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COAL TAR ENAMEL- LOID-11

COAL TAR BASED PIPELINE COATING

PRODUCT DATA SHEET


DESCRIPTION
Loid-T11 Enamel is a thermoplastic polymeric coating produced from plasticization of coal
tar pitch, coal and its distillates followed by addition of inert filers. Loid-11 Enamel is
produced in accordance with standards BS 4164, AWWA C203 and IS 10221.
ADVANTAGES & SALIENT FEATURES
When used together with Loid-7 Primer B/Loid-3 Primer, Glass Fibre Inner wrap and coal
tar impregnated glass fibre outer wrap LOIDWRAP it provides long-term protection to
pipelines.

Permanent corrosion protection

Resistance to soil bacteria and marine organism

Low moisture absorption

Good electrical insulation

Insolubility in hydrocarbon

Excellent adhesion to metal

Retention to form under soil pressure

Ease of application

Good flexibility and temperature susceptibility

Resistant to Cathodic disbanding

Inertness to soil chemicals

APPLICATION METHODOLOGY
Loidcoat Enamel to be the broken into small pieces of approx. 2 Kgs. And loaded into the
kettle. It is advisable to first melt the material under slow firing till half the tank capacity and
then to add new material and start agitation periodically to avoid carbonization.

Enamel to be heated and maintained at application temperature. Excessive heating to be


avoided and it is very important to have a temperature recorder fitted to the kettle all the
time which must be calibrated time to time.
The maximum temperature of the enamel should never exceed 245 oC, enamel above this
temperature should be rejected, if when tested out of specification.
Enamel held at application temperature for more than four hours should be rejected, if
when tested out of specification.
The left over material from the previous batch can be added to the fresh material at the rate
of 10% maximum per batch.
Any material recovered from the reused batch should not be reused and is to be rejected.
Enamel should not be applied to primed pipe when metal temperature is below 7 oC and the
pipe to be coated should be free from dust, dirt, oil and moisture.
For best results, application should be carried out at either 5 oF or 3oC above dew point.
Best bonding is achieved in this case.
STORAGE

To be stored in clean area to avoid contamination

For bulk liquid storage the temperature to be maintained from 180 oC-210oC

PACKAGING AND SHIPPING INFORMATION

Standard 220 Kgs. MS Drum

Drums are marked for easy identification grade and batch number

Silicone coated paper bags also available

Loidcoat enamel can also supplied in tanker loads in liquid condition after taking into
consideration the distance to be covered and arrangements at the unloading point.

For overseas shipment, packed drums loaded in containers or shipped as bulk


cargo.

HEALTH AND SAFETY

Use of gloves and filler type masks are recommended in the application area

Eye protection glasses recommended when enamel is on use, in event of contact


wash eyes with cold water and seek medical advice

Cream to be applied to skin before commencing work

Ventilation must be adequate in area of application

For life protection use CO2 or dry powder

STANDARD SPECIFICATION SHEET


COAL TAR ENAMEL (LOID T-11)
Sl.
No.

CHARACTERISTICS
SPECIFICATION
GRADES

1.

Softening Point Deg.


C
Filler Content % by
mass
Density at 25oC,
g/cm2
Flow time, Seconds
At 230oC
At 240oC
Penetration, 10I mm
At 25oC / 100 gm / 5
s
45/46.1/48oC / 50
gm / 5s
Sag, Maximum, mm
70/71oC C/24 hrs.
80oC C / 24 hrs.
Low Temp. Cracking
&
Disbonding
-30oC
-28.9 oC
-25oC
-23.3oC
-20oC
Bend at 0o C/4 oC
First Crack, Min., mm
Initial
After heating
Disbanded area, Max,
mm2
Initial
After Heating
Impact Test
Disbonded area, Max,
mm2

2.
3.
4.
5.

6.
7.

8.

9.

STANDARD RANGE
AWWA-C-203-02
Type-1
Type-2

105/15

BS-4164-02
105/8
120/5

104-116

104-116

105-116

105-116

120-130

25-35

25-35

25-35

25-35

25-35

1.4-1.6

1.4-1.6

1.4-1.6

1.4-1.6

1.4-1.6

9-16

9-16

9-26

5-10

10-20

10-20

5-12

1-9

12-30

15-55

15-55

8-30

3-16

1.6
-

1.6
-

1.5
-

1.5
-

1.5

None

N/A

None

None
N/A

N/A
N/A

None
-

None

20
15

15
10

2,000
3,000

3,000
5,000

15,000

0o C

(i) Direct

(ii) Indirect
25 C (i) Direct
(ii) Indirect
Peel Test (Max.) mm
27/30o C
o

10

38/40o C
49/50o C
60/60o C
71/70o C
11

Fineness Filler
through 200 mesh %
by weight, min.
Cathodic Disbonding
in 28 days, mm, Max.

