Professional Documents
Culture Documents
Art:10.1007/s00603 011 0209 7 PDF
Art:10.1007/s00603 011 0209 7 PDF
DOI 10.1007/s00603-011-0209-7
ORIGINAL PAPER
Received: 7 September 2011 / Accepted: 18 November 2011 / Published online: 29 November 2011
Springer-Verlag 2011
1 Introduction
Rock masses normally consist of blocks of intact rocks
separated by joints, faults or interfaces. Even intact rocks
are categorised as an inhomogeneous, discontinuous
material, on both small and large scales, because they
contain cracks, voids and pores, normally induced by historical thermal, mechanical and/or chemical actions and
reactions. The study of brittle fracture and its relationship
to material damage, fatigue and strength is central in many
rock engineering disciplines, including rock fracture and
damage mechanics, rock cutting, drilling and blasting.
Research on understanding rock cracking, fracture and
fatigue behaviour under various loading conditions, such as
static, cyclic and impact loading, has attracted many
investigators in recent years (Celestino and Bortolucci
1995; Ingraffea 1981; Petros et al. 2003; Zhenyu and
Haihong 1990). Inglis (1913) first confirmed that a maximum tensile stress that is many times larger than the
applied loading stress can be generated at the boundary of
the ellipse modelling crack geometry.
The tensile strength of rocks is much lower than its
compressive strength. Rock is a brittle material and
because all brittle materials are weak in tension, the tensile
strength of rock becomes one of the most important
parameters influencing its deformability and fracture
toughness. The difficulties associated with performing a
direct uniaxial tensile test on a rock specimen have led to a
number of indirect methods for assessing tensile strength.
In 1978, the Brazilian test was officially proposed by the
International Society for Rock Mechanics (ISRM) as a
suggested method for determining the tensile strength of
rock materials (ISRM 1978). The mechanical behaviour of
rock under static loading has been thoroughly investigated.
However, rock reaction to cyclic, repetitive stresses
123
328
123
N. Erarslan, D. J. Williams
329
Fig. 2 Microcrystalline quartz cement (a), and Quartz (Q) mineral in microcrystalline quartz and primary cryptocrystalline cement (b)
Youngs
modulus
(GPa)
Poissons
ratio
UCS (MPa)
BTS
(MPa)
Max = 25
Max = 0.26
Max = 190
Max = 15
Min = 19
Min = 0.22
Min = 97
Min = 8.0
Fig. 3 a Prepared BTS disc specimens, b disc specimen with strain gauges placed between loading jaws
123
330
123
N. Erarslan, D. J. Williams
3 Results of Tests
3.1 Results of Static Tests
The tested Brisbane tuff specimens under loading arcs are
shown in Fig. 5. In the present tests on Brisbane tuff disc
specimens, loading with the Brazilian jaws caused central
tensile cracking at the centre of the disc specimens with the
occurrence of several fractures branching from the diametral plane.
The details of the test results for the two different
Brisbane tuff specimens, NST35 and NST207, are given in
Table 2. Two typical stressstrain curves from standard
Brazilian tests are shown in Fig. 6.
3.2 Results of Cyclic Tests
During the monotonic tests on Brazilian disc specimens, it
was found that the standard BTS test caused catastrophic
failure of the disc specimens, rather than the expected
tensile splitting failure initiated by a central crack. For this
331
NST35
NST207
NST35
NST207
Replicate 1
26.29
24.58
12.36
11.56
Replicate 2
24.39
19.45
11.47
9.15
Replicate 3
Replicate 4
25.42
23.49
20.98
21.86
11.96
11.05
9.87
10.28
Replicate 5
25.97
25.06
12.22
11.79
Average
25.11
22.38
11.81
10.53
Percentage
decrease in
failure load
Smax (as % of
static failure
load)
Fmax
(failure
load, kN)
100
23
95
21.8
90
90
20.7
20.7
98
268
10
10
90
20.7
104
10
90
20.7
190
10
80
18.4
3,456
20
80
18.4
