Phn 1: in dn khu vc th nghim

BI 2
XC NH TNG ST TRONG
NC
Bui Nhm Ngy
lm
th
nghim
1
3,4
20/09/2016
2
5,6
22/09/2016
3
7,8
27/09/2016
4
1,2
29/09/2016
BI 3
XC NH HM LNG SUNFAT
TRONG NC
Bui Nhm Ngy
lm
th
nghim
1
5,6
20/09/2016
2
7,8
22/09/2016
3
1,2
27/09/2016
4
3,4
29/09/2016

BI 1
XC NH KIM CA NC
Bui Nhm Ngy
lm
th
nghim
1
1,2
20/09/2016
2
3,4
22/09/2016
3
5,6
27/09/2016
4
7,8
29/09/2016
BI 4

XC NH HM LNG
CACBONIOXIT TRONG KHNG KH
XUNG QUANH

Bui Nhm
1
2
3
4

7,8
1,2
3,4
5,6

Ngy
lm
nghim
20/09/2016
22/09/2016
27/09/2016
29/09/2016

th

Phn 2: In ha cht v dng c mi nhm

BI 1
XC NH KIM CA NC
1. i tng mu:

01 mu Nc my phng th nghim
03 Mu nc phng th nghim do gio vin
chun b
2. Phng php phn tch: Phn tch th tch( chun )
Mi mu sinh vin lm 4 ln ly kt qu x l s
liu
3. Dng c v ha cht cn thit
T
T
1
2
3
4
5

Ha cht

a
im
Ch th mu Trn
phenolphthalei bn
n 0,05 %
Ch th mu Trn
methyl da cam bn
0,05 %
Dd
Na2S2O3 Trn
0,1N
bn
Dd NaOH 1N
Trn
bn
Dd
Na2CO3 Trn
0,02N
bn

Dd H2SO4 1N

Yu cu

Ghi ch

KTV pha

1 l nh git 2
nhm dng chung

KTV pha

1 l nh git 2
nhm dng chung

KTV pha

1 l nh git 2
nhm dng chung
ng trong l 100
ml
KTV chun b 1 cc
sch sy kh
sv cn ha cht, 1
bnh nh mc 500
ml, 1 chai kh,
sch ng dung
dch sau khi pha

KTV pha
SV pha t Na2CO3 tinh
th c PTN sy
1050C v trong bnh
ht m (cn 0,503 g
Na2CO3 chuyn qua
phu vo bnh nh
mc 500 ml, thm
nc ct n vch
mc)
SV pha t H2SO4 c
trong t ht(eo gng
tay, ly khong 250 ml
nc ct cho vo bnh
nh mc 500 ml, thm

Pha xong chuyn

ra chai kh sch
ly lm dung
dch lu tr

Phn cng
nhim v

1
nhm
pha dng
chung cho
2 nhm

1
nhm
pha dng
chung cho
2 nhm

Dung
dch
H2SO4 0,02N

14 ml H2SO4 c vo,
thm nc n vch
mc)
SV Pha t dung dch
Dung dch H2SO4 1N
(20 ml H2SO4 1N vo
bnh nh mc 1lit,
thm nc ct n
vch mc)

Pha xong chuyn

ra chai ly lm
dung dch chun,
trc khi thc hin
cn chun li bng
dung dch Na2CO3
0,02N

1
nhm
pha dng
chung cho
2 nhm

Gi :
- Mt nhm s pha dung dch H2SO4 1N, H2SO4 0,02N
- Mt nhm s pha dung dch Na 2CO3 0,02N, chun
li dung dch H2SO4 0,02N
Dng c th nghim
T
T

Tn dng c

n v
S lng Dng
tnh
cho
mt chung
nhm

Buret 25ml

Ci

Bnh tam gic 250 Ci

ml

3
4

Giy ch th vn Hp
nng
My o pH
Ci

ng nghim 16

Ci

08

ng ong 100ml

Ci

04

7
8

Gi ng nghim
Ci
Pi pet 25 ml chia Ci
vch

1
2

02
04

02

08
(04
bnh
1
buret)
01

Tng
(cho
2
nh
m)
04

16

02
x

Mc ch

Cha dung dch

chun H2SO4
0,02 N
Ly
mu

chun
Ktra s b pH
ca mu
o pH chnh xc
ca mu
Lm ng i
chng
Ly mu vo
bnh nh mc
ng
Ly lng chnh
xc -Dung dch

