Professional Documents
Culture Documents
ICCSA
ICCSA
ICSAAM 2015
The 6th International Conference on
Structural Analysis of Advanced Materials
8-11 September, 2015, Porto, Portugal
Porto, Portugal
8 - 11 September, 2015
Committees
Chairmen
Published by:
INEGI Instituto de Engenharia Mecnica e Gesto Industrial
Front cover figures credits:
VC Pinto, PMGP Moreira
Editor ICSAAM2015 book of abstracts: VC Pinto, PMGP Moreira, PJS Tavares
ISBN: 978-972-8826
http://icsaam2015.inegi.up.pt
Sponsors
University of Patras
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Contents
Committees ............................................................................................................... 2
Sponsors .................................................................................................................... 5
Contents .................................................................................................................... 6
Welcome from President of the INEGI - Institute of Science and Innovation in
Mechanical and Industrial Engineering................................................................... 12
Welcome from Conference Chairs .......................................................................... 13
Conference Overview.............................................................................................. 14
About Porto............................................................................................................. 16
Conference site ....................................................................................................... 18
Meetings rooms ...................................................................................................... 18
Plenary Invited Speakers ......................................................................................... 22
Prof. Raj Das ........................................................................................................ 22
Modelling extreme deformation and dynamic behaviour of materials using
multi-scale techniques and mesh-less methods ............................................. 22
Prof. Mrio Vaz ................................................................................................... 24
Structural Monitoring and Biomechanics ....................................................... 24
Prof. Antnio Torres Marques ............................................................................ 26
Thermoset versus Thermoplastic composites: from raw materials and semiproducts to final parts..................................................................................... 26
Prof. George Papanicolaou ................................................................................. 28
A comparative study of nanotube-epoxy interphasial interaction in CNT and
TNT-epoxy matrix nanocomposites ................................................................ 28
Prof. Stefan Pastrama ......................................................................................... 30
Prof. Gabriel Jiga ................................................................................................. 33
Material and shape crash-box influence on the evaluation of the impact
energy absorption capacity during a vehicle collision .................................... 33
Prof. Alberto DAmore ........................................................................................ 35
Constitutive law describing the strength degradation of fiber reinforced
composites subjected to cyclic loading........................................................... 35
Prof. Rui Miranda Guedes ................................................................................... 37
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Session 2B ............................................................................................................... 77
DIGITAL IMAGE CORRELATION MEASUREMENTS IN AN INNOVATIVE RAILWAY
CAR BODY UNDERFRAME 3-POINT BENDING TEST ............................................ 78
DIGITAL IMAGE CORRELATION FOR STRUCTURAL HEALTH MONITORING OF AN
INNOVATIVE PROPOSAL FOR SEISMIC RESISTANT STRUCTURES........................ 79
WIRELESS STRAIN GAUGE FOR COMPOSITE MATERIALS.................................... 81
INFLUENCE OF ULTRASOUNDS IN THE DAMPING CAPACITY OF ALUMINIUM
ALLOYS ................................................................................................................ 82
ACOUSTIC EMISSION MONITORING FRACTURE OF A COMPOSITE MATERIAL ... 83
Session 3A ............................................................................................................... 85
INFLUENCE OF DEFORMABILITY OF HORIZONTAL DIAPHRAGMS IN THEIR PLAN
ON THE SEISMIC LOADS DISTRIBUTION TO RESISTING WALLS ........................... 86
A MODERN METHODOLOGY OF DESIGN OF THREE-DIMENSIONAL STRUCTURES
BY A GENETIC ALGORITHMS APPROACH ............................................................ 88
SURFACE STRUCTURAL INHOMOGENEITIES AND FRACTAL PROPERTIES OF MnO2
SEMICONDUCTOR THIN FILMS ........................................................................... 90
MULTIBODY DYNAMICS SIMULATION OF AN ELECTRIC BUS WITH FLEXIBLE
PARTS .................................................................................................................. 91
FINITE ELEMENT ANALYSIS IN THE DESIGN OF PATIENT-SPECIFIC OSTEOTOMIES
GUIDES. CASE STUDY .......................................................................................... 92
HOMOGENIZATION OF A FIBRED STRUCTURE WITH A CONDITION ON THE
INTERFACE MATRIX-FIBRE .................................................................................. 94
Session 3B ............................................................................................................... 95
DEVELOPMENT OF COMPOSITE MATERIALS DATABASE FOR AEROSPACE
CERTIFICATION .................................................................................................... 96
DYNAMIC BEHAVIOR OF COMPOSITE PLATES MADE WITH GREEN MATERIALS 97
MACROPOROUS GREEN CERAMICS BY SIMULTANEOUS RECYCLING OF COAL
ASH AND GLASS WASTES .................................................................................... 99
GREEN COMPOSITE MATERIALS: THE BREAKING NEW GROUND ABC-MATRIX
.......................................................................................................................... 101
COMPOSITE MAGNETIC MICROWIRES SANDWICH STRUCTURE FOR SENSOR
APPLICATION ..................................................................................................... 103
Session 4A ............................................................................................................. 105
CRACK INITIATION ANALYSIS UNDER MEAN STRESS EFFECT IN 2024 T351 ALALLOY ................................................................................................................ 106
8
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
MONITORING THE FLY ASH DISPERSION IN EPOXY MATRIX AND ITS EFFECT ON
THE THERMOMECHANICAL PROPERTIES OF THE OBTAINED COMPOSITES ..... 183
EFFECT OF PIGMENTS ADDITION ON PROPERTIES OF THE ISOTACTIC
POLYPROPYLENE ............................................................................................... 185
USE OF DIFFERENT ACIDS FOR THE EXTRACTION OF CHROMIUM CONTAINED IN
ASH FROM THE INCINERATION OF WASTE LEATHER........................................ 187
HYDROGEN GAS SENSORS BASED ON PALLADIUM/SILICON OXIDE/SILICON
CARBIDE SANDWICH STRUCTURES ................................................................... 188
DIFFERENCES IN DEGRADATION MECHANISM OF THE STANDARD AND THE NEW
- CORE-SHELL CATALYST DURING AMMONIA OXIDATION PROCESS ................ 190
RELATIONSHIP OF CHEMICAL SURFACE TREATMENTS OF STRUCTURAL
ALUMINUM ALLOY TO STRENGTH OF GLUED JOINT ........................................ 191
INFLUENCE OF TEMPERATURE ON MECHANICAL PROPERTIES OF
POLYPROPYLENE SANDWICH PANEL AND COMPARE THE MECHANICAL
PROPERTIES OF THE ALUMINUM HONEYCOMB PANELS.................................. 193
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
As President of INEGI, it is with great pleasure that I welcome you to the 6th
International Conference on Structural Analysis of Advanced Materials.
INEGI pledged its commitment to the subject of this conference several years ago,
and has been doing research work in the area that has not gone unnoticed. As an
interface institute between the University and the Industry, we are bound by the
numerous practical issues on the subject brought to our attention by the
companies and research institutions we partner, the projects we embrace or the
discoveries of our scholars and research teams. Structural analysis of advanced
materials issues arise naturally on real-life parts, and those are precisely the sort
of subjects our industrial partners make a living of, and therefore we either study
or analyse as part of our daily work.
I wish you all a fruitfull meeting and may the consequences of this conference fuel
important work for new researchers and results for the industry and the Society
at large.
Warm regards,
Alcibiades Paulo Guedes
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Conference Overview
Portugal is the newest addition to the organizing committee of the International
Conference on Structural Analysis of Advanced Material ICSAAM conferences
and it is therefore the first time this exclusive conference is hosted in Porto from 8th
to 11th September, 2015.
ICSAAM was launched in 2005 and is a partnership effort from INEGI, University
of Patras and University Politehnica of Bucharest, Romania.
For its 6th edition, ICSAAM 2015 conference authors were invited to submit work
and present papers and posters in all relevant fields of Structural Analysis of
Advanced Materials.
ICSAAM 2015 aims at bringing together scientists and engineers from around the
world in the attempt to exchange recent experiences in research and development
activities in the field of Structural Analysis of Advanced Materials. The topics to
be covered by the conference include all thematic areas of current research and
industrial applications. Main topics of the conference are:
Materials
Polymers and Polymer Matrix Composites
Ceramic and Metallic Matrix Composites
Nano-composites
Biomaterials and medical applications
Smart materials
Green composites
Sandwich structures
Degradation and Prediction
Damage and Fracture
Fatigue (Mechanical, Thermal)
Durability and Reliability
Large deformations
Impact
Water absorption
Analytical and Numerical Modeling
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Experimental techniques
NDT-NDI
Thermal Analysis
Mechanical Testing
Vibration Analysis
Dynamic Behavior
Manufacturing Techniques
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
About Porto
Portos cultural and social life is warmingly waiting our visitors.
It is situated on North of Portugal.
Discover more on: www.portocvb.com or on http://www.cm-porto.pt/
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Photos: https://www.flickr.com/photos/visitportoandnorth/sets
Videos: https://vimeo.com/visitportoandnorth
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Conference site
The conference will take place in the Faculty of Sciences at the University of
Porto (Faculdade de Cincias da Universidade do Porto).
With origins dating back to the eighteenth century, the University of Porto is
currently the largest education and research institution in Portugal. The venue is
located in a quiet area with several green gardens with remarkable views to the sea,
the Douro river and its historical bridges, the world famous Porto wine cellars and
the UNESCO World Heritage Ribeira.
The Faculty facilities are excellent and serve, each year, a large number of similar
events.
Boavista area with its world renowned Casa da Msica (The House of Music),
shopping centers shops and hotels are a few minutes walk away. An modern and
very efficient public transportation system (subway, buses, trams) connects in a
few minutes to all major interest points in the city but also to the airport, train
stations and well as the several well known beaches and seaside towns both north
and south of Douro River.
Meetings rooms
Room Newton
Room Galileu
Room A and B
More information on: Usefull tips paper
__ Room Galileu
__ Room Newton
__ Room A
__ Room B
__ Coffee-break /
lunch lounge
area
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Conference banquet
Casa da Msica Restaurant
Av. da Boavista, 604-610
4149-071 Porto, Portugal
Before banquet, there will be a guided tour to Casa da Msica beginning at
18:30. Organizing staff will lead participants to Casa da Msica.
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
(Directions)
Conference tour
Visit Douro Full Day (By Boat and Train, with Lunch included)
11 September Friday
Up by train to Rgua and downstream by boat to Porto.
08h30 Meeting at S. Bento Railway Station in Porto.
All on board for a Cruise towards Rgua to enjoy a delightful journey along the
river Douro, through an untouched landscape of wonderful high hills, lush Porto
vineyards, picturesque villages and traditional towns.
09h10 - Departure by train to Rgua
11h08 - Arrival at Rgua
11h30 - Shipping at Rgua Quay
Departure to Porto // Port Wine on board
12h00 - Lunch on board
13h45 - Carrapatelo Dam (Flood-gate, unlevelling 35 meters)
16h30 - Crestuma-Lever Dam (Flood-gate, unlevelling 14 meters)
18h00 - Arrival at Vila Nova de Gaia Quay
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Dr Raj Das is a principle investigator of the Centre for Advanced Composite Materials, and a faculty
member of the Mechanical Engineering Department of the University of Auckland, New Zealand. His
current areas of interest include impact response and failure of composite materials, numerical
modelling using mesh-less methods, multi-scale modelling, nano-machining, dynamic fracture,
damage tolerance based structural optimisation. Dr Das received a PhD in the field of failure analysis
and structural optimisation from Monash University, Australia. He developed a range of damage
tolerance based optimisation tools, which have been adopted by Australian aerospace industries for
optimum designs for fracture strength and fatigue life. Dr Das subsequently worked as a Research
Associate in the University of Manchester, UK. On his return to Australia, Dr Das joined the
Commonwealth Scientific and Industrial Research Organisation (CSIRO) as a Senior Research
Scientist, where he contributed to the development of mesh-less SPH method for a range of
applications. Dr Raj Das has established strong linkages with aerospace, rail and marine industries
and active collaboration with national and international academic institutions. Dr Das is a member of
the National Committee on Applied Mechanics, and is an adjunct professor of the University of
Quebec, Canada.
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24
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Figure 1 - Sensor for 2D shear force assessment in the plantar region of patients with diabetic
neuropathy, (Patent pending).
------------------------------------------------
Mario Vaz joined the Faculty of Engineering of the University of Porto teaching staff in 1985.
Throughout his professional life took part in several research projects in the area of inspection of
structures and characterization of its behavior under load, as well as in developing methods of
inspection based on the use of laser radiation. He was also involved in several projects of technology
transfer and expertise in various accidents involving structures. Currently his main research interest
are focused on Solid Mechanics, Holographic interferometry, NDT of Composites, Dynamic of
Materials, Biomechanics, Experimental Mechanics, Image Processing.
25
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Thermoset versus Thermoplastic composites: from raw materials and semiproducts to final parts
Abstract
Although only recently thermoplastic matrices have been used in long and continuous fibre
reinforced composites replacing with success thermosetting matrices, the number of their
applications is increasing due to their better ecological and mechanical performance. A
comparison will be made regarding advantages and disadvantages of both systems and their
future evolution and applications perspectives.
The use of long/continuous fibre reinforced thermoplastic matrix composites involves,
however, great technological and scientific challenges since thermoplastics present much
higher viscosity than thermosettings, which makes much difficult and complex the
impregnation of reinforcements and consolidation tasks.
Two major technologies are being used to allow wet reinforcing fibres with thermoplastic
polymers: i) the direct melting of the polymer and, ii) the intimate fiber/matrix contact prior
to final composite fabrication. Continuous fibre reinforced thermoplastic matrix preimpregnated tapes (PCTs) are, for example, produced by direct melting processes.
Alternatively, intimate contact processes allow producing cheap and promising preimpregnated materials, such as, commingled fibres and powder coated towpregs.
Sometimes, thermoplastic compatibilizers were added to the matrices to improve their
adhesion and facilitate impregnation to reinforcements.
Different thermoplastic matrices and fibres raw-materials were used in a case study to
manufacture pultruded composites for commercial applications (glass and carbon fibre/
polypropylene) and for advanced markets (carbon fibre/Primospire).
Other semi-products, like tape, may be used and the forming processing conditions are
described.
The towpregs, PCTs and commingled fibres were processed into composite bar profiles
using the laboratorial pultrusion line.
To produce composite profiles, the pre-impregnated materials are guided into the preheating furnace to be heated up to the required temperature. Then, they enter in the
pultrusion heated die to be heated and consolidated to the required size and, after cooled
down in the cooling die to solidify.
A die to allow producing a 202 mm2 bar-shaped profile has been designed and
manufactured.
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
interphase model a comparison of the interphasial characteristics of CNT-Epoxy and TNTEpoxy resin systems was made. Interesting results concerning the nanotube-polymer
interphase characteristics were derived (Fig. 1a and 1b).
tE_0.01*(Ei-Em)
ExpDec1 of tE_0.01*(Ei-Em)
0,030
tE_0.01*(Ei-Em)
ExpDec1 of tE_0.01*(Ei-Em)
0,016
0,014
0,025
0,020
0,015
0,010
0,005
0,012
0,010
0,008
0,006
0,004
0,002
0,000
0,000
0,2
0,4
0,6
0,8
0,1
1,0
0,2
0,3
0,4
0,5
0,6
0,7
0,8
0,9
1,0
kE
kE
(a)
(b)
------------------------------------------------
Prof. George Papanicolaou complete his Degree in Physics from National University of Athens in
1971 and hisDr. Engn. In Applied Mechanics from National Technical University of Athens in
1980. Professor has research experience in several groups like the Composite Materials Group,
Washington, USA and in the fields of Measurement Techniques, Analysis Methods, Transducers and
Electronic Instrumentation, Bruel & Kjaer, Naerum, Denmark. He has been the Director of Section of
Applied Mechanics, Dept. of Mechanical Engineering, University of Patras (July 1990 - Dec. 1992)
and ). Acting Head of the Mechanical Engineering Dept., Univ. of Patras (Sept. 1993- Sept.1997).
Nowadays, he is Full Professor of Mechanics of Polymers and Composites, Dept. of Mechanical
Engng., Univ.of Patras. He received the silver medal for excellent research work on Crack
Propagation Problems in Rubber-Modified Polymers, Cambridge (U.K.) (1987). He is also Doctor
Honoris Causa, (Dr. of Honour) University Politehnica of Bucharest (1998).
Author and co-author of more than 200 papers in recognized scientific journals, one monograph and
several book chapters. Leader of 8 European Projects and numerous national research and industrial
projects. devoted to optical metrology and development of innovative measurement systems based on
interferometric and noncoherent methods.
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Abstract
In order to diagnose lung cancer, the most lethal one today, medical doctors perform a
trans-bronchial biopsy. First, this is planned by examining a number of Computed
Tomography (CT) scan slices. Then, the procedure is performed by introducing a video
bronchoscope into the bronchi as far as the diameter of the bronchoscope permits. A biopsy
forceps is inserted through the bronchoscope channel and the biopsy is blindly performed,
but the success rate of the procedure is not very high. In the case of such procedure, better
results were reported following the use of electromagnetic navigation bronchoscopy (ENB)
with a steerable instrument.
The authors of this paper have developed a novel system, called NAVICAD 1 for spatial
guidance of a customized bronchoscopic forceps used to reach peripheral targets beyond
the place allowed by the size of the diameter of the video bronchoscope. When
bronchoscope diameter is too big to advance, the user extends only the navigation forceps
further to the peripheral target. The navigation is then performed using the virtual
bronchoscopy image from the fourth window of CT and the instantaneous position of the
forceps tip overlaid on the 3D model presented in the third window. The biopsy using the
forceps can be performed when the target is reached. Improved diagnosis is accomplished
via enhanced navigation, targeting, and anatomical structure differentiation.
The paper describes the virtual bronchoscopy method implemented in the NAVICAD
system, developed based on a GPU implementation of the Marching Cubes algorithm for
extracting surfaces from volumes using Open Computing Language (OpenCL) and Open
Graphics Library (OpenGL), [3]. This algorithm has 4 stages: 1. Data transfer. Dataset is
stored as a 3D texture on the GPU of NVidia Quadro 6000 professional graphics solution
model; 2. Reconstruction of the surface of the lung tissue using the Marching Cubes
algorithm; 3. Rendering of the surface extracted in the previous step; 4. Navigation using
collision detection and resolution through an algorithm developed by the authors.
In virtual bronchoscopy, the user navigates through the CT volume; the virtual navigation
camera must be forced to remain inside the airways surface. In Image Guided Therapy
30
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
(IGT) tracking, the virtual camera is attached to the tracking tool that is moving always
inside the airways tubes. But, due to various errors, the tool could be placed outside the
airways. A Collisions Engine class is used in the application, that detects and solves the
collisions of the virtual camera with the airways surface. The virtual airways surface is
formed by more 200.000 triangles. In order to reduce the computations that could slow
down the application, the triangles are stored in an efficient manner, such that the
intersections line-triangle are tested only on the triangles found in the vicinity of the line
segment: the surface is covered with boxes, each box stores the triangles that intersect it;
the tests are calculated only on the triangles stored in the boxes intersected by the line
segment (Fig. 1). In step 1, first the intersection between line and the triangle plane is
computed, than barycentric coordinates are used to test if the intersection is inside the
triangle. An artificial structure generated mathematically is used to test the collisions
algorithms. Virtual bronchoscopy and IGT tracking are performed on CT scans of a
medical phantom (Fig. 2).
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Acknowledgements
The research leading to these results has received funding from EEA Financial Mechanism 2009 2014 under the project EEA-JRP-RO-NO-2013-1-0123 - Navigation System For Confocal Laser
Endomicroscopy To Improve Optical Biopsy Of Peripheral Lesions In The Lungs (NAVICAD),
contract no. 3SEE/30.06.2014.
------------------------------------------------
Stefan Dan Pastrama, is working as Professor at the Department of Strength of Materials from
University Politehnica of Bucharest, Romania.
His research interests cover fracture mechanics of metals and composites and biomechanics. He has
published papers in ISI journals as International Journal of Pressure Vessels and Piping, Fatigue and
Fracture of Engineering Materials and Structures, Materials and Design, Engineering Fracture
Mechanics, International Journal of Fracture. Prof. Pastrama conducted biomechanics research
projects and was invited researcher in the team of University of Porto in two European projects in
structural integrity of aeronautical structures. He co-authored two books with subjects from structural
integrity. He has reviewed scientific papers in International Journal of Structural Integrity and other
journals in the same scientific field. Prof. Pastrama is Member in the International Scientific
Committee of the Danubia-Adria Society on Experimental Mechanics
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Material and shape crash-box influence on the evaluation of the impact energy
absorption capacity during a vehicle collision
Abstract
During a light collision between two vehicles or a vehicle and an obstacle, the internal
structure of the car is irrecoverably damaged. In order to limit as much as possible the body
in white defacement the new vehicles are equipped with so called crash boxes situated in
front and rear of the car.
Conflicting requirements with respect to saving weight and increasing vehicle
crashworthiness at the same time, pose a major challenge in automotive design. Many
devices have been designed to study impact energy absorption during a collision and hence
protect the vehicle components and passengers. Today, aluminium in its various product
forms (sheet, extrusions, die castings) is an established automotive lightweight material
offering excellent weight saving potential, including crashworthiness applications for
passive vehicle safety. Modern ductile aluminium alloys have an outstanding ability to
absorb impact energy in case of accidents.
The purpose of our study is to analyze the influence of the crash box material in order to
reduce the side member permanent deformations, since once damaged, this component,
even repaired, will never assure a good safety in case of major collision.
Although the speed necessary for of a car homologation is 16 km/h, a second purpose of
this paper is to identify the influence of the velocity upon the crash box behaviour.
Consequently, a numerical study has been undertaken to investigate axial crushing
responses, energy absorption performance of empty & foam filled steel and aluminium
concentric tubes with different density of foam.
For comparison four different materials have been taken into account for the simulations of
the crash box:
a) automotive steel H360, with E = 200 GPa and yield limit of 420 MPa;
b) TRIP steel, with E = 200 GPa and yield limit of 550 MPa;
c) Aluminium extrusion 6008T7, with E = 70 GPa and yield limit 250 MPa;
d) 6061 aluminium alloy, with E = 70 GPa and yield limit of 200 MPa.
Concerning the filling material, low-density polymeric (non-metallic) foams have been
widely used in several engineering applications. In this paper, different types of
polyurethane foams, with different densities varying from 100 kg/m3 to 350 kg/m3 are
wide-spread in the energy absorption and impact applications due to their excellent energy
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
absorbing capability. In the automotive industry, the new regulations in the Federal Motor
Vehicle Safety Standards (FMVSS) require the use of polymeric foam materials inside
motor vehicles to protect the occupants during accidents.
The crash box has been modelled in two different configurations:
a) rectangular caisson shape (height h = 90 mm, width b = 80 mm and thickness t = 2 mm);
b) hexagonal shape (diagonal of 90 mm and thickness t = 2 mm).
Nowadays, crash boxes are manufactured from automotive steel an advanced high
strength steel with carefully selected chemical compositions and multiphase
microstructures resulting from precisely controlled heating and cooling processes.
Crash box, with whom a vehicle is equipped at the front end of its front side frame, is one
of the most important automotive parts for crash energy absorption. In case of frontal crash
accident, for example, crash box is estimated to be collapsed with absorbing crash energy
prior to the other car components such that the damage of the cabin frame is minimized the
vehicle occupants having the possibility to save their lives.
According to the new regulations, it has been strictly required to satisfy both reduction of
body weight and improvement of crash worthiness and consequently, regarding the crash
box, it is absolutely necessary to ensure high energy absorption using cross sections with
minimum thickness.
However, it happens that these boxes do not work as designed when a thin sheet is applied
as the material for a crash box manufacturing, being difficult to acquire sufficient energy
absorption only through the thin walls.
In several studies attention is focused upon finding an optimum cross sectional shape of a
crash box to ensure high capability for energy absorption without crash bead.
------------------------------------------------
Prof. Gabriel Jiga graduated the University POLITEHNICA of Bucharest in 1986 in the field of
Manufacturing Engineering. I obtained a Ph.D. in 1996 with a thesis entitled "Considerations of
calculus and implementation of some efficient composites in Industry and military
equipments". Since 2004, I am professor in the Department of Strength of Materials, Faculty of
Engineering and Management of Technological Sytesms (Industrial Engineering) from University
POLITEHNICA of Bucharest. Since 2008 I am vice-dean responsible with International Cooperation
in the frame of the same faculty. Author and co-author of more than 60 papers published in
prestigious journals or presented in International Conferences and Symposiums and author (coauthor) of 10 books in the field of Strength of materials, Numerical methods in engineering,
Fundamentals of composite materials.
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------------------------------------------------
Alberto DAmore born in Naples (Italy) on July 25th 1956. He is married with two sons. His home is
at Via Roma 48, Somma Vesuviana, 80049 (NA), Italy. He is an Associate Professor of Materials
Science and Technology at The Second University of Naples-SUN Department of Industrial and
Information Engineering , Via Roma, 19, 81031, Aversa (CE), Italy.
The research activities of Professor DAmore focus on Polymer Processing and properties, Structureproperties-relationships of high performance composites, Structural relaxation, Environmental and
Physical aging of polymers, Rheology and Viscoelasticity of complex systems, Adhesives, Polymer
modified cements, Nano-composites, Biomaterials, thin films. Professor DAmore published more
than 130 papers on International Journals and books. He edited several international books
(NovaScience Publishers, Apple Academic Press, Brill Leiden).
He is Editor, Associate and/or Guest Editor of International Journals (AIP- Conference Proceedings,
MTDM- Mechanics of Time Dependent Materials, Polymer Composites, Materiale Plastice, Journal
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------------------------------------------------
R. M. Guedess research focuses on polymer based composite materials. His main interest is in
durability and long-time prediction of mechanical behavior of composite structures. More recently
has been working in biodegradable medical devices for ligament repair. He received his MSc in
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials___________
Structural Engineering (1992) and PhD in Mechanical Engineering from the University of Porto
(1997). In 1997 he joined the Mechanical Engineering Department of the University of Porto. He
received his Habilitation in Mechanical Engineering from the University of Porto in 2012. He has
published more than 60 papers in scientific journals, 9 book chapters and edited 1 book.
