MDI Jade

2006 6 5

E-mail:huangjw@mail.csu.edu.cn
Telephone:0731-8836426
QQ406089079


X
X

Jade

MDI Jade 5.0 6.5

2006 7 8

E-mail:huangjw@mail.csu.edu.cn
Telephone:0731-8836426
QQ406089079

Jade .................................................................................................................1
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PDF ...........................................................................................15
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PDF .......................................................................................................20
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RIR................................................................................24
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RIR................................................................................................................49
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 Jade

Jade

1 MDI Jade
Jade
2 File | Patterns...

Jade PDF Jade

Jade Jade
Jade Windows .Raw
X

Jade
AutoCAD
CAD CAD

1
File | Patterns...

File|Thumbnail

File
2
1
Jade
MDI ASCii Pattern Files(*.mdi) JADE
JADEJADE
JADE\demofiles
RINT-2000 Binary pattern files(*,raw)
Jade import ascii pattern files(*.TXT)
Jade
Jade
*.*
2

2
Windows
3

1Read

2Add

Add
Jade

JADE
JADE

File-Save-Setup Ascii Export

TXT DAT

80

Import /Export

Save

B
Browse
L

CWClick Here for Setup Menu

Setup 1st Data Point

Set Theta Field

17
16 17 2
ID
SAVE
C MDI
MDI MDI
JADE demo8.MDI

Setup Scan ID
Set Start Angle
Set Final Angle
Set step angle
Set Dwell Time
Set X-ray anode
Set Wavelength
Set Data Count
Set Date & Time
Set 1st Data Pint
Set Data Pints/Line

1 1 0
0
2 8
1

MDI

06-05-06 00:31
15.0
.02 .15 Cu 1.54056
91
87
81
82
80
85
84
94
115
91
112
93

80.0
89
85
85

3251
93
84
87

90
92
88

88
93
85

File

Patterns Thumbnail
Save

Save-Primary Pattern as *.txt

*.txt

Origin

Full Range(View )
2smooth,

Save-Setup Ascii Export Jade Export

Import)

Scan ID
Wavelength Cu
*.TXT *.DAT

Browse
Jade
Edit
Preferences

Copy

Files- Save-Primary Pattern as *.txt

Preferences

Jade

Display-Keep PDF overlays for New Pattern File:

PDF PDF2.dat

PDF
Jade

PDF

ICSD
10

Report-Estimate Crystallite Size from FWHM Values:

PDF
PDF-Setup ICDD PDF MDI Jade
ICDD PDF Jade ICDD PDF
PDF-Setup PDF
Options

Cell Refinement:
Calculate Stress
View
Zoom window-Full Range Zoom Windows-Display Range
Zoom

Report
//

PDF

Jade

Read
Add
/

11

9-15

BG
BE
BG

BG

Cubic Spline
K2
Strip K-alpha2-Ka1/Ka2 Ratio 2.0
K2

Strip K-alpha2-Ka1/Ka2 Ratio 2.0 X

K K
K K
K

12

K K K1 K2
2/1 K2
K2

Edit- Preferences Report-Estimate Crystallite Size from FWHM

Values

R 9%

PDF S/M

13

Jade

HKL

14

PDF

PDF
JADE PDF2

PDF2 2004 1-54 65 70-89 2003

54 PDF

1 PDF

2 PDF-Setup

PDF2

Browse
PDF2

3 PDF2 PDF2.DAT Find

BROWSE
4 PDF2 PDF2 14
Select All
JADE

5Go 10

1 JADE5 JADE6
2PDF2002 PDF2003 JADE5 PDF2004 28

WINDOWS2000

15

2
3

PDF

2 100
3

3
FeO Fe
FeO
Fe

Jade

1S/M
Use chemistry filter PDF
S/M Focus on Major PhasesOKSearch/Match Display

PDF

16

Search/Match Display PDF

100 FOMFOM

PDF

Use chemistry filter

OK
S/M Focus on Minor Phases S/M Focus on Trace Phases

Al,Sn,O,Ag Sn-O
Sn O

17

LiMnO
Fe
OFe

OCl

PDF

S/MJade 5 Painted Peaks

99.9%
Jade

PDF 140000

///

18

PDF

Report

Jade Report-Phase ID Report

19

PDF

31-785
PDF
8 PDF

PDF

20

PDF

Fe
O OK Fe-O

21

Jade

Report-Peak Search Report

Save.IDE

Report-Peak ID(Extended)

Save.PID

22

I%=100.IDE RIRK

23

RIR

RIR
1978 ICDD PDF RIR K
Al2O3() 11
/ K Al 2 O 3 =
A

IA
KA
=
A
Al 2 O 3
I Al 2O 3
K

K
ABC A PDF
RIR A K

K AlA 2O 3
K AlB 2O 3
K AlC 2O 3
B
C
= 1 KA = A
KA = A

K = A
K Al 2O 3
K Al 2O 3
K Al 2O 3
A
A

N X

WX =

I Xi
N

K AX
i= A

Ii
K Ai

A I=AN N
AB RIR

WA =

IA
IA +

IB
K AB

WB =

IB
= 1 WA
I B + I A K AB

MDI Jade RIR

2Report-Peak ID(Extended)
I%=100 .PID

3Report-Report-Peak Search Report

.IDE.