Pi pet 10 ml chia Ci
vch

04

1
0

Cc thy tinh 100 ci

ml kh, sch c
m

1
1
1
2
1
3
1
4
1
5

Chai ng ha Ci
cht 1 lt
Chai ng ha ci
cht 500 ml
Cn phn tch 4 s ci

Tha cn

ci

Bnh tia nc ct

ci

05

chun
-Mu phn tch
Ly lng chnh
xc: -Dung dch
chun
-Mu phn tch
Cn
mu
Na2CO3,
ly
dung dch chun
vo buret

1
2

02

04

Cn cht chun
Na2CO3
Dng
ly
Na2CO3
Dng:
-Trng dng c
-Pha ha cht

Quy trnh tin hnh th nghim

Tin hnh o s b pH ca mu nc
Nu mu c pH > 8,3: Ly 100ml mu vo bnh nn, thm 3 git ch th mu
phenolphthalein. Chun bng dung dch H2SO4 0,02N ht V1 (ml). Ghi li gi tr V1
tnh kim phenol (P).
Nu mu c pH < 8,3: Ly 100 ml mu vo bnh nn, thm 3 git ch th mu
methyl cam (hay 3 git ch th mu hn hp). Lm hai ng i chng, cho vo hai ng
nghim mi ng 25 ml mu, ng th nht thm 1 ml H 2SO4 1N v 1 git methyl cam.ng
th hai thm 1 ml NaOH 1N v 1 git methyl da cam. Chun mu bng dung dch
H2SO4 cho n khi dung dch c mu da cam (mu gia hai ng i chng). Nu dng
ch th hn hp, ti im kt thc dung dch c mu xm. Ghi th tch V 2 ml H2SO4
0,02N dng tnh kim metyl da cam .

BI 2
XC NH HM LNG TNG ST TRONG NC

1. i tng mu:
01 mu Nc my phng th nghim
02 Mu nc phng th nghim do gio vin
chun b
2. Phng php phn tch: Phn tch trc quang
Mi mu sinh vin lm 3 ln ly kt qu x l s
liu
3. Dng c v ha cht cn thit
TT
1
2

Ha cht

a
im
T
HCl c.
ht
Dung
dch Trn
bn
hydroxylamin
NH2OH.HCl

Yu cu

Ghi ch

eo gng tay vo ly
ha cht
KTV pha
Ha
tan
50g
NH2OH.HCl
trong
500ml nc ct

Chun b 2 chai
trong t ht
-Pha thnh 500 ml
chia thnh 2 nhm
-Bo qun dng
trong c qu trnh
th nghim

Dung dch m Trn

amoni
acetat bn
(NH3C2H3O2)

KTV pha t tinh th

amoniacetat
-Ha
tan
250
g
NH3C2H3O2 trong
150ml nc ct,
thm 700ml axit

-Pha thnh 1000ml

chia
thnh
2
nhm, mi nhm
500 ml
-Bo qun dng
cho c qu trnh
th nghim

Chun b

-1 Cc 250
ml
-1
bnh
nh mc
500 ml
-2 chai
250ml
-1 cc 500
ml
-1
bnh
nh mc
1000 ml
-2
chai
ng 500

Dung
dch Trn
phenanthroline bn
(C12H8N2.H2)