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
ICSAAM2015 Program
Program Overview
Tuesday 08/09
Wednesday 09/09
Thrusday 10/09
9:00-9.30
OPENING SESSION
9:30-10:15
10:15-11:00
11:00-11:30
COFFEE-BREAK
COFFEE-BREAK
COFFEE-BREAK
LUNCH
LUNCH
11:30-12:15
12:15-12:30
12:45-14:15
14:15-15:30
15:30-16:00
16:00-17:00
17:00-17:30
Session 1A
Session 1B
LUNCH
Session 2A
Session 2B
COFFEE-BREAK
Session 3A
Session 3B
17:30-18:00
Poster Session 1
18:00-19:30
WELCOME COCKTAIL
RECEPTION
Session 4A
Session 4B
COFFEE-BREAK
Session 5A
Session 6
COFFEE-BREAK
Session 5B
CONFERENCE BANQUET
19:30-23:00
39
Session 7
CLOSING SESSION
Friday 11/09
CONFERENCE TOUR
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
Technical Program
August 14th, 2015
TUESDAY, 8 September 2015
TUE, 09:00 - 09:30
OPENING SESSION
Room Newton
Welcome to Participants
(Conference Co-Chairs)
Welcome Address
MONDAY, 24 JUNE 2013
TUE, 09:30 - 10:15
PLENARY LECTURE 1.1
Room Newton
Modelling extreme deformation and dynamic behavior of materials using multi-scale techniques and meshless methods
Professor Raj Das
(University of Auckland, New Zeland)
Chair: Professor George Papanicolaou (University of Patras)
WED, 10:15 - 11:00
COFFEE-BREAK
40
Lounge
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
TUE
Session 1A
11:30-12:45
TOPIC: Testing I
Chair: Mrio Vaz
Ref:
Title and Author (s)
#15
Investigation of the mechanical properties of
carbon nanotube reinforced composites and
their evaluation using a cylidrical RVE
M. Konstantakopoulou, G. Kotsikos
#27
Mechanics crack growth-based fatigue
evaluation considering crack closure and
equivalent initial flaw size
A.S.F. Alves, J.A.F.O. Correia, A.M.P. De Jesus,
P.J.S. Tavares, P.M.G.P. Moreira
#26
Theoretical and experimental study of specimens
with stress concentrators in dependance of
stress triaxiality Donka Ana Maria Comanici,
Viorel Goanta, Paul Doru Barsanescu
#66
Deformability behaviour of new cobalt based
alloys
Alexandru Ghiban, Brandusa Ghiban, Nicolae
Serban, Cristina Maria Bortu
#58
Experimental investigation on Self-healing
efficiency of doped Fiber Reinforced Plastics with
Thermoplastic micro-Particles
A. Kotrotsos, A. Baltopoulos, S. Tsantzalis, X.
Tsilimigkra, P.Tsokanas, V. Kostopoulos
TUE
Session 1B
11:30-12:45
TOPIC: Nanocomposites
Chair: Viviana Correia Pinto
Ref:
Title and Author (s)
#20
Effect of clay modifier on the rheometric behavior
and mechanical/thermal aging properties of
styrene-butadiene rubber-clay nanocomposites
E. M. Sadek, D. E. El-Nashar, S.M.Ahmed
#42
A comparative study of nanotube-epoxy
interphasial interaction in CNT and TNT-epoxy
matrix nanocomposites
G.C. Papanicolaou, D.V. Portan
#43
#46
#55
LUNCH
41
Lounge
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
TUE
Session 2A
Room A
14:15-15:30
TOPIC: Polymers and Polymer Matrix Composites
Chair: Gabriel Jiga
Ref:
Title and Author (s)
#7
Fiber length influence and filament interaction on
single and multifilaments
Alexander Maier, Armin Salimi, Ralf Schledjewski
#22
#68
#77
#59
TUE
Session 2B
Room B
14:15-15:30
TOPIC: NDT-NDI techinques & others
Chair: Paulo Tavares
Ref:
Title and Author (s)
#35
Digital image correlation measurements in
an innovative railway car body underframe
3-point bending test
Tiago Ramos, Shayan Eslami, Paulo J.
Tavares, P. M. G. P. Moreira
#36
Digital image correlation for structural
health monitoring of an innovative
proposal for seismic resistant structures
Tiago Ramos, Andr Furtado, Shayan
Eslami, Sofia Alves, Hugo Rodrigues,
Antnio rede, Paulo J. Tavares, P.M. G. P.
Moreira
#70
Wireless strain gauge for composite
materials
melko Miroslav, Praslika Duan,
Draganov Katarna, Lipovsk Pavol, Kn
Viktor, Bajs Jn
#71
Influence of ultrasounds in the damping
capacity of aluminium alloys
H. Puga, V.H. Carneiro
#19
COFFEE-BREAK
42
Lounge
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
TUE
Session 3A
16:00-17:30
TOPIC: Analytical and Numerical Modeling I
Chair: Srgio Tavares
Ref:
#3
#4
#6
#30
#92
#11
Room
A
TUE
Session 3B
Room
16:00-17:30
B
TOPIC: Polymer Matrix Composites, Sandwich and Green
Composite Structures
Chair: George Papanicolaou
Ref:
Title and Author (s)
#81
Development of composite materials database for
aerospace certification
Ho-Sung Lee, Kyung-Ju Min
#82
#84
#52
#8
POSTER SESSION
Exhibition Area
WELCOME RECEPTION
COCKTAIL RECEPTION
by courtesy of Taylors
Taylors Port
43
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
COFFEE-BREAK
Lounge
LUNCH
44
Lounge
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
WED
Session 4A
14:15-15:30
Room
A
TOPIC: Fatigue
Chair: Stefan Dan Pastrama
Ref:
Title and Author (s)
#18
Crack initiation analysis under mean stress effect in
2024 T351 Al-alloy
Mustapha Benachour, Nadjia Benachour, Mohamed
Benguediab
#28
Stress intensity factors of a compact mixed mode
specimen: finite element analysis
S. M. O. Tavares, D. Peixoto, P. J. Tavares, P.M.G.P.
Moreira
#85
Comparison between three fatigue damage models
and experimental results for composite materials
submitted to spectrum loading
Mohammed Bousfia, M. Aboussaleh, B. Ouhbi
#86
Fatigue Analysis of a Hopper Knuckle Connection of
a 181k Ton DWT Bulk Carrier under Global and Local
Loads
V K Kapnopoulou, P A Caridis
#62
Study of effect of R-ratio on fatigue crack growth
using Artificial Neural Network
K.N.Pandey, Chetan Swaroop
WED
Session 4B
Room
14:15-15:30
B
TOPIC: Manufacturing Techniques
Chair: Pedro Moreira
Ref:
Title and Author (s)
#14
Viability analysis of double cold wire gas metal arc
welding process
R. A. Ribeiro, P. D'Angelo Assuno, E.M. Braga
#34
#89
#73
#88
COFFEE-BREAK
45
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Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
WED
Session 5A
Room
16:00-17:30
A
TOPIC: Analytical and Numerical Model II
Chair: Paulo Tavares de Castro
Ref:
Title and Author (s)
#78
Three dimensional free vibration analysis of rotating
Functionally Graded cylindrical shells in thermal
environment
Abbas Ali Jami,Esmaeil Bahmyari
#5
#16
#72
#76
WED
Session 5B
16:00-17:30
TOPIC: Testing II
Chair: Jos Correia
Ref:
Title and Author (s)
#63
Effect of aluminosilsesqioxane addition and
various curing conditions on the
thermomechanical properties of glass fiber
reinforced epoxy composite
Danuta Matykiewicz, Mateusz Barczewski, Beata
Dudziec
#75
Validation of the dynamic behavior of composite
materials with discontinuities
Mihaela Sava, Anton Hadr, Ioan Pruanu,
Florin Baciu, Stnescu Marius Marinel
#90
#65
#66
#1
BANQUET
46
Room
B
Casa da Msica
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
COFFEE-BREAK
Lounge
LUNCH
47
Lounge
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
THU, 14:15-15:30
Session 6
Room Newton
TOPIC: Degradation, durability and corrosion
Chair: Rui Miranda Guedes
Ref:
Title and Author (s)
The electrochemical investigation on corrosion behavior of two titanium aluminide in aqueous
#23
#24
#25
#74
#87
environments
Alexandra Banu, Marcu Maria, Alexandru Paraschiv, Oana Trusca
New coatings for short-term oxidation protection of titanium aluminide at 850C
Maria Marcu, Alexandra Banu, Luminita Georgescu,Cristina Juganaru
DSC analysis of titanium aluminde correlated with short term oxidation behavior
Alexandra Banu, Marcu Maria, Elena Anghel, Cristian Doicin
Degradation analysis of fiber-metal laminates under service conditions to predict their
durability
A.Viandier, D. Stefaniak, C. Hhne, M. Sinapius
A complete characterization study of anomalous behaviour of hygrothermally aged FRPs
Sotirios A. Grammatikos, Mark Evernden
THU, 15:30-16:00
COFFEE-BREAK
THU, 16:00-17:00
Session 7
TOPIC: Polymers and Polymer Matrix Composites II
Chair: Daniel F. O. Braga
Ref:
Title and Author (s)
Stable and degradable all-aliphatic polyurethane elastomers
#2
#10
#95
Lounge
Room Newton
Milena prkov, Magdalena Serkis, Rafa Porba, Ji Hodan, Jana Kredatusov, Luka
Machov, Dana Kubies
The accelerated effect of nanoparticles on the degradation of the thermomechanical
properties of a bio-based polymer
Evagelia Kontou
Optimization of the hybrid viscoelastic interphase model
Psarra Erato, Papanicolaou George
CLOSING SESSION
Conference Organizing Committee
48
Room Newton
Book of abstracts of the 6th International Conference on Structural Analysis and Advanced Materials__________________________________________________
POSTER SESSION
Exhibition Area
Dynamic mechanical properties of PLA and PLA/CNT-COOH biodegradable nanocomposites thin film
Viviana Correia Pinto, Marta Martins, Nuno Rocha, Rui Miranda Guedes
Experimental and numerical analysis of creep and stress relaxation behaviour of PLA-PCL fibres
Ctia Martins, Viviana Correia Pinto, Rui Miranda Guedes, Antnio T. Marques
Preparation of PVP Polymer Electrolytes and their Application in Solid State Dye Sensitized Solar Cells
D.I. Giannopoulos, D.A. Chalkias, G.C. Papanicolaou
Low energy impact and post impact behavior of epoxy matrix-woven flax fabric composites
D.A. Chalkias, A.F. Koutsomitopoulou, G.C. Papanicolaou
Strain rate effects in micro and nano TiO2 epoxy resin particulate composites
A.E. Manara, L.C. Kontaxis, G.C. Papanicolaou
Thermal Shock Cycling Effect on the Flexural Stress Relaxation Behavior of Glass-Epoxy Composites
E.A. Tsiangou, L.C. Kontaxis, G.C. Papanicolaou
The double role of fibers as reinforcements and heating elements for polymer curing in thermoset matrix-fiber
composites
I. E. Chontzoglou, L.C.Kontaxis, G.C. Papanicolaou
Modeling the Mechanical Degradation Due to Moisture Absorption in Polymer Matrix Composites
P.D. Fotou, G.C. Papanicolaou
Modeling and Experimental Investigation of the inclusion geometry and concentration effect on the quasistatic properties of a semi-green epoxy matrix
F.K. Kozaniti, L.C. Kontaxis, G.C. Papanicolaou
Development of a Starch Reinforced Chios mastic- olive oil matrix new green composite material
D.E. Anastasiou, L.C. Kontaxis, G.C. Papanicolaou
Nitinol layered composites: manufacturing and electrical properties
E.J. Pappa, G.C. Psarras, D.V. Portan, G.C. Papanicolaou
Thermomechanical characterization of epoxy/carbon black/graphene oxide hybrid nanocomposites
A. Stimoniaris, D. Gournis, M. Karakassides, C. Delides
Monitoring the fly ash dispersion in epoxy matrix and its effect on the thermomechanical properties of the
obtained composites
Adamos Stimoniaris, Haralampos Zois, Athanasios Kanapitsas, Michael Karakassides, Constaninos Delides
Effect of pigments addition on properties of the isotactic polypropylene
Mateusz Barczewski, Bartomiej Hoffmann
Use of Different Acids for the Extraction of Chromium Contained in Ash from the Incineration of Waste Leather
Alexandru Ghiban, Brandusa Ghiban, Nicolae Serban, Cristina Maria Bortun
Hydrogen gas sensors based on Palladium/Silicon Oxide/Ailicon Carbide sandwich structures
Jenica Neamtu, Florea Craciunoiu, Dragos Ovezea, Razvan Pascu
Differences in degradation mechanism of the standard and the new - core-shell catalyst during ammonia
oxidation process
Jarosaw Pura, Piotr Kwasniak, Halina Garbacz, Joanna Zdunek, Zbigniew Laskowski, Maciej Gierej
Relationship chemical surface treatments for aluminum structural bond strength
Vinov Lenka, Jarmil Vlach, Konek Jan
Influence of temperature on mechanical properties of polypropylene sandwich panel and compare the
mechanical properties of the aluminum honeycomb panels
Lukasova Vera, Kavan Pavel
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Abstracts
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
Session 1A
TUE, 11:30-12:45
Room A
TOPIC: Testing I
Chair: Mrio Vaz
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#15
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#26
ABSTRACT
The literature presents several results as respects to multiaxial tests of stress concentrators
specimens. Different types of specimens were used accordingly to the stress triaxiality as follows:
butterfly specimen for high stress triaxiality degree, plane specimen for medium state of triaxiality
and cylindrical specimen for low degree of triaxiality. This paper proposes theoretical and
experimental study on two types of specimens: cylindrical and plane (flat) specimens with stress
concentrators.
a)
b)
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
a)
b)
Fig. 3. a) Shear stress of the area with stress concentrators ; b) Principal directions of the stresses.
This article shows the results of experimental determinations, finite element analysis and
theoretical study of two types of specimens and it aims to obtain high stress state in failure
section (volume), more uniform stress distribution and stress ratio to be constant till failure.
References
[1] M. DUNAND, D. MOHR: ON THE PREDICTIVE CAPABILITIES OF THE SHEAR MODIFIED GURSON
AND THE MODIFIED MOHRCOULOMB FRACTURE MODELS OVER A WIDE RANGE OF STRESS
TRIAXIALITIES AND LODE ANGLES, JOURNAL OF THE MECHANICS AND PHYSICS OF SOLIDS 59
(2011), PP. 13741394.
[2] L. MALCHER, E.N. MAMIYA: AN IMPROVED DAMAGE EVOLUTION LAW BASED ON
CONTINUUM DAMAGE MECHANICS AND ITS DEPENDENCE ON BOTH STRESS TRIAXIALITY AND
THE THIRD INVARIANT, INTERNATIONAL JOURNAL OF PLASTICITY 56 (2014), PP. 232261.
[3] P. ALLEN: MASTERS THESIS: HYDROSTATIC STRESS EFFECTS IN METAL PLASTICITY, JULY 20,
2000.
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#66
,2
Currently, both removable and fixed prostheses are made from Co-Cr-Mo alloys, which possess
good corrosion resistance owing to the appropriate microstructure, but present low
machinability. Occasionally, allergic responses to the constituents of the base metal alloys are
observed. However most adverse tissue reactions attributed to the wearing of a base metal
removable prosthesis, were manifestations of an improper design or a poor fit. Being the major
component, cobalt imparts to the alloy its intrinsic corrosion resistance. On the other side, Ti is
one of the best biocompatible metals and is widely used as implant. In addition, the total weight
of a prosthesis can be reduced by Ti incorporation in the alloy composition. The purpose of this
paper is to develop new dental materials with superior mechanical performance and corrosion
resistance as well as high biocompatibility. The attention was focused on the possibility to obtain
a new class of cobalt based alloy by Ti addition. Different compositions of the CoCrMo base
system were produced in a cold crucible melting furnace, in argon protective atmosphere. The
present paper take in consideration the fomability behaviour of these alloys. The investigations
were carried out in laboratory conditions by investigation the upsetting behaviour in a range of
temperature about 950-1300C. The tested samples were analysed at stereomicroscope and
scaning microscope. Finaly it was established the best range of temperature for hot plastic
forming of these class of material.
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
Fig.1: Outline of specimen preparation: 1) Addition of particles in the epoxy. 2) Mechanical mixing by hand
at room temperature for 30 min. 3) Addition of the curing agent and mixing. 4) Making of the GF and CF
reinforced laminas. 5) Preparation of the unmodified and modified CFRP and GFRP laminates by the hand
o
lay-up method. 6) Curing at room temperature for 24 h and at 60 C for 10 h.
Material Groups
Plies
16
% wt healing agent
Mechanical Experiments
7%
7%
Table 1. Material groups, number of plies, % wt of the healing agent in the matrix and type of experiments.
References
[1] G. WILLIAMS, R. TRASK, I. BOND, A SELF-HEALING CARBON FIBRE REINFORCED POLYMER FOR
AEROSPACE APPLICATIONS, COMPOSITES: PART A, 38; 1525-1532 (2007).
[2] J. BAUR, E. SILVERMAN, CHALLENGES AND OPPORTUNITIES IN MULTIFUNCTIONAL
NANOCOMPOSITE STRUCTURES FOR AEROSPACE APPLICATIONS, MRS BULLETIN, 32; 328-334
(2007).
[3] K. LOH, D. RYU, MULTIFUNCTIONAL MATERIALS AND NANOTECHNOLOGY FOR ASSESSING
AND MONITORING CIVIL INFRASTRUCTURES, SENSOR TECHNOLOGIES FOR CIVIL
INFRASTRUCTURES, 1; 295-326 (2014).
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
Session 1B
TUE, 11:30-12:45
Room B
TOPIC: Nanocomposites
Chair:Vivana Correia Pinto
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#20
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
References
[1] B. OREGAN, M. GRATZEL, A LOW-COST, HIGH-EFFICIENCY SOLAR CELL BASED ON DYE
SENSITIZED COLLOIDAL TIO2 FILMS, NATURE 353 (1991) 737.
[2] Y. YAN, J. WANG, Q. CHANG, M. BABIKIER, H. WANG, H. LI, Q. YU, S. GAO, S. JIAO,
FABRICATION OF MESOPOROUS TIO2 ELECTRODES BY CHEMICAL TECHNIQUE FOR DYE-SENSITIZED
SOLAR CELLS, ELECTROCHIMICA ACTA 94 (2013) 277.
[3] Z. LAN, J. WU, J. LIN, M. HUANG, A HIGHLY EFFICIENT DYE-SENSITIZED SOLAR CELL WITH A
BLOCKING LAYER AND TICL4 TREATMENT TO SUPPRESS DARK REACTION, ENERGY SOURCES, PART
A: RECOVERY, UTILIZATION AND ENVIRONMENTAL EFFECTS 36 (2014) 1810.
[4] K.-J. HWANG, D.-W. PARK, S. JIN, S. O. KANG, D. W. CHO, INFLUENCE OF DYE CONCENTRATION
ON THE LIGHT SCATTERING EFFECT IN DYE-SENSITIZED SOLAR CELL, MATERIALS CHEMISTRY AND
PHYSICS 149 (2015) 594.
[5] H. LIU, L. LIANG, T. PENG, H. F. MEHNANE, B. SEBO, S. BAI, Z. YU, W. YU, W. LIU, S. GUO, X.
ZHAO, ENHANCE THE PERFORMANCE OF DYE-SENSITIZED SOLAR CELLS BY BALANCING THE LIGHT
HARVESTING AND ELECTRON COLLECTING EFFICIENCIES OF SCATTERING LAYER BASED
PHOTOANODES, ELECTROCHIMICA ACTA 132 (2014) 25.
[6] T. SAWATSUK, A. CHINDADUANG, C. SAE-KUNG, S. PRATONTEP,G.TUMCHARERN, DYESENSITIZED SOLAR CELLS BASED ON TIO2MWCNTS COMPOSITE ELECTRODES: PERFORMANCE
IMPROVEMENT AND THEIR MECHANISMS, DIAMOND & RELATED MATERIALS 18 (2009) 524.
[7] W. FENG, Y. FENG, Z. WU, A. FUJII, M. OZAKI, K. YOSHINO, OPTICAL AND ELECTRICAL
CHARACTERIZATIONS OF NANOCOMPOSITE FILM OF TITANIA ADSORBED ONTO OXIDIZED
MULTIWALLED CARBON NANOTUBES, JOURNAL OF PHYSICS: CONDENSED MATTER 17 (2005)
4361.
[8] H. H. KYAW, T. BORA, J. DUTTA, ONE-DIODE MODEL EQUIVALENT CIRCUIT ANALYSIS FOR ZNO
NANOROD-BASED DYE-SENSITIZED SOLAR CELLS: EFFECTS OF ANNEALING AND ACTIVE AREA, IEEE
TRANSACTIONS ON NANOTECHNOLOGY 11 (2012) 763.
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References
[1] PAPANICOLAOU, G. C.; ZAOUTSOS, S. P.; CARDON A.H., FURTHER DEVELOPMENT OF A DATA
REDUCTION METHOD FOR THE NONLINEAR VISCOELASTIC CHARACTERIZATION OF FRPS.
COMPOSITES, PART A, 1999, 30 (7), 839-848.
[2] PAPANICOLAOU, G. C.; XEPAPADAKI, A. G.; PAVLOPOULOU, S.; ZAOUTSOS, S. P. ON THE
INVESTIGATION OF THE STRESS THRESHOLD FROM LINEAR TO NONLINEAR VISCOELASTIC
BEHAVIOUR OF POLYMER-MATRIX PARTICULATE COMPOSITES. MECH. TIME-DEPEND. MATER.,
2009, 13 (3), 261-274.
[3] PAPANICOLAOU, G. C.; KONTAXIS, L. C.; KOUTSOMITOPOULOU, A. F.; ZAOUTSOS, S. P. STRESS
RELAXATION BEHAVIOR OF STARCH POWDEREPOXY RESIN COMPOSITES. J. APPL. POLYM. SCI.,
2015.
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#55
In 1999 it was reported that porous TiO2 nanostructures could be fabricated by electrochemically
anodizing a Ti sheet in an acid electrolyte containing a small amount of hydrofluoric acid (HF).
Since then, many research groups have paid considerable attention to this field; because
anodization opens up ways to easily produce closely packed tube arrays with a self-organized
vertical alignment (Fig. 2) [3]. Depending on several experimental parameters combination,
different TiO2 nanotubes geometries can be obtained. These parameters include time of
anodization, type of electrolyte used, voltage applied, etc. In the present investigation, a specific
combination of the above parameters has been selected in order to develop nanotubes with
optimum geometry and achieve single lap adhesive joints with high bonding strength. Bond
strength is studied by means of three point bending experiments while nanostructural topography
is investigated by means of SEM observations.
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References
[1] A.M. PEREIRA, J.M. FERREIRA, F.V. ANTUNES, P.J. BRTOLO (2010) ANALYSIS OF
MANUFACTURING PARAMETERS ON THE SHEAR STRENGTH OF ALUMINIUM ADHESIVE SINGLELAP JOINTS, JOURNAL OF MATERIALS PROCESSING TECHNOLOGY 210, 610617
[2] T.C. SILVA, L.C.S NUNES (2014) A NEW EXPERIMENTAL APPROACH FOR THE ESTIMATION OF
BENDING MOMENTS IN ADHESIVELY BONDED SINGLE LAP JOINTS, INTERNATIONAL JOURNAL OF
ADHESION AND ADHESIVES VOLUME 54, PAGES 1320
[3] D. V. PORTAN, K. PAPAEFTHYMIOU, E. ARVANITA, G. JIGA, G. C. PAPANICOLAOU (2012) A
COMBINED STATISTICAL AND MICROSCOPIC ANALYSIS OF TIO2 NANOTUBES SYNTHESIZED UNDER
DIFFERENT ELECTROCHEMICAL ANODIZING CONDITIONS, J MATER SCI (2012) 47:4696-4705
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Session 2A
TUE, 14:15-15:30
Room A
TOPIC: Polymers and Polymer Matrix Composites I
Chair: Gabriel Jiga
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#7
Recently, the need for high-performance, low-weight structures has been growing and the
demand for polymer matrix composites (PMCs) that have high specific strength and stiffness will
continue to grow. Glass fibers are the most widely used reinforcement in PMCs. Approximately
90% of PMC products contain glass fibers. Glass fiber-reinforced plastics (GFRPs) are used to
manufacture various products such as fishing rods, storage tanks, and marine structures. It has
been reported that glass fibers show unique characteristics during manufacturing. The mechanical
performance of these composites results not only from a combination of the fiber and matrix
properties and the ability to transfer stresses across the fibermatrix interface. It is well known
that the strength of glass fibers increases with increasing strain rate. However for constant strain
rates other phenomena may exist which decrease the tensile strength further on. For example
variables such as the fiber content, diameter, orientation and the interfacial strength depending
on the free fiber length are of prime importance to the final balance of mechanical properties and
especially for the manufacturing of composite parts. As another property during manufacturing
the interaction of filaments for example tow friction becomes more and more an important
mechanism in the production and processing of high performance parts.
For example the continuous manufacturing processes the Winding - Process has to deal with
different dry roving lengths at the feeding system of the machine before the actual
manufacturing. In addition to that a necessary load on the roving bundle must be supplied to gain
good manufacturing results in the end. In actual winding processes it often appears that the
preloaded fiber bundle fails to a lower strength than the given tensile strength out of the data
sheet. The reason for such a behavior is a combination of free fiber length and in that case a
change in the statistical distribution of the tensile strength, the necessary preload on the fibers
and the interaction between filaments during the tensile load [1-3].