775
20
80
18.4
18,723
20
80
18.4
121,000
20
80
16.1
12,047
30
70
16.1
74,515
30
70
16.1
500,000
30
70
16.1
560,000
30
70
16.1
800,000
30
70
16.0
800,000a
30
No failure
123
332
N. Erarslan, D. J. Williams
Sample
Amplitude
% SUL
Ultimate
load (kN)
Number of
cycles
up to failure
Indirect
tensile
strength (ITS)
Reduction in
ITS (%)
NST207-Rp1
10
17.4
2,583
8.2
24.1
NST207-Rp2
10
15.6
2,384
7.3
32.5
NST207-Rp3
10
18.1
2,723
8.5
21.3
17.03
2,563
8.0
25.9
Average
NST207-Rp1
20
17.5
2,195
8.2
24.1
NST207-Rp2
20
15.4
1,887
7.2
33.4
NST207-Rp3
Average
20
14.6
15.9
1,679
1,920
6.8
7.4
37.1
31.5
NST207-Rp1
30
17.3
1,906
8.1
25.0
NST207-Rp2
30
15.2
1,334
7.1
34.3
NST207-Rp3
30
16.1
1,556
7.5
31.0
16.2
1,598
7.6
30.1
42.0
Average
NST207-Rp1
40
14.0
738
6.5
NST207-Rp2
40
14.4
992
6.7
40.0
NST207-Rp3
40
16.8
1227
7.9
29.3
15.0
985
7.0
37.1
Average
Fig. 8 Comparison of loadstrain curves of Brazilian disc specimens tested under static and increasing cyclic loading with various amplitudes
123
333
permanent strain show that both the axial and lateral strain
curves increase with the number of cycles, but at different
rates. A slight deviation from linearity is evident only in
the final stage of vertical diametral strain prior to failure,
whereas remarkable deviation from linearity is evident in
horizontal diametral strain (see Fig. 10a). The axial stress
level at which the axial strain departs from linearity marks
the beginning of the onset of unstable crack growth, as
defined by Bieniawskie (1967). This generally occurs at an
axial stress level between 70 and 85% of the short-term
peak strength of cylindrical specimens. The dominant
mechanism causing this increase in axial strain is sliding
along inclined surfaces. These occur in the region characterised by the most significant structural changes to the
specimen, with the density of microcracks increasing sevenfold. As seen from Fig. 10b, the fatigue damage of rock
can be attributed to the continuous accumulation of stressinduced fracture damage. Examinations of the horizontal
diametral strain changes reveal relatively high stiffness
values up to 9 kN when the load is first applied to the
specimen (the lateral stiffness term represents the change in
the lateral strain rate under diametral compressive loading).
Fig. 9 Tested Brazilian disc specimens under: a static loading, and b, c cyclic loading
123
334
N. Erarslan, D. J. Williams
123
335
123
336
N. Erarslan, D. J. Williams
Fig. 14 Damage and small grains in the matrix of failed Brisbane tuff disc specimen tested under cyclic loading
Fig. 15 Damage and fracturing in the matrix of failed Brisbane tuff disc specimens tested under monotonic loading
123
337
Fig. 16 a, b Typical transcrystalline cracks, and c, d intercrystalline and intracrystalline cracks on the failure surfaces of Brisbane tuff disc
specimens tested under monotonic loading
indicate the fracturing mechanism of rock fatigue is produced by the combination of splitting (opening) due to
stress-induced fatigue cracks and frictional sliding (shear),
causing crushing at the grain boundaries during each
loading and unloading cycle around loosened grains.
Some dust grains were observed around the loosened
grains using a higher magnification (see Fig. 18). In general, contact points at grain boundaries are regions of stress
concentration. Transgranular cracks were often found
emanating from these regions. However, these small particles around the grains may also be explained by the
indentation of the grains. It is possible for stiffer grains
(indenters) to exert an indentation pressure on the surface
of the weaker matrix during each loadingunloading cycle.
It is well known that some special cracks, such as radial
cracks, propagate through the surface of a material during
unloading of indenters (Tiryaki, 2008; Whittaker et al.
1992).