12

Service Temp. oC
Interior Lining
Exterior Lining

13

14

Recommended
application
temperature, oC

10,323
3,871

6,452
1,290

10,000
-

No
Peeling
No
Peeling
No
Peeling
No
Peeling
No
Peeling

No
Peeling
No
Peeling
No
Peeling
No
Peeling
No
Peeling

3.0

3.0

3.0

3.0

3.0

3.0

3.0

3.0

90

90

32.2
71.1
230
240

32.2
71.1
230
240

- 30 to
+65
250 max.

- 20 to + - 5 to
5
+65
250 max. 260 Max.

As per Customer request, the following additional Tests may be done :


Sl.No.

Characteristics / Standard

1.

Volume resistivity, Min., Ohm cm (ASTM D-176)

2.

Di-Electric Strength Min., KV/mm (Between 2.54


mm gap (ASTM D-176)

Specification
1013
25 KV (10 KV/mm)

In addition to the above, Coal Tar Enamel conforming to AWWA-C-203 (Type & II), BS
(Three Grades) and those specified by customers are also manufactured.

SYNTHETIC PRIMER LOID- T 7


PRODUCT DATA SHEET

DESCRIPTION
Loid T-7 is a chlorinated based synthetic primer, which is modified and adjusted with
plasticizers and stabilizer in blend of special solvents. The all season Loid-T-7 is designed
to dry faster under all temperature conditions. Its quick drying characteristic develop a bond
with Loid-T-11 under most difficult field conditions and permit pipe sections to be hot coat
and wrapped eliminating primer contamination.
Loid-T-7 Conforms to AWWA C-203/1997
British Standard
BS 4164/1897
Properties
Test Method

Characteristics
Flow time (4 mm cup) at
23oC / Sec
Flash Point
(Abel Closed cup)oC
Volatile Matter
(105oC - 110oC) %
Drying Time, minutes

USES

Limits
Max.
60

BS 3900, Part A6

Min.
35

BS 2000, Part 170-

23

BS 4165, App. A

75

BS 4165 App P

15

- ADVANTAGES

It is all season primer and designed to dry faster under all temperature conditions.

Its free flowing property permit coverage of 10-12 m2 per Liter on new pipe surface
while old and rough pipe require 10% to 20% extra coverage depending upon pipe
surface.

It can be used for internal coating of pipes as it has not taste or odour.

APPLICATION METHODOLOGY
PIPE SURFACE PREPARATION
Before applying Loid-T-7 pipe surface preparation is of the utmost importance. There are a
number of suitable methods of pipe cleaning including:
(a)

Sand or grit blasting.

(b)

Mechanical scraping and wire brushing.

Each method has its own attractions.


Method (a) is the most full proof and medium / fine grit gives best results. Sand creates a
dust hazard and shot is susceptible to oil contamination and can cause deep impingement
on the steel surface which leads to a low primer coverage rate. An enclosed recalculating
blasting cabinet gives best results as it eliminates contamination and is easy to control.
Method (b) is used on line travel for over the ditch coating, but is not as reliable as
method (a). Any dust remaining on the pipe must be blown off with compressed air.
It should be clearly understood that before any mechanical cleaning operation takes place
all oil and grease should be removed from the pipe surface using a suitable solvent.
PRIMER APPLICATION
The prime pipe should have a uniform film of primer, free from runs, drips or missed spots.
It is most important that the steel surface of the pipe should be above the dew point before
application of any protective coatings. If any doubt exists regarding this, the pipe should be
warmed, e.g. by means of hot air blown through the pipe to warm it to a temperature of
30oC 40oC. Synthetic Primer should not be applied when the temperature of the pipe
surface is above 60oC. The use of fast drying synthetic primer eliminates the need to coat
the primed pipe within a specified period of time.
PACKAGE AND STORAGE
Available in standard 20 litres and 200 litres M.S. Drums. Special packaging available on
customers request. Loid-T-7 is to be stored in sealed container in cool place to avoid
evaporation.

HEALTH AND SAFETY

Smoking welding and flash to be avoided in application area.

Use solvent proof gloves and rubber boots, eye protection glasses during
application.

In event of contact, wash eyes with cold water and seek medical advice.