Dung dch lu Trn

bn
tr st

Dung

dch
chun
st

acetic
(CH3COOH) m
c. Lc u.
KTV pha t tinh th
phenanthroline
-Cch 1: Ha tan
500mg
1,10
phenanthroline(C12H8N2
.H2) trong 500ml nc
ct, khuy v un ti
80oC ( khng c un
si)
-Cch 2: Cho 50ml
nc ct vo trong cc
cha
500
mg
phenanthroline
C12H8N2.H2O, thm 10
git axit m c,
khuy u n khi tan
hon ton, pha long
thnh 500ml.
-Khng s dng khi
dung dch c mu.
KTV pha t mui Mo
- Rt 10ml H2SO4 m
c vo 25ml nc ct
v thm vo 0,702 g
Fe(NH4)2(SO4)2.6H2O.
Sau khi dung dch ng
nht, thm tng git
KMnO4 cho n khi
xut hin mu hng
nht khng i. Pha
thnh 500ml vi nc
ct (1,00ml = 200g
Fe).
SV pha t dung
dch st lu tr
-(Ly 25 ml dung dch
lu tr st cho vo bnh
nh mc 500ml, thm

ml

-Pha thnh 500 ml,

chia mi nhm 250
ml
- Bo qun dng
cho c qu trnh
th nghim

-1
bnh
nh mc
500 ml
-2
chai
250ml
-cc c m
100ml

-Pha thnh 500 ml

2 nhm dng
chung
-Bo qun dng
cho c qu trnh
th nghim

-1
bnh
nh mc
500 ml
-1 cc 100
ml
-1
chai
thy
tinh
500 ml

Pha vo bnh nh
mc 500 ml, mi
nhm dng ring,
pha dng trong
tng
bui
th
nghim

-2
bnh
nh mc
500ml
-2
pipet
bu 25 ml

Dung

dch Trn
bn
NaOH
30%

CH3COOH c

H2SO4 c

10

KMnO4

11

Nc ct

T
ht
T
ht
T
PTN
Trn
bn

nc ct ti vch nh
mc
(1,00ml
=
10,00g Fe).
KTV pha t NaOH tinh
th.
Cn
-Cn 300g NaOH vin
vo cc sau cho t
t vo cc ( c sn
700 ml nc), khuy
u cho tan ht

Pha thnh 1000ml

chia 2 nhm, mi
nhm 500 ml
-Bo qun dng c
trong qu trnh th
nghim

-1
bnh
nh mc
1000 ml
- 1 cc
500ml
-2
chai
nha 500
ml

Dng cho KTV pha ha cht

Mi nhm 2 chai 500 ml

Gi : sinh vin t tho lun b tr cch lm th nghim,

phn cng nhim v sao cho nhanh chng v hiu qu
Dng c th nghim
TT

Tn dng c

Bnh nn 125ml Chi

hoc 250 ml
c
Bnh nh mc
500 ml

n
v
tnh

S
ln
g
cho
mt
nh
m
10

Dn
g
chun
g

01

03

Tng
Mc ch
(cho 2
nhm
)

20
04

X l mu trc khi em o
quang
-mi nhm cn 01 pha
dung dch st chun( 2 nhm
=02)
-KTV dng 03 pha
+Dung dch lu tr st,
+Dung dch phenanthroline

Bnh nh mc
50 ml
Bnh nh mc
25 ml
ng ong 50 ml

a thy tinh

Qu bp

02

04

Gng tay

02

04

R ng nghim

Ci

10
11

Gi pipet
Pi pet bu 25 ml

ci
Ci

1
2

2
4

12

Pi pet 25 ml chia
vch
Pi pet 10 ml chia Ci
vch

14

Pi pet 5 ml chia
vch

15

Pi pet 2 ml chia
vch
Pi pet 1 ml chia
vch

02

04

04

08

13

16

17

Cc
250

thy
ml

Chi
c
Chc

10

20

14

Chi
c
Ci

tinh ci
kh,

KTV

01

+Dung dch hydroxylamin

nh mc mu sau khi x
l
ng dung dch chun lp
ng chun
Ly mu vo bnh nn x
l
Khy dung dch khi pha ha
cht
Ly dung dch:
-01 trn bn
-01 trong t ht
eo khi ly ha cht c hi,
gy n mn da, bng nh
H2SO4 c, HCl c
ng:
-Bnh nn
-Bnh nh mc
Ly lng chnh xc
- Dung dch chun
-Mu phn tch
10 ml<Ly mu vi lng <
25ml
Ly lng chnh xc
-Dung dch m,
-Dung dch chun
Ly lng chnh xc:
-Dung dch chun,
-Dung dch phenanthroline,
- dung dch hydroxylamine,
-Ly dung dch HCl c khi
x l mu
Ly :
-Dung dch NaOH
- Dung dch HCl c,
-Dung dch chun,
- Dung dch hydroxylamin
-Cn
pha
dung
dch
hydroxylamin