From loadstrain plots it was determined that fatigue
fracturing is a continuous process of ongoing and
123
338
N. Erarslan, D. J. Williams
Fig. 17 Scanning electron microscope images of the fractured surfaces of the Brisbane tuff disc specimens: a, b loosened grains and typical
intercrystalline cracks around grains, and c, d extracted grains from the tuff matrix
Fig. 18 Scanning electron microscopic images of the fractured surfaces of Brisbane tuff disc specimens
123
4 Discussion
Monotonic loading, sinusoidal cyclic loading and increasing cyclic loading tests were conducted on Brazilian disc
specimens. The reduction in ITS was determined to be 30%
with sinusoidal loading, whereas increasing cyclic loading
caused a maximum reduction in ITS of 35%; these percentages are in comparison to the ITS values obtained
under monotonic loading. Besides the decrease in ITS
value, the fracturing mechanism of rock material was found
to be very different under monotonic and cyclic loading,
with excessive amounts of dust and small grains found in
cyclically failed specimens. This observation suggests that
opening tensile fracturing is not the only effective fracturing mechanism in rock fatigue damage. As the preexisting cracks and deformities in the rock disc specimen
do not necessarily align with the principal stress direction,
shear type or mixed type fracturing mechanisms are also
possible around inclined pre-existing cracks in a disc
specimen. Consequently, sliding and shear effects of crack
surfaces are believed to be the principal source of excessive
microfracturing in cyclic tests. The dilation of the cracks
along the diametral axial direction results in greater lateral
strain compared with diametral axial strain. This shows that
unstable crack propagation has been started in the specimen. Unstable crack propagation continues to the point at
which the numerous fatigue-induced microcracks coalesce
into larger cracks, and the rock can no longer support
loading cycles. It is believed that the subcritical failure of
rock, which is characterised by the development of a large
number of microcracks, is possible even prior to the
appearance of the main fatigue cracks in cyclically loaded
specimens.
The SEM images showed that transgranular and intergranular cracks are the main mechanisms of rock fatigue.
This may make an explanation to fatigue researches, which
has reported that a massive amount of microfractures and
irreversible damage accumulation are the main causes of
rock fatigue (Carfagni and Salvatore 2000; Holcomb 1981;
Pino et al. 1999). The SEM images also revealed many
small particles on failure surfaces, small grains and dust
around grain boundaries. However, it is still unknown how
the loading cycles break the bonds between the grains and
the rock matrix to produce intergranular cracks around
grain boundaries. Two possible mechanisms can be inferred from the SEM image analysis in this research: (1)
stiffer grains (i.e., quartz and feldspar minerals) act on the
339
5 Conclusion
The ITS response to cyclic loading was found to be different from that under static loading in terms of the lower
ultimate load and different fracturing mechanisms. A
macro-scale splitting crack with a sharp and rough surface
was found along the diametral compressive loading direction under monotonic loading, whereas an excessive
amount of small particles and dust was produced under
cyclic loading. In this research, various experimental
observations of cyclic loading tests with varying amplitudes have indicated that increasing cyclic loading is more
effective at ITS degradation of rocks than sinusoidal
compressive cyclic loading. The reduction in ITS was
found to be 33% with sinusoidal loading, whereas
increasing cyclic loading caused a maximum reduction in
ITS of 37%. In addition, no post-peak behaviour was
observed in the loadstrain plots of either the monotonic or
the cyclic loading tests. The Brazilian disc specimens
failed violently during both the monotonic and cyclic tests.
The SEM imaging results enable some of the qualitative
features of the fatigue damage process in Brisbane tuff to
be inferred. SEM investigations revealed that grain
boundaries play an important role in rock fatigue. The
largest cracks follow the grain boundaries and microcracks
generally start to form at the grain boundaries or voids.
Grain de-cohesion seems to be the source of large cracks.
Further, transgranular cracks were observed during rock
123
340
fatigue. Secondary cracks were seen on the fracture surfaces of one cyclically fractured specimen, but no such
secondary cracks were found on any of the static fracture
surfaces. The main characteristic was grain breakage under
cyclic loading, which probably starts at points of contact
between grains and is accompanied by the production of
very small fragments, probably due to frictional sliding
within the weak matrix. It is believed that contact points at
grain boundaries are the regions of stress concentration
(i.e., indenters). Transgranular cracks may emanate from
these regions, and intergranular cracks sometimes pass
through these contact points. Once cracking starts, there is
a steady progression of damage and a general loosening
of the rock, which is a precursor to the formation of
intergranular cracks.
Acknowledgments Acknowledgement is made to Leighton Contractors who provided core samples of Brisbane tuff from the CLEM7
Project and to Professor Ted Brown AC, Les McQueen, Mark Funkhauser and Rob Morphet of Golder Associates Pty Ltd for their
assistance and advice. The work described forms part of the first
authors PhD research carried out within the Golder Geomechanics
Centre at The University of Queensland. The first author was supported by an Australian Postgraduate Award/UQRS and the Golder
Geomechanics Centre.
References
Atkinson BK (1984) Subcritical crack growth in geological materials.
