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Predicting Grain Size Evolution Alloy 718
Predicting Grain Size Evolution Alloy 718
The following paper was selectedby the Awards Subcommitteeof the International Symposium
on Superalloys as a co-winner of the Best PaperAward for the Ninth Symposium. The selection
was basedon the following criteria: originality, technical content, pertinence to the superalloy
and gasturbine industries and clarity and style.
Predicting Grain Size Evolution of Udimet Alloy 718 during the Cogging Processthrough
Use of Numerical Analysis
B.F. Antolovich and M.D. Evans
Predicting Grain Size Evolution of UDIMET@ alloy 718 During the Cogging Process Through the Use of
Numerical Analysis
Bruce Antolovich* Mike Evans**
Special Metals Corporation,4317 Middle SetlementRd, New Hartford, NY*
Electralloy, 175 Main St., Oil City, PA**
Abstract
A semi-automatedfinite element analysis program, in conjunction with user written subroutines, has been demonstrated to successfully predict therm0 mechanical histories
and grain size evolution. Double cone compression
specimenswere found to be highly efficient for generating
data for the recrystallization behavior of UDIMET@ alloy
718. Recrystallization behavior was modelled as having
two distinct regimes, dynamic and static; both of which
were modelled using typical Mehl-Johnson-Avrami forms.
This type of modelling capability is expectedto improve the
efficiency of the ingot-billet conversion processas well as
making possible the development of unique products such
as dual property billet.
Introduction
Superalloys 2000
Edited by T.M. Pollock, R.D. Kissinger, R.R. Bowman,
K.A. Green, M. McLean, S. Olson. and J.J. Schima
TM.5 (The Minerals, Metals &Materials Society), 2OiXl
39
Recrystallization Models
The literature contains a great number of articles concerning
recrystallization and cogging of nickel base superalloys.
[l-6] These models have generally taken one of three
forms as statedpreviously. Regardlessof the model, there
are two well accepted regimes of recrystallization along
with a slightly controversial third type. In general, during
load application, an original unrecrystallized grain may
recrystallize dynamically. If 100% dynamic recrystallization is not achievedthe remaining unrecrystallized portions
of the original grain may undergo further recrystallization
without additional strain input. Some authors call this
meta-dynamic recrystallization since the principal driving
force for recrystallization is the removal of dislocations
introduced in the previous deformation. The third regime
is static recrystallization and grain growth in which the
principal driving force is the reduction of grain boundary
energy. The factors affecting each of these types of
recrystallization for any given material are :
1. Static
l Hold time
l Residual dislocation density
l Temperature
0 Initial grain size
2. Dynamic
0 Strain
0 Strain rate
l Temperature
3. Meta-Dynamic
l Strain
0 Strain rate
l Temperature
0 Initial grain size
l Hold time
Regardlessof the recrystallization model chosen, dynamically recrystallized and meta-dynamically recrystallized
grain size may be reduced by increasing the total strain or
strain rate. Increasing the temperatureor hold time tends to
increasethe meta-dynamic or statically recrystallized grain
size.
Material
The material chosen for this study was UDIMET@ alloy
7 18. Its nominal composition is shown in Table I.
This author has chosen to model the recrystallization phenomenon by breaking it down into dynamic and static
componentswithout addressingthe meta-dynamic possibilities. The modelling is Mehl-Johnson-Avrami based[7,8]
with critical strains and strain rates to achieve static and
dynamic recrystallization respectively.
40
Dynamic Recrystallization
1. Material
2. Heat exchangeenvironment
3. Billet geometry
4. Die geometry
5. Die movementparameters
6. Reheatfurnace temperature
7. Number of reheats
8. Number of passesper reheat
9. Billet advanceper bite(trave1 increment acrossdies)
10. Draft per bite
11. Billet rotation per pass
ddarn =
I-exp
[-+J]
clz
(1)
(2)
Where E is the applied strain, k, n, Cl and m are material constants, 60.6 is the strain required to achieve 50%
recrystallization and Z is the traditional Zener-Hollomon
parametergiven by:
Q
z = Eexp
*
( RT >
(3)
Static Recrystallization
Static recrystallization will only ocurr if there has been
sufficient accumulation of plastic strain. (i.e. Ep >
~SRXC& If this is achieved,then the fraction recrystallized
and recrystallized grain size will be given by:
X sta
with trJ.5
d sta
I-exp
to.5
C 2 $-donzZn~
(do,
[-hk(&)n]
(4)
4 Z)
(5)
Experimental Procedures
Generating recrystallization data for the three recrystallization modesrequires sampleswith different initial grain size,
temperature, hold time, strain and strain rate. In order
to reduce the time and expense of testing, double cone
compressionspecimenswere chosen due to their ability to
generate a wide variety of strains and strain rates within
a single specimen. A typical double cone geometry and
strain variation is shown in Figure 1. Similar variations are
found for the strain rate as shown in Figure 2.
lime (see)
Pass
1
2
3
4
5
6
7
8
9
10
11
12
Advance
(mm)
per Bite
CenterlinepSpmDlbution:
Lonpihldnal
-&ml,
,,oBM -7m -700 xE.3 UN -633 -500 -453 -4a -SE0 .wl -2uI
Llx@tinal Position(ml)
,,o.am -760 -mo 6Yl bw -550 -600 460 40
0.0
f!a.8
jo.,.- ~ /
454 -wJ
::i:
-32 -24 .28 -26 -24 .P
46
46 4,
42 -10
o.60
.x2
40
-20 48
16
14
12
-10
Radial .%aka~s~bution:
Rsdia,pEai& (ml,
~tinsl
wi
(mm,
-750 -ml 650 a9 -550 -Km 460 4l
0.6(~
-33 400
.a
$ 0.6 -
0.6
1::d
i?
3
; 0.7 .
3
0.6 -
0.6
0.6
10
0.6
-32 -xl
c
.a
m c
-26 -24 22 a
m c
-18 -16 -14 -18 -10
Figure 8:
measured 25
Radial SP~t~s;button:
Rdbl Poritm (mm)
.
.
:j
0.0 .
5
5;: 0.6 .
0.6 -
,I
0.6
10
-30
.a
.a
-2,
.a
-18
-16
-14
-12
-10
recrystslhzed
graa
5128
91
Center Primary
Center ALA
Edge Primary
m
0
Practice 1
Practbce 2
Edge ALA
tle : 0355R266lNC716
Volume
,,aot,on
0, dyrrrlllL
rocrystullllulloll
Conclusions
References
Applications
Given the fact that the disk forger has areas in the disk
which receive little deformation and little potential for grain
size refinement, one elegant solution is to supply billet with
an appropriate heterogeneousgrain size. Through careful
attention to reheattemperatures,bite advance,bite draft and
die speed,it is theoretically possible to produce such a billet.
The amountof industrial trials required in the past to perfect
this processwere prohibitive. In theory and practice, these
billets may now be produced.
1939.
46
47