Tensile strength of glass fibers exhibits statistical Weibull type distribution and significant size
dependence. In the present work besides the size effect a possible length dependency will be
investigated for tow bundles and single filaments. These analyses will be based on the needs of
manufacturer for continuous manufacturing processes. As very import information the maximum
strength of dry fiber filaments depending on the actual fiber length will be investigated. This is
crucial for adjusting the feeding system of the reinforcements to the actual manufacturing
machine.
For the first part in this work, a systematic analysis of glass fiber samples with different lengths
influencing the mechanical strength of fiber bundles and single filaments will be introduced.
Therefore the statistical number of voids based on the different manufacturing of glass fibers will
be discussed and additional to that the influence of the raising number of voids based on the
raising testing sample dimension will be taken into consideration. As a next step glass fibers were
tested with different gauge lengths. The length effect will be analyzed based on the Weibull
statistics. As a next step the interaction between filaments (Fig. 1) during the tensile load will be
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
investigated and the result will be taken into consideration to describe the performance of fiber
bundles during manufacturing.
Fig. 1 Filament interaction depending on free fiber length during tensile test
References
[1] J.L. THOMASON. THE INFLUENCE OF FIBER LENGTH, DIAMETER AND CONCENTRATION ON
THE IMPACT PERFORMANCE OF LONG GLASS-FIBER REINFORCED POLYAMIDE 6,6.
COMPOSITES: PART A 40 (2009) 114124
[2] N. SATO, T. KURAUCHI, S. SATO, O. KAMIGAITO. REINFORCING MECHANISM BY SMALL
DIAMETER FIBER IN SHORT FIBER COMPOSITES.
J COMPOS MATER 1998;22:85073.
[3] B. CORNELISSEN, B. RIETMAN, R. AKKERMAN. FRICTIONAL BEHAVIOUR OF HIGH
PERFORMANCE FIBROUS TOWS: FRICTION EXPERIMENTS.
COMPOSITES: PART A 44 (2013) 95104
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#22
Emerging Materials Research Unit, Faculty of Technology, University Ferhat Abbas 1, Stif
19000, Algeria, amelhamma@yahoo.fr
3
Department of Industrial Engineering, University of Trento, Polo Scientifico e Technologico,
F.Ferrari, Via Sommarive 9, 38123 Trento, Italy
ABSTRACT
In this study, a comparison between the degradation behaviour of starch-grafted-polypropylene
reinforced with 30 %.wt of kenaf fibres (S-g-PP/KF) and the virgin matrix (S-g-PP) were carried out,
when materials were subjected to outdoor weathering. The morphology of weathered samples
has shown a discoloration and cracking after 5 months of exposure (Fig.1-a, b, c, d). This is due to
wetting and drying cycles between the exposed surfaces and interior sections and probably to the
degradation of exposed materials [1].
(a) S-g-PP before aging
Fig. 1 Micrographs of unweathered a)- S-g-PP matrix & b)- S-g-PP/KF composite and 160 days outdoor
weathered c)- S-g-PP & d)- /KF composites.
The evolution of crystallinity index of S-g-PP and its composite (Fig.2) has shown an increase in
values with exposure time. This explains retrogradation phenomena of the matrix containing
starch, induced by the climatic conditions such as the high humidity % 60% and the low
temperature range (0-5C) above Tg values. However, composite crystal linity was more affected
by weathering than the net matrix.
Fig. 2 Evolution of the crystallinity index of S-gPP & S-g-PP/KF with exposure period
Youngs modulus evolution as illustrated in Fig.3, exhibited a decrease for both, matrix and its
composite, with outdoor weathering. However, neat matrix was less affected for exposure period
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
less than 2 months (-30% decrease), than the composite (-60% decrease). After that, matrix
modulus still decrease, while, composite ones were found to increase. The same trend was also
observed for the tensile stress at break (Fig.4). This behaviour could be explained, in one side, by
the changes in samples crystallinity directly affecting the modulus of composite [2]. And on
another side, to the decrease in molecular weight and macromolecular chain length due to C-C
bond cleavage occurring in the S-g-PP samples [3]. This affected the deformation of samples
which is reduced progressively for the neat samples as shown in Fig.5.
Fig. 4 Evolution of tensile stress of S-g-PP & S-gPP/KF with exposure period
Fig. 5 Evolution of tensile strain of S-g-PP & S-gPP/KF with exposure period
For short outdoor weathering periods (below 2 months), all exposed samples display a drop off in
h*, which is less pronounced. For longer ones (beyond 2 months), the viscosity still decreases for
neat matrix samples, however, composite ones have shown closest values as unweathered one.
This behaviour indicates a competition between crosslinking reactions and chain scissions
degradation mechanism, at the later degradation stages for composite samples, against chain
scission reactions governing the degradation mechanism of neat matrix.
b)
a)
Fig. 6 Complex viscosity dependency of a) S-g-PP & b) S-g-PP/KF before and after outdoor weathering
References
[1] TEMIZ A, YILDIZ UC, AYDIN I, EIKENES M, ALFREDSEN G, OLAKOGLU G. APPLIED SURFACE
SCIENCE. 2005;250(14):35-42.
[2] ZHOU J, MA Y, ZHANG J, TONG J. JOURNAL OF APPLIED POLYMER SCIENCE.2009;112(1):99106.
[3] RABELLO MS, TOCCHETTO RS, BARROS LA, DALMEIDA JRM, WHITE JR. PLASTICS, RUBBER AND
COMPOSITES 2001;30 (3):132-40.
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The objective of this work is in a first time, the synthesis of materials geopolymers from two types
of activator solutions concentrated prepared respectively with two different bases NaOH and
KOH. These solutions have been mixed thereafter (after 24 hours) with the kaolin previously
heated under 550C in order to obtain geopolymers samples, while optimizing the Si/Al ratio.
Secondly, the study of the influence of the partial and total substitution of the metakaolin by a
portland cement is thrown in the goal to decrease the delays of hold (beginning and end) of the
gopolymer material at the fresh state. Thereafter, the physical (bulk density) and mechanical
properties of the samples at hardened state, notably the constraints limit of compression and the
resistances in traction are investigated.
The results showed that the use of the activator solution containing KOH during the preparation
of the activator solution increases the solubility between KOH and silica gel. However, the
solution based on sodium hydroxide (NaOH) promotes obtaining better mechanical resistances in
the geopolymer materials. Otherwise, the partial substitution of metakaolin by cement portland
improves the mechanical resistances on compression but to a certain doorstep before inverse
effect appears.
Finally, recommendations and perspectives are proposed in adequacy with the used raw materials
and the mechanical performances of the geopolymers materials.
References
ALCNTARA E, CHEESEMAN CH, KNIGHT J, LOIZIDOU M., 2000. PROPERTIES OF ALKALI-ACTIVATED
CLINOPTILOLITE. CEM CONCR RES; 30: 16416.
BAKHAREV T., 2005. GEOPOLYMER MATERIALS PREPARED USING CLASS F Y ASH AND ELEVATED
TEMPERATURE CURING. CEM CONCR RES; 35:12241232.
BAKHAREV T, SANJAYAN J, CHENG Y., 2002. SULFATE ATTACK ON ALKALI-ACTIVATED SLAG
CONCRETE. CEM CONCR RES; 32:2116.
DAVIDOVITS. J., 1994. GEOPOLYMERS: MAN-MADE ROCKS GEOSYNTHESIS AND THE RESULTING
DEVELOPMENT OF VERY EARLY HIGH STRENGTH CEMENT, J. MATER. EDUC. 16: 91139.
MARTNEZ-RAMREZ S, BLANCO-VARELA MT, EREA I, GENER M., 2006. POZZOLANIC REACTIVITY
OF ZEOLITIC ROCKS FROM TWO DIFFERENT CUBAN DEPOSITS: CHARACTERIZATION OF REACTIONS
PRODUCTS. APPL CLAY SCI; 32: 4052.
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Department of petroleum applications, Egyptian Petroleum Research Institute, Nasr city, 11727,
Cairo, Egypt, basharosh_00@yahoo.com
ABSTRACT
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Rosin is a suitable candidate for preparing liquid crystalline epoxy curative and resin. The fully biobased system show good dynamic mechanical properties and thermal stability.
Acknowledgements
This project was supported financially by the Science and Technology Development Fund (STDF),
Egypt, Grant No. 4225.
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ABSTRACT
Polymer composites are widely used in engineering fields due to their specific properties.
However, deteriorations generated in service cause catastrophic failure in materials. In view of
this, scientists have drawn inspirations by natural biological systems and their ability to heal an
external wound, to develop a similar repair system within a material. The aim is to reduce the
repeated repairs and extend the life time of the materials, without compromising the overall
mechanical performance. In light of this issue, self healing composites attract a considerable
interest for their potential to undertake an autonomous in situ repair of damage [1-2]. Several
conceptual approaches for implementing self healing functionality within a material have already
been explored and reported the past ten years. Self healing materials can be classified in two
main categories: (i) the intrinsic, where polymers are able to heal themselves under chemical
interactions, (ii) the extrinsic in which the healing system is stored and incorporated into the
material in advance. The first category utilizes the inherently reversible bonding in the matrix
polymer to affect healing via thermally reversible reactions [3]. The second can be separated in
two basic different modes: microcapsules containing a healing system that will be released upon
crack damage and an embedded vascular network which serves as reservoir for the distribution of
the healing system. Implementing the healing functionality during manufacturing process, healing
activation upon damage and monitoring are the main domains to be considered in the design of
self healing composites. The present study assesses the feasibility to implement the self healing
functionality within a composite material, during manufacturing, in a repeatable manner. Ideally,
this process could be achieved with the minimal disruption of the final composite in terms of its
structural integrity.
Fig. 1 Schematic of (a) Self healing strategies (b) self healing stage
he reversible polymers direction consists of three main material categories. The first category
includes polymers that are based on covalent bonds while the second regards the materials based
on Diels Alder and Retro Diels-Alder reaction. The third category encompasses materials based on
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References
[1] BLAISZIK B.J., KRAMER S.L.B., OLUGEBEFOLA S.C., MOORE J.S., SOTTOS N.R., WHITE S.R., " SELF
HEALING POLYMERS AND COMPOSITES", ANNUAL REVIEW OF MATERIALS RESEARCH, 2010,
40:179-211
[2] WU D.Y., MEURE S, SOLOMON D., " SELF-HEALING POLYMERIC MATERIALS: A REVIEW OF
RECENT DEVELOPMENTS", PROGRESS IN POLYMER SCIENCE, 2008, 33:479-522
[3] PINGKARAWAT K., BHAT T., CRAZE D. A., WANG C. H., VARLEY R. J., AND MOURITZ A. P.,
''HEALING OF CARBON FIBRE-EPOXY COMPOSITES USING THERMOPLASTIC ADDITIVES'', POLYMER
CHEMISTRY, 2013,10:1039
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Session 2B
TUE, 14:15-15:30
Room B
TOPIC: NDT-NDI techniques and others
Chair: Paulo Tavares
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Fig. 1 Strain in y direction (yy) comparison between simulation and DIC measurements for the last
monitored step.
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Corner Crushing
Fig. 2 Displacement field, strain field and detailed view for the right half of the wall, in the in-plane test.
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Fig. 3 LVDT and DIC results comparison for both in-plane and out of plane tests.
References
[1] H. R. H. V. A. C. A. J. M. S. R. VICENTE, "PERFORMANCE OF MASONRY ENCLOSURE WALLS:
LESSONS LEARNED FROM RECENT EARTHQUAKES," EARTHQUAKE ENGINEERING AND VIBRATION,
VOL. 11, NO. 1, PP. 23-34, 2012.
[2] C. C. A. A. A. H. R. ANDR FURTADO, "GEOMETRIC CHARACTERISATION OF PORTUGUESE RC
BUILDINGS WITH MASONRY INFILL WALLS," EUROPEAN JOURNAL OF ENVIRONMENTAL AND CIVIL
ENGINEERING, VOL. IN PRESS, 2015.
[3] J. V. H. S. D. LECOMPTE, "CRACK DETECTION IN A CONCRETE BEAM USING TWO DIFFERENT
CAMERA TECHNIQUES," STRUCTURAL HEALTH MONITORING, VOL. 5, NO. 1, PP. 59-68, 2006.
[4] J. B. F. P. F. H. MICHEL KNTZ MARC JOLIN, "DIGITAL IMAGE CORRELATION ANALYSIS OF
CRACK BEHAVIOUR IN A REINFORCED CONCRETE BEAM DURING A LOAD TEST," CANADIAN
JOURNAL OF CIVIL ENGINEERING, VOL. 33, NO. 11, PP. 1418-1425, 2006.
[5] E. T. E. F. J. F. DESTREBECQ, "ANALYSIS OF CRACKS AND DEFORMATIONS IN A FULL SCALE
REINFORCE CONCRETE BEAM USING A DIGITAL IMAGE CORRELATION TECHNIQUE,"
EXPERIMENTAL MECHANICS, VOL. 51, PP. 879-890, 2011.
[6] N. M. A. H. SALMANPOUR, "APPLICATION OF DIGITAL IMAGE CORRELATION FOR STRAIN
MEASUREMENTS OF LARGE MASONRY WALLS," APCOM & ISCM, ZURICH, 2013.
[7] F. M. M. A. S. R. GHORBANI, "FULL-FIELD DEFORMATION MEASUREMENT AND CRACK
MAPPING ON CONFINED MASONRY WALLS USING DIGITAL IMAGE CORRELATION,"
EXPERIMENTAL MECHANICS, VOL. 55, PP. 227-243, 2014.
[8] M. J. E. G. ABRAHAM SAVITSKY, "SMOOTHING AND DIFFERENTIATION OF DATA BY SIMPLIFIED
LEAST SQUARES PROCEDURES," ANALYTICAL CHEMISTRY, VOL. 36, NO. 8, PP. 1627-1639, 1964.
[9] Y. Z. VYACHESLAV V. VOLKOV, "DETERMINISTIC PHASE UNWRAPPING IN THE PRESENCE OF
NOISE," OPTIC LETTERS, VOL. 28, NO. 22, 2003.
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ABSTRACT
The article deals with the possibility of wireless sensor creation with magnetic microwires
embedded in a composite material. Conventional strain gauge measuring methods cover surface
stress measurement, however measurement inside the material is limited. Strain gauges have one
significant disadvantage - galvanic connection between sensor and sensing device. Magnetic
microwires [1] offer the ability to create a built-in sensor inside the material. No galvanic
connection is needed and no structure violation will occur. Moreover, sensor itself reacts to
several physical quantities [2] and special measuring method allows us the possibility to measure
this parameters simultaneously. These advantages make this technology application very
perspective and interesting [3]. Experimental results confirm this statement and are discussed in
the article.
References
[1] A.V. ULITOVSKI, METHOD OF CONTINUOUS FABRICATION OF MICROWIRES COATED BY GLASS
RU PATENT NO128427, (3.9.1950)
[2] R. SABOL, R. VARGA, J. HUDAK, J. BLAZEK, D. PRASLICKA ET AL. , J. APPL. PHYS. 111.
053919(2012)
[3] M. SMELKO, D. PRASLICKA, J. BLAZEK , ICMT 2013, P. 1521-1525. - ISBN 978-80-7231-918-3
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ABSTRACT
The use of light-alloys is necessary in specific applications that require both mechanical strength,
reduced system mass and high damping characteristics. This is the case of industrial fields such as
aerospace, aeronautics, railway and transportations in general. As the value per added structural
weight in this fields may be extremely high, it is mandatory to select materials with low density
that are able to sustain structural loads [1]. Additionally, the life expectance of mechanical
components and the noise that is generated by this structures when they are subjected to
dynamic loads is directly related to the damping capacity of the materials. Thus, it is necessary to
develop techniques that can improve the referred characteristic in materials, for example by
microstructural modification of the base material [2]. In this study, was evaluated the effect of
Ultrasound grain refinement [3] in the Al7075 alloy and if this technique is a viable and an
interesting opportunity to be used in the production of light-weight structural components with
enhanced damping capacity. The referred technique is applied directly to the metal mold were
the liquid metal is casted [4], forming ingots from which the samples are drawn. The evaluation of
the enhanced damping capacity is obtained by Dynamic Mechanical Analysis (DMA). This
technique was applied in samples with and without Ultrasound treatment. The values of the
internal friction (tan ) were determined, using a single-cantilever clamping configuration. The
results suggest that the grain refinement, achieved by the Ultrasounds, is able to enhance the
damping capacity of this Aluminium alloy and therefore is an interesting path for further
development and to be applied in the referred industrial fields.
References
[1] E. PHIL, C. SOUTIS (EDS). POLYMER COMPOSITES IN THE AEROSPACE INDUSTRY, ELSEVIER,
2014.
[2] Y. ZHANG, N. MA, Y. LE, S. LI, H. WANG. MECHANICAL PROPERTIES AND DAMPING CAPACITY
AFTER GRAIN REFINEMENT IN A356 ALLOY MATERIALS LETTERS, VOL.59, PP.2174-2177, 2005.
[3] H. PUGA, J. BARBOSA, S. COSTA, S. RIBEIRO, A.M.P. PINTO, M. PROKIC. INFLUENCE OF
INDIRECT ULTRASONIC VIBRATION ON THE MICROSTRUCTURE AND MECHANICAL BEHAVIOR OF
AL-SI-CU ALLOY, MATERIALS SCIENCE AND ENGINEERING A, VOL.560, PP. 589-595, 2013.
[4] N.Q. TUAN, H. PUGA, J. BARBOSA, A.M.P. PINTO. GRAIN REFINEMENT OF AL-MG-SC ALLOY BY
ULTRASONIC TREATMENT, METALS AND MATERIALS INTERNATIONAL, VOL.21 NO.1, PP.72-78,
2015.
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Fig. 1. The experimental equipment (left), the composite sample (up) and the transducers attached (bottom
right)
The finite elements simulation provided information on directivity and signal velocity. The
processed experimental signals revealed the increase of the AE activity, the approximate
localization of cracks locations and values for the signal level. The devices used attach the
transducer to the laminate surface proved to be adequate, even for large displacements/strains.
References
[1] J. KAISER: UNTERSUCHUNG BER DAS AUFTRETEN VON GERUSCHEN BEIM ZUGVERSUCH
(STUDY ON THE OCCURRENCE OF NOISE IN THE TENSILE TEST), PH.D. THESYS, TECHNISCHEN
UNIVERSITT MNCHEN 1950.
[2] A.S. PAIPETIS, D.G. AGGELIS DAMAGE ASSESSMENT IN FIBROUS COMPOSITES USING ACOUSTIC
EMISSION,
ACOUSTIC EMISSION, DR. WOJCIECH SIKORSKI (ED.), ISBN: 978-953-51-0056-0, INTECH, (2012),
AVAILABLE FROM: HTTP://WWW.INTECHOPEN.COM/BOOKS/ACOUSTIC-EMISSION/DAMAGEASSESSMENT-IN-FIBROUS-COMPOSITES-USING-ACOUSTIC-EMISSION
[3] T. BIDLINGMAIER, A. WANNER, S. RITTER, WAVEFORM-BASED ANALYSIS OF ACOUSTIC
EMISSION FROM FIBER FRACTURE IN MODEL COMPOSITE PLATES, REV. PROG. QUANT.
NONDESTR. EVAL., 17, 517-524, 1998
[4] C. G. KOH, G. Q. QIAO, S. T. QUEK, DAMAGE IDENTIFICATION OF STRUCTURAL MEMBERS:
NUMERICAL AND EXPERIMENTAL STUDIES, STRUCT. HEALTH MONIT, 2(1), 4155, 2003.
[5] Z. SU, L, YE, FUNDAMENTAL LAMB MODE-BASED DELAMINATION DETECTION FOR CF/EP
COMPOSITE LAMINATES USING DISTRIBUTED PIEZOELECTRICS, 3(1), 4368, 2004.
[6] J. J. SCHOLEY, P.D.WILCOX,, C.K.LEE, M.I. FRISWELL, M.R.WISNOM, ACOUSTIC EMISSION IN
WIDE COMPOSITE SPECIMENS, ADV. MAT. RES., 13-14, 325-332, 2006.
[7] A.MAL, F. RICCI, S. BANERJEE, F. SHIH, A CONCEPTUAL STRUCTURAL HEALTH MONITORING
SYSTEM BASED ON VIBRATION AND WAVE PROPAGATION, 4(3), 283293, 2005.
[8] S.S. KULKARNI AND J.D. ACHENBACH, STRUCTURAL HEALTH MONITORING AND DAMAGE
PROGNOSIS IN FATIGUE, 7(1), 3749, 2008.
[9] V. GIURGIUTIU, A. CUC, EMBEDDED NON-DESTRUCTIVE EVALUATION FOR STRUCTURAL
HEALTH MONITORING, DAMAGE DETECTION, AND FAILURE PREVENTION, SHOCK VIBR. DIG., 37,
83-105, 2005
[10] D. ALJETS, A. CHONG, S. WILCOX, K HOLFORD, ACOUSTIC EMISSION SOURCE LOCATION IN
PLATE-LIKE STRUCTURES USING A CLOSELY ARRANGED TRIANGULAR SENSOR ARRAY, J. ACOUSTIC
EMISSION, 28, 85-98, 2010.
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Session 3A
TUE, 16:00 -17:30
Room A
TOPIC: Analytical and Numerical Modeling I
Chair: Srgio M. O. Tavares
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#3
In the buildings, the floors play a very important role in the overall seismic behavior of the
structure. They act as horizontal diaphragms, which collect the inertial forces, transmit them to
the vertical structural elements, and make these elements interdependent to resist at the
horizontal seismic action. However, this function depends strongly on their relative rigidity
compared to the one of the vertical resistant veils. For the analysis of structures, diaphragms
(floors) are classified as rigid, flexible and semi- rigid, based on this relative rigidity. If a diaphragm
is considered as rigid, it can distribute horizontal forces to vertical elements in proportion to their
relative rigidities. In this case, the deformation of the diaphragm will be insignificant compared to
the one of the vertical elements. In return, in a flexible diaphragm the distribution of horizontal
forces to vertical elements is independent of their relative rigidity and deformation of the
diaphragm will be substantially large compared to the one of vertical elements. The flexible
diaphragm distributes lateral loads to vertical elements as a series of simple beams. In reality, no
diaphragm is perfectly rigid or perfectly flexible. However, the diaphragms can be considered as
rigid or flexible in order to simplify the analysis. In the case where the deformations of the
diaphragm and vertical elements are similar, the diaphragm cannot reasonably be assumed as
rigid or flexible. It is therefore considered as semi-rigid. The analysis of structural systems
containing semi-rigid diaphragms is complex, because this analysis should take into account the
relative stiffness of all structural elements including diaphragms. The distribution of lateral loads
of a semi-rigid diaphragm can be considered as a continuous beam supported on elastic supports.
It has generally recognized that the modeling of non-rigid floor behavior is much more complex
than the one of rigid floors. For many years, the simplified elastic methods of calculation have
usually used in the design of structures based on skewered models by concentrated masses and
equivalent stiffness, since they are easy to implement and well understood by Engineers.
However, this approach can provide only limited understanding of the real seismic behavior, the
linear response of a structure with flexible floors under the seismic action in terms of
displacement, is largely unexplored. Some seismic standard (European or American), to overcome
these disadvantages; recommend the use of specific methods based on the principle of finite
elements which could give good indications on the seismic behavior of the structure. In Algeria,
since the earthquake of Boumerdes town, the frame structures showed their limit and their
inefficiency with respect to the seismic actions. To attenuate the risk of possible catastrophes, the
Algerian seismic Standard (RPA), modified in 2003, recommends the use of the reinforced
concrete veils like resistance systems. This change in method of construction should encourage
the engineers of structures to give a special attention for the allowed assumption and never
checked in the occurrence, the rigidity of the floors. Indeed, if this latter one has manifestly
allowed when the resistant systems has constituted by frames; it is necessary to ensure
consequently, in the case of veils, of this rigidity because the distribution of the seismic actions
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can move away from the one corresponding to an infinitely rigid diaphragm. In practice, therefore
a certain ambiguity covers the deformation of the floors in their plan like the diversity of criteria
used in the international seismic standard in force. In addition, the comparison of the different
international seismic standard makes clear the range of the limits characterizing the rigidity of a
diaphragm. Some criteria can show enormous differences as the proportions of openings in a
floor.
To get round this ambiguity about the criteria used by the existing standard, case studies are
necessary. That is the purpose of this present study, using numerical simulation where the
stresses and strains calculated in the floors and resistant veils can bring a response to apprehend
the flexibility of the horizontal diaphragms (floors) in their plan by the use of computer codes
based on the finite elements method. By this manner, we will try to establish limits, non-existent
in the Algerian seismic standard (RPA), for taking into account their influence on the lateral loads
distribution.
References
[1] GARDINER D. R., BULL D.K. AND CARR A. J. INTERNAL FORCES OF CONCRETE FLOOR
DIAPHRAGMS IN MULTI-STOREY BUILDINGS, DEPARTMENT OF CIVIL ENGINEERING, UNIVERSITY
OF ANTERBURY, CHRISTCHURCH.(2008) NZSEE CONFERENCE.
[2] RECOMMENDATIONS OF A NZSEE STUDY GROUP ON EARTHQUAKE RISK BUILDINGS, NEW
ZEALAND OF SOCIETY FOR EARTHQUAKE ENGINEERING ASSESSMENT AND IMPROVEMENT OF
THE STRUCTURAL PERFORMANCE OF BUILDINGS IN EARTHQUAKES, JUNE (2006).
[3] AKHIR L. THE EFFECTS OF DIAPHRAGM COMPONENTS IN RESISTING LATERAL STABILITY OF
PRECAST CONCRETE FRAMES,VOT 75139,6 NOVEMBER (2006).
[4] SCHIERLE G G, PHD,FAIA DESIGN FOR EARTHQUAKE SAFETY NATIONAL CONVENTION AND
DESIGN EXPOSITION, JUNE (2006).