18

19

sch,c m
Cc thy
500
ml
sch ,c m
Cc thy
100
ml
sch ,c m

tinh
kh,

KTV

02

-Cn pha dung dch m

-Cn pha NaOH

tinh
kh,

02

01
(KTV
)

03

-Cn pha dung dch st lu

tr
Cn
pha
dung
dch
phenanthrolin
ng:
-Dung dch m(01 cho mi
nhm)
-Dung dch st lu tr (01
chung cho 2 nhm)
ng:
-Dung dch hydroxylamine
-Phenanthroline
ng dung dch NaOH 30%

20

Chai thy tinh Ci

ng ha cht
500 ml

01

21

Chai thy tinh ci

ng ha cht
250 ml
Chai nha ng ci
ha cht
Bp in
ci
Cn phn tch 4
s

02

04

01

02

22
23
24

25

Cn k thut 2 ci
s

26

a thy tinh

27

28
29

30

02

Chi
c
Bi thy tinh hoc Hn(
bt
mn
h)

Giy ch th vn Hp
nng
My o pH
Chi
c

My quang ph

Chi
c

4
01

2
Vi
mn
h
nh
2
01

01

un x l mu
Cn:
-Cht chun
-Thuc th
KTV Cn ha cht pha:
- Dung dch m ,
- Dung dch NaOH,
-Dung dch tc nhn kh
(hydroxylamine)
Khuy u dung dch khi pha
ha cht
Trnh hin tng si qu
mnh khi un dung dch

o s b pH ca dung dch
o pH ca dung dch sau khi
x l mu, trc khi mang i
o hp th
o hp th ca
-Dung dch chun

31

Cuvet thch anh

32

Tha cn

33

Bnh tia nc ct

34

Bt nha

35
36

Giy nhn
Giy cun

37

Phu thy tinh

Chi
c
Chi
c
chai

02

04

Chi 01
c
Cun
Cun

02

Chi
c

x
x

01
01

01

-Mu
ng mu khi o trong my
quang ph
Cn ha cht th nghim
Dng:
- Trng dng c.
-Pha long dung dch
ng dung dch thi sau khi
o mu
Ghi mu v dn mu
Lau kh b ngoi cuvet khi o
mu
Chuyn ha cht pha vo
bnh nh mc

Quy trnh tin hnh th nghim

2. THC HNH XC NH HM LNG ST TNG CNG TRONG NC (Fe tc):

2.1. Chun b mu:

- Ra tt c dng c thy tinh bng axit HCl m c, trng li bng nc ct trc
khi s dng.( Nhm loi b st bm trn thnh dng )
- Mu phi c lc u trc khi phn tch,
- Ly 50ml mu cho vo bnh nn. Nu th tch mu c hm lng st cao hn 200g,
s dng mt lng mu t hn v pha thnh 50 ml. Thm 2ml HCl m c v 1ml
NH2OH.HCl. Thm vi vin bt vo bnh nn, un si n khi th tch cn khong 15
20ml
- Lm ngui mu nhit phng, chuyn dung dch vo bnh nh mc 50ml, chnh
pH v khong 2,8-3,5 bng (NaOH 30%)
2.2. Lp ng cong chun
S dng dung dch chun c nng 1ml = 10g Fe.
Pha lot dung dch chun st nh sau :
Bng 2.4. Lot dung dch chun st
STT bnh nh mc 25 1
2
3
4
5
M1 M2
ml
V dd chun (ml)
0
2,5 5
7,5 10
V mu
15
15
V HCl m c (ml)
1,0
0
0
V dd NH2OH.HCl (ml)
2,5
0
0

