B GD&T

Trng i hc SPKT
Khoa CNHH&TP

CNG HA X HI CH NGHA VIT NAM

c lp T do Hnh phc
**********

Chng trnh Gio dc i hc

Ngnh o to: Cng ngh thc phm

Trnh o to: i hc

Chng trnh o to: Cng ngh thc phm

cng chi tit hc phn

1. Tn hc phn: Thc hnh ha phn tch

MT

M hc phn: ANCH235651

2. Tn ting: Analytical Chemistry Practice

3. S tn ch: 1
Phn b thi gian: 15 tun (2 tit l thuyt + 0*2 tit thc hnh + 6 tit t hc/ tun)
4. Cc ging vin ph trch hc phn
1/ GV ph trch chnh: ThS. H Th Yu Ly
2/ Danh sch ging vin cng GD: ThS. Phan Th Anh o
5. iu kin tham gia hc tp hc phn
Mn hc tin quyt: ton cao cp 1, 2, 3, vt l i cng A1 v A2, ha i cng, ha
hu c, ha sinh i cng, Ha phn tch MT
6. M t tm tt hc phn
Trang b cho ngi hc nhng k nng thc hnh. Pha ch ha cht, thc hnh thnh tho
k thut chun , xc nh c thi im dng chun qua k nng pht hin c s thay
i mu sc ca dung dch chun . Tnh ton c cc sai s lin quan n kt qu phn tch.
Thit lp cng thc tnh ton cc kt qu phn tch. Hiu ng cc phng php x l v iu
chnh quy trnh phn tch ph hp vi iu kin thc t phng th nghim. Nhn thc v thit
lp cc phng php bo v, ci thin mi trng trong v xung quanh phng th nghim. Bit
cch x l cc s c v an ton trong phng th nghim... ng thi lm nn tng cho vic thc
hin cc mn hc thc hnh ngh, n kha lun tt nghip.
Gip cho ngi hc c phng php tip cn, k nng thc hnh phn tch cht bng
phng php chun , t c nhng nh hng c th v kh nng hc tp, nghin cu v
pht trin ngh nghip ca mnh.
7. Mc tiu hc phn (Course Goals)
Mc tiu
(Goals)

M t
(Goal description)
(Hc phn ny trang b cho sinh vin:)

Chun u ra
CTT

G1

Nm vng kin thc chuyn mn trong lnh vc thc hnh nh 1.1, 1.2, 1.3
lng bng phng php ha hc: an ton PTN, s dng dng c
o, pha ch ha cht, k thut nh phn, xc nh im dng nh
phn, tnh kt qu, x l s liu, nh gi kt qu.

G2

Thnh tho s dng thit b, dng c s dng trong qu trnh th

2.1, 2.2, 2.4,
nghim. Kh nng phn tch, gii thch v lp lun gii quyt cc
2.5
vn lin quan n kt qu phn tch.C k nng chuyn
mn: o c ngh nghip, trung thc, xc nh mc
tiu v nh hng ngh nghip.

G3

K nng lm vic nhm, giao tip v kh nng c hiu cc ti 3.1; 3.2; 3.3
liu k thut bng ting Anh.

G4

Kh nng vn dng, xc nh cht trong i tng mu mi 4.1; 4.5

trng

8. Chun u ra ca hc phn.
Chun
u ra HP

M t
Chun u
ra CDIO
(Sau khi hc xong mn hc ny, ngi hc c th:)
G1.1 Nm c phng php tip cn v phng php lun ca mn hc
1.1
Trnh by c nguyn tc ca s i mu trong qu trnh nh phn.
1.2
G1.2
Phng php chun axit-baz, oxy ha kh, kt ta v to phc.
Nm vng v vn dng cc cng thc tnh ton v chuyn i cc
1.3
G1.3 loi nng vo thc hnh pha ch v xc nh nng v hm

G1

G1.4

lng cc cht.
Nm vng nguyn tc c kt qu t dng c o v biu din kt qu

phn tch, x l v nh gi kt qu phn tch.

S dng ng, thnh tho dng c o. Hiu r qu trnh nh phn,
G2.1
gii thch ng s i mu trong qu trnh nh phn.
G2

2.1.1

G2.2

p dng cc kin thc l thuyt vo thc hnh: gii thch hin tng,
thit lp cng thc, nhn thc thi im dng chun .