[5] SARKISSIAN L., KHALILI K. JAHROMI AND ZAHRAI S.M. IMPACT OF JOISTS DIRECTION ON THE
DIAPHRAGM BEHAVIOR OF COMPOSITE FLOOR SYSTEMS JSEE: VOL. 8, NO. 1 / 29, SPRING (2006).
[6] DHIMAN B. AND SUDHIR K.J. SEISMIC ANALYSIS OF ASYMMETRIC BUILDINGS WITH FLEXIBLE
FLOOR DIAPHRAGMS JOURNAL OF STRUCTURAL ENGINEERING ASCE / 1169 AUGUST (2004).
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#6
PCB "Argo',Israel
NTU "KhPI", Ukraine
ABSTRACT
The significant influence of fractal layer on electrical characteristics of MDS capacitors was
reported earlier. This feature as well as the developed surface microrelief ob MnO2 films are
responsible for the interest in investigating the fractal properties of this compound.The theory of
scattering by a porous solid was developed by Wong [1], and the theory main formula is as
follows: I(q) ~ constant x q-D .( Here D is the surface fractal dimension that shows fractal
behavior ).
Fig. 1. Logarithmic dependence of the SAXS intensity I vs the wavevector q for the
semiconductor layer: ( experimental
)
data; ( ___ )- approximation to the linear range.
On the graph, the coefficient of the curved part slope, which can be closely approximated by line
, (Fig.1) is:
= -dlgI(q)/dlgq = 2.87
(1)
Comparison result (1) with the Wong's formula (1) gives ( for = D ) the value of D=2.87. Obtained
D value coincides with the previously [1] found value of surface fractal dimensionality in a
sintered niobium powder pellet with high accuracy, D =2,81.
References
[1] PO-ZEN WONG, PHYS.REV B 32 (1985) 7417.
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#30
INEGI Institute of Science and Innovation in Mechanical and Industrial Engineering, Porto,
Portugal
ABSTRACT
In the design stage of a bus, as well as any other road vehicles, it is important to understand its
response to different critical maneuvers, such as curves, bumps and emergency braking. Virtual
simulations can give worthwhile information and knowledge about the behavior of these vehicles
under these different conditions, allowing faster, cheaper and more precise design. However,
numerical models of passenger buses are not straightforward due to the multiple elements that
interact with each other and with nonlinear responses, making it harder to predict their behavior
to different requests. In this case study, an electric bus dynamic behavior was analyzed for
different conditions. This study was fundamental for design decisions since the batteries mass
increases the center of gravity, which may instigate risks of instability. Aiming a multibody
dynamics study, a model in MSC ADAMS/Car was built taking into account the dynamic
interactions of the different components. Parameters quantification, as mass, moment of inertia
of major elements and also characteristic curves of springs, dampers, bushings and bumpstops,
among others were defined, supporting the problem definition and to describe the bus behavior,
understanding if the suspension elements are well chosen. This allows to describe the bus
behavior, and to understand if the suspension elements are well chosen. Mass and moments of
inertia were determined from the geometry and material density of the different components.
Through a literature review, were found the spring characteristic curves and experimentally were
measured the dampers characteristic curves. Remaining components were characterized by
standard values proposed by MSC ADAMS/Car. A sensitivity analysis showed that these standard
values have low influence in the results.
A multibody simulation in MSC ADAMS taking into account the flexibility of each part in the model
was performed. Although a coupled simulation between Abaqus and MSC ADAMS is possible
allowing to consider the stiffness of each part and estimate the stress due to the different critical
maneuvers. An MNF file considering the stiffness and mass matrix of the model was generated in
Abaqus, and then used in MSC ADAMS considering the stiffness of the different parts. This
coupled simulation allowed to estimate in a more accurate way the mechanical behavior of the
electric bus structure.
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Acknowledgements
The work has been funded by the Partnerships in Priority Areas Programme PN II of MEN
UEFISCDI, through the Agreement 5/2014.
References
[1] HU Y, YUAN ZS, KEPLER CK, ALBERT TJ, YUAN JB, DONG WX, SUN XY, WANG CT (2014)
DEVIATION ANALYSIS OF C1-C2 TRANSARTICULAR SCREW PLACEMENT ASSISTED BY A NOVEL
RAPID PROTOTYPING DRILL TEMPLATE: A CADAVERIC STUDY. J SPINAL DISORD TECH 27(5):E181-6
[2] THIENPONT E, SCHWAB PE, FENNEMA P (2014) A SYSTEMATIC REVIEW AND META-ANALYSIS
OF PATIENT-SPECIFIC INSTRUMENTATION FOR IMPROVING ALIGNMENT OF THE COMPONENTS IN
TOTAL KNEE REPLACEMENT. BONE JOINT J 96-B:105261
[3] LEVINE JP, PATEL A, SAADEH PB, HIRSCH DL, COMPUTER-AIDED DESIGN AND
MANUFACTURING IN CRANIOMAXILLOFACIAL SURGERY: THE NEW STATE OF THE ART, J
CRANIOFAC SURG. 2012, 23(1):288-93
[4] BIBB R, MEDICAL MODELING: THE APPLICATION OF ADVANCED DESIGN AND DEVELOPMENT
TECHNIQUES IN MEDICINE. WOODHEAD PUBLISHING LIMITED, 2006.
[5] BAGARIA, V., RASALKAR, D., BAGARIA, S.I., ILYAS, J., MEDICAL APPLICATIONS OF RAPID
PROTOTYPING - A NEW HORIZON, ADVANCED APPLICATIONS OF RAPID PROTOTYPING
TECHNOLOGY IN MODERN ENGINEERING, DR. M. HOQUE (ED.), 2011
[6] RADERMACHER K ET AL (1998) COMPUTER ASSISTED ORTHOPAEDIC SURGERY WITH IMAGE
BASED INDIVIDUAL TEMPLATES. CLIN ORTHOP RELAT RES 354:283
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Session 3B
TUE, 16:00 -17:30
Room B
TOPIC: Polymer matrix composites, sandwich composites structures and green composites
Chair: George Papanicolaou
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In order to observe the dynamic behavior of the considered plates, numerical simulations were
carried out in addition to the experimental determination of the eigen frequencies of these
materials [3,4].
One of the forms shape of the plate captured experimentally [5] is presented in the Figure 2.
Acknowledgement
The work has been funded by the Sectoral Operational Programme Human Resources
Development 2007-2013 of the Ministry of European Funds through the Financial Agreement
POSDRU/159/1.5/S/132397
References
[1] GIBSON, R.F. (1994). PRINCIPLES OF COMPOSITE MATERIAL MECHANICS, MC GRAW-HILL, ISBN
0-07-113335-6, USA.
[2] BUZDUGAN, G., MIHAILESU, E., RADES, M. (1986). VIBRATION MEASUREMENT, MARTINUS
NIJHOFF PUBLISHERS, ISBN 90-247-3111-9, ROMANIA.
[3] RADES, M. (1986). EFECTUL ATASARII VIBRATORULUI ASUPRA RASPUNSULUI DINAMIC AL
STRUCTURILOR, BULETINUL IPB, SERIA MECANICA, TOMUL XLVIII, PAG. 50-59.
[4] RADES, M. (1976). COMPENSAREA MASELOR LA MASURAREA IMPEDANTELOR MECANICE,
STUDII SI CERCETARI DE MECANICA APLICATA, VOL 4, TOMUL 35, OCTOMBRIE-DECEMBRIE,
PAG. 547-568.
[5] FRISWELL, M.I., MOTTERSHEAD, J.E., FINITE ELEMENT MODEL UPDATING IN STRUCTURAL
DYNAMICS, KLUVER ACADEMIC PUBLISHERS, ISBN 0-7923-3431-0, THE NETHERLANDS.
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#84
University Politehnica Bucharest, Centre for Surface Science and NanoTechnology, Romania
2
Scientific Research Centre for CBRN Defence and Ecology, Bucharest, Romania
3
University Politehnica Bucharest, Faculty of Applied Chemistry and Material Science, Romania
ABSTRACT
The energy industry generates yearly great amounts of coal ash accompanied by a lot of work for
transport and storage by landfill which cause negative environmental impacts such as leaching of
potentially toxic substances into soils and groundwater [1,2]. The best way to solve the disposal
problem of ash is to decrease the quantity for disposal with utilization of such waste. To deal with
these problems, our paper assesses the recycling of coal ash generated in thermal power plants in
conjunction with the re-use of waste glass. Due to its unique properties combination: i.e. thermal
insulating, chemically corrosion resistance, lightweight, rigid, waterproof and low cost, these
foam ceramic materials could be an alternative for application in building industry and other
fields. Various processing methods have been developed to produce porous ceramics, such as:
replica [3], sacrificial template [4] and direct foaming method [5]. The foaming agent could be
used to prepare a foam ceramics includes carbonates, sulphates, carbon, SiC, etc.
The chemical composition analysis (by X-ray fluorescence and atomic absorption) indicates that
the coal ash consists mainly of Si, Al, Ca and Fe oxides. The ash type is silico-aluminous with a
composition close to clay lands. The chemical composition of the investigated waste is given in
the table bellow.
%
SiO2
TiO2
Al2O3
coal
ash
49.7
0.77
20.95
71.48
0.07
2.33
glass
MgO
CaO
MnO
Na2O
K2O
P2O5
SO3
LOI
8.96
2.48
9.25
0.08
0.21
1.55
0.2
0.59
5.06
0.31
5.26
8.96
12.98
0.04
0.5
Fe2O3
Preliminary measurements of radioactivity show the existence of 226Ra and 232Th, the irradiation
on radiation protection being at a level, close but lower than of the health admitted norms. Such
comprehensive characterization helps to find out the appropriate ways of ash recycling, giving
also the useful information about the power plant combustion efficiency.
In our research the porous ceramics was obtained by high temperature foaming process. As main
starting materials were used coal fly ash and bottom ash and various glass wastes and silicon
carbide (SiC) as foaming agents.
o
(1)
(2)
2-
(3)
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
2-
Property
Porosity, %
Bulk density, kg/m
Expansion rate
Compression
strength, MPa
73- 82
3
261.3
3.5 - 4.8
0.92 -1.12
CONCLUSIONS
The development of porous ceramic by high temperature foaming process was effective by using
as starting materials 85% bottom coal ash and 15% glass waste and SiC as foaming agent.
226
232
Preliminary measurements of radioactivity on coal ash show the existence of Ra and Th, the
irradiation on radiation protection being at a level, close but lower than of the health in the
admitted norms.
Due to its unique properties combination: i.e. thermal insulating, chemically corrosion resistance,
lightweight, rigid, waterproof and low cost, these foam glass materials could be an alternative for
application in building industry and other fields.
Acknowledgements
This work was partially supported by the Romanian Executive Unit for Financing Higher
Education, Research Development and Innovation (Grant no. nr.283/2014 - Collaborative applied
research projects).
References
[1] G. FERRAIOLO, M. ZILLI, A. CONVERTI, FLY ASH DISPOSAL AND UTILIZATION, J. CHEM.
TECHNOL. BIOTECHNOL. 47 (1990) 281305.
[2] C.L. CARLSON, D.C. ADRIANO, ENVIRONMENTAL IMPACT OF COAL COMBUSTION RESIDUE, J.
ENVIRON. QUAL. 22 (1993) 227247.
[3]. NOR MAAM, HONG LC, AHMAD ZA, AKIL HM. PREPARATION AND CHARACTERI-ZATION OF
CERAMIC FOAM PRODUCED VIA POLYMERIC FOAM REPLICATION METHOD. JMATER PROCESS
TECHNOL 2008;207(13):2359.
[4]. ANDERSSON L, BERGSTRM L. GAS-FILLED MICROSPHERES AS AN EXPANDABLE SACRIFICIAL
TEMPLATE FOR DIRECT CASTING OF COMPLEX-SHAPED MACROPOROUS CERAMICS. J EUR CERAM
SOC 2008;28(15):281521.
[5]. BARG S, SOLTMANN C, ANDRADE M, KOCH D, GRATHWOHL G. CELLULAR CERAMICS BY
DIRECT FOAMING OF EMULSIFIED CERAMIC POWDER SUSPENSIONS. J AM CERAMSOC
2008;91(9):28239.
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The product behaves in an especial way, compared to other similar materials or to alternative
combinations of its ingredients and it is given the name ABC (Advanced Bean Composite). The
production process is environmental friendly, with insignificant environmental impact, since it
uses raw materials of plant origin, there are zero gas emissions and the sub-products can be used
as animal feed. The process is fast and easy and non laborious, using ordinary laboratory
equipment.
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(b)
(a)
The developed new matrix is a 100% green material, totally biodegradable, totally recyclable,
environmental friendly. ABC-Matrix is suitable to be easily reinforced with a great variety of
reinforcements (Fig. 2 and 3) to produce a series of novel composite materials covering a long
range of mechanical properties mimicking materials as rubber, plastics and more, breaking new
ground in green composite materials scientific research.
References
[1] F.P. LA MANTIA, M. MORREALE, "GREEN COMPOSITES: A BRIEF REVIEW, COMPOSITES PART A:
APPLIED SCIENCE AND MANUFACTURING", COMPOSITES PART A: APPLIED SCIENCE AND
MANUFACTURING, VOLUME 42, ISSUE 6, JUNE 2011, PP. 579588
[2] O. FARUK, A.K. BLEDZKI, H.P. FINK, M. SAIN, BIOCOMPOSITES REINFORCED WITH NATURAL
FIBERS: 20002010, PROG. POLYM. SCI. 2012, 37, 15521596
[3] X.Z. TANG, P. KUMAR, S. ALAVI, K.P. SANDEEP, RECENT ADVANCES IN BIOPOLYMERS AND
BIOPOLYMER-BASED NANOCOMPOSITES FOR FOOD PACKAGING MATERIALS, CRIT. REV. FOOD
SCI. NUTR. 2012, 52, 426442
[4] L.L. MCKINNEY, W.F.SOLLARS, E.A. SETZKORN, STUDIES ON THE PREPARATION OF SOY BEAN
PROTEIN FREE OF PHOSPHORUS, J. BIOL.CHEM. 1949
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#8
Dpto. Facultad de Quimica, Universidad del Pas Vasco UPV/EHU, San Sebastian, Spain
2
Laboratory of Magnetism, University of Bialystok, Bialystok, Poland
3
IKERBASQUE, Basque Foundation for Science, Bilbao, Spain
ABSTRACT
The study of the magnetic properties of glass-covered amorphous microwires is a topic of growing
technological interest related to their peculiar magnetic behaviour such as magnetic bistability
and giant magnetoimpedance effect (GMI). The GMI effect provides opportunities for the use of
magnetic wires in sensor elements. Optimization of amorphous wires for sensor applications
requires investigation of their electric and magnetic properties. Because the GMI effect is mainly a
surface effect, the surface magnetic structure of the microwires should be investigated for this
optimization.
Microwire has a sandwich structure: axially magnetized inner core, radial or circularly magnetised
outer shell and pirex-glass covering. There are three lines of study of the composite microwires:
magneto-optical Kerr effect (MOKE) magnetometry, MOKE polarizing microscopy (Fig. 1) and
MOKE-modified SixtusTonks method to study the surface domain wall dynamics [1]. The main
idea of our experiments is MOKE without external magnetic field: the studies have been
performed in the presence of the circular magnetic field that was produced by electric current
flowing along the microwire.
Magnetic domain imaging of the microwire surface was performed by MOKE optical polarizing
microscopy in reflection mode. Surface magnetic domains were observed because the different
in-plane components of the surface magnetization transform to blackwhite contrast when
polarized light reflects from the cylindrically shaped microwire surface. Therefore, images of the
domain structures (Fig. 2) obtained by MOKE microscopy show differences of the in-plane
magnetization components (Fig.1).
Fig. 2 Image of surface magnetic domain structure. Red arrows show domain wall motion.
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The surface magnetic hysteresis loops were obtained using a magneto-optical magnetometer. A
polarized light of HeNe laser was reflected from the wire to the detector. When the longitudinal
Kerr effect was used, the rotation of the angle of the light polarization was proportional to the
magnetization, which was parallel to the plane of the light. When the transverse Kerr effect was
used, the intensity of the reflected light was proportional to the magnetization, which was
perpendicular to the plane of the light. An electric current flowing along the wire produced a
circular magnetic field. An axial magnetic field was produced by the pair of Helmgolz coils.
It was discovered the great variety of the domain structures as a response to such external
parameters as magnetic field, high frequency electric current, tension and torsion stresses,
temperature, etc. It permits us to predict and control the details of the magnetization reversal in
microwires to optimize the functioning of magnetic sensors.
References
[1] A. CHIZHIK, J. GONZALEZ, MAGNETIC MICROWIRES: A MAGNETO-OPTICAL STUDY, PAN
STANFORD PUBLISHING PTE. LTD., SINGAPORE, 2014.
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Session 4A
WED, 14:15 -15:30
Room A
TOPIC: Fatigue
Chair: Stefan Dan Pastrama
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#18
In recent years it has been recognized that the fatigue failure process involves three phases, crack
initiation, crack propagation and finally, the unstable crack growth to fracture of components. The
aim of this work is to present mean stress effect on fatigue failure in 2024 T351 aluminium alloy
used in aircraft components. In this investigation, fourth bending fatigue test was carried out to
evaluate evolution in initiation fatigue life under specified fatigue loading level from notched
specimens. A crack initiation law was developed using opening stress theory. Fractography
analysis was conducted in order to show the effect of mean stress on fractured surfaces. In
initiation phase, crystallographic fracture was apparent.
The experimental study was performed on 2024 T351 Al-alloy. The chemical composition of
studied material and mechanical properties are reported in others authors works [1]. Bars with a
rectangular section 1010 mm2 in 2024 aluminum alloy were loaded under four point bending
specimen. Evolution of fatigue initiation lives for a crack between 105 and 120 m under mean
stress effect are summarised in Table 1. Detected initiation crack lengths remain lower than the
grain size. The applied loadings cycles characterized by P loading amplitude until final fracture
are shown in Fig. 1. It is noticed that initiation fatigue lives increase with decreasing in mean
stress (mean loading) and increasing in stress ratio R from 0.1 to 0.3. This conclusion is confirmed
in studies conducted by all researchers for 2024 Al-alloys [2-4]. The transition from R=0.1 and
R=0.3 represents a decrease in amplitude loading P from 2727 KN 1928 KN and has increased
initiation fatigue life from 15400 cycles to 37800 cycles. This difference represents a decrease rate
of 2.45 times.
The evolution in the number of initiation cycles depending on the load ratio, R or mean stress is
shown in figure 2. This evolution is approximated by an exponential function given on the same
figure. It covers the area of 103 to 104 cycles. Under applied spectrum loading, fatigue crack
initiation life varies from 4% to 7% of the total fatigue failure. The fatigue fracture surfaces were
examined on SEM to obtain more detailed information on crack growth contributions of different
load cycles. The fractured surfaces indicate crystallographic fracture near the notch and in
initiation zone as illustrated in Fig 3a. Due to the high applied load in initiation stage, secondary
cracks are presents Fig 4b.
Table 1: Effect of mean or stress ratio on fatigue initiation Lives Ni
R
0.1
0.2
0.3
Pmax (KN)
2.755
2.755
2.755
Pmoy (KN)
1.515
1.653
1.791
P (KN)
2.727
2.203
1.928
106
ai (m)
115
105
120
Ni (Cycles)
15400
24000
37800
Nf (Cycles)
382000
569500
547000
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3,0
40000
2,5
Nombre de cycle Ni
30000
2,0
1,5
20000
Ni = 9812,3e4,49 R
r2 = 1
10000
1,0
0,5
100 000
200 000
300 000
400 000
500 000
600 000
0,1
0,2
0,3
0,4
Rapport de charge R
Notch
Secondary cracks
at boundary grains
Fig. 3. Fractography of fractured surfaces in initiation stage for 2024 aluminium alloy at R=0.1
(a) fracture surface near the notch (b) At (a=3.23 mm, da/dN=7.8010-6 mm/cycles)
References
[1] M. BENACHOUR, A. HADJOUI, M. BENGUEDIAB, N. BENACHOUR. EFFECT OF THE AMPLITUDE
LOADING ON FATIGUE CRACK GROWTH. PROCEDIA ENGINEERING 2, 121-127, 2010.
[2] S. PEARSON. INITIATION OF FATIGUE CRACK IN COMMERCIAL ALUMINIUM ALLOYS AND THE
SUBSEQUENT PROPAGATION OF VERY SHORT CRACKS. ENGNG. FRACT. MECH. 7, 235-247, 1975.
[3] N. RANGANATHAN, H. ALDROE, F. LACROIX, F. CHALON, R. LEROY, A. TOUGUI. FATIGUE CRACK
INITIATION AT A NOTCH. INT. J. FATIGUE 33, 492-499, 2011.
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#28
INEGI Institute of Science and Innovation in Mechanical and Industrial Engineering, Porto,
Portugal
ABSTRACT
Material fracture mechanics properties are commonly obtained by standardized and well
stablished specimens. However, since the standards are focused on mode I material
characterization, other specimens have been developed in order to describe the fracture behavior
of materials in mode II and mode III.
A compact mixed mode specimen was developed by H.A. Richard, [1], aiming to characterize
materials in mixed mode loading taking in to account tension and shear loading (mode I and mode
II). H.A. Richard labeled this specimen as new compact shear specimen (NCS specimen). This
NCS specimen can be tested in a multipurpose grip system, due to its capacity to load the
specimen with different directions, from 0 degrees to 90 degrees, correspond to pure mode I to
pure mode II, respectively.
This research revisits this specimen and the respective stress intensity factor calibration using
numerical models. The crack behavior is modeled using the eXtended Finite Element Method
(XFEM) and the stress intensity factors were calculated for different conditions using the stress
field simulated with conventional finite element models (FEM) with post-processing technique
proposed by R. Krueger. [2]: modified virtual crack closure technique (mVVCT).
These models allowed to understand how the grip system allots the load to the specimen and, the
respective the stress field and the principal stress direction. In addition, it allows to reexamine the
stress intensity factor calibration proposed by H.A. Richard for different conditions.
References
[1] RICHARD, H. A. "A NEW COMPACT SHEAR SPECIMEN." INTERNATIONAL JOURNAL OF
FRACTURE 17.5 (1981): R105-R107.
[2] KRUEGER, R. "VIRTUAL CRACK CLOSURE TECHNIQUE: HISTORY, APPROACH, AND
APPLICATIONS." APPLIED MECHANICS REVIEWS 57.2 (2004): 109-143.
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#85
ABSTRACT
Thanks to their excellent fatigue resistance and low weight ratio, today; composite materials are of
great importance in humanity life, either in civil or military fields such as aerospace, automotive,
marine and as is usual, each material reaches failure towards the end of his life which is manifested by
the occurrence of fractures. Until now, researchers put their efforts into service in order to achieve
accurate and general models for predicting damage of this mysterious material. On our side, we
compared three fatigue damage models in order to see the most accurate and consistent with our
experimental results. Throughout the work, we adopted a stationary ergodic Gaussian random
loading.
First, we conducted a thorough study of the interlaminar fracture of composite laminates subjected to
stochastic loads. The choice of this failure mode was inspired by the fact that this failure mode is most
predominant among others; moreover, it is more dangerous because its invisible and undetectable
and occurs suddenly between the layers of material. The results of the experiments carried out with
graphite epoxy composite laminates [ 45/0/90]3s, were compared to the predictions of three models
namely: Linear damage model based on the law of Miner, damage mathematical expectancy E (t) and
stiffness degradation model.
Second time, following an analysis of the results, we found that the three models mentioned
above are close to the experimental results. We see that the correlation is the best for the
stiffness degradation model. On the other hand, the effects of load sequence and interaction are
not taken into account in linear damage model, which can lead to some difference between the
model predictions and experimental results.
References
[1] DIAO X, YE L, MAI YW. A STATISTICAL MODEL OF RESIDUAL STRENGTH AND FATIGUE LIFE OF
COMPOSITE LAMINATES. COMPOS SCI TECHNOL 1995; 54:329336.
[2] ADDEN S, HORST P. STIFFNESS DEGRADATION UNDER FATIGUE IN MULTIAXIALLY LOADED
NON-CRIMPED-FABRICS. INT J FATIGUE 2010; 32:108122.
[3] M. ABOUSSALEH AND R. BOUKHILI. LIFE PREDICTION FOR COMPOSITE LAMINATES
SUBMITTED TO SERVICE LOADING SPECTRA. JUNE 1998; VOL. 19. P. 241-245.
[4] YUNG-LI LEE, TANA TJHUNG. CHAPTER 3 - RAINFLOW CYCLE COUNTING TECHNIQUES. METAL
FATIGUE ANALYSIS HANDBOOK 2012. P. 89-114.
[5] DOWLING NE. FATIGUE-FAILURE PREDICTIONS FOR COMPLICATED STRESSSTRAIN HISTORIES.
J MATER ASTM 1972; 7(1):7187.
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[6] WATSON P, DABELL BJ. CYCLE COUNTING AND FATIGUE DAMAGE. SYMPOSIUM ON
STATISTICAL ASPECTS OF FATIGUE TESTING, WARWICK UNIVERSITY, 1975.
[7] PASSIPOULARIDIS VA, PHILIPPIDIS TP. A STUDY OF FACTORS AFFECTING LIFE PREDICTION OF
COMPOSITES UNDER SPECTRUM LOADING. INT J FATIGUE 2009; 31:40817.
[8] ZHEN GAO AND TORGEIR MOAN. FREQUENCY-DOMAIN FATIGUE ANALYSIS OF WIDE-BAND
STATIONARY GAUSSIAN PROCESSES USING A TRIMODAL SPECTRAL FORMULATION. INTER J OF
FATIGUE 2008; 30. P.19441955.
[9] REIFSNIDER KL, SCOTT C, JERMY D. COMPOS SCI TECHNOL 2000; 60:2539.
[10] ZHAI HONGJUN, YAO WEIXING. A SURVEY ON STIFFNESS REDUCTION MODELS OF FIBER
REINFORCED PLASTICS UNDER CYCLIC LOADING. ADV MECH 2002;32(1):6980.