24

RIR

4PDF PDF

.PDF RIR

25

X
100% 100%

1
100%
100%

100%
100%

Jade

100%

100
75 75% X

1
2
3

26

5Report-Peak Profile Report

27

Jade

Print
Copy bmp Word
bmp
Save bmp,jpgJade 6
Setup

Ctrl

AJade

# 1

28

1
2 K2
3
4

R=R
R
5%

Too Many Profiles in Zoom

29

Window

Fitted Profiles

30

Jade

NIST-LaB6Silicon-640
Si
Si 300 24
Jade
K2

AnalyzeFWHM Curve Plot

File Save FWHM Curve of Peaks

EditPreferences

31

Save

View FWHM Curve

32

FWHM
FWHM

FWS
Jade

FW ( S ) D = FWHM D FW ( I ) D
D 1-2
2
D=1 D 1
D

Size =

K
FW ( S ) * COS ( )

Size nmK K=1 X (nm)FWS

(Rad)(Rad)

30nm 1-100nm 100nm

33

Strain(

d
FW ( S )
)=
d
4 tan( )

Strain
3

Hall FWS
111222200400

FW ( S ) * COS ( )

sin( )

sin( )

2 Jade K2
3Report-Size & Strain Plot
//

D =1-2

4 Size only, Strain Only, Size/strain

5 D
6
7 Save Export

34

Report-Peak
Profile ReportXS
Hall e

ax 2

1
1

2
1 + ax
(1 + ax 2 ) 2

D D

1
1

2
1 + ax
(1 + ax 2 ) 2

(nm)

(nm)

(nm)

(nm)

1-1

0.199

0.371

113.9536

0.0916

195.9855

0.1277

158.7912

1.0883

156.2434

0.4359

1-2

0.211

0.375

90.6067

0.0869

132.3290

0.1417

110.0600

1.1052

110.9986

0.4446

2-1

0.184

0.373

222.6750

0.1000

693.0338

0.1099

512.3432

1.0968

476.0173

0.4356

2-2

0.189

0.369

154.7003

0.0956

341.3761

0.1159

265.1053

1.0799

253.7272

0.4304

3-1

0.196

0.352

108.6920

0.0819

169.7103

0.1241

138.3940

1.0078

138.9321

0.4046

3-2

0.197

0.364

114.3239

0.0886

192.8584

0.1253

155.5487

1.0587

154.2437

0.4242

4-1

0.185

0.359

162.3217

0.0919

360.7296

0.1111

276.4588

1.0375

266.5034

0.4135

4-2

0.194

0.367

126.8964

0.0919

235.1226

0.1218

184.9637

1.0714

182.3276

0.4284

5-1

0.198

0.379

124.3676

0.0967

235.4637

0.1265

186.3562

1.1221

182.0625

0.4484

5-2

0.210

0.386

97.2854

0.0943

154.5340

0.1405

126.5458

1.1516

126.1217

0.4621

6-1

0.196

0.398

166.9377

0.1083

433.6488

0.1241

326.6098

1.2021

309.0655

0.4782

6-2

0.198

0.398

151.5527

0.1074

360.9569

0.1265

276.3212

1.2021

262.9436

0.4786

7-1

0.178

0.349

202.0796

0.0896

525.8895

0.1027

394.7144

0.9950

374.2278

0.3958

7-2

0.178

0.346

191.1997

0.0880

467.9151

0.1027

352.4236

0.9823

337.1795

0.3910

21=44.662 1=0.109 22=98.913 2=0.147

35

Jade

NIST-LaB6Silicon-640

K2
Analyze-Theta Calibration F5

Save Curve

Calibrate Patterns on Loading Automatically

36

PDF

102-103nm

Al

K2

PDF PDF Al
Al
Options-Cell Refinement

PDF

37

RefineJade

.abc
PDF

RefineCalc

38

Jade

Options | D-Spacing & hkl...

PDF
2000
Same d-Spacing d

.HKL
d(nm)

hkl

2-Theta

6.0353

100

14.6652

4.2676

110

12

20.7972

D (g/cm^3) = W * Z / V / 0.6022169
(W = , V =
) Z Z

39

20 XX
1961 E.Mchearauch
Xsin2X

XX
2sin2M
2
=0153045 2sin2
=K2/sin2= KM
=0 2
2
2 HKL
0 2
0 2 2 HKL

Jade6.0
2

3
Options-Calculate Stress

40

4
Psi-Angle
5
Fit OneFit All
6
1
Parabolic FitJade

Jade
2
Fit All

(d d 0 )
% = A + B * sin( ) 2
d

d0=0 d0
d0d0

4
EDS
5
Y = B * X B = Stress *

1 +
E
E

tensile stress
compressive stress
6LPA
-
LPA--

(1 + cos 2 2 )(1
LPA =

tan
)
tan

sin 2

LPA* LPA
LPA

41

7
Print
Ctrl+Print
Copy
Copy
Save(*.wmf)
Save(*.ksi)
42

21-22

0.28-0.3

19.6

0.28

Al

7.03

0.345

12.98

0.364

13.25

0.333

WC

53.44

0.22

Ti

11.57

0.321

Ni

21.2, 19.9-22.0

0.31,0.3-0.32

Ag

8.27

0.367

40.888

0.233

9
Jade 5 2

Jade
2

43

Jade

Shift Ctrl
Read

Ctrl Reset

44

Shift

Offset 10 10

(0) ID

2
3D
View-Overlays in 3D 3D

3D

45

K2

Fit All OverlaysJade

46

Report

MDI Jade 6
Options-Calculate Stress

()

Fit All OverlaysJade

Report 1
23
Crystallinity

47

48

 RIR

RIR
14 PDF RIR PDF
RIR
Jade 5 RIR Jade 6

PDF-Retrival

4 RIR
2-4 Calc MDI
1
RIR

RIR

49

JADE

2006 6 5

50