2.2.1

G2.3

C kh nng t tm kim ti liu, t nghin cu, trnh by v gii

quyt cc vn lin quan ti ni dung th nghim

2.2.3

G3.1

C kh nng lm vic trong cc nhm tho lun v gii quyt cc 3.1.1, 3.1.2,
vn lin quan n bi th nghim
3.2.6

G3.2

Hiu c cc thut ng ting Anh dng trong ha phn tch, thc

hnh ha phn tch mi trng

G3

G4

1.4

3.3.1

G4.1 Xc nh c i tng cn phn tch trong mu thc t

4.3.2

G4.2 Vn dng phng php phn tch ha hc ph hp vi i tng,

iu kin phng th nghim

4.4.1

G4.3 X l v bo co kt qu

4.4.3

9. Ti liu hc tp
-

Sch, gio trnh chnh:

1. Bi ging Thc hnh Ha Phn tch, bin son: H Th Yu Ly, 2009.

Sch tham kho:

2. Nguyn Bch Tuyt, L Xun Mai, Th nghim ha phn tch, i hc Quc gia
TP.HCM, 2003
10. nh gi sinh vin:
- Thang im: 10
- K hoch kim tra nh sau:
Hnh
thc

Ni dung

Thi im

Cng c
KT

Chun
u ra

T
l

KT

KT

(%)

Bi tp
BT1

BT2

BT3

BT4

BT5

BT6

30

Tnh ton lng cn cn ly pha ch

ha cht

Tun 1

Bi tp nh
trn lp

G1.1, 1.3

Mc ch, nguyn tc, cch tin hnh xc

nh NaOH v H3PO4

Tun 2

Bi tp nh
trn lp

G1.1, 1.2,
1.3, 1.4,
2.1, 2.2,
2.3, 3.1

Mc ch, nguyn tc, cch tin hnh xc

nh Na2CO3, hn hp NaOH v Na2CO3

Tun3

Bi tp nh
trn lp

G1.1, 1.2,
1.3, 1.4,
2.1, 2.2,
2.3, 3.1

Mc ch, nguyn tc, cch tin hnh xc

nh KMnO4 v Fe2+

Tun 4

Bi tp nh
trn lp

G1.1, 1.2,
1.3, 1.4,
2.1, 2.2,
2.3, 3.1

Mc ch, nguyn tc, cch tin hnh xc

nh Na2S2O3 v Cu2+

Tun 5

Bi tp nh
trn lp

G1.1, 1.2,
1.3, 1.4,
2.1, 2.2,
2.3, 3.1

Mc ch, nguyn tc, cch tin hnh xc

nh Cl-, cng ca nc v Al3+

Tun 6

Bi tp nh
trn lp

G2.2, 3.1,
4.1, 4.2,
4.3

Kim tra gia k - bi tp ln

Ni dung kim tra
1. Nguyn tc xc nh cht, cch
tin hnh
2. Nguyn nhn gy sai s
3. Xc nh nng cc cht trong
mu cho
4. Phn loi phng php phn tch

10

Tun 6
G1.1, 1.2,
1.3, 1.4,
2.1, 2.2.
2.3, 3.1

Thi cui k

50

- Ni dung bao qut tt c cc chun u

ra quan trng ca mn hc.
- Thi gian lm bi 10 pht chun b/
SV

Thi vn p

G1.1, 1.2,
1.3, 3.1,
3.2, 2.1,
2.2

11. Ni dung chi tit hc phn:

Chun u
Tun
1

Ni dung
Bi 1: An ton phng th nghim
hng dn cch s dng cc dng c o
pha ch ha cht
Bi 2: Pha dd oxalic chun, xc nh nng dung dch NaOH v

ra hc
phn
G2.1, 2.2,
2.3,
3.2.

3.1,

dung dch H3PO4

A/ Ni dung v PPGD trn lp (2)
- Cc ni dung GD trn lp:
- Cc ni dung GD trn lp:
1.1. Ni quy phng th nghim
1.2. S cu trong phng th nghim
1.3. Nhng iu cn ch khi lm vic trong phng th nghim phn tch
nh lng
1.4. Cch s dng mt s dng c thy tinh
1.5. Cch lm sch cc dng c thy tinh
1.6. Thao tc pha ch ha cht
2.1. Xc nh nng dung dch NaOH
2.1.1. Mc ch, nguyn tc
2.1.2. Pha ch H2C2O4 0,1N, thc hnh xc nh nng NaOH
2.2. Xc nh nng dung dch H3PO4
2.1.1. Mc ch, nguyn tc
2.1.2. Thc hnh xc nh nng NaOH
- PPGD:
+ Thuyt trnh
+ Lm trnh din
+ Tho lun nhm
B/ Cc ni dung cn hc nh (4)
+ Lm bi tp nh GV giao v vit bo co
2

+ c thm ti liu lin quan v ngnh o to

Bi 3: Pha dung dch HCl 0,1N Xc nh nng dung dch Na 2CO3 G2.1,
v hn hp NaOH ln Na2CO3 (1/5/2)
A/ Ni dung v PPGD trn lp (6)
3.1. Xc nh nng dung dch Na2CO3
3.1.1. Mc ch, nguyn tc
3.1.2. Pha ch HCl 0,1N, thc hnh xc nh nng Na2CO3
3.2. Xc nh nng dung dch hn hp NaOH ln Na2CO3
3.1.1. Mc ch, nguyn tc
3.1.2. Thc hnh xc nh nng hn hp NaOH ln Na2CO3
- PPGD:
+ Thuyt trnh
+ Lm trnh din

2.3,
3.2.

