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    Bahtiar Nurhakim
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    The document is an SEM-EDS analysis of a sample. It includes information about the instrument used, acquisition parameters such as voltage and time, and a table displaying the quantitative elemental analysis of the sample using the ZAF method. The analysis found carbon at 7.5% mass, oxygen at 14.74% mass, sodium at 5.7% mass, phosphorus at 9.57% mass, and sulfur at 0.62% mass.

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    The document is an SEM-EDS analysis of a sample. It includes information about the instrument used, acquisition parameters such as voltage and time, and a table displaying the quantitative elemental analysis of the sample using the ZAF method. The analysis found carbon at 7.5% mass, oxygen at 14.74% mass, sodium at 5.7% mass, phosphorus at 9.57% mass, and sulfur at 0.62% mass.

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    13 views1 page

    4

    Uploaded by

    Bahtiar Nurhakim
    The document is an SEM-EDS analysis of a sample. It includes information about the instrument used, acquisition parameters such as voltage and time, and a table displaying the quantitative elemental analysis of the sample using the ZAF method. The analysis found carbon at 7.5% mass, oxygen at 14.74% mass, sodium at 5.7% mass, phosphorus at 9.57% mass, and sulfur at 0.62% mass.

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    Title
    : IMG2
    -------------------------Instrument
    :
    Volt
    : 18,00 kV
    Mag.
    : x 1,000
    Date
    : 2016/03/24
    Pixel
    : 1280 x 960

    30
    30 m
    m
    3000

    900
    600

    NiKa

    PKa

    Acquisition Parameter
    Instrument
    : 6390(LA)
    Acc. Voltage : 18.0 kV
    Probe Current: 1.00000 nA
    PHA mode
    : T4
    Real Time
    : 81.11 sec
    Live Time
    : 50.00 sec
    Dead Time
    : 38 %
    Counting Rate: 4681 cps
    Energy Range : 0 - 20 keV

    NiKb

    1200

    FeKa
    FeKb

    1500

    FeKesc

    Counts

    1800

    SKa SKb

    2100

    CKa

    2400

    OKa
    FeLl FeLa NiLl
    NaKa NiLa

    2700

    300
    0
    0.00

    3.00

    6.00

    9.00

    12.00

    15.00

    18.00

    21.00

    keV
    ZAF Method Standardless Quantitative Analysis
    Fitting Coefficient : 0.2827
    Element
    (keV)
    Mass%
    Error%
    Atom%
    Compound
    Mass%
    K
    C K
    0.277
    7.50
    0.19
    1.6568
    O
    K
    0.525
    14.74
    0.13
    19.6572
    Na K
    1.041
    5.70
    0.24
    2.9069
    P K
    2.013
    9.57
    0.11
    11.2951
    S K
    2.307
    0.62
    0.09
    0.7691

    JED-2300

    AnalysisStation

    Cation
    19.66
    29.00
    7.81
    9.72
    0.61

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