NaOH (30%)
V dd m NH3C2H3O2 (ml)
V dd phenanthroline (ml)
H2O (ml)
C mg/l

1,0
7,5
2,5
11,5 8
0
1

0
5,5 3
2
3

0,5 0.5
4

0
0.5

Nu mu b c v c mu, thay v s dng nc ct lm mu chun trng, s dng chnh

mu lm mu chun trng v x l mu qua tt c cc bc nh trong qu trnh thc hin
nhng khng cho phenanthrolin.

BI 3: XC NH HM LNG SUNFAT TRONG NC

1. i tng mu:
01 mu Nc my phng th nghim
02 Mu nc phng th nghim do gio vin
chun b
2. Phng php phn tch: Phn tch trc quang
Mi mu sinh vin lm 3 ln ly kt qu x l s
liu

3. Dng c v ha cht cn thit

TT

Ha cht

Dung dch m:

a
i
m
Tr
n
bn

Dung dch Bari Tr

n
clorua 33%

Yu cu

Ghi ch

Chun b

KTV pha

-Pha thnh 1000

ml chia u cho 2
nhm (mi nhm
500 ml)
-Bo qun dng
trong c qu trnh
th nghim

-1 cc 250
ml
-1
bnh
nh mc
1000 ml
- 2 chai
500 ml

Ha
tan
30g
MgCl2.6H2O,
5g
CH3COONa.3H2O , 1 g
KNO3 v 20 ml CH3COOH
(99%) trong 500 ml nc
ct ,pha thnh 1000ml.
-Pha thnh 500 ml -1 cc 250
KTV pha
Cn 165 g BaCl2 ha tan chia u cho 2 ml

bn

nhm( mi nhm
250 ml)
-Bo qun dng
trong c qu trnh
th nghim
-Pha thnh 1000
ml chia cho 2
nhm ( mi nhm
500 ml)
- Bo qun dng
trong c qu trnh
th nghim

vi 335 ml nc ct

Dung dch sunfat Tr

SV pha t tinh th
chun (1,00 ml= n
Na2SO4
bn

2147,9 mg Na2SO4 khan +

100 g SO4 )
nc ct pha thnh 1000
ml.( hoc Ly chnh xc
10,4 ml H2SO4 0.0200N
chun + nc ct
=
100ml)
Dng cho KTV pha ha cht
MgCl2.6H2O

4
5
6
7
8

-1
bnh
nh mc
500 ml
-1 cc 50
ml
kh
sch
-1
bnh
nh mc
1000 ml
- 1 phu
thy tinh

CH3COONa.3H2O

KNO3
CH3COOH
Nc ct

Tr
n
bn

Mi nhm 2 chai 500 ml

Gi :
Dng c th nghim
TT

Tn dng c

Bnh nh mc Ci
1000 ml
Bnh nh mc
500 ml
Bnh nh mc Chc

2
4

n
v
tnh

S
ln
g
cho
mt
nh
m

Dn
g
chun
g

Tng
Mc ch
(cho 2
nhm
)

KTV
(02)
KTV
(01)
16

-Pha dung dch m

-Pha dung dch chun
-Pha dung dch BaCl2
32

ng dung dch chun lp

5
6
7

25 ml
ng ong 100 ml Chi
c
a thy tinh
Ci
Qu bp
Phu thy tinh

x
1

01
2

02
x

04
01

R ng nghim

Ci

10
12

Gi pipet
ci
Pi pet 25 ml chia
vch
Pi pet 10 ml chia Ci
vch
Pi pet 5 ml chia
vch
Pi pet 2 ml chia
vch
Cc thy tinh
250 ml c m