2.2,
3.1,

+ Tho lun nhm

B/ Cc ni dung cn hc nh (4)
+ Lm bi tp nh GV giao v vit bo co
3

+ c thm ti liu lin quan v ngnh o to

Bi 4: Pha dung dch KMnO4, xc nh chun dung dch KMnO4
bng H2C2O4, xc nh hm lng Fe2+ (1/5/2)
A/ Ni dung v PPGD trn lp (6)
4.1. Xc nh nng dung dch KMnO4
4.1.1. Mc ch, nguyn tc
4.1.2. Pha ch KMnO4 0,1N, thc hnh xc nh chnh xc nng
KMnO4
4.2. Xc nh hm lng Fe2+
4.1.1. Mc ch, nguyn tc
4.1.2. Thc hnh xc nh hm lng Fe2+
- PPGD:
+ Thuyt trnh
+ Lm trnh din
+ Tho lun nhm
B/ Cc ni dung cn hc nh (4)
+ Lm bi tp nh GV giao v vit bo co

+ c thm ti liu lin quan v ngnh o to

Bi 4: Pha dung dch KMnO4, xc nh chun dung dch KMnO4 G2.1,
bng H2C2O4, xc nh hm lng Fe2+ (1/5/2)
A/ Ni dung v PPGD trn lp (2)

2.3,

2.2,
3.1,

3.2.

5.1. Xc nh nng dung dch KMnO4

5.1.1. Mc ch, nguyn tc
5.1.2. Pha ch KMnO4 0,1N, thc hnh xc nh chnh xc nng
KMnO4
5.2. Xc nh hm lng Fe2+
5.1.1. Mc ch, nguyn tc
5.1.2. Thc hnh xc nh hm lng Fe2+
- PPGD:
+ Thuyt trnh
+ Lm trnh din
+ Tho lun nhm
B/ Cc ni dung cn hc nh (4)
+ Lm bi tp nh GV giao v vit bo co
+ c thm ti liu lin quan v ngnh o to
5

Bi 5: Pha dung dch Na2S2O3, xc nh chun ca dung dch G2.1,

2.2,

Na2S2O3, xc nh Cu2+ bng phng php iod (1/5/2)

A/ Ni dung v PPGD trn lp (6)

2.3,

3.1,

3.2.

6.1. Xc nh nng dung dch Na2S2O3

6.1.1. Mc ch, nguyn tc
6.1.2. Pha ch Na2S2O3, 0,1N, thc hnh xc nh chnh xc nng
Na2S2O3
6.2. Xc nh Cu2+ bng phng php iod
6.1.1. Mc ch, nguyn tc
6.1.2. Thc hnh xc nh Cu2+
- PPGD:
+ Thuyt trnh
+ Lm trnh din
+ Tho lun nhm
B/ Cc ni dung cn hc nh (4)
+ Lm bi tp nh GV giao v vit bo co
+ c thm ti liu lin quan v ngnh o to

bi 6: Pha dung dch NaCl, xc nh Cl - bng phng php kt ta. G2.1,

2.2,

Bi 7: Xc nh cng ca nc v Al 3+ bng phng php 2.3,

3.1,

complexon (1/5/2)
A/ Ni dung v PPGD trn lp (6)

4.1,

7.1. Phng php mohr xc nh Cl7.1.1. Nguyn tc

7.1.2. Pha ch NaCl, 0,1N, thc hnh xc nh chnh xc nng Cl7.2. Phng php ch th hp ph xc nh Cl7.2.1. Nguyn tc
7.2.2. Thc hnh xc nh chnh xc nng Cl7.3. Xc nh cng ca nc
7.3.1. Nguyn tc
7.3.2. Thc hnh xc nh cng ca nc
7.4. Xc nh Al3+
7.3.1. Nguyn tc
7.3.2. Thc hnh xc nh Al3+
- PPGD:
+ Thuyt trnh
+ Lm trnh din
+ Tho lun nhm
B/ Cc ni dung cn hc nh (4)

3.2,
4.2, 4.3.

+ Lm bi tp nh GV giao v vit bo co
+ c thm ti liu lin quan v ngnh o to

12. o c khoa hc:

+ Cc bi bo co nu b pht hin l sao chp ca nhau s b tr 100% im qu trnh,
nu mc nghim trng s b cm thi cui k c ngi s dng bi chp v ngi cho chp bi.
+ Sinh vin khng hon thnh nhim v th b cm thi.
+ Sinh vin thi h th c 2 ngi thi h v nh thi h s b nh ch hc tp hoc b ui
hc.
+ Trung thc vi s liu thc hnh
13. Ngy ph duyt ln u tin:
14. Cp ph duyt:
Trng khoa

Trng B MN

Ngi bin son

Ths. H Th Yu Ly
Ths. Phan Th Anh o
Cp nht ln 1

Ngi cp nht

Trng b mn

Cp nht ln 2

Ngi cp nht

Trng b mn