Ting. 4 - Bab 8 (2) - Slide

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Step 2:

[Solution] Describe a detailed procedure involved in the preparation of salt based on the
experimental plan in Step 1

Langkah 2:

[Penyelesaian] Menghuraikan prosedur penyediaan garam secara terperinci berdasarkan pada rancangan eksperimen dalam Langkah 1

A) Preparation of zinc carbonate salt


Penyediaan garam zink karbonat
Zinc nitrate solution
Larutan zink nitrat

Sodium
solution
Larutan
karbonat

Zinc
carbonate
precipitate
Mendakan
zink
karbonat

Retort stand
Kaki retort
Zinc
carbonate
precipitate
Mendakan
zink
karbonat

Zinc
carbonate
precipitate
Mendakan
zink
karbonat

carbonate
natrium

50cm3 of 1.0 mol dm-3 zinc nitrate solution is


poured into a beaker containing 50cm3 of 1.0
mol dm-3 sodium carbonate. The mixture is
stirred with a glass rod.
50cm3 larutan zink nitrat 1.0 mol dm-3 dituang
ke dalam bikar yang mengandungi 50cm3
larutan natrium karbonat 1.0 mol dm-3.
Campuran dikacau dengan rod kaca.

Zinc
carbonate
precipitate is formed
Mendakan
zink
karbonat terhasil

The mixture is filtered


Campuran dituras

The precipitate formed is


rinsed with distilled water
Mendakan
terbentuk
dibilas dengan air suling

B) Preparation of zinc sulphate salt


Penyediaan garam zink sulfat
Zinc carbonate precipitate
Mendakan zink karbonat

Excess zinc carbonate powder


Serbuk zink karbonat berlebihan
Zinc sulphate solution
Larutan zink sulfat

Dilute
sulphuric
acid
Asid sulfurik cair
Zinc sulphate solution
Larutan zink sulfat

50cm3 of 1.0 mol dm-3 sulphuric acid is heated slowly. The


residue/precipitate is added a little at a time until excess into the
sulphuric acid solution. The mixture is stirred with glass rod.
50cm3 asid sulfurik cair 1.0 mol dm-3 dipanaskan dengan
perlahan-lahan. Baki turasan/mendakan ditambah sedikit demi
sedikit sehingga berlebihan ke dalam asid sulfurik cair. Campuran
dikacau dengan rod kaca.

Zinc sulphate crystals


Hablur zink sulfat
Zinc sulphate crystals
Hablur zink sulfat

The crystals are dried by


pressing them between
the sheets of filter paper
Hablur garam dikeringkan
dengan menekannya di
antara helaian kertas
turas

The crystals are rinsed with


cold distilled water
Hablur garam dibilas dengan
air suling yang sejuk

The mixture is filtered to remove excess zinc


carbonate powder
Campuran dituras bagi menyingkirkan serbuk
zink karbonat berlebihan

Zinc
sulphate
crystals
Hablur zink sulfat

The crystals formed are filtered


Hablur garam yang terbentuk
dituras

The filtrate
is heated until
saturated
Hasil
turasan
dipanaskan
sehingga tepu

Saturated zinc sulphate solution


Larutan tepu zink sulfat

The saturated solution is allowed to


cool to room temperature until
crystals are formed
Larutan
tepu
yang
terhasil
disejukkan kepada suhu bilik
sehingga hablur garam terbentuk

Chemical equations/Persamaan kimia:


a) Preparation of zinc carbonate salt/Penyediaan garam zink karbonat:
Zn(NO3)2 (aq/ak) + Na2CO3 (aq/ak) ZnCO3 (s/p) + 2NaNO3 (aq/ak)
b) Preparation of zinc sulphate salt/Penyediaan garam zink sulfat:
ZnCO3 (s/p) + H2SO4 (aq/ak) ZnSO4 (aq/ak) + CO2 (g/g) + H2O (l/ce)

Diagram 8.4

Diagrammatic procedures of the preparation of zinc sulphate salt

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