J Geophys Res 89:40774114
Attawel PB, Farmer IW (1973) Fatigue behaviour of rock. Int J Rock
Mech Min 10:19
Bagde MN, Pedros V (2005) Fatigue properties of intact sandstone
specimens subjected to dynamic uniaxial cyclical loading. Int J
Rock Mech Min 42(2):237250
Bagde MN, Pedros V (2009) Fatigue and dynamic energy behaviour
of rock subjected to cyclical loading. Int J Rock Mech Min
46:200209
Bieniawskie ZT (1967) Mechanism of brittle rock fracture: part II
experimental studies. Int J Rock Mech Min 4(4):407423
Burdine NT (1963) Rock failure under dynamic failure conditions.
SPE 3:18
Carfagni S, Salvatore W (2000) The characterisation of marble by
cyclic compression loading: experimental results. Mech Cohes
Frict Mat 5:535547
Celestino TB, Bortolucci AA (1995) Determination of rock fracture
toughness under creep and fatigue. In: Proceedings of the 35th
U.S. symposium on rock mechanics. Reno, New York,
pp 147152
Costin LS, Holcomb DJ (1981) Time-dependent failure of rock under
cyclic loading. Tectonophys 79:279296
123
N. Erarslan, D. J. Williams
Evans AG, Fuller ER (1974) Crack propagation in ceramic materials
under cyclic loading conditions. Metall Trans 5:2729
Evans AG, Linzer M, Russell LR (1974) Acoustic emission and crack
propagation in polycrystalline alumina. Mater Sci Eng
15:253261
Gatelier N, Pellet F, Loret B (2002) Mechanical damage of an
anisotropic porous rock in cyclic triaxial tests. Int J Rock Mech
Min 39:335354
Gottlieb L, Moore PJ (1981) Vibratory cutting of brown coal. Int J
Rock Mech Min 18:335339
Hadly K (1976) The effect of cyclic stress on dilatancy: another look.
J Geophys Res 81:24712474
Haimson BC (1978) Effect of cyclic loading on rock. In: Dynamic
geotechnical testing. ASTM STP 654:228245
Haimson BC, Kim CM (1971) Mechanical behaviour of rock under
cyclic fatigue. Rock Mech 3:845863
Holcomb DJ (1981) Memory, relaxation, and microfracturing in
dilatant rock. J Geophys Res 86(B7):62356248
Hood M, Alehossein HA (2000) Development in rock cutting
technology. Int J Rock Mech Min 37(12):297305
Inglis CE (1913) Stresses in a plate due to the presence of cracks and
sharp corners. T Inst Nav Archit 55:219246
Ingraffea AR (1981) Mixed mode fracture initiation in Indiana
limestone and westerly granite. In: Proceedings of the 22nd U.S.
symposium on rock mechanics. Cambridge, MA, pp 186191
ISRM (1978) Suggested methods for determining tensile strength of
rock materials. Int J Rock Mech Min 15:99103
Nemat-Nasser S, Deng H (1994) Strain rate effect on brittle failure in
compression. Acta Metall Mater 42:10131024
Petros V, Bagde MN, Holub K, Michalcik P (2003) Comparison of
changes in the strength and the deformation behavior of rocks
under static and dynamic loading. In: The 10th Congress of the
ISRM, Technology Roadmap for Rock Mechanics, Johannesburg, South Africa, pp 899902
Pino DR, Narducci P, Royer-Carfagni G (1999) A SEM investigation
on fatigue damage of marble. J Mater Sci Lett 18:16191622
Roxborough FF (1963) Cutting rocks with picks. Min Eng (Littleton)
132:445452
Roxborough FF (1968) Coal ploughing. Col Eng 12(16):6671
Singh SK (1989) Fatigue and strain hardening behaviour of
greywacke from the flagstaff formation, NSW. Eng Geol
26:171179
Tiryaki N (2008) Numerical analysis of rock fracturing by various
indenters. Dissertation, Hacettepe University, Ankara, Turkey
Whittaker BN, Singh RN, Sun G (1992) Rock fracture mechanics,
principles, design and applications. Elsevier, Amsterdam
Zhang ZX, Kou SQ, Yu J, Yu Y, Jiang LG, Lindqvist PA (1999)
Effects of loading rate on rock fracture. Int J Rock Mech Min
36(5):597611
Zhao J, Li HB (2000) Experimental determination of dynamic tensile
properties of a granite. Int J Rock Mech Min 37:851861
Zhenyu T, Haihong M (1990) An experimental study and analysis of
the behaviour of rock under cyclic loading. Int J Rock Mech Min
27(1):5156