[11] TALREJA R. FATIGUE OF COMPOSITE MATERIALS. TECHNOMIC PUBLISHING COMPANY; 1987.
[12] RATWANI MM, KAN HP. COMPRESSION FATIGUE ANALYSIS OF FIBER COMPOSITES. IN:
AIAA/ASME/ASCE/AHS 21ST STRUCTURES, STRUCTURAL DYNAMICS AND MATERIALS
CONFERENCE, PART 1, MAY 1980, SEATTLE, WASHINGTON, USA, PP. 27984.
[13] SCHN J, BLOM AF. LOAD-RATIO DEPENDENCE ON FATIGUE LIFE COMPOSITES. PARIS: ICCM,
1999.
[14] SCHN J, BLOM AF. FATIGUE LIFE PREDICTION AND LOAD CYCLE ELIMINATION DURING
SPECTRUM LOADING OF COMPOSITES. INT J FATIGUE 2002; 361-367.
[15] MILLER KJ. METAL FATIGUE-A NEW PERSPECTIVE. IN: ARGON AS, EDITOR. TOPICS IN
FRACTURE AND FATIGUE. BERLIN: SPRINGER-VERLAG; 1992. P. 30930.
[16] PAGANO N, SCHOEPPNER G. DELAMINATION OF POLYMER MATRIX COMPOSITES: PROBLEMS
AND ASSESSMENT. IN: KELLY A, ZWEBEN C, EDITORS. COMPREHENSIVE COMPOSITE MATERIALS.
OXFORD: PERGAMON; 2000. P. 433528.
[17] JM. HODGKINSON. MECHANICAL TESTING OF ADVANCED FIBER COMPOSITES. CRC PRESS,
2000.
[18] SR. REID AND G. ZHO. IMPACT BEHAVIOR OF FIBER-REINFORCED COMPOSITE MATERIALS
AND STRUCTURES. CRC PRESS, 2000.
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#86
V K Kapnopoulou , P A Caridis
1
ABSTRACT
Fatigue and fracture problems arose the last few decades, as HTS-steels were introduced to the
shipbuilding industry. To ensure that the steel structure will fulfill its intended function, a fatigue
assessment of the structure by a detailed fatigue analysis should be performed [1]. In the present
study, fatigue evaluation is conducted through the structural hot spot approach which estimates
the structural stress range at the hot spot. The structural hot spot approach implemented here, is
based on the idea of excluding the nonlinear stress peak from the structural stress, due to the fact
that the designer might not be certain about the exact geometry of the weld toe at an early
design stage. Thus, the effect of the notch is implicitly included in the experimental S-N curves. [2]
The aim of this study is to establish the fatigue life of a ship detail which is considered as hot spot,
using the finite element method by the use of Abaqus/CAE. A ship of 181k Ton DWT Bulk Carrier is
employed and the detail that is sub-modeled is the lower hopper knuckle connection. The cargo
hold model extents longitudinally by two hold lengths ( + 1 + ) and transversely by its full
breadth.
The elements that are employed are 4-noded shell elements (S4), quadrilateral, with 4 integration
points. According to the CSR Rules [3], the mesh should preferably represent the actual plate
panels between stiffeners so that the stresses for the control of yield and buckling strength can be
read and averaged from the results directly [3]. In this model, the mesh is a size of 0.425x0.425
when the typical longitudinal stiffener spacing is 0.85m. Linear, elastic analysis is performed
because linear elastic material behavior can be presumed as only localized yielding is allowed by
most design codes [2, 3].
Due to the size of the ship being over 200m, CSR Rules identify four loading conditions to be taken
into consideration; Homogenous, Alternate, Heavy Ballast and Normal Ballast [3]. In each loading
condition, a Hogging and Sagging load case is explored. In Alternate condition two separate cases
are examined; one with the cargo loads applied to the outer holds and one at the center hold thus
emphasizing the hogging and sagging effect on the structure. Therefore, the loads applied to the
model are a wave bending moment; either sagging or hogging, a cargo/ballast load and the
hydrodynamic pressure.
The lower hopper knuckle connection at the midship is one of the locations that CSR Rules
consider as hot spots in a Bulk Carrier and is sub-modeled [3]. To establish the fatigue life of the
hot spot of the detail, a fine mesh is generated at the hot spot. In order to increase efficiency, the
density of the mesh is explored through a mesh dependence analysis. At the structural stress
range calculation the transverse to the ship stress, is considered [2]. It is found that the most
affected area is at the hopper plate, hence the structural stress range calculation concerns this
area.
Figure 1 shows the cargo hold model (1a) and the sub-model (1b). Figure 2 illustrates the submodel with the fine mesh zone at the hopper knuckle connection on the left side (2a) whereas on
the right (2b), it focuses on the red circle area as illustrated at Figure 2a of the connection
showing the stress at the hopper plate.
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
(a)
(b)
In the present study results of the stress distribution (Figures 2a-2b) are presented for the
Alternate Condition which is considered the most critical. Table 1 presents the results of fatigue
life of the hopper knuckle connection. It is revealed that Alternate Condition draws the most
damage compared to all the other conditions due to the cargo load being spread in a way that
enhances the hogging-sagging effect to the structure. Therefore, it is considered as the most
critical situation and is proposed to be taken as a critical case when examining ways to reduce the
structural hot spot stress range, as means of increasing fatigue life.
(a)
(b)
Fig. 2: Results from the most critical condition-Alternate (a) and the right figure (b) zooms in to the red
circle of figure 2a.
Table 1: Results of the Cumulative Damage Ratio (D) and Fatigue Life for the hot spot of the connection
Final D
Fatigue Life (years)
Hot Spot
1,068
23,39(<25)
References
[1] P A CARIDIS., 2000, THE STEEL STRUCTURE OF THE SHIP; LOCAL STRENGTH
ISSUES, 1ST EDITION, ATHENS: G. ARGIROPOULOS LTD
[2] E NIEMI, W FRICKE, SJ MADDOX, 2006, FATIGUE ANALYSIS OF WELDED
COMPONENTS; DESIGNERS GUIDE TO THE STRUCTURAL HOT SPOT STRESS
APPROACH, 1ST EDITION, WOODHEAD PUBLISHING
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ABSTRACT
Two different crack growth-based fatigue analysis are presented for fatigue life prediction in this
paper. The first proposed method is based on an equivalent initial flaw size (EIFS). The EIFS is
determined by the Kitagawa-Takahashi diagram [3]. The second method proposed is crack
closure. This analysis strongly affects the fatigue crack growth rate. Accounting for crack closure in
fatigue life prediction models allows the description of mean stress effects on fatigue life [6].
This latter approach is applied to a notched plate made of P355NL1 steel. Fatigue crack growth
data of the material is evaluated using CT specimens, covering several stress R-ratios. Also, S-N
fatigue data is available for the double notched plate, covering stress R-ratios equal to 0, 0.15 and
0.3. The crack propagation model takes into account stress ratio effects, account for propagation
threshold and a correction for plasticity. Stress intensity factors are computed using the J-integral
technique. The performances of predictions are analyzed and deviations discussed [7].
References
[1] KITAGAWA H., TAKAHASHI S. APPLICABILITY OF FRACTURE MECHANICS TO VERY SMALL
CRACKS OR CRACKS IN THE EARLY STAGE. PROC. OF THE 2ND INT. CONF ON MECH. BEHAVIOUR
OF MATERIALS, ASM, 627631, 1976.
[2] FERNNDEZ-CANTELI A., BRIGHENTI R., CASTILLO E. TOWARDS A PROBABILISTIC CONCEPT OF
THE KITAGAWA-TAKAHASHI DIAGRAM. PROCEEDINGS OF THE 4TH INTERNATIONAL CONFERENCE
ON CRACK PATHS (CP 2012), GAETA, ITALY, 2012, 1041-1048.
[3] XIANG Y., LU Z., LIU Y. CRACK GROWTH-BASED FATIGUE LIFE PREDICTION USING AN
EQUIVALENT INITIAL FLAW MODEL. PART I: UNIAXIAL LOADING. INTENATIONAL JOURNAL OF
FATIGUE, VOL. 32, NUM. 2, PP. 341-349, 2010.
[4] SAVAIDIS G., SAVAIDIS A., ZERRES P., VORMWALD M. MODE I FATIGUE CRACK GROWTH AT
NOTCHES CONSIDERING CRACK CLOSURE. INTENATIONAL JOURNAL OF FATIGUE, VOL. 32, NUM.
10, PP. 1543-1558, 2010.
[5] CASTILLO E., FERNNDEZ-CANTELI A. A GENERAL REGRESSION MODEL FOR LIFETIME
EVALUATION AND PREDICTION, INT. J. FRACT., 2001; 107, PP. 117137.
[6] FISCHER C., SCHWEIZER C., SEIFERT T., ASSESSMENT OF FATIGUE CRACK CLOSURE UNDER INPHASE AND OUT-OF-PHASE THERMOMECHANICAL FATIGUE LOADING USING A TEMPERATURE
DEPENDENT STRIP YIELD MODEL. INTERNATIONAL JOURNAL OF FATIGUE, VOL. 78, PP. 2230,2015.
[7] ALVES A. S. F., SAMPAYO L.M.C.M.V., CORREIA J.A.F.O., DE JESUS A.M.P., MOREIRA P.M.G.P.,
TAVARES P.J.S., FATIGUE LIFE PREDICTION BASED ON CRACK GROWTH ANALYSIS USING AN
EQUIVALENT INITIAL FLAW SIZE MODEL: APPLICATION TO A NOTCHED GEOMETRY. PROCEDIA
ENGINEERING OF THE 1ST INTERNATIONAL CONFERENCE ON STRUCTURAL INTEGRITY [ACCEPTED]
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Session 4B
WED, 14:15 -15:30
Room B
TOPIC: Manufacturing Techniques
Chair: Pedro Moreira
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#14
ABSTRACT
The shipbuilding industry is fundamental to the regional development of Amazon Region due to
its natural calling expressed in the extension of its navigable rivers. One increasing issue of local
shipbuilding industry as a whole is its productivity rate that should be as high as possible to allow
international competition with other naval industries.Thinking on this issue the Materials
Characterization Laboratory (LCAM) of the Federal University of Par (UFPA) developed the called
Double Cold Wire Gas Metal Arc Welding (DCW - GMAW) process, which consists of the injection
of two cold wires (non energized) in the direction of the welding pool besides the energized wire
of the conventional GMAW process, these two wires profit of the heat produced by the electric
arc that was not used to melt the hot wire (energized) or transferred to the weld piece, and,
consequently, are melted and deposited on the weld piece increasing the deposition rate and
decreasing the Heat Affected Zone (HAZ), due to the fact that these cold wires act as heat sinks,
diminishing the heat transferred to the base metal and the consequent distortions. This work
aims to compare the operational behavior of the conventional GMAW and DCW - GMAW
processes and the metallurgical, mechanical and geometrical features of the steel welds produced
by these welding processes. The automated welds were conducted on flat plates with an electrical
source in positive Direct Current (DC+), in a flat position and under protection of 75% Argon (Ar)
and 25% Carbon Dioxide (CO2) gas mixture, in a welding workbench constituted of an automated
welding displacement system, a energized wire feeding system and an additional two cold wire
feeding systems. The weld beads were made with the electrode AWS 70S-6 wire applied to ASTM
131 steel grade A as base metal. The base metal had the following dimensions: 150 x 60 x 53 x 9
mm. The input variables were the electrode wire feeding rate (10, 12 and 14m/min), a constant
welding speed (40cm/min) and feeding rates of the non-energized wires (20%, 40%, 60%, 80%
and 100% of the electrode wire feeding rates). The evaluation of the deposits was based in their
geometrical characteristics (Width (W), Height (H) and Penetration (P) and Dilution (D)),
microhardness values in Vickers and general characteristics of the resulting micrographies. The
microstructural characterization consisted of qualitative analysis of the micrographies obtained
by standard metallographic procedures. The DCW - GMAW welding process showed a good
operational stability and lower incidence of splash compared to the conventional GMAW process.
Also showed good geometrical characteristics, with adequate P/W ratios and absence of defects
such as finger and porosities. Besides, the DCW - GMAW processes showed a higher deposition
rate, as expected, when compared to the usual GMAW process. The micrographies showed that
there were microstructural variations among the welded samples by the usual GMAW, and DCW
- GMAW processes for similar welding conditions. The hardness profiles collected in the weld
metal fusion zone showed a hardness increase in this region DCW - GMAW in a feeding rate
higher than 60% of non-energized wires, which can be related to the increase of second phase
non-aligned ferrite.
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#34
INEGI Institute of Science and Innovation in Mechanical and Industrial Engineering, 4200-465
Porto, Portugal
ABSTRACT
Friction Stir Welding (FSW) is a solid-state joining technique that has seen remarkable
developments during the last decade. Due to its numerous benefits over the conventional welding
techniques along with growing industrial demands for lightweight design structures [1], FSW
found its way to be one of the main attractions of engineering subjects. FSW process is based on
the generation of frictional heat, between the FSW tool and the parent material surface, under an
axial force [2]. Originally, this method was used for welding metallic materials, which are hard or
somehow impossible to weld with conventional techniques.
However, due to polymeric materials significant consumption growth in the industry, recently,
FSW has been utilized for pursuing the possibility of implementing this technique for welding
polymers together with different configurations. Nevertheless, polymeric materials behave
differently than metallic ones, and up to this point, scarce investigations have been done in this
specific area.
This article reviews the previous studies, which have investigated for welding polymers using FSW
technique. A brief historical review is performed in order to analyse tool developments, welds
strength and the most effective welding parameters for different polymeric materials. New
materials, configurations and test specifications are currently under investigations, including the
possibility for dissimilar materials joining, taking FSW to a new phase in industrial applications.
References
[1] BILICI, M.K., A.. YKLER, AND M. KURTULMU THE OPTIMIZATION OF WELDING PARAMETERS
FOR FRICTION STIR SPOT WELDING OF HIGH DENSITY POLYETHYLENE SHEETS. MATERIALS &
DESIGN, 2011. 32, 4074-4079 DOI: 10.1016/J.MATDES.2011.03.014.
[2] REZGUI, M.A., ET AL. APPLICATION OF TAGUCHI APPROACH TO OPTIMIZE FRICTION STIR
WELDING PARAMETERS OF POLYETHYLENE. EPJ WEB OF CONFERENCES, 2010. 6, 07003 DOI:
10.1051/EPJCONF/20100607003.
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Institute of Science and Innovation in Mechanical and Industrial Engineering (INEGI), University of
Porto, Campus da FEUP, Av. Roberto Frias, 400, 4200-465 Porto, Portugal
2
LAETA, IDMEC, Instituto Superior Tcnico, Universidade de Lisboa, Av. Rovisco Pais, 1049-001
Lisboa, Portugal
3
Faculdade de Engenharia da Universidade do Porto, Campus da FEUP, Av. Roberto Frias, s/n,
4200-465 Porto, Portugal
ABSTRACT
Lightweight construction although has always been a goal of every structural designer has
become ever more relevant with regulatory imposition of fuel efficiency goals in the
transportation industry together with customer perception of fuel efficiency and environmental
friendliness. In the pursuit of better, more lightweight structural designs, the adoption of new
materials such as lightweight alloys and new manufacturing processes are required. Joining
aluminum alloys was normally a concern due to their poor weldability properties, but the
advancements in adhesive bonding technology and the development of solid state welding such
as friction stir welding (FSW) [1], has increased the possibilities of application of theses alloys in
structural design. In FSW the interaction of a non-consumable tool rotating and traversing along
the joint line creates a welded joint through visco-plastic deformation and consequent heat
dissipation resulting in temperatures below the melting temperature of the materials being
joined. In contrast with conventional fusion processes, FSW creates low distortions, excellent
mechanical properties in the weld zone, and allows for execution without a shielding gas, and is
suitability to weld all aluminum alloys. These characteristics have not only generated vast interest
in the research community but also industrial applications of FSW may be found in the literature
[2]. Adhesive bonding (AB) has garnish much attention from structural designers, since it is a
technology capable of efficiently joining dissimilar materials and vast differentiation exists in
adhesives resulting in the existence of specific adhesives for particular applications and
requirements. The research in adhesive bonding is vast and broad, from fracture mechanics [3] or
self-healing and thermally expandable particles in adhesive joints [4] to application cases [5, 6].
Adhesive bonding has also been used together with other joining methods to form hybrid joints,
since AB complements very well the benefits of other technologies. Spot welding, riveting,
clinching [7] along with many other joining processes have been used in conjunction with AB to
form these hybrid joints. As FSW is a relatively more recent technology, studies regarding hybrid
joints made with FSW are more uncommon. One study found in the literature was the one by
Chowdhury et al. in [8] where friction stir spot welded bonded dissimilar joints of magnesium and
aluminium were produced and tested. The hybrid bonded joints shown improvement in lap shear
strength and failure energy regarding the only friction stir spot welded joints. Fatigue life was
improved as well when using adhesive in the friction stir spot welded. Hybrid FSW and AB joints of
AA6082 aluminium alloy will be studied in this work.
References
[1] THOMAS, W.M., E.D. NICHOLAS, J.C. NEEDHAM, M.G. MURCH, P. TEMPLESMITH, AND C.J.
DAWES, IMPROVEMENTS RELATING TO FRICTION WELDING, E.P. OFFICE, EDITOR. 1993.
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
[2] KUSUDA, Y., HONDA DEVELOPS ROBOTIZED FSW TECHNOLOGY TO WELD STEEL AND
ALUMINUM AND APPLIED IT TO A MASS-PRODUCTION VEHICLE. INDUSTRIAL ROBOT: AN
INTERNATIONAL JOURNAL, 2013. 40(3): P. 208-212.
[3] CHAVES, F.J., M. DE MOURA, L. DA SILVA, AND D. DILLARD, FRACTURE CHARACTERIZATION OF
BONDED JOINTS USING THE DUAL ACTUATOR LOAD APPARATUS. JOURNAL OF ADHESION SCIENCE
AND TECHNOLOGY, 2014. 28(5): P. 512-524.
[4] BANEA, M.D., L.F. DA SILVA, R.D. CAMPILHO, AND C. SATO, SMART ADHESIVE JOINTS: AN
OVERVIEW OF RECENT DEVELOPMENTS. THE JOURNAL OF ADHESION, 2014. 90(1): P. 16-40.
[5] KADIOGLU, F. AND R.D. ADAMS, FLEXIBLE ADHESIVES FOR AUTOMOTIVE APPLICATION UNDER
IMPACT LOADING. INTERNATIONAL JOURNAL OF ADHESION AND ADHESIVES, 2015. 56: P. 73-78.
[6] SCHIEL, M., S. KRELING, C. UNGER, F. FISCHER, AND K. DILGER, BEHAVIOR OF ADHESIVELY
BONDED COATED STEEL FOR AUTOMOTIVE APPLICATIONS UNDER IMPACT LOADS.
INTERNATIONAL JOURNAL OF ADHESION AND ADHESIVES, 2015. 56: P. 32-40.
[7] MORONI, F., A. PIRONDI, AND F. KLEINER, EXPERIMENTAL ANALYSIS AND COMPARISON OF
THE STRENGTH OF SIMPLE AND HYBRID STRUCTURAL JOINTS. INTERNATIONAL JOURNAL OF
ADHESION AND ADHESIVES, 2010. 30(5): P. 367-379.
[8] CHOWDHURY, S., D. CHEN, S. BHOLE, X. CAO, AND P. WANJARA, LAP SHEAR STRENGTH AND
FATIGUE BEHAVIOR OF FRICTION STIR SPOT WELDED DISSIMILAR MAGNESIUM-TO-ALUMINUM
JOINTS WITH ADHESIVE. MATERIALS SCIENCE AND ENGINEERING: A, 2013. 562: P. 53-60.
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#73
ABSTRACT
Manufacturing industry is one of the most important industries in the developed countries. This
industry uses different machining techniques like drilling, turning, milling as well as the
combination of those techniques.
Depending on machining aim and for each cutting tool there are different combinations of
parameters, like feed rate, spindle speed, axial or radial depth of cut to obtain different results in
terms of quality of machined surface and tool wear. Each cutting parameters combination will
result in a different surficial roughness of workpiece and tool life. However, it is very difficult to
define the best combination that provides the lower surface roughness and maximum tool life [1].
One of the most important features in the manufacturing industry is to predict the surface
roughness and tool life for a particular combination of machining parameters in order to choose
the best combination for producing a part [2, 3]. Furthermore, is essential to reduce the costs for
the required quality.
This paper presents a study of Taguchi design application to optimize surface quality in a CNC
milling operation. Maintaining good surface quality usually involves additional manufacturing cost
or loss of productivity. The Taguchi design is an efficient and effective experimental method in
which a response variable can be optimized, given various control and/or noise factors, using
fewer resources than a factorial design. This study includes feed per tooth, cutting speed and
radial depth of cut as control factors. An orthogonal array of L9(34) was implemented and the
ANOVA analyses were carried out to identify the significant factors affecting surface roughness as
well as the determination of optimal cutting combination by seeking the best surface roughness
(response) and signal-to-noise ratio.
In this study we have machined a cylindrical hardened plastic mould steel (GMTC 1.2738)
specimen using a milling tool provided by Palbit which the reference is PLUS 49095 / WNHU
04T310.
The experimental work was done in the milling machine Deckel Maho DMC 63V and the cutting
parameters were combined agreeing the defined Taguchi orthogonal array (table 1), the only
parameter maintained fixed was the axial depth with a value of 0.3 mm. Between each
experiment, the roughness was measure on three different points of specimen using a portable
surface roughness tester (Mitutoyo SJ-301).
The results were analyzed and statistical treated to obtain the best combination in terms of
surficial roughness and the influence of each cutting parameter in the surface quality.
In the table 1 is presented the Taguchi orthogonal array, the average of the measured roughness
and the signal to noise ratio which, is this case, was chosen the smaller is the better in order to
minimize the surface roughness.
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Book of abstracts of ICSAAM2015, The 6 International Conference on Structural Analysis and Advanced Materials
Vc
[m/min]
150
150
150
180
180
180
200
200
200
fz
[mm/tooth]
0,1
0,15
0,2
0,1
0,15
0,2
0,1
0,15
0,2
Ae
[mm]
0,075
0,1
0,125
0,1
0,125
0,075
0,125
0,075
0,1
Roughness
[m]
2,44
2,39
2,6
2,19
1,94
2,18
2,05
2,28
2,03
S/N
[dB]
-7,776
-7,567
-8,286
-6,834
-5,751
-6,757
-6,217
-7,168
-6,172
Analyzing the table 1, is possible to observe that the cutting parameters combination of
experiment 5 gives the lower value of roughness and signal to noise ratio.
With all the roughness measurements, was implemented an ANOVA analysis using the
Statgraphics software. The results are shown in table 2.
Source of Variance
MAIN EFFECTS
A:Vc
B:fz
C:ae
RESIDUAL
TOTAL
2
2
2
2
8
0,133433
0,00343333
0,0100333
0,0379
F-Ratio
P-value
3,52
0,09
0,26
0,2212
0,9169
0,7907
Evaluating the ANOVA analysis, it is possible to observe that the most important factor is the
Cutting Speed (Vc) with a P-value=0,22 and the feed rate (fz) has the lower effect in the value of
roughness. Due to the low number of degrees of freedom, we must be cautious with the results,
however for a preliminary test, the results are good enough for the industry application.
References
[1] NALBANT, M., GKKAYA, H. AND SUR, G. (2007). APPLICATION OF TAGUCHI METHOD IN THE
OPTIMIZATION OF CUTTING PARAMETERS FOR SURFACE ROUGHNESS IN TURNING. MATERIALS &
DESIGN, 28(4): 1379-1385.
[2] GHANI, J.A., CHOUDHURY, I.A. AND HASSAN, H.H. (2004). APPLICATION OF TAGUCHI METHOD
IN THE OPTIMIZATION OF END MILLING PARAMETERS. JOURNAL OF MATERIALS PROCESSING
TECHNOLOGY, 145(1): 84-92.
[3] ZHANG, J.Z., CHEN, J.C. AND KIRBY, E.D. (2007). SURFACE ROUGHNESS OPTIMIZATION IN AN
END-MILLING OPERATION USING THE TAGUCHI DESIGN METHOD. JOURNAL OF MATERIALS
PROCESSING TECHNOLOGY, 184(1-3): 233-239.
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#88
STRUCTURAL GLASS MATERIAL FOR MEMBERS AND PARTS OF LOADCARRYING STRUCTURES IN CIVIL ENGINEERING
Marcela Karmaznov, Jindrich Melcher, Ondej Peek
Brno University of Technology, Faculty of Civil Engineering
ABSTRACT
The paper is focused on the problems of properties of structural glass and its usage in the
members and parts of load-carrying structures of building constructions. Glass as a traditional
material is usually used for transparent fills of window or door openings, but recently it is also
used for load-carrying structures, the most often as a material of load-carrying parts of wall or
roof claddings, but still more often also for parts of usual load-carrying structures, like as
staircases, floors, roof structures and of course, their partial parts, but also, for example, largevolume aquariums. The essential part of this paper presents the overview of some selected
results of the verification of structural glass used for several various types of structures, which
have been performed on the paper authors workplace in the period of about 20 last years. For
the verification of mentioned glass structures the experimental, analytical and numerical methods
have been applied.
There are many various types of components made of structural glass, from the viewpoint of
chemical composition, technological treatment and structural composition. The basic type of
construction glass is clear float glass. Increasing in mechanical strength can be achieved by
tempering or toughening. Due to cooling, the tensile stress occurs inside the structure of
tempered glass, while on the surface the compressive stress occurs. It is classified as a safety
glass. Another type of heat-strengthened glass is semi-hardened partially tempered glass. Its
mechanical properties are not changed during the gradual heating up to 200 C and are not
affected by temperatures below freezing. Laminated safety glass is composed of two or more
panes of tempered or heat-strengthened glass, with intermediate foil.
a)
b)
c)
d)
Fig. 1 Examples of typical glass structures of buildings: a) Audio-Video Center in San Francisco; b)
Lincoln Center in New York; c) Waterloo Station in London; d) International Forum in Tokyo
a)
b)
c)
d)
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Fig. 2 Examples of large glazed facades with stiffening fins: a) South Bank University in London; b)
Holiday Inn in Paris; c) Burj Al Arab Hotel in Dubai; d) Harbour Grand Kowloon Hotel in HK.