1
2

2
4

02

04

13
14
15
18

19

21

22

25

26

Cc thy tinh 50
ml kh, sch c
m
Chai thy tinh Ci
ng ha cht
500 ml

Chai thy tinh ci

ng ha cht
250 ml
Cn phn tch 4
s

Cn k thut 2 ci

ng chun v o mu
ong nc ct khi pha dung
dch
Khy dung dch khi pha ha
cht
Ht dung dch:
Chuyn dung dch cn pha
vo bnh nh mc
ng:
-ng ong
-Bnh nh mc
ng pipet cho mi nhm
10 ml<Ly mu vi lng <
25ml
Ly lng chnh xc:
-Dung dch chun
Ly lng chnh xc:
-Dung dch chun,
-Ly dung dch BaCl2

KTV

02

-Cn BaCl2
- Cn ha cht pha dung dch
m

01

Cn Na2SO4 pha dung dch

chun

02

04

01

02

ng:
-Dung dch chun (01 cho
mi nhm)
-Dung dch m (01 cho mi
nhm)
ng:
-Dung dch BaCl2

01

01

Cn:
-Cht chun
-Cn ha cht i pha dung
dch m
KTV Cn ha cht pha:

27

s
a thy tinh

31

My quang ph

32

Cuvet thch anh

33

Tha cn

34

Bnh tia nc ct

34

Bt nha

35
36

Giy nhn
Giy cun

KTV
Chi
c
Chi
c

Chi
c
Chi
c
chai

02

04

Chi 01
c
Cun
Cun

02

01

x
x

01
01

- Dung dch BaCl2

Khuy u dung dch khi pha
ha cht
o hp th ca
-Dung dch chun
-Mu
ng mu khi o trong my
quang ph
Cn ha cht th nghim
Dng:
- Trng dng c.
-Pha long dung dch
ng dung dch thi sau khi
o mu
Ghi mu v dn mu
Lau kh b ngoi cuvet khi o
mu

Quy trnh tin hnh th nghim

2.

THC HNH XC NH HM LNG SUNFAT TRONG NC

a) Chun b ng chun theo th t sau:

Bng 2.7. Lot dung dch chun sunfat
STT bnh nh mc 10ml
1
2
3
2DD SO 4 chun (5ppm) (ml)
0
2,5 5
Mu (ml)
m (ml)
5
BaCl2 33 % (ml)
2
H2O (ml)
18 15,5 13

4
7,5

5
10

10,5 8

M1

M2

15

15

Lc u ha tan hon ton BaCl2 thnh dung dch ng nht.

b) o hp thu A ca dung dch tham chiu v mu trn my quang ph = 420nm.
V ng cong chun v so snh, ghi kt qu. Thi gian o khng qu 5 pht trnh
lng ng kt ta BaSO4. Nu c ca mu vt qu 20mg/l, cn pha long mu n
khong thch hp.
Ch : Nu mu c hoc c nhiu cn l lng, cn phi lc trc khi ly mu.

BI 4: XC NH HM LNG CO2 TRONG KHNG KH

1. i tng mu:
2. Phng php phn tch: Hp th CO2 vo mt lng
chnh xc dung dch Ba(OH)2, chun lng
Ba(OH)2 d xc nh hm lng CO2 hp th
Mi mu sinh vin lm 3 ln ly kt qu x l s
liu
3. Dng c v ha cht cn thit
TT

Ha cht

a
im
dch Trn
bn

Dung
barit:

Dung dch axit Trn

ocxalic
100 bn
ppm:

Dung
dch Trn
phenolphthale bn
in 0,1%:

11

Nc ct un Trn
si ngui
bn

Yu cu

Ghi ch

Chun b

KTV pha
Cn
0,7
g
Ba(OH)2.8H2O v 0,04
g BaCl2 ho tan bng
nc ct un si
ngui, nh mc thnh
500 ml, lc dung dch
thu c, chun li
nng bng dung
dch axit axit ocxalic
100 ppm

Pha thnh 500 ml,

2
nhm
dng
chung, trc khi
lm th nghim
cn chun li
-Lm th nghim
hm no pha hm

-1 bnh nh
mc 500 ml
-1 cc cn 50
ml
-1 chai 500
ml

SV pha t tinh th
H2C2O4.2H2O
(Ho tan 0,5632 g
H2C2O4.2H2O bng nc
ct un si ngui
sau nh mc thnh
1 lt (1ml = 0,1 ml
cacbon ioxyt).
KTV pha
Cn
0.1g
phenolphthalein
pha
trong 100 ml cn 900.

