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Toma de Muestras de Aguas
Toma de Muestras de Aguas
BSI
BRITISH STANDARD
Water quality
Part 6: Sampling
Section 6.5 Guidance on sampling of
drinking water and water used for food
and beverage processing
BS 6068-6.5:
1991
ISO 5667-5:
1991
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
BS 6068-6.5:1991
Date
Comments
BS 6068-6.5:1991
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
Contents
Page
Committees responsible
Inside front cover
National foreword
ii
1
Scope
1
2
Normative references
1
3
Sampling equipment
1
4
Sampling procedure
1
5
Sampling technique
4
6
Safety precautions
5
7
Volume of sample, handling of samples
5
8
Sample identification and records
6
9
Quality assurance of sampling and training of sampling personnel
6
Annex A (normative) Report Sampling of drinking water and water
used for food and beverage processing
7
Annex B (informative) Bibliography
8
Publication(s) referred to
Inside back cover
BSI 03-1999
BS 6068-6.5:1991
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
National foreword
This Section of BS 6068, which has been prepared under the direction of the
Environment and Pollution Standards Policy Committee is identical with
ISO 5667-5:1991 Water quality Sampling Part 5: Guidance on sampling of
drinking water and water used for food and beverage processing.
The international standard was prepared by subcommittee 6, Sampling, of
Technical Committee 147, Water quality, of the International Organization for
Standardization (ISO) with the active participation and approval of the UK.
BS 6068 is being published in a series of Parts subdivided into Sections that will
generally correspond to particular international standards. Sections are being, or
will be, published in Parts 1 to 7, which together with Part 0, are listed below.
Part 0: Introduction;
Part 1: Glossary;
Part 2: Physical, chemical and biochemical methods;
Part 3: Radiological methods;
Part 4: Microbiological methods;
Part 5: Biological methods;
Part 6: Sampling;
Part 7: Precision and accuracy.
Cross-references
International standard
ISO 2859-1:1989
ISO 5667-1:1980
ISO 5667-2:1991
ISO 5667-3:1985
ISO 8199:1988
a In
ii
preparation
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
BS 6068-6.5:1991
This Section of BS 6068 is one of a group of standards dealing with the sampling
of specific types of water. It should be read in conjunction particularly with
BS 6068-6.1, BS 6068-6.2 and BS 6068-6.3 which deal respectively with the
design of sampling programmes, sampling techniques and the preservation and
handling of samples. The general terminology used is in accordance with that
established by ISO/TC 147, Water quality, and more particularly, with the
terminology on sampling given in BS 6068-1.2.
A British Standard does not purport to include all the necessary provisions of a
contract. Users of British Standards are responsible for their correct application.
Compliance with a British Standard does not of itself confer immunity
from legal obligations.
Summary of pages
This document comprises a front cover, an inside front cover, pages i to iv,
pages 1 to 8, an inside back cover and a back cover.
This standard has been updated (see copyright date) and may have had
amendments incorporated. This will be indicated in the amendment table on
the inside front cover.
BSI 03-1999
iii
iv
blank
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Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
ISO 5667-5:1991(E)
1 Scope
2 Normative references
1)
3 Sampling equipment
Reference should be made to ISO 5667-2 for
sampling equipment and requirements for
materials in contact with the sample, and to
ISO 5667-3 for cleaning of sample containers.
4 Sampling procedure
4.1 Sampling location
Detailed guidance, including statistical
consideration, is given in ISO 5667-1.
The sampling location and local safety regulations
(see clause 6) influence the method of sample
collection. Before collection of the sample, it should
be decided whether some of the analyses are to be
performed on site. On-site analysis is recommended
particularly for such determinands as odour, taste,
pH, chlorine, ozone, dissolved oxygen, acid (base)
capacity, carbon dioxide, electrical conductivity, and
for the assessment of the temperature of the water
and the ambient air and the visual inspection of the
sample. Cognizance should also be taken of any
national regulations requiring on-site analysis.
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
ISO 5667-5:1991(E)
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
ISO 5667-5:1991(E)
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
ISO 5667-5:1991(E)
5 Sampling technique
Before collecting the sample, the water should
normally be allowed to flow freely for the time
required by the sampling purpose (see also clause 4
and 5.3).
5.1 Sampling for physical, chemical and
radiological analysis
When sampling from taps, usually of the
distribution system or the service reservoir, the
water should be allowed to flow slowly into the
sampling container and to overflow. Samples that
are to be preserved, and microbiological samples
should not be filled to overflowing (see also 5.3).
Then the completely filled container should be
stoppered tightly and checked for the absence of air
bubbles.
For the determination of oxygen or dissolved gases
it is necessary to use a hose, attached to the tap or
pump outlet, that reaches the bottom of the sample
container. The water should be allowed to flow
slowly into the sampling container through the
hose, then it should be handled as described in this
subclause.
Reference should be made either to ISO 5667-3 or
the Sampling and preservation of samples clause
of the respective analytical International Standard
for detailed instructions concerning the handling of
samples after sampling.
Sampling for particulate matter is not normally
performed on a routine basis. To obtain a
representative sample it is necessary to
sample at a location where particulate matter
is uniformly distributed in the pipe, by sampling
from systems with turbulent flow as far away as
practicable from any obstructions such as bends
or valves and sampling from a straight length of
pipe;
withdraw a representative sample from the
bulk fluid by, for example, sampling
isokinetically via a sampling probe protruding
into the pipe and facing into the direction of flow;
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
ISO 5667-5:1991(E)
6 Safety precautions
It is essential that personnel responsible for the
design of sampling programmes and for carrying out
sampling operations ensure that the requirements
of relevant national safety regulations are taken
into account and complied with and that the
sampling personnel are informed of the necessary
precautions to be taken in sampling operations.
For further information reference should be made to
ISO 5667-1.
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
ISO 5667-5:1991(E)
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
ISO 5667-5:1991(E)
Annex A (normative)
Report Sampling of drinking water and water used for food and beverage
processing
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
ISO 5667-5:1991(E)
Annex B (informative)
Bibliography
[1] Guidelines for drinking-water quality, World Health Organization, Vol. 1, Recommendations, 1984.
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
BS 6068-6.5:1991
Publication(s) referred to
BSI 03-1999
Licensed Copy: Institute Of Technology Tallaght, Institute of Technology, Fri Aug 04 13:04:41 BST 2006, Uncontrolled Copy, (c) BSI
BSI
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