Among many known and interesting glass structures over the world, the following selected
examples can be mentioned as typical: In Fig. 1, staircase grades, as well as the vertical support
structure of the walls reinforced by transverse ribs, are made of glass; the wall structure stiffened
by twisted rope is indicated in Fig. 1b; high glazed external walls of buildings need to stiffen by
load-carrying steel structure forming a support system of glass cladding, with regard to the
considerable effects of pressure and suction of the wind; Fig. 1c and Fig. 1d show constructions of
the glass walls with a supporting system forming by the rods and struts; the most spread systems
are the large glazed building facades with the stiffening ensured by the transverse glass fins see
examples in Fig. 2. Authors workplace deals with the problems of structural glass already longterm. Some selected examples of the verification of structural glass intended for different types of
members and parts of civil structures are shown in Fig. 3. Fig. 3a shows one of the first
experiments of this type, which was used for the verification test of the resistance of glass panels
of the railing at the bridge "Vysoina" in Velk Mezi, for the load effects corresponding with
pressure and sucking of the wind. Fig. 3b is an illustration of one of the test specimens failed
within the experimental verification of the panels intended for the bus station roofing in Ostrava.
In both cases the effective vacuum testing method has been applied for the uniform load
simulating wind effects. As another example of the behaviour of the panels made of structural
glass, the failure of the specimen composed of three-layer insulating glass intended for cladding
buildings is indicated in Fig. 3c. Within the verification and evaluation of glass structures, also
numerical models have been utilized, similarly as for example in the case of assessment of the
causes of the accident of the aquarium at ZOO see Fig. 4.
a)
b)
c)
Fig. 3 Selected examples of experimental verification of structural glass components
a)
b)
Fig. 4 Illustration of fracture of aquarium walls and appropriate numerical model in ANSYS
References
HALDMAN, M, LUIBLE, A. AND OVEREND, M. STRUCTURAL USE OF GLASS, ZURICH: ETH ZURICH,
2008, 215 PP. ISBN 3-85748-119-2.
GORIS, A. BAUTABELEN FUR INGENIEURE: MIT BERECHNUNGSHINWEISEN UND BEISPIELEN, KLN,
WOLTERS KLUWER DEUTCHLAND GMBH (IN GERMAN LANGUAGE), 2008, 555 PP. ISBN 978-38041-5236-6.
MELCHER, J. AND KARMAZNOV, M. PROBLEMS OF BEHAVIOR AND ANALYSIS OF GLASS
STRUCTURAL MEMBERS WITH RESPECT TO THEIR APPLICATION IN CONSTRUCTION, IN PROC. OF
THE SEVENTH INTL STRUCTURAL ENGINEERING AND CONSTRUCTION CONFERENCE ISEC-7
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Session 5A
WED, 16:00 -17:30
Room A
TOPIC: Analytical and Numerical Modeling II
Chair: Paulo Tavares de Castro
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N 10 10 ). Their distribution is
fatigue loading (number of loading cycles varied in the range =
determined by the level of nominal stresses N and by the theoretical stress concentration
0
factor .
The problem related to distribution of es is solved using analytical, numerical or experimental
methods. Here the type of eS distribution depends on resistance of the material to elastic
(Young's modulus E ) and plastic deformations (hardening modulus m ). Material properties in
case of low-cycle fatigue depend on N and eS . As the values of N , N and are increased and
the value of m is decreased the nonuniformity of eS is magnified. This leads to the development
of local cyclic damages d that depend on eS and N . To describe them the Neiger-Coffin relation
is used.
As damages d reach critical values dC in stress concentration zones, a large number of
microcracks nCN are being initiated. The number of microcracks nNC in the laboratory specimens
at the initial stage of loading lies in the range of 10 to 20. The crack growth rate dl / dN depends
on d , eS and N . When d and N are further increased, the number of growing cracks nCN starts
to reduce gradually while their growth rate rises up.
At the final stage one can see a single crack (nCN = 1) that is growing at a high rate dl / dN . This
stage of damage accumulation and single crack growth is characterized by a transition from
multiple crack development mode of failure ( nNC >> 1 ) to critical main crack destruction mode of
failure (nNC = 1) .
The process of initiation and growth of low-cycle fatigue cracks in stress concentration zones is
characterized by the deflection from well-known Paris Erdogan crack growth law. Initial multiple
cracks in zones of intensive damage d grow at higher rates dN / dl than it could have been
expected according to classical equations of cyclic fracture mechanics.
The paper presents the results of experiments and calculations for fields of deformations eS and
emax and damages d , number of cracks nNC and crack growth rates dl / dN . The experiments
were carried out on flat specimens with holes ( = 2.5) . The specimens were made of steels
used in construction of pressure vessels that have different yield points y and hardening
moduli m .
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force, which is transferred right before and after the joint, cannot be equally distributed.
Consequentially an additional bending load of pane 4 has to be considered.
(v) Superposition: Subsequently, the resulting stress / strain distribution in the joint cross section
can be calculated by superposition of the results obtained in step (i), (iii) and (iv).
The results presented below are based on the following assumptions: L = 583 mm, t = 10 mm, tint =
1.52 mm, Youngs modulus E = 67,000 MPa, case 1 interlayer shear modulus G = 182 MPa, case 2
interlayer shear modulus G = 7 MPa.
Figure 2 illustrates the predicted strain distribution according to the model in the longitudinal
direction as well as along the joint cross section for both cases of G. The prediction is compared to
the strain distribution obtained by FE simulations, as well as in experimental tests.
The strain distributions in figure 2 indicate that the prediction obtained with the
analytical model corresponds well to the results obtained from FE simulations and
experimental tests. Figure 2: Comparison of the analytical model to results obtained by FE
simulations and experimental tests: (a) and (b) strain distribution along the x and y-directions
respectively with E/G 370 and F = 4,001 N; (c) and (d) strain distribution along the x and ydirections respectively with E/G 9,500 and F = 4,020 N
The load-bearing behavior of a spliced laminate with linear elastic material properties under
tensile load can be described with an analytical model, which is based on the load redistribution
due to stiffness and bending of a sandwich element. The results indicate that the joint has a
significant influence by considerably increasing the maximal strain. Furthermore, the joint shows a
wide-reaching influence zone.
References
[1] VOLKERSON, O.: DIE NIETKRAFTVERTEILUNG IN ZUGBEANSPRUCHTEN NIETVERBINDUNGEN
MIT KONSTANTEM LASCHENQUERSCHNITT. LUFTFAHRTFORSCHUNG, 15, 41-47, (1938).
[2] STAMM, K.; WITTE, H.: SANDWICHTRAGKONSTRUKTIONEN BERECHNUNG, FERTIGUNG,
AUSFHRUNG. SPRINGER-VERLAG; WIEN, NEW YORK, (1974).
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ABSTRACT
A constitutive model for a mechanical analysis is a relationship between the response of a body
(for example, strain state) and the stress state due to the forces acting on the body, which can
include the environmental effects. A wide variety of material behaviours are described with a few
different classes of constitutive equations [1].
The hyperelastic models have been used extensively to model the non-linear behaviour and
anisotropic material, since the soft tissues under large deformations often regain their elasticity.
The constitutive behaviour of hyperelastic materials is defined in terms of deformation energy
potential [2].
In this study, were performed simulations of Newtonian fluid flow in channels with disorders such
as the aneurysms. The main goals of these simulations were to analyse the fluid flow in the
channels and the mechanical behaviour of channels walls. The material used for channels was the
PDMS which has a hyperelastic behaviours and to simulate that structure were used different
constitutive models, under the same conditions, aiming to analyse the most appropriate model
for this type of study. Thus, the deformations suffered were visualized on the walls of the
channels, caused by the internal pressure induced by the internal fluid.
It was used Ansys - Fluent software, to perform the simulation of the Newtonian fluid flow
(glycerin, with well-known properties and sufficient viscosity to measure the pressure drops), in
order to determine the speed and the internal pressure. This pressure, approximately 11.742e-6
MPa for an input flow rate of 300 L/min, was imported into the channels in Ansys - Static
Structural, in order to be able to evaluate and analyse the deformations and stresses in the
channel wall, caused by internal pressure induced by the fluid flow. To do this, was used the most
known hyper-elastic constitutive models.Six constitutive models were simulated, they being:
Ogden 2nd and 3rd Order, Yeoh 2nd and 3rd Order and Mooney-Rivlin 5 and 9 Parameter. All the
analysed constitutive models converged for a solution.
The obtained results of numerical simulations for these six models showed little variation among
them. This small variation is explained because the flaw rate used in the Fluent simulation
induced a low pressure within the channel which caused a small deformation field and for these
values all the constitutive models could follow the material mechanical behaviour. If the internal
pressure is much higher, probably the results obtained for the different constituent models will be
very different. In Fig. 1 is presented an example of the resulted obtained for two different
constitutive models.
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Figura 1 - Total deformation occurred in the channel wall calculated by the constitutive model of MooneyRivlin 5 Parameter and Yeoh 3rd Order, respectively.
In the Table 1 is present the comparison among the maximum and minimum displacements
obtained in the FEM simulations. It is possible to verify that the obtained displacements are very
low for all the analysed models, even for maximum values. The standard deviation is also low that
indicates the calculated values tend to be very close to the average and range from 0.755E-4 and
0.05E-8 for the maximum and minimum values.
Tabela 1 Maximum and minimum values of the different models and mean and standard deviation
corresponding.
Constitutive model
Mooney-Rivlin 5 Parameter
Mooney-Rivlin 9 Parameter
Ogden 2nd Order
Ogden 3rd Order
Yeoh 2nd Order
Yeoh 3rd Order
Average
Standard deviation
In summary, it is concluded that any constitutive model referred to above, can be applied to such
studies, allowing the study behaviour of the PDMS channel wall, particularly for the analysis of
stress and displacement field on the aneurysm. In further studies it would be interesting analyse
the channel wall behaviour for higher internal pressures and for a Non Newtonian fluid which the
properties were more close to blood.
References
[1] P. R. FERNANDES, P. BARTOLO, TISSUE ENGINEERING: COMPUTER MODELING,
BIOFABRICATION AND CELL BEHAVIOR, EDITED BY SPRINGER, COMPUTATIONAL METHODS IN
APPLIED SCIENCES, LISBON PORTUGAL, 2014.
[2] J. MART, A. OLIVER, J. FREIXENET, R. MART, DIGITAL MAMMOGRAPHY: 10TH
INTERNATIONAL WORKSHOP, EDITED BY SPRINGER, INSTITUTE OF INFORMATICS AND
APPLICATIONS, UNIVERSITY OF GIRONA, CATALONIA, SPAIN, PG. 729, JUNE 2010.
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Institute of Science and Innovation in Mechanical and Industrial Engineering, University of Porto
Rua Dr. Roberto Frias, 4200-465 Porto, Portugal.
2
Faculty of Engineering, University of Porto, Rua Dr. Roberto Frias, 4200-465 Porto, Portugal.
3
Department of Civil-Environmental Engineering and Architecture, University of Parma, Viale G.P.
Usberti 181/A, 43100 Parma, Italy.
4
Department of Construction and Manufacturing Engineering, University of Oviedo, Campus de
Viesques, 33203 Gijn, Spain.
ABSTRACT
The Kitagawa-Takahashi (KT) diagram [1] represents a boundary in terms of crack size and stress
range for which infinite fatigue lifetime of structural or mechanical components can be safely
ensured due to non-propagating micro- and macrocracks [2]. The fatigue life assessment can be
related to the classical fatigue limit concept, based on experimental S-N curves, and the threshold
stress intensity factor range or threshold value of the cyclic J-integral, based on fracture
mechanics using propagation laws.
In this paper, a procedure is proposed to obtain the probabilistic Kitagawa-Takahashi diagram for
structural components. This procedure is based on the equivalent initial flaw size (EIFS) model [34] and is supported by the probabilistic S-N model proposed by Castillo and Fernndez-Canteli [5].
With the EIFS concept and based on fracture mechanics, particularly on elastoplastic cyclic Jintegral, the initial defects of the structural components will be taken into account. This approach,
combined with the probabilistic S-N field, allows the generation of the probabilistic distribution of
the EIFS. Also, a probabilistic KT diagram (P-KT) is presented as an alternative way to understand
the distribution of the EIFS. The procedure proposed is applied to a notched plate made of
P355NL1 steel. The performances of predictions are analyzed and deviations discussed.
References
[1] KITAGAWA H., TAKAHASHI S. APPLICABILITY OF FRACTURE MECHANICS TO VERY SMALL
CRACKS OR CRACKS IN THE EARLY STAGE. PROC. OF THE 2ND INT. CONF ON MECH. BEHAVIOUR
OF MATERIALS, ASM, 627631, 1976.
[2] FERNNDEZ-CANTELI A., BRIGHENTI R., CASTILLO E. TOWARDS A PROBABILISTIC CONCEPT OF
THE KITAGAWA-TAKAHASHI DIAGRAM. PROCEEDINGS OF THE 4TH INTERNATIONAL CONFERENCE
ON CRACK PATHS (CP 2012), GAETA, ITALY, 2012, 1041-1048.
[3] XIANG Y., LU Z., LIU Y. CRACK GROWTH-BASED FATIGUE LIFE PREDICTION USING AN
EQUIVALENT INITIAL FLAW MODEL. PART I: UNIAXIAL LOADING. INTENATIONAL JOURNAL OF
FATIGUE, VOL. 32, NUM. 2, PP. 341-349, 2010.
[4] SAVAIDIS G., SAVAIDIS A., ZERRES P., VORMWALD M. MODE I FATIGUE CRACK GROWTH AT
NOTCHES CONSIDERING CRACK CLOSURE. INTENATIONAL JOURNAL OF FATIGUE, VOL. 32, NUM.
10, PP. 1543-1558, 2010.
[5] CASTILLO E., FERNNDEZ-CANTELI A. A GENERAL REGRESSION MODEL FOR LIFETIME
EVALUATION AND PREDICTION, INT. J. FRACT., 2001; 107, PP. 117137.
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Session 5B
WED, 16:00 -17:30
Room B
TOPIC: Testing II
Chair: Jos Correia
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Glass fiber reinforced epoxy resin composites have become very attractive engineering materials
in recent years and have extensively replaced popular metallic and polymeric materials in many
industrial application [1-2]. The polyhedral oligomeric silsesquioxanes (POSS) which are inorganic
organic modifiers may be used as additives, catalytic agent, reinforcement, processing aids and
flame retardants in the epoxy compositions [3-5]. Therefore, the aim of this study was to verify
the influence of aluminosilsesquioxane (POSS) addition on thermo mechanical properties of glass
fiber reinforced epoxy composite prepared at various curing conditions.
The following components were used in this studies: epoxy resin Epidian 6 (E6) based on
bisphenol A, triethylenetetramine as a curing agent (both produced Chemical Works OrganikaSarzyna, Poland) and bis(heptaphenylaluminosilsesquioxane) (POSS) C84H70Al2O24Si14
(synthesis by Department of Organometallic Chemistry, Faculty of Chemistry, Adam Mickiewicz
University, Poland
The epoxy composites were fabricated in a mould using hand lay-up with glass woven fabrics (GF).
Two different types of epoxy composites were produced: first group of samples only with glass
woven fabrics and second group of samples with glass woven fabrics and 1wt %POSS as the epoxy
resin modifier. Composites were cured at ambient temperature (20C) for 24 h and post-cured for
2 h at the different temperatures: 80C, 100C, 120C, 140C and 160C.
The dynamic-mechanical properties of the post-cured samples were investigated by DMTA
measurements in a torsion mode, at frequency f = 1 Hz in the temperature range between 25C
and 150C, and at heating rate 2C min. Detailed analysis of storage modulus vs. temperature
curve provides information about stiffness, degree of cross - linking and fibre/matrix interfacial
bonding of materials [6]. Plots of the storage modulus G and tan versus temperature T for
representative types of composites are shown in Figures 1. The composites with POSS indicated
more constant properties (G at 25 C) during various curing conditions when compared to the
reference sample. The values of the glass transition temperature of the composites increase
together with the increase of the temperature post-curing. The increase of the composites glass
transition temperature indicated that a post-curing process had occurred.
The composites modified with POSS showed more stable properties at higher post-curing
temperatures than reference sample. Hence, these types of composites can be used as
construction materials with resistance to temperature changes.
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Fig.1 The DMTA curves of the E6_GF and E6_GFPOSS samples post-cured at 140C
References
[1] BORREGO LP, COSTA JDM, FERREIRA JAM, SILVA H., COMPOSITES PART B: 2014, 62, 65-72
[2] KLING S., CZIGNY T., COMP. SCI. TECH. 2014, 99, 82-88
[3] CHO H., LIANG K., CHATTERJEE S., PITTMAN JR. CU., J INORG ORGANOMET POLYM 2005,15,
541-553
[4] CONSTANTIN F., GAREA S.A., IOVU H., U P B SCI BULL SERIES B 2010, 2 (2),103-114
[5] CHRUCIEL JJ., LENIAK E., PROGRESS IN POLYMER SCIENCE 2015, 41,67-121
[6] JAWAID M., ABDUL KHALIL H.P.S., OMAR S. ALATTAS COMPOSITES: PART A, 2012, 43, 288293
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0
-10
29 Hz
-20
-30
-40
-50
-60
-70
-80
0
40
80
120
160
200
[Hz]
240
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280
320
360
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In order to observe the dynamic behavior of the considered specimens, numerical simulations
were carried out in addition to the experimental determination of the eigenfrequencies of these
materials [4].
The dynamic modulus of elasticity is influenced by the non-uniformity coefficient, calculated from
[5]. The greater the number of defects, an increasing value of the non-uniformity coefficient is
obtained and the modulus of elasticity decreases as shown in Figure 2.
Acknowledgement
The work has been funded by the Sectoral Operational Programme Human Resources
Development 2007-2013 of the Ministry of European Funds through the Financial Agreement
POSDRU/159/1.5/S/132397
References
[1] TANAKA, M., AND OTHERS, INFLUENCE OF NON-UNIFORM FIBER ARRANGEMENT ON TENSILE
FRACTURE BEHAVIOR OF UNIDIRECTIONAL FIBER/EPOXY MODEL COMPOSITES, COMPOSITE
INTERFACE, 12(3-4), 2005, P. 365-378.
[2] JARVE, E.V., KIM, R., STRENGTH PREDICTION AND MEASUREMENT IN MODEL MULTILAYERED
DISCONTINUOUS TOW REINFORCED COMPOSITES, JOURNAL OF COMPOSITE MATERIALS, 38(1),
2004, P. 5-18.
[3] GIBSON, R.F. (1994). PRINCIPLES OF COMPOSITE MATERIAL MECHANICS, MC GRAW-HILL, ISBN
0-07-113335-6, USA.
[4] FRISWELL, M.I., MOTTERSHEAD, J.E., FINITE ELEMENT MODEL UPDATING IN STRUCTURAL
DYNAMICS, KLUVER ACADEMIC PUBLISHERS, ISBN 0-7923-3431-0, THE NETHERLANDS.
[5] BOLCU. D., STNESCU, M.M., CIUC, I., DUMITRU, S., SAVA, M., THE NON-UNIFORMITY FROM
THE COMPOSITE MATERIALS REINFORCED WITH FIBER GLASS FABRIC, MAT. PLAST., 51(1), 2014, P.
97-100.
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(a)
(b)
Fig. 1 (a) Microstructure image of iron particles (b) Scanning electron microscope image of elastomer
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Fig. 2. (a) Photographic image of experimental set up for deformation test (b) Schematic diagram of testing.
Fig. 3 (a) Hysteresis loss of the MSE samples (b) Force versus time curve of the MSE samples at various
magnetic intensity.
Acknowledgement
Authors acknowledge for the work carried out at Technical University of Liberec.
References
[1] M . KALLIO, THE ELASTIC AND DAMPING PROPERTIES OF MAGNETO RHEOLOGICAL
ELASTOMER, 2005.
[2] JARMIL VLACH, HOANG SY TUAN, BOHDANA MARVALOV: EXPERIMENTAL AND NUMERICAL
RESEARCH OFMAGNETO-SENSITIVE ELASTOMERS. 47TH INTERNATIONAL CONFERENCE OF
EXPERIMENTAL STRESS ANALYSIS. SYRCHOV, JUNE 8-11, 2009, CZECH REPUBLIC, PP.283-290, ISBN
978-80-7372-483-2.483-2.
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Research Unit: Materials, Processes and Environment (UR/MPE), University of Boumerdes, 35000
Boumerdes, Algeria, fadyesdid@yahoo.fr
ABSTRACT
The work undertaken deals with the valorisatin of industrial waste .To do so it was a good idea to
proceed to different studies namely :
A characterization carried on crude vegetable oils from sunflower (feedstock) has provided a
good understanding of their lubricating character, resulted in a publication. The study of
industrial waste which is actually wash water following a neutralization of refining a crude oil
vagtale resulted in a communication. The separation of the wash water has demonstrated that
the presence of the soap and neutral oil forming a stable emulsion with the qualities of
biodegradable surfactants also followed by a communication. Following its recovery, we have
proceeded the characterization of this proven biodegradable water to lubricating properties a
multi-use that have been two communications followed a study of a biomass (for the soap)
another statement on the identification of a viscous fluid (concerning oil)
For the valorisation of industrial waste, we have decided for its use as food for leather tanning.
Preliminary tests were encouraging for its use as a lubricant fibrillar, and this , after rechomage
. In addition to that, we have alaboared many formulations, with different percentages ,
based on commercials food associated to wash water which shall be our subject of discussion
for the presente conference . These formulations were submitted to different oleo-chemical tests
and gave satisfactory result.Physiocomcaniques tests carried on formal tests concerning the
NAPPA in the wet bleu state ( trivalent chromium tanned leather ) were verified and gave
convincing results for the tanners .
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Session 6
THU, 16:00 -17:30
Room B
TOPIC: Degradation, durability and corrosion
Chair: Rui Miranda Guedes
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Institute of Physical Chemistry Ilie Murgulescu, Splaiul Independentei 202, Bucharest, Romania
2
. Politehnica University from Bucharest, Splaiul Independentei 313, Romania
alexandrabanu14@yahoo.com
ABSTRACT
In literature, there are a lot of data concerning the mechanical properties of titanium alumides
materials and correlation between the chemical composition and their capability to undertake
and transmit efforts at high temperatures. Less data exist about the corrosion behavior, even this
is a challenging and the most limiting characteristic. Through these data, those about corrosion
behavior in aqueous environments are less than oxidation data.
The poor resistance of these materials in chlorides and sulphates is one of most important
characteristic for their utilization in waste burning equipment or aero and hydro components in
contact with salted water.
This work have as main task the corrosion behavior study of two titanium aluminides (chemical
composition Table 1) in synthetic seawater using voltametric and EIS techniques in order to
identify the influence of chemical composition and structure on corrosion behavior and of
coatings necessity for these applications. The alloys structure and corrosion products analysis is
done using SEM, EDAX, Raman and XRD techniques. The used aggressive environment with
chemical composition of: NaCl 243,6gL-1; KCl 0.67gL-1; CaCl2x2H2O 1,36gL-1; MgSO4x7H2O 6,29gL-1;
MgCl2x6H2O 4,66 gL-1; NaHCO3 0,18 gL-1 was prepared from Aldrich reagents.
Table 1 Chemical composition of titanium aluminides (at%)
Samples
Ti
Al
Nb
Zr
Mo
o- TiAl
50
22
25
2 -Ti3Al
68
19
10
As is shown in the figures 1 and 2 orto titanium aluminide in cast form presents a better
electrochemical behavior in seawater environment.
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References
[1] D. ALVARADO, P.A SUNDARAM , A STUDY OF THE CORROSION BEHAVIOR OF GAMMA
TITANIUM ALUMINIDE IN 3.5 WT% NACL SOLUTION AND SEAWATER, CORROSION SCIENCE 49
(2007) 37323741
[2] Y. XIONG, S. ZHU, F. WANG, SYNERGISTIC CORROSION BEHAVIOR OF COATED TI60 ALLOYS
WITH NACL DEPOSIT IN MOIST AIR AT ELEVATED TEMPERATURE, CORROSION SCIENCE 50 (2008)
1522
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Fig 1 SEM image (SEI) showing the Al2O3 coating aspect: compact layer having some superficial
microcracks
- it can be seen in the BSE image in fig.2 that a 10-20 um depth diffusion zone from the NiCrAlY
toward the support, during the high temperature exposure; the EDS spectrum collected from one
of these areas (fig.3)demonstrated that the most obvious diffusion tendency is shown by nickel.
References
[1] C. LEYENS, M. PETERS, Titanium and titanium alloys: fundamentals and applications, WileyVCH Verlag GmbH, Wenheim, 2003.
[2] J. XIA, X.Y. LI, C.X. LI, H. DONG, The structural and mechanical property characterisation of
thermal oxidation treated g-based titanium aluminide, Thin Solid Films 458 (2004) 212222.
[3] G. MOSKAL, Thermal barriers coatings: characteristic of microstructure and properties,
generation and directions of development of bonds, Journal of Achievements in Materials and
Manufacturing engineering, 37 (2013) 323-331.
[4] S.L. DRAPER, B. A. LERCH, J. M. PEREIRA, K. MIYOSHI, Durability Assessment of Gamma TiAl
Final Report, NASA/TM2004-21230
[5] M. KEMDEHOUNDJA, J.L. GROSSEAU-POUSSARD, J.F. DINHUT, Raman microprobe
spectroscopy measurements of residual stress distribution along blisters in Cr2O3 thin films, Appl.
Surf. Sci. 256 (2010) 27192725.
