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    Orgo Lab 1 Calculations

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    VictoriaMcKaba
    1. You started with 25g of a compound and lost 5g after recrystallization. The percent recovery is calculated as 20g recovered divided by 25g original times 100, which is 80%. 2. For a compound A with a partition coefficient of 6 between water and ethyl acetate, if 15g dissolved in 100mL water and 20mL ethyl acetate is added, 6g will transfer to the ethyl acetate layer, leaving 6.81g in the water layer. 3. To calculate specific rotation, take the observed rotation in degrees and divide by the concentration in g/mL and cell length in dm to obtain [α].

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    Orgo Lab 1 Calculations

    Uploaded by

    VictoriaMcKaba
    111 views2 pages
    1. You started with 25g of a compound and lost 5g after recrystallization. The percent recovery is calculated as 20g recovered divided by 25g original times 100, which is 80%. 2. For a compound A with a partition coefficient of 6 between water and ethyl acetate, if 15g dissolved in 100mL water and 20mL ethyl acetate is added, 6g will transfer to the ethyl acetate layer, leaving 6.81g in the water layer. 3. To calculate specific rotation, take the observed rotation in degrees and divide by the concentration in g/mL and cell length in dm to obtain [α].

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    For CHM 205

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    1. You started with 25g of a compound and lost 5g after recrystallization. The percent recovery is calculated as 20g recovered divided by 25g original times 100, which is 80%. 2. For a compound A with a partition coefficient of 6 between water and ethyl acetate, if 15g dissolved in 100mL water and 20mL ethyl acetate is added, 6g will transfer to the ethyl acetate layer, leaving 6.81g in the water layer. 3. To calculate specific rotation, take the observed rotation in degrees and divide by the concentration in g/mL and cell length in dm to obtain [α].

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    © All Rights Reserved
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    111 views2 pages

    Orgo Lab 1 Calculations

    Uploaded by

    VictoriaMcKaba
    1. You started with 25g of a compound and lost 5g after recrystallization. The percent recovery is calculated as 20g recovered divided by 25g original times 100, which is 80%. 2. For a compound A with a partition coefficient of 6 between water and ethyl acetate, if 15g dissolved in 100mL water and 20mL ethyl acetate is added, 6g will transfer to the ethyl acetate layer, leaving 6.81g in the water layer. 3. To calculate specific rotation, take the observed rotation in degrees and divide by the concentration in g/mL and cell length in dm to obtain [α].

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
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    of 2

    Orgo Lab 1 Calculations:

    Experiments 0&1
    Quiz 1
    1. You started with 25 g of a compound. After recrystallization you
    lost 5g of the compound. Calculate the percent recovery of the
    compound.
    25g 5g = 20g
    20g/25g x 100 = 80%
    Experiment 2
    Quiz 2
    2. Assume an organic compound A has a partition coefficient
    between water nd ethyl acetate equal to 6, and 15 g of A
    dissolved in 100mL of water. If 20mL of ethyl acetate are added,
    calculate how much of A remains in the water layer.
    6g =

    6g =
    1500

    or

    6g =

    120x = 1500-100x

    220x =

    x = 1500/220 = 6.81g in H20


    Experiment
    Data:
    .106g Benzoic Acid used
    0.096 Benzoic Acid recovered
    Used 2mL MtBE
    Used 3mL H2O
    3. C2 =

    C1 =

    KD =
    Experiment 3a
    Quiz 3a
    4. Calculate Rf values for the two spots below and show the
    equation you used to obtain these values.

    Rf = distance from origin / total length

    A.

    B.
    Experiment 6
    Quiz 6
    5. Calculate the specific rotation of a substance that is dissolved in
    a solvent at concentration of 0.5g/mL and that has an observed
    rotation of -10 as determined with a 0.5 dm cell
    Specific rotation =

    Experiment
    Data:
    3.48g amine
    7mL solution
    -11.538 observed optical rotation
    6. C =
    L = 1.0
    [] =

    Optical purity =

    (-) enantiomer

    100-58.4 = 41.6% () racemic


    Total (-) amine = 58.4% + (0.5 x 41.6) = 79.2%
    Total (+) amine = (0.5)(41.6) = 20.8%

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