COAL TAR TAPE


HOT APPLIED COAL TAR TAPE
PRODUCT DATA SHEET
DESCRIPTION
Loid Tape is a hot applied, factory made, prefabricated coal tar coating in tape form for
underground gas, oil and water pipelines. Loidtape is composed of specially formulated
plasticized coal tar coating completely saturated and bonded to both sides of a high tensile
strength fabric. Loidtape is manufactured in accordance with AWWA C-203 and IS 10221.
Characteristics

Technical Specification
Range
Min.
Max.
65
121
3
20
20
30
1.25

Softening Point
Penetration 25oC
Filter Percentage
Weight average
(Kg/sqm/mm)
Breaking strength in
longitudinal direction
Adhesion to prime steel
Holiday Test
Impact Test
Thickness MM
Cathodic Disbondment, 28
days (mm)
Service temperature C

Test Method
ASTMD 36
AWWA C-203
ASTMD 2415
ASTMD 146

0.7

AWWA C-203

Passes
Passes
Passes
2
-

4
5

AWWA C-203
AWWA C-203
AWWA C-203
AWWA C-203
BS4164-87

60

USES
Loidtape is used to protect underground or submerged metal surface from corrosion and
electrolysis.
It is commonly used in:

Oil and gas pipelines

Tanks underground structures and fittings

Water and sewage pipelines

Fire hydrant lines

Pipe joints, fittings and couplings

ADVANTAGES

Ease of application and low application cost

Uniform coating thickness

High water and electrical resistance

Cathodic disbanding resistivity

Resistance to soil bacteria, marine organisms, root growth

Resistance to petroleum products, acids & alkalies

Resistance to damage due to impact of backfill

Good flexibility and temperature susceptibility

Excellent adhesion to metal surfaces

Environment friendly

Good resistance to abrasion

OUTERWRAP
OUTERWRAP FOR PIPELINES
PRODUCT DATA SHEET
DESCRIPTION
Loidwrap is manufactured to meet the requirements of AWWA C-203 and IS-10221. The
fibre glass mat is impregnated with coal tar that is fully compatible with Loidcoat Enamel
manufactured in accordance with AWWA C-203 & BS-4164. Loiwrap surface is dusted with
inorganic parting agent, to prevent sticking with the roll. It s tensile strength is more than
adequate to allow trouble free application with high speed wrapping machines.

Property
Characteristics
Base Material : Non Woven
Fibre Glass Tissue Based
A. Weight gm/M2
Finished outerwrap
A. Weight gm/m2
B. Thickness: min; mm
C. Tensile Strength
(Average Longitudinal
Transverse
D. Pliability

Values
AWWA C-203

E. Weight loss on heating

2% max.

83
580 732
0.76 Min
Min;
6130 N/M of width
4730 N/M of width
No cracking

ADVANTAGES

HIGH ELECTRICAL RESISTANCE

RESISTANCE TO BACTERIA

MOISTURE PROOF

CONTROLLED POROSITY

REINFORCED

HIGH TENSILE STRENGTH

ROT PROOF

EXCELLENT RESISTANCE TO SOIL EROSION

APPLICATION
Suitable for use in factory, line travel and hand repair application. The depth of penetration
of Lloydwrap can be controlled by tension and Lloydcoat enamel temperature. The overall
coating thickness can be controlled by speed of application, Lloydcoat enamel temperature
and Lloydwrap tension.
A minimum overlap of 13 mm at a tension is to be given to avoid wrinkles, buckles and
defects and at the same time allowing bleed outs between laps.
PACKAGING AND SHIPPING INFORMATION
Rolls can be supplied in cardboard carlons and wooden pallets. For overseas supplies it
can be in loose or box packaging and transported in containers. Special packaging on
customer request also available. Available in rolls upto 300 mtr. Length and different width
as per requirement.
HEALTH SAFETY AND STORAGE

Use of gloves, goggles and facemasks are recommended during application.

To be stored in coo, dry and covered place, away from heat and naked flames.

COAL TAR PITCH LOID T


PRODUCTION DATA SHEET
Coal Tar Pitch is of high fixed carbon content and as well as of good binding properties.
Loid T is produced from high temperature Coal Tar procured from different steel plants
and in accordance with latest technology under strict process and quality control by highly
experience and qualified technicians.
This reflects in quality of Pitch, as follows:

Low volatile

High fixed carbon

Low ash content

No meso phase

Good wettability

Good thermal stability during storage

USES

Coal Tar Pitch is mainly used as binder material for the production of anode for
Aluminum Smelting Industry.

CTP is also applied to graphite electrode for Electric Arc furnace (EAF) for steel
industry.

As a water proofing agent.

As refractory material.

Isolated aromatic base chemicals for the production of dyes, inks, pesticides,
plasticizers, solvents, surfactants.

Aromatic oils for the production of Carbon Black.

PACKAGE & STORAGE


Available in both solid (lump & pencil size) and liquid form. Solid Pitch available in 50 Kg.
HDPE bags, 1 M.T. Jumbo bags and in Drums. Liquid Pitch is supplied to especially made
tanker.

HEALTH & SAFETY

Smoking, Welding and Flash to be avoided in working placing.

Used heat proof gloves, safety boots, dust / gas protective nose mask and eye
protection glass during handling the material.

In event of contact eyes with cold water and seek medical advise.

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