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References
[1] M. MARCIUS, M. RISTIC, M. IVANDA, S. MUSIC, FORMATION AND MICROSTRUCTURE OF
NICKEL OXIDE FILMS, JOURNAL OF ALLOYS AND COMPOUNDS 541 (2012) 238243
[2] P.M. SOUSA, A.J. SILVESTRE, O. CONDE, CR2O3 THIN FILMS GROWN AT ROOM TEMPERATURE
BY LOW PRESSURE LASER CHEMICAL VAPOUR DEPOSITION, THIN SOLID FILMS 519 (2011) 3653
3657
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#74
Institute of Composite Structures and Adaptive Systems, DLR - German Aerospace Center,
Germany, aurelie.viandier@dlr.de
Institute of Adaptronics and Functional integration, Technical University of Braunschweig,
Germany
ABSTRACT
High-performance industries such as aviation, aerospace or automobile require structures with
high specific strength and stiffness along with outstanding damage tolerance, fire resistance,
fatigue and impact resistance. One possibility to meet these numerous demands is a judicious
combination of different materials. In this regard, Fibre-Metal Laminates (FMLs), advanced
materials consisting of layers of polymer matrix composite alternated with metal foils as in Fig. 1,
are developed and benefit from growing attention. The present study focuses on FMLs composed
of carbon-fibre reinforced plastic (CFRP, based on Prepreg HexPly 8552/AS4) and stainless steel
1.4310 (AISI 301). This material choice is based on the similar mechanical properties of both parts,
especially strength and stiffness, in order to reach a high structural efficiency. As a heterogeneous
system, it is expected to ally the beneficial properties as well as compensate the weaknesses of its
sole constituents, while fulfilling its service life requirements. Nevertheless, the hybrids durability
and reliability under operating conditions is of concern [1-2]. Indeed, FMLs based on carbon fibres
and metal alloys are expected to experience degradation over time in service. In fact, since the
CFRPs resin can absorb moisture, carbon fibres are electrically conductive and CFRP plies are in
direct contact with the steel sheets, stainless steel could undergo the natural and inevitable
process of corrosion. Yet, corrosion inevitably leads to the detrimental change of the chemical,
physical and mechanical properties of the material. Therefore, the reactions taking place inside
the FML should be investigated and the properties deterioration described.
The study's objective is hence to comprehend the undergone
degradation at the CFRP/metal-interface in order to allow predicting
the change in mechanical properties of the FML subjected to
hygrothermal conditions. For this purpose, an appropriate testing is
selected given the materials, the corrosion forms that might occur for
this particular system and the service conditions. Conventional
methods based on physical changes are hence hardly feasible but it is
possible to observe chemical state changes utilizing electrochemical
techniques. The latter are commonly used for the study of metals
corrosion and receive increasing attention for studying CFRP as selfFig. 1 CFRP/stainless
sensing
materials for health monitoring applications. The two
steel-FML
electrochemical tests utilized are:
- Potentiodynamic polarisation - the recording of the polarization curves of steel and CFRP taken
separately by means of a potential sweep over a broad range. Subsequently, the curves are
overlapped to have an insight into the galvanic corrosion behaviour of the heterogeneous system
as in Fig. 2.
- Electrochemical impedance spectroscopy (EIS) - the measurement of the electrode response to a
low amplitude sinusoidal potential modulation. It permits to characterize electrochemical
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processes taking place in the vicinity of the electrode through the determination of an equivalent
electrical circuit [3]. Thus, the electrolytes resistance, the double layer capacitance and the
materials polarization resistance can be defined; and kinetic parameters can be extracted. In
addition, EIS is a non-destructive technique (NDT) and can be coupled with mechanical testing.
Besides, both techniques require the same experimental configuration: a three-electrode test
setup connected to a potentiostat (here a Vertex from Ivium Technologies). The probe under
study works as the working electrode, a Ag/AgCl-electrode serves as reference electrode and a
Pt/C-foil as the counter electrode.
Fig. 2: Overlapping of the polarisation curves for determining the corrosion parameters
The methods could be implemented with success and led to the following results. The polarization
measurements show that CFRP forms a galvanic corrosion cell with stainless steel; the carbon
composite being the systems cathode (more positive potential) and steel the anode. Besides, the
system displays a critical potential difference of 397 mV. So stainless steel corrodes and pits
appear on its surface. The polarisation tests also enable determining all corrosion parameters
including the systems galvanic current density of 23.1 nA/mm indicating the corrosion rate; its
galvanic potential of 50 mV ie. the energy barrier from which the corrosion occurs; and the
polarisation resistance of each material - the parameter to be improved in order to slow down the
FMLs degradation. It is noted that EIS permits at best to define the materials polarisation
resistance since it dissociates it from the ohmic drop. Thus, the steel presents a higher
polarisation resistance (about 8,943 ) than CFRP (352 ), which is supposedly due to its passive
behaviour. Nonetheless, the pit formation implies the local destruction of the passive oxide layer.
In the end, carrying out potentiodynamic polarisation and EIS is a powerful approach to foresee
the galvanic corrosion behaviour of FMLs under service conditions.
Acknowledgements
The authors wish to thank the following persons from the InES-Institute at TU Braunschweig: Prof.
Ulrike Krewer for hosting and enabling the performance of pre-tests in her lab; Daniel Schrder for
discussions on and assistance for the polarization measurements; Nina Bge for friendly advice.
References
[1] T. SINMAZELIK, E. AVCU, M.. BORA, AND O. OBAN. A REVIEW: FIBRE METAL LAMINATES,
BACKGROUND, BONDING TYPES AND APPLIED TEST METHODS. MATERIALS AND DESIGN,
32(7):3671-3685, 2011.
[2] Z. PENG AND X. NIE. GALVANIC CORROSION PROPERTY OF CONTACTS BETWEEN CARBON
FIBER CLOTH MATERIALS AND TYPICAL METAL ALLOYS IN AN AGGRESSIVE ENVIRONMENT.
SURFACE AND COATINGS TECHNOLOGY, 215(0):85-89, 2013.
[3] M.E ORAZEM AND B. TRIBOLLET. ELECTROCHEMICAL IMPEDANCE SPECTROSCOPY. JOHN
WILEY & SONS, 2008.
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Session 7
THU, 16:00 -17:00
Room B
TOPIC: Polymers and Polymer Matrix Composites II
Chair: Daniel F. O. Braga
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The set of analytical methods (enabling the multiscale material characterization from the
segmental up to macroscopic levels) revealed that all-aliphatic three-componental polycarbonatebased PU films can be considered as hydrolytically and thermally stable elastomeric materials
keeping excellent mechanical properties within the period up to 12 months. On the other hand,
four-componental PU elastomeric films containing in addition oligomeric D,L-lactide-based linker
can be considered as efficient and prosperous biodegradable materials.
Acknowledgement
The Authors wish to thank the financial support of the Grant Agency of the Czech Republic (Czech
Science Foundation, project No. 13-06700S).
References
[1] PRKOV M, PAVLIEVI J, STRACHOTA A, PORBA R, BERA O, KAPRKOV L, BALDRIAN J,
LOUF M, LAZI N, BUDINSKI-SIMENDI J. NOVEL POLYCARBONATE-BASED POLYURETHANE
ELASTOMERS: COMPOSITION-PROPERTY RELATIONSHIP. EUROP POLYM J 2011;47(5):959-972.
[2] PORBA R, PRKOV M, BROOV L, LAZI N, PAVLIEVI J, STRACHOTA A. ALIPHATIC
POLYCARBONATE-BASED POLYURETHANE ELASTOMERS AND NANOCOMPOSITES. II.
MECHANICAL, THERMAL, AND GAS TRANSPORT PROPERTIES. J APPL POLYM SCI 2013;127(1):329341.
[3] PRKOV M, MACHOV L, KOBERA L, BRUS J, PORBA R, SERKIS M, ZHIGUNOV A.
MULTISCALE APPROACH TO THE MORPHOLOGY, STRUCTURE, AND SEGMENTAL DYNAMICS OF
COMPLEX DEGRADABLE ALIPHATIC POLYURETHANES. J APPL POLYM SCI 2015;132(10):41590.
[4] PORBA R, KREDATUSOV J, HODAN J, SERKIS M, PRKOV M. THERMAL AND MECHANICAL
PROPERTIES OF MULTIPLE-COMPONENT ALIPHATIC DEGRADABLE POLYURETHANES. J APPL
POLYM SCI 2015; 132:41872.
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Fig.1 : Creep strain versus time of PLA and its nanocomposites, at various aging time periods.
Creep strain data were simulated by employing linear viscoelastic models. The accelerated creep
strain at the tertiary creep stage, has been successfully modeled by a nonlinear viscoplastic model
[4], while the stress-strain curves were predicted with the same set of parameters.
It must be concluded that at the particular aging conditions studied, silica nanoparticles
accelerate the degradability of PLA, having a higher impact on Youngs modulus, and creep
response.
References
[1] S. K. SAHA AND H. TSUJI. EFFECTS OF MOLECULAR WEIGHT AND SMALL AMOUNTS OF D-
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Laboratory of Solid Mechanics, Ecole Polytechnique, Route de Saclay, 91128, Palaiseau, France
Department of Mechanical and Aeronautical Engineering, Composite Materials Group, University
of Patras, Patras 26500, Greece
ABSTRACT
In this study, the hybrid viscoelastic interphase model [1] meets its optimization development,
incorporating assumptions which extend models influence and validity. In composite materials,
by the term hybrid interphase, it is meant the interphase material having a volume fraction that
represents the percentage of the bulk matrix surrounding the reinforcement, in which a specific
matrix property is strongly affected by the existence of the reinforcement. The hybrid interphase
thickness represents the maximum radial distance from the inclusion to the matrix boundary, a
regime where all the properties exponentially vary [2]. This third phase includes micro-cracks,
stress concentrations [3-5], residual stresses etc, having properties that are strongly affected not
only by the presence of the reinforcement, but also by the imperfect bonding between the
constituent materials. Thus, it is a possible region for failure initiation, while it exhibits a timedependent response, as a matrix-modified viscoelastic material [6-8].
According to the hybrid interphase model, the interphasial thickness is not a constant value, but it
depends on the property considered at the time, as well as on the creep time. In addition, the
parameter of the imperfect bonding is introduced through the degree of adhesion [9]. Despite
models indisputable effectiveness and significant contribution to the field of interphase
modeling, the assumptions of a time-dependent adhesion coefficient and Modulus come to
enhance the analytical expressions, providing a better description of the conflicting
microstructural phenomena occurring in the interphasial regime.
In the present investigation, experimental findings were initially modeled by means of the
originally developed model. The experimental outputs combined with analytical and numerical
results gave a better understanding of the viscoelastic response of long fiber polymer composites.
The application of the model carried out on Epoxy Resin/Luffa Cylindrica (ER/LC) specimens,
subjected to tensile creep at 9.6 MPa stress level (20% of max).
To go one step further, the effective response was recalculated based on the new assumptions,
which were successively added to the model. The adhesive bonds were stochastically distributed
along fibers longitudinal direction, turning the RVE into 2D, depicting a more realistic condition of
the interphase, formed during the manufacturing process. Poissons ratio affects the variation of
the interphasial thickness vs. time and thus it was, also, taken into account in the calculations. The
local - global strains were defined through experiments and homogenization schemes.
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Fig. 1. Left: Luffa Cylindrica fibers, reinforcement of epoxy resin specimens; right: Creep Compliance curves
of pure resin and ER/LC, stress level: 20% of Su
Fig. 2. Interphase Modulus Ei vs. position through the interface thickness for: left: the original hybrid
interphase model; right: the optimized hybrid interphase model taking into account the degradation of
interfacial bonds.
References
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Poster Session
TUE, 17:30 -18:00
Exhibition Area
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Fig. 1 Results for relaxation modulus and strain variation, at a constant load, for PLA, PLA/CNTCOOH0.3 and PLA/CNT-COOH0.7, at 37C.
Tensile tests results revealed tensile strength of PLA was around 61.04 MPa and between 65.75
and 73.40 MPa for PLA/CNT-COOH nanocomposites, depending on their weight percentage of
nanofillers, followed by the plastic regime, ending up on the specimen break. Youngs modulus for
PLA was determined as 4.1 GPa, being improved for nanocomposites, between 4.2 and 4.9 GPa.
Augmentation of toughness, Youngs modulus and tensile strength simultaneously are the most
valuable functionality of these of PLA/CNT-COOH nanocomposites, comparing to previous studies,
indicating a real load transfer from PLA-matrix to nanofillers. Poissons ratio results indicate
mixtures isotropy.
After 1hour, relaxation modulus for PLA was about 1.2 GPa, 1.7 GPa for PLA/CNT-COOH.3 and
2GPa for PLA/CNT-COOH.7. PLA and PLA/CNT-COOH nanocomposites demonstrate nonlinear
viscoelastic behaviour. Storage modulus for PLA/CNT-COOH nanocomposites was higher than the
PLA one, verifying the same tendency on tensile tests.
References
[1] L. S. NAIR, C. T. LAURENCIN, BIODEGRADABLE POLYMERS AS BIOMATERIALS, PROGRESS IN
POLYMER SCIENCE, 32, 762-798, 2007.
[2] D. W. HUTMACHER, SCAFFOLDS IN TISSUE ENGINEERING BONE AND CARTILAGE,
BIOMATERIALS, 21, 2529-2543, 2000.
[3] R. AURAS, L.-T. LIM, S. SELKE, H. TSUJI. POLY(LACTIC ACID): SYNTHESIS, STRUCTURES,
PROPERTIES, PROCESSING, AND APPLICATIONS. POLYMER ENGINEERING AND
TECHNONOLOGY. NEW JERSEY, USA: JOHN WILEY & SONS, 2010.
[4] A.C. VIEIRA, J. C. VIEIRA, J. M. FERRA, F. D. MAGALHES, R. M. GUEDES, A. T. MARQUES.
MECHANICAL STUDY OF PLA-PCL FIBERS DURING IN VITRO DEGRADATION, JOURNAL OF THE
MECHANICAL BEHAVIOR OF BIOMEDICAL MATERIALS, 4(3):451-60, 2011.
[5] D882 ASTM STANDARD TEST METHOD FOR TENSILE PROPERTIES OF THIN PLASTIC SHEETING:
ASTM INTERNATIONAL: WEST CONSHOHOCKEN, 2012.
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Ctia Martins1,2, Viviana Correia Pinto1,2, Rui Miranda Guedes1,2,3, Antnio T. Marques1,3
1
INEGI Institute of Science and Innovation in Mechanical and Industrial Engineering, 4200-465
Porto, Portugal
2
LABIOMEP, Laboraty of Biomechanics of Porto, University of Porto, 4200-465 Porto, Portugal
3
Department of Mechanical Engineering, Faculty of Engineering, University of Porto, 4200-465
Porto, Portugal
ABSTRACT
Current solutions for soft tissues replacements based on biodegradable polymers are susceptible
to visco-elastoplastic behavior which may lead to the device failure. When they are submitted to
large deformations, above the elastic limit, in dynamic or static loading conditions, these materials
will progressively accumulate permanent deformation, which part of it is internal damage, due to
creep and fatigue [1]. Biodegradable devices can fail in long term due laxity or by sudden failure
and, in the case of polymers, creep and fatigue interactions occur at low temperature and these
two phenomena are coupled [1]. An ideal scaffold for ligament repair must display a similar
mechanical behaviour to the natural ligament, being essential to analyze and reproduce
viscoelastic behaviour of the scaffold for the medical device production.
In this work, the focus was given to the study of creep and stress relaxation behaviour of PLA-PCL
fibres and the Burgers model was used to describe the experimental data. PLA-PCL fibres (
0.5mm, length: 80mm), dry and saturated specimens with normal saline solution (0.9% NaCl),
were tested under static and dynamic mechanical loading conditions, i.e. tensile, creep and stress
relaxation tests. Saturated samples were placed in a recipient containing the solution for at least 2
hours, for mimic the human body environment. Additionally, a dropper was used to moisten the
samples and efforts were made to ensure that all the specimens remained saturated throughout
the mechanical tests. The different creep and stress relaxation levels were defined based on
tensile strength (dry specimens: 237.75MPa; saturated specimens: 232.22MPa) and maximum
strain (dry specimens: 76.57%; saturated specimens: 77.40%) values collected from tensile tests
data (engineering curve).
The most linear region of the different creep and relaxation curves are represented in Fig. and
Fig. 2 respectively (in a log-log scale). A linear approach was used in order to calculate creep and
stress relaxation rates.
a
Fig. 1- Creep rate at multiple levels: (a) dry specimens; (b) saturated specimens.
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Fig. 2: Relaxation rate at multiple levels: (a) dry specimens; (b) saturated specimens.
Creep experimental data was used to obtain the Burgers model parameters [2]. Fig. 3 depicts a
good fit of the model to the experimental data. Similarly, experimental stress relaxation data was
used to test the model.
The prediction of stress relaxation behavior using the Burgers model may be considered
qualitatively satisfactory in spite of the assumptions implied by this simple model.
st
References
[1] VIEIRA, A., ET AL., TIME-DEPENDENT DAMAGE ON BIODEGRADABLE DEVICES. JOURNAL OF
BIOMECHANICS, 2012. 45: P. S59.
[2] FINDLEY, W. N., CREEP AND RELAXATION OF NONLINEAR VISCOELASTIC MATERIALS (WITH AN
INTRODUCTION TO LINEAR VISCOELASTICITY). 1976, NEW YORK: DOVER PUBLISHER, INC.
[3] PROVENZANO, P.P., ET AL., APPLICATION OF NONLINEAR VISCOELASTIC MODELS TO DESCRIBE
LIGAMENT BEHAVIOR. BIOMECH MODEL MECHANOBIOL, 2002. 1(1): P. 45-57.
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References
[1] B. OREGAN, M. GRATZEL, A LOW-COST, HIGH-EFFICIENCY SOLAR CELL BASED ON DYE
SENSITIZED COLLOIDAL TIO2 FILMS, NATURE 353 (1991) 737.
[2] A. F. NOGUEIRA, C. LONGO, M. -A. DE PAOLI, POLYMERS IN DYE SENSITIZED SOLAR CELLS:
OVERVIEW AND PERSPECTIVES, COORDINATION CHEMISTRY REVIEWS 248 (2004) 1455.
[3] M. SINGH, V. K. SINGH, K. SURANA, B. BHATTACHARYA, P. K. SINGH, H. -W. RHEE, NEW
POLYMER ELECTROLYTE FOR ELECTROCHEMICAL APPLICATION, JOURNAL OF INDUSTRIAL AND
ENGINEERING CHEMISTRY 19 (2013) 819.
[4] J. WU, P. LI, S. HAO, H. YANG, Z. LAN, A POLYBLEND ELECTROLYTE (PVP/PEG+KI+I2) FOR DYESENSITIZED SOLAR CELLS, ELECTROCHIMICA ACTA 52 (2007) 5334.
[5] Y. YAN, J. WANG, Q. CHANG, M. BABIKIER, H. WANG, H. LI, Q. YU, S. GAO, S. JIAO,
FABRICATION OF MESOPOROUS TIO2 ELECTRODES BY CHEMICAL TECHNIQUE FOR DYESENSITIZED SOLAR CELLS, ELECTROCHIMICA ACTA 94 (2013) 277.
[6] M.-S. KANG, J. H. KIMB, J. WON, Y. S. KANG, DYE-SENSITIZED SOLAR CELLS BASED ON
CROSSLINKED POLY(ETHYLENE GLYCOL) ELECTROLYTES, JOURNAL OF PHOTOCHEMISTRY AND
PHOTOBIOLOGY A: CHEMISTRY 183 (2006) 15.
[7] W. ZHAO, H. BALA, J. CHEN, Y. ZHAO, G. SUN, J. CAO Z. ZHANG, THICKNESS-DEPENDENT
ELECTRON TRANSPORT PERFORMANCE OF MESOPOROUS TIO2 THIN FILM FOR DYE-SENSITIZED
SOLAR CELLS, ELECTROCHIMICA ACTA 114 (2013) 318.
[8] H. H. KYAW, T. BORA, J. DUTTA, ONE-DIODE MODEL EQUIVALENT CIRCUIT ANALYSIS FOR ZNO
NANOROD-BASED DYE-SENSITIZED SOLAR CELLS: EFFECTS OF ANNEALING AND ACTIVE AREA,
IEEE TRANSACTIONS ON NANOTECHNOLOGY 11 (2012) 763.
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LOW ENERGY IMPACT AND POST IMPACT BEHAVIOR OF EPOXY MATRIXWOVEN FLAX FABRIC COMPOSITES
D.A. Chalkias, A.F. Koutsomitopoulou, G.C. Papanicolaou+
Composite Materials Group (CMG) Department of Mechanical & Aeronautical Engineering,
University of Patras, Patras, GR-26500, Greece, gpapan@mech.upatras.gr
ABSTRACT
Predicting the residual properties after impact of polymeric composites is an important issue in
determining their ability to post impact loading. Low-energy impact damage is often internal and
invisible, but can minimize the residual strength of the material [1-3]. Epoxy matrix-woven flax
fabric composite panels, designed of four laminates, were fabricated using a simple open
molding, hand lay-up, manufacturing process. This work presents the results of experimental
investigations concerning low-energy impact tests on the composites, as also the very good
correlation between experimental and analytical results of their post impact behavior, by applying
two analytical models developed by the corresponding author [4, 5]. Experimental impact tests
were performed according to ASTM standards using an instrumented falling weight impact testing
machine, from increasing impact heights until visible damage in composite was induced (see Fig.
1). The progressive damage due to increased impact energy levels was studied, as also the
variation of the maximum impact load and absorbed energy/impact energy as a function of
impact energy was calculated. The maximum damage zone, in all experiments, existed on the
back face of the impacted composite panels, where cracks appeared in direction of 45 with
respect to woven fibers and proceed in the radial direction from the center of the panel for higher
impact-energy level (> 2.507 J). This pattern of cracking is characteristic of woven composites [6].
At impact-energy 3.76 J, the composite appeared to lose 60% of the maximum strength in
bending, while the modulus was almost halved. The mechanical properties degradation of the
composites was approached through quasi-static characterization in 3-point bending of composite
beams sectioned from composite panels, investigating in addition the spread of damage in the
panel. For this purpose, four strips were taken symmetrically from both sides of the panels, and
the fifth one was obtained from the central panel area, thus containing the impact zone (see Fig.
2).
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References
[1] W. J. CANTWELL, J. MORTON, THE IMPACT RESISTANCE OF COMPOSITE MATERIALS- A
REVIEW, COMPOSITES 22 (1991) 347.
[2] M. O. W RICHARDSON, M. J. WISHEART, REVIEW OF LOW-VELOCITY IMPACT PROPERTIES OF
COMPOSITE MATERIALS, COMPOSITES PART A 27 (1996), 1123.
[3] S. ALBRATE, IMPACT ON LAMINATED COMPOSITE MATERIALS, APPLIED MECHANICS REVIEW
44 (1991) 155.
[4] G. C. PAPANICOLAOU, C. D. STAVROPOULOS, D. E. MOUZAKIS, J. KARGER-KOCSIS, RESIDUAL
TENSILE STRENGTH MODELLING OF POLYMER-POLYMER MICROLAYER COMPOSITES AFTER
LOW ENERGY IMPACT. PLASTICS, RUBBER AND COMPOSITES PROCESSING AND APPLICATIONS
26 (1997) 412.
[5] G. C. PAPANICOLAOU, T. V. KOSMIDOU, A. S. VATALIS, C. G. DELIDES, WATER ABSORPTION
MECHANISM AND SOME ANOMALOUS EFFECTS ON THE MECHANICAL AND VISCOELASTIC
BEHAVIOR OF AN EPOXY SYSTEM, JOURNAL OF APPLIED POLYMER SCIENCE 99 (2006) 1328.
[6] P. N. B. REIS, J. A. M. FERREIRA, P. SANTOS, M. O. W. RICHARDSON, J. B. SANTOS, IMPACT
RESPONSE OF KEVLAR COMPOSITES WITH FILLED EPOXY MATRIX, JOURNAL OF COMPOSITE
STRUCTURES 94 (2012) 3520.
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Fig. 1 SEM image of epoxy resin reinforced with TiO2 micro-particles (0.2 m, Wf =20%)
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Fig. 2 SEM image of epoxy resin reinforced with TiO2 nano-particles (21 nm, Wf =3%)
References
[1] G.C. PAPANICOLAOU, C. BAXEVANAKIS. "VISCOELASTIC MODELLING AND STRAIN-RATE
BEHAVIOUR OF PLASTICIZED POLY(VINYL CHLORIDE)." J. MATER. SCI., 1991, 26, 4323-4330.
[2] S.BARRE, T. CHOTARD AND M.L. BENZEGGAGH. "COMPARATIVE STUDY OF STRAIN RATE
EFFECTS ON MECHANICAL PROPERTIES OF GLASS FIBRE-REINFORCED THERMOSET MATRIX
COMPOSITES". COMPOSITES, PART A., 1996, 27,1169-1181.
[3] D.P. PIOLETTI, L.R. RAKOTOMANANA,J.-F. BENVENUTI, P.-F. LEYVRAZ. "VISCOELASTIC
CONSTITUVE LAW IN LARGE DEFORMATIONS: APPLICATION TO HUMAN KNEE LIGAMENTS AND
TENDON." J. BIOMECH., 1998, 31,753-757.
[4] P.S.THEOCARIS; G.C.PAPANICOLAOU; E.A.KONTOU "THE EFFECT OF FILLER-VOLUME FRACTION
AND STRAIN RATE ON TENSILE PROPERTIES OF IRON-EPOXY PARTICULATE COMPOSITES", J. REINF.
PLAST. COMPOS. 1982, 1(3), 206-224
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Fig. 2 Relaxation Curves of undamaged and damaged specimens after 12,24,36,48 thermal shock cycles
References
[1] PAPANICOLAOU, G. C.; XEPAPADAKI, A. G.; TAGARIS, G. D. EFFECT OF THERMAL SHOCK
CYCLING ON THE CREEP BEHAVIOR OF GLASS-EPOXY COMPOSITES. COMPOS. STRUCT., 2009, 88
(3), 436-442.