Pha thnh 1000

ml, chia u cho 2
nhm (mi nhm
500 ml)
-Bo qun dng
trong c qu trnh
th nghim

-1 bnh nh
mc 1000 ml
-1 cc cn 50
ml
-2 chai 500
ml

-Pha thnh 100 ml

(dng chung cho
c 2 nhm)
-Bo qun dng
cho c qu trnh
th nghim

-1 bnh nh
mc 100 ml
-1 l nh git
100ml
-1 cc cn 50
ml

Mi nhm 2 chai 500 ml

Gi : sinh vin t tho lun b tr cch lm th nghim,

phn cng nhim v sao cho nhanh chng v hiu qu

Dng c th nghim
TT

Tn dng c

n
v
tnh

1
2

Ci
ci

Bnh nn 250 ml
Bnh nh mc
1000 ml
Bnh nh mc
500 ml
Bnh nh mc
100 ml
a thy tinh

Qu bp

R ng nghim

8
9

3
4

10

Chi
c
Chc
Ci

Dn
g
chun
g

Tng
Mc ch
(cho 2
nhm
)

06
01

01

01

02

04

Ci

Gi pipet
ci
Pi pet 10 ml chia Ci
vch
Buret
ci

1
1

2
2

01

02

11

Cc thy tinh 50 ci
ml kh, sch,c
m

12

Chai thy tinh Ci

ng ha cht
500 ml

13

S
ln
g
cho
mt
nh
m
03

Cn phn tch 4 Chi

s
c

KTV

01

03

(KTV 03
)
01

Chun lng d Ba(OH)2

Pha dung dch axitoxalic 100
ppm
Pha dung dch barit
Pha dung dch ch th
phenolphtalein
Khy dung dch khi pha ha
cht
Ly dung dch:
-01 trn bn
-01 trong t ht
ng:
-ng bnh nn
-ng qu bp
ng pipet
-Ly dung dch hp th
-Cha dung dch chun axit
oxalic
Cn pha dung dch :
-Barit
-Axit oxalic
-Phenolphtalein
ng:
-Dung dch axit oxalic (01 cho
mi nhm)
-Dung dch barit (01 chung
cho 2 nhm)
Cn:
-Cht chun
-Thuc th

14

18

My ht khng Chi
kh SKC
c
B hp th kh
Chi
c
a thy tinh
Chi
c
Tha cn
Chi
c
Bnh tia nc ct chai

19

Bt nha

20

Giy nhn

Chi 01
c
Cun

19

Giy cun

Cun

01

20

Phu thy tinh

Chi
c

01

15
16
17

x
01

02

02

04

02
x

01

Ht khng kh v dung dch

hp th
Cha dung dch hp th
Khuy u dung dch khi pha
ha cht
Cn ha cht th nghim
Dng:
- Trng dng c.
-Pha long dung dch
ng dung dch thi
Ghi thng s mu v dn ln
mu
Lau kh b ngoi cuvet khi o
mu
Chuyn ha cht pha vo
bnh nh mc

1. THC HNH XC NH HM LNG CO2 TRONG KHNG KH

Ly vo 3 ng hp th mi ng 10ml dung dch barit,cho mi ng 1 git
phenolphatalein 0,1% dung dch c mu hng, ni vi my ht, bt cng tc v ht vi
tc 1lt/pht trong 10 pht( hoc khi dung dch trong ng hp th u tin nht mu),
tt my chuyn ton b dung dch trong ng hp th vo bnh nn ,trng ng hp th
bng nc ct ri gp c vo bnh nn, ly dung dch thu c chun li lng d
Ba(OH)2 bng dung dch axit oxalic 100 ppm n mt mu.
Chun ng thi mu trng vi 30ml dung dch barit v 3 git phenolphthalein
0.1 %.