[2] RAY, B. C. THERMAL SHOCK AND THERMAL FATIGUE ON DELAMINATION OF GLASS FIBER
REINFORCED POLYMERIC COMPOSITES. J. REINF. PLAST. COMPOS., 2005, 24(1). 111-116.
[3] FERRY, J. D. VISCOELASTIC PROPERTIES OF POLYMERS JOHN WILEY AND SONS: NEW YORK,
1980.
[4] MULIANA, A. NONLINEAR VISCOELASTIC-DEGRADATION MODEL FOR POLYMERIC BASED
MATERIALS. INT. J. SOLIDS STRUCT., 2014, 51 (1), 122-132.
[5] PAPANICOLAOU, G. C.; KONTAXIS, L. C.; KOUTSOMITOPOULOU, A. F.; ZAOUTSOS, S. P. STRESS
RELAXATION BEHAVIOR OF STARCH POWDER-EPOXY RESIN COMPOSITES. J. APP. POLYM. SC.,
2015, 132 (12).
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Fig. 1 The experimental setup: Carbon Fiber rowing as heating medium for the polymerization of Epoxy
resin
References
[1] G.C. PAPANICOLAOU, D. MOUZAKIS, COMPOSITE MATERIALS, KLEIDARITHMOS PUBL.,
ATHENS, 2007
[2] S.VERBIS, A.KOTROTSOS, G.C.PAPANICOLAOU, AN INNOVATIVE TECHNIQUE FOR CURING OF
THERMOSETS AND SELF HEALING OF THERMOPLASTICS, THE 5TH INTERNATIONAL CONFERENCE
ON STRUCTURAL ANALYSIS OF ADVANCED MATERIALS (ICSAAM), 23-26 SEPTEMBER 2013, KOS,
GREECE
[3] Y. A. CENGEL, A. GHAJAR, HEAT AND MASS TRANSFER, 4TH EDITION, TZIOLAS
PUBLICATIONS, 2012
[4] I. VARDAKOSTAS, G.C. PAPANICOLAOU, THERMAL STRESSES IN FIBROUS COMPOSITE
MATERIALS AND APPLICATION HYBRID INTERPHASE MODEL, FINAL YEAR THESIS, UNIVERSITY OF
PATRAS, 2005
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experimental values
theoretical values
experimental values
theoretical values
0,0
0.0
(Ec-E0)/E0
(Ec-E0)/E0
-0,1
-0,2
-0,3
-0.1
C1= -0.18
T =18h
Distilled water
Immersion temperature=600C
1
10
-0,4
10
100
C1= -0.57
T=49h
Sea water
Immersion temperature=400C
100
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Wood flour-Polypropylene
Flax unidirectional fabric-Epoxy (11L)
0.1
experimental values
theoretical values
experimental values
theoretical values
0.0
0.0
-0.1
(Ec-E0)/E0
(Ec-E0)/E0
-0.1
-0.2
-0.3
vf=0.51
C1= -0.14
T =480h
Distilled water
Immersion temperature=250C
-0.4
-0.5
10
-0.2
-0.3
-0.4
10
100
0.6
0.4
vf=0.16
C1= 0.92
T =950h
experimental values
theoretical values
0.5
0.3
vf=0.2
C1= 1.1
T =950h
0.4
(Ec-E0)/E0
(Ec-E0)/E0
1000
100
0.5
wf=0.4
C1= -0.7
T =1470h
Distilled water
Immersion temperature=26.70C
-0.5
0.2
0.1
0.3
0.2
0.0
0.1
-0.1
Distilled water
Immersion temperature=200C
Distilled water
Immersion temperature=200C
0.0
1000
1000
Fig. 1. Comparison between experimental points and theoretical predictions for different material systems.
As it is obvious from the diagrams shown above, a very satisfactory agreement between
experimental points and values derived from the theory can be observed.
References
[1] P.S. THEOCARIS, G.C. PAPANICOLAOU, E.A. KONTOU, INTERRELATION BETWEEN MOISTURE
ABSORPTION, MECHANICAL BEHAVIOR, AND EXTENT OF THE BOUNDARY INTERPHASE IN
PARTICULATE COMPOSITES, JOURNAL OF APPLIED POLYMER SCIENCE, VOL. 28, ISSUE 10, PP.
3145-3153, (1983).
[2] G.C. PAPANICOLAOU, TH.V. KOSMIDOU, A.S. VATALIS, C.G. DELIDES, WATER ABSORPTION
MECHANISM AND SOME ANOMALOUS EFFECTS ON THE MECHANICAL AND VISCOELASTIC
BEHAVIOR OF AN EPOXY SYSTEM, JOURNAL OF APPLIED POLYMER SCIENCE, VOL. 99, ISSUE 4, PP.
1328-1339, (2006).
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Fig. 1 Comparison between experimental values and theoretical predictions as derived from property
prediction model (PPM) for the Flexural modulus of the Glass Fiber (3mm) hybrid epoxy matrix composites
investigated
Fig. 2 Comparison between experimental values and theoretical predictions as derived from property
prediction model (PPM) for the Flexural Strength of the Glass Fiber (3mm) hybrid epoxy matrix composites
investigated.
References
[1] PAPANICOLAOU, G. C.; KONTAXIS, L. C.; KOUTSOMITOPOULOU, A. F.; ZAOUTSOS, S. P. STRESS
RELAXATION BEHAVIOR OF STARCH POWDEREPOXY RESIN COMPOSITES. J. APPL. POLYM.
SCI., 2015.
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In the current investigation, Chios Mastic was used as the base ingredient to produce a new food
grade and totally green composite material [1-3]. Chios Mastic traditionally collected was treated
thermally to evaporate the natural occurring essential oils and to overcome the consequent
brittleness of the material, taking care not to overheat it. A small quantity of olive oil is added,
followed by starch micro-globules addition at elevated temperature and constant agitation until
saturation is obtained.
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Then, the pigment is transferred to molds and left to cool slowly to room temperature. This new
composite material contains 50% (w/w) solid starch as reinforcement and shows significant
strength compared to pure matrix. The residual composite is a food grade plastic, totally green,
100% recyclable and biodegradable. It is easy to be prepared, and has no significant
environmental impact. The emitted essential oils can be collected and used as a food flavoring or
perfume. Mechanical characterization will be made to describe the properties of the composite
and prefigure the possible uses of this new and promising material.
References
[1] SOTIRIOS PARASCHOS, PROKOPIOS MAGIATIS, SOFIA MITAKOU, KALLIOPI PETRAKI, ANTONIOS
KALLIAROPOULOS, PETROS MARAGKOUDAKIS, ANDREAS MENTIS, DIONYSSIOS SGOURAS,
ALEXIOS-LEANDROS SKALTSOUNIS, IN VITRO AND IN VIVO ACTIVITIES OF CHIOS MASTIC
GUM EXTRACTS AND CONSTITUENTS AGAINST HELICOBACTER PYLORI, IN
VIVO, SEPTEMBER 2012 26:5 777-785.
[2] ADEODATO VIEIRA, M. G., DA SILVA, M. A., DOS SANTOS, L. O., AND BEPPU, M. M.
NATURALBASED PLASTICIZERS AND BIOPOLYMER FILMS: A REVIEW, EUROPEAN POLYMER
JOURNAL, 2011, 47: 254- 263.
[3] ALESSANDRO GANDINI,, TALITA M. LACERDA, FROM MONOMERS TO POLYMERS FROM
RENEWABLE RESOURCES: RECENT ADVANCES, PROGRESS IN POLYMER SCIENCE, JANUARY
2015.
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Individual phases of hybrid composites were evaluated dielectrically for reference reasons.
Results were discussed, on the basis of the interphasial phenomena existing at the separating
surfaces between the individual layers of the hybrid composites.
References
[1] CLMENT SANCHEZ, BEATRIZ JULIN, PHILIPPE BELLEVILLE, MICHAEL POPALL (2005)
APPLICATIONS OF HYBRID ORGANICINORGANIC NANOCOMPOSITES, J. MATER. CHEM., 15, 35593592, DOI: 10.1039/B509097K
[2] VICTOR BIRMAN, K. CHANDRASHEKHARA, SUKHENDU SAIN (1996) AN APPROACH TO
OPTIMIZATION OF SHAPE MEMORY ALLOY HYBRID COMPOSITE PLATES SUBJECTED TO LOWVELOCITY IMPACT, COMPOSITES: PART B 27B, 439-446
[3] ATHANASIOS KANAPITSAS, CHRISTOS TSONOS, CONSTANTINOS G. DELIDES, GEORGIOS C.
PSARRAS (2013) THERMOGRAVIMETRIC AND DIELECTRIC STUDY OF ER/BATIO3/ZNO COMPOSITES,
MACROMOLECULAR SYMPOSIA, VOLUME 331-332, ISSUE 1, PAGES 181188, OCTOBER 2013
[4] GEORGIA N. TOMARA, ARIADNI P. KERASIDOU, ANASTASIOS C. PATSIDIS, PANAGIOTA K.
KARAHALIOU, GEORGIOS C. PSARRAS, STAVROULA N. GEORGA, CHRISTOFOROS A. KRONTIRAS
(2015) DIELECTRIC RESPONSE AND ENERGY STORAGE EFFICIENCY OF LOW CONTENT TIO2POLYMER MATRIX NANOCOMPOSITES, COMPOSITES PART A: APPLIED SCIENCE AND
MANUFACTURING, VOLUME 71, PAGES 204211
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MONITORING THE FLY ASH DISPERSION IN EPOXY MATRIX AND ITS EFFECT
ON THE THERMOMECHANICAL PROPERTIES OF THE OBTAINED
COMPOSITES
Adamos Stimoniaris1, 4*, Haralampos Zois2, Athanasios Kanapitsas3, Michael
Karakassides4, Constaninos Delides1
1
Fig. 1 SEM fracture image and EDS map spectrum of FA/ER 5%w/w composite.
Table I. Fly Ash chemical composition
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(a)
(b)
(c)
Fig. 2 (a) SEM fracture image with EDS spectrum of Si, O, Ca and
EDS spectra (b) Ca and (c) Si of FA/ER 5%w/w composite.
In addition, the dynamic mechanical and thermogravimetric measurements [8] were also
employed to characterize the thermomechanical performance of the composites with parameter
the sonication time (Fig.3).
These results can be used to tailor the mechanical and thermal properties of syntactic foams
based on the application parameters. In addition the fabrication of new composites addresses the
disposition problem of fly ash as well as brings down the production cost giving an economical
and eco-friendly solution.
References
[1] K.W. WONG, R.W. TRUSS, COMPOS. SCI. TECHNOL. 52, 361-368 (1994).
[2] J. GU, ET AL. MATER. SCI. ENG. A 452-453, 614-618 (2007).
[3] I. AHMAD, A. MAHANWAM, J. MINER. MATER. CHARACT. ENG. 9,183-198 (2010).
[4] R.S. RAJA, ET AL. INT. J. MIN. MET. MECH. ENG. 1 (1), 34-37 (2013).
[5] MATTHEW LABELLA, STEVEN E. ZELTMANN, VASANTH CHAK. SHUNMUGASAMY, NIK. GUPTA,
PRAD. K. ROHATGI., FUEL 121 (1), 240-249 (2014).
[6] AJIT KUM. SENAPATI, AB. BHATTA, SAT. MOHANTY, P.C. MISHRA, B.C.ROUTRA, INTER. JOUR.
OF INNOVATIVE SC. AND MODERN ENGIN. (IJISME) 2 (3) 4-9 (2014).
[7] D.T. KOUNTOURAS, A. TSOUKNIDAS, G.E. KIOURTSIDIS, AND S.M. SKOLIANOS, JOUR. OF
MATERIALS ENGINEERING AND PERFORMANCE 22 (8), 2210-2218 (2013).
[8] ZOIS H., STIMONIARIS A., KANAPITSAS A., KARAKASSIDES M. AND DELIDES C., 10TH HELLENIC
POLYMER SOCIETY CONFERENCE 4-6 DECEMBER, PATRA (2014).
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Isotactic polypropylene (iPP) is one of the most often used thermoplastic polymer due to its low
price, good processability, mechanical properties and chemical resistance. Despite more than
forty years of researches modification of this polymeric material is current problem. Even low
amounts of additives or fillers incorporated to polypropylene matrix may cause strong
heterogeneous nucleation effect and influence on structure and properties of modified polymer.
Therefore, purposeful addition of specially designed nucleating agents (NA) became the interest
of many studies. Nucleating agents are additives which provide additional nuclei that accelerate
crystallization process and promote nucleation for crystal growth. As a result, a larger amount of
smaller spherulites is generated. Actual three different polymorphic phases in isotactic
polypropylene are known: monoclinic (), hexagonal () and triclinic (). Most of the pigments
reveal a good nucleating ability and led to increase polypropylene crystallinity level. Moreover,
some of them are described in literature as highly effective nucleating agents that promote
crystallization of hexagonal phase in polypropylene. The aim of our studies was to assess the
influence of two different quinacridone pigments addition on the mechanical and thermal
properties of isotactic polypropylene.
Commercial isotactic polypropylene Moplen HP500J with MFR=10 g/10 min (230C. 2.16 kg) from
Basell Orlen Polyolefins (Poland) was modified with two quinacridone pigments: Hostaperm Red
Violet ER 02 (-quinacridone) and Hostaprem Red E5B 02 (-quinacridone) delivered by Clariant
(Switzerland). Both pigments in various amounts (0.01; 0.05; 0.1; 0.5; 1; 2 wt %) were
incorporated into polymer matrix in melt processing by twin screw extrusion, test specimens were
formed via injection molding process (Fig. 1).
The influence of pigments addition on mechanical properties was investigated by tensile test. The
effect of quinacridone pigments amount on thermal properties of modified isotactic
polypropylene was assessed by differential scanning calorimetry (DSC). In order to understand the
differences in modification efficiency and changes in polymorphism of polypropylene matrix
caused by incorporation of pigments, wide angle X-ray scattering experiments were prepared.
Both pigments act as highly effective nucleating agents provide to strong increase of crystallinity
level which results in changes of mechanical properties of the modified isotactic polypropylene.
Differences between polypropylene samples nucleated by two different pigments may be
attributed to different heterogeneous nucleation behavior dependent of pigment type. As it was
proved by WAXS investigations addition of -quinacridone (E5B) provided to partially
crystallization of polypropylene in hexagonal phase. For -quinacridone (ER 02) modified
polypropylene no evidence of -phase was observed.
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Fig. 1. Polypropylene injection molded samples containing various amounts of - and -quinacridone
pigment
References
[1] KARGER-KOCSIS, J. (1999). POLYPROPYLENE - AN A-Z REFERENCE. DORDRECHT - BOSTON
LONDON: KLUVER ACADEMIC.
[2] GAHLEITNER M., GREIN C., KHEIRANDISH S., WOLFSCHWENGER J. NUCLEATION OF
POLYPROPYLENE HOMO- AND COPOLYMERS, INTERNATIONAL POLYMER PROCESSING 26(1), 2-20,
2011.
[3] VARGA J. SUPERMOLECULAR STRUCTURE OF ISOTACTIC POLYPROPYLENE, JOURNAL OF
MATERIALS SCIENCE, 27(10), 2557-2579, 1992.
[4] STERZYNSKI T., CALO P., LAMBLA M., THOMAS M. TRANS- AND DIMETHYL QUINACRIDONE
NUCLEATION OF ISOTACTIC POLYPROPYLENE, POLYMER ENGINEERING AND SCIENCE, 37, 19171927, 1997.
[5] STERZYNSKI T. PROCESSING AND PROPERTY IMPROVEMENT IN ISOTACTIC POLYPROPYLENE BY
HETEROGENEOUS NUCLEATION, POLIMERY, 45, 786-791, 2000.
[6] BRODA J. NUCLEATING ACTIVITY OF THE QUINACRIDONE AND PHTHALOCYANINE PIGMENTS IN
POLYPROPYLENE CRYSTALLIZATION, JOURNAL OF APPLIED POLYMER SCIENCE, 90, 3957-3964,
2003.
[7] BRODA J. STRUCTURE OF POLYPROPYLENE FIBERS COLOURED WITH A MIXTURE OF PIGMENTS
WITH DIFFERENT NUCLEATING ABILITY, POLYMER, 44, 6943-6949, 2003.
[8] GRADYS A., SAJKIEWICZ P., MINAKOV A. A., ADAMOVSKY S., SCHICK C., HASHIMOTO T., SAIJO
K. CRYSTALLIZATION OF POLYPROPYLENE AT VARIOUS COOLING RATES, MATERIALS SCIENCE AND
ENGINEERING, 413-414, 442-446, 2005.
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ABSTRAC
Our study is to use the potential of different acids for the extraction of chromium from the
bottom ash obtained by incineration of the leather waste shavings. Benzohydroxamic acid
(BHA), citric and oxalic acid were chosen because of their high extraction efficiency of chromium
in form of Cr (III). The preliminary experiments showed that the extracted chromium with
Benzohydroxamic (BHA), citric and oxalic acid have a potential tanning capacity. This method has
potential for application to environmental and industrial problems concerning chromium waste.
References
[1] Bartlett R.J. and Kimble JM. (1976), Behaviour of chromium in soils: Trivalent Forms.J.Environ.
Qual. 5, 379 386.
[2] Dugenest S.C.J; Casabianca H. and Grenier-Loustalot M.F (1999a), Municipal solid waste
incineration bottom ash: characterization and kinetic studies of organic matter. Environmental
science and technology, 33(7), 1110 -1115.
[3] Eddings, E.G. and light, J.S. (1992), Fundamental Studies of Metal Behavior During Dolids
Incineration. Combust. Sci.Technol., 85, 375 485.
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Fig. 1. The fabricated of four MOSiC structures (with 18, 24, 36, 68 m diameter of gates).
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The microstructures of Pd thin films (50nm thickness) were investigated by Field Emission
Scanning Electron Microscopy (FESEM-FIB) Zeiss-Auriga Germany.
Acknowledgements
This work was supported by the grants of the Romanian National Authority for Scientific Research,
ANCSI&UEFISCDI, project PCCA number 204/2012
References
[1] F. SERINA, K. Y. S. NG, C. HUANG, G. W. AUNER, L. RIMAI AND R. NAIK, PD/ALN/SIC THIN-FILM
DEVICES FOR SELECTIVE HYDROGEN SENSING, APPL. PHYS. LETT. 79,3350-3352 (2001).
[2] R. N. GHOSH, P. TOBIAS, S. EJAKOV AND B. GOLDING, INTERFACE STATES IN HIGH
TEMPERATURE SIC GAS SENSING, PROC. IEEE SENSORS 2002, 2, 1120-1125, PAPER 6-4 (2002).
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Faculty of Material Science an Engineering, Warsaw university of Technology, Wooska 141, 02507 Warsaw, Poland
2
Precious Metal Mint, Weteranw 95, 05-250 Radzymin, Poland
ABSTRACT
The most common catalysts for the ammonia oxidation process are 80m diameter platinumrhodium wires knitted or woven into a form of a gauze. In the aggressive environment and under
extreme conditions (temperature 800-900C, intensive gas flow and pressure) precious elements
are drained from the surface of the wires. Part of this separated material quickly decompose on
the surface in form of characteristic cauliflower-shape protrusions, second part of material
decompose on located beneath palladium capture gauzes and the other part is lost.
Despite of the use of capture gauzes, platinum loss during oxidation process is significant and
strongly determine profitability of the process. Other economic disadvantage is the value of
precious metals catalyst itself, when only part of the material located on the surface of the wires
works as a catalyst. This problem brings the idea of core-shell catalyst which ones core is made of
less expensive, but still high temperature resistant material and shell is made of common-known
platinum-rhodium alloy. There were several attempts to produce ammonia oxidation catalyst like
this, that is also able to work in existing industrial reactors. The main problem was the insufficient
durability of the joint between the core and the shell.
In our investigation we focused on effects of the degradation of gauze made of standard Pt-Rh
wires and the new gauze made of core-shell wires. Bi-alloy structure of the material was obtained
using powder metallurgy, and complex plastic processing. In this case both, shell and core are
made of alloys
from the same materials group and are characterized by wide range of mutual solubility. The
manufacturing method and selection of materials allowed to obtain gentle gradient joint between
core and shell of the wires. This eliminate some of disadvantages of the joint without transition
zone (like thermal and mechanical properties mismatch of the materials).
Changes in the spatial morphology of the wires after 1 month exploitation were examined using
X-ray Computer Microtomography (XCT). The XCT researches allowed obtaining threedimensional models of studied wires and their structure quantitative characterization.
Observations of surface were performed using a Scanning Electron Microscope (SEM) with Energy
Dispersive Spectroscopy device (EDS) to obtain chemical composition.
Microscope observations and microtomography analysis showed that all wires surfaces were
strongly developed by etching and deposition processes occurring under extreme conditions.
Analyzed wires differed slightly in rate of degradation and morphology of the characteristic
cauliflower-shape protrusions. Also small differences in elements distribution on surface of the
wires were observed. Obtained results can be basis of further investigation on improvement of
precious metals catalysts in high temperature chemical applications.
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ABSTRACT
This article is focused on the chemical coating of structural adhesive joints of the constructive
aluminum alloy EN-AW 6082. The samples were glued by the epoxy resin Epoxy 1200. Glued joints
which represent the modern method of jointing materials where the most important aspect is the
low consumption fasteners and resulting reduction in product weight. Glued connections are
usually designed so as to transfer shear, thrust and combined load. Their strength depends on the
physical and chemical properties associated materials, their surfaces and properties of the
adhesive.
Main objective of this work was to increase the strength of the glued joint that had been
chemically treated dilute hydrochloric acid or sulfuric acid. This type epoxy resin was not chosen
only because it is widely available, but also has very good mechanical properties and chemical
resistance to non-oxidizing acids. Samples of glued joints were subjected to shear strength. These
findings may be used to produce light metal and fiber reinforced composites.
Glued joint
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References
[1] CRITCHLOW, G. W., ET AL. STRATEGIES FOR THE REPLACEMENT OF CHROMIC ACID ANODISING
FOR THE STRUCTURAL BONDING OF ALUMINIUM ALLOYS. INTERNATIONAL JOURNAL OF
ADHESION AND ADHESIVES, 2006, VOL. 26, P. 419453.
[2] ZHANG J. ET AL.: THE BONDING STRENGTH AND CORROSION RESISTENCE OF ALUMINIUM
ALLOY BY ANODIZING TREATMENT IN A PHOSPHORIC ACID MODIFIED BORIC ACID/SULFURIC
ACID BATH. SURF. COAT. TECHNOL., 2008, VOL. 202, P. 31493156.-4
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Fig. 2 Test specimen with dimensions of 50x50x25 mm, intended for the pressure tests
Fig. 3 Test specimen with dimensions of 50x220x25 mm intended for test the bend
References
[1] HJEK, PETER. BUILDING STRUCTURES 10: BEARING STRUCTURES I. ED. 2ND, REWORKING.
PRAGUE: CTU PUBLISHING HOUSE, 2000, 259 PP. ISBN 80-010-2243-9.
[2] MATOUKOV, DAGMAR. STRUCTURAL ENGINEERING I.: SUPPORTING STRUCTURES I. 1ST ED.
OSTRAVA: VB - TECHNICAL UNIVERSITY, 1997, 182 PP. ISBN 80-707-8503-9.
[3] EN 13964 ED. SECOND SUSPENDED CEILINGS - REQUIREMENTS AND TEST METHODS. PRAGUE:
CZECH OFFICE FOR STANDARDS, METROLOGY, TESTING, 2015.
[4] HSSLER, RDIGER A WOLFGANG KUNZE. THERMISCHE EIGENSCHAFTEN POLYMERER
WERKSTOFFE: DMA - DSC - TGA - TMA; STOFFSAMMLUNG THERMOANALYTISCHER MESSUNGEN.
1. AUFL. ESCHBORN: TA-INSTRUMENTS, 2007. ISBN 978-3-940184-01-6.
[5] ASTM C364 / C364M-07(2012), STANDARD TEST METHOD FOR EDGEWISE COMPRESSIVE
STRENGTH OF SANDWICH CONSTRUCTIONS, ASTM INTERNATIONAL, WEST CONSHOHOCKEN, PA,
2012, WWW.ASTM.ORG
[6] ASTM C365 / C365M-11A, STANDARD TEST METHOD FOR FLATWISE COMPRESSIVE
PROPERTIES OF SANDWICH CORES, ASTM INTERNATIONAL, WEST CONSHOHOCKEN, PA, 2011,
WWW.ASTM.ORG
[7] ASTM C393 / C393M-11E1, STANDARD TEST METHOD FOR CORE SHEAR PROPERTIES OF
SANDWICH CONSTRUCTIONS BY BEAM FLEXURE, ASTM INTERNATIONAL, WEST CONSHOHOCKEN,
PA, 2011, WWW.ASTM.ORG
[8] WOLVEGA PANELEN & COMPOSITES: COMPOSITES [ONLINE]. 2015 [CIT. 2015-07-22].
DOSTUPN Z: HTTP://WWW.WOLVEGAPANELEN.NL/COMPOSITES.ASPX
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Chairmen
Pedro Moreira (INEGI/FEUP, Portugal) (chairman)
Gabi Jiga (UPB, Romania) (co-chairman)
George Papanicolaou (UP, Greece) (co-chairman)
Organizing Committee
Mrio Vaz, University of Porto, Portugal
Paulo Tavares de Castro, University of Porto, Portugal
Paulo Tavares, INEGI, Portugal
Pedro Moreira, INEGI/FEUP, Portugal local chairman
Rui Miranda Guedes, University of Porto, Portugal
Tiago Ramos, INEGI, Porto
Viviana Correia Pinto, INEGI, Porto
Joaquim Silva Gomes, University of Porto, Portugal
Mrio Vaz, University of Porto, Portugal
Paulo Tavares de Castro, University of Porto, Portugal
Srgio Tavares, INEGI, Portugal