MTB > RSRegress 'Yield' = C5 C6 C7 C5*C5 C6*C6 C7*C7 C5*C6 C5*C7 C6*C7;

SUBC>
Order C8;
SUBC>
InUnit 1 0;
SUBC>
Levels -1,68179283050743 1,68179283050743 -1,68179283050743
1,68179283050743 &
CONT> -1,68179283050743 1,68179283050743;
SUBC>
Brief 2.

Response Surface Regression: Yield versus A; B; C

The analysis was done using coded units.
Estimated Regression Coefficients for Yield
Term
Constant
A
B
C
A*A
B*B
C*C
A*B
A*C
B*C

Coef
100,666
2,138
2,289
-2,513
-10,656
-35,156
-27,156
8,132
-7,425
-13,081

S = 13,6417
R-Sq = 66,31%

SE Coef
5,564
6,208
6,208
6,208
10,164
10,164
10,164
13,642
13,642
13,642

T
18,093
0,344
0,369
-0,405
-1,048
-3,459
-2,672
0,596
-0,544
-0,959

PRESS = 8855,23
R-Sq(pred) = 0,00%

P
0,000
0,738
0,720
0,694
0,319
0,006
0,023
0,564
0,598
0,360

R-Sq(adj) = 35,98%

Analysis of Variance for Yield

Source
Regression
Linear
A
B
C
Square
A*A
B*B
C*C
Interaction
A*B
A*C
B*C
Residual Error
Lack-of-Fit
Pure Error
Total

DF
9
3
1
1
1
3
1
1
1
3
1
1
1
10
5
5
19

Seq SS
3662,00
77,89
22,08
25,31
30,50
3291,74
46,37
1916,92
1328,46
292,37
66,12
55,12
171,12
1860,95
1001,61
859,33
5522,95

Adj SS
3662,00
77,89
22,08
25,31
30,50
3291,74
204,55
2226,45
1328,46
292,37
66,12
55,12
171,12
1860,95
1001,61
859,33

Adj MS
406,89
25,96
22,08
25,31
30,50
1097,25
204,55
2226,45
1328,46
97,46
66,12
55,12
171,12
186,09
200,32
171,87

F
2,19
0,14
0,12
0,14
0,16
5,90
1,10
11,96
7,14
0,52
0,36
0,30
0,92

P
0,119
0,934
0,738
0,720
0,694
0,014
0,319
0,006
0,023
0,676
0,564
0,598
0,360

1,17

0,435

Estimated Regression Coefficients for Yield using data in uncoded units

Term
Constant
A
B
C

Coef
100,666
1,27146
1,36130
-1,49445

A*A
B*B
C*C
A*B
A*C
B*C

-3,76749
-12,4296
-9,60113
2,87500
-2,62500
-4,62500

Surface Plots of Yield

Hold Values
A 0
B 0
C 0
100
Yield

100

80

Yield

60

40

-2
A

-2

80
60

40
0
-2
B

-2

50

-2
A

100
Yield

75

-2

Contour Plots of Yield

B*A

C*A

-1

-1

-1

-1

Yield_2
< 40
40
60
60
80
80 100
> 100

C*B
1

-1

-1

MTB > RSRegress 'Filtration Time' = C5 C6 C5*C5 C6*C6 C5*C6;

SUBC>
Order C7;
SUBC>
InUnit 1 0;
SUBC>
Levels -1,4142135623731 1,4142135623731 -1,4142135623731
1,4142135623731;
SUBC>
Brief 2.

Response Surface Regression: Filtration Time versus A; B

The analysis was done using coded units.
Estimated Regression Coefficients for Filtration Time
Term
Constant
A
B
A*A
B*B
A*B

Coef
41,200
-2,786
2,061
7,425
4,925
12,000

S = 4,69655
R-Sq = 67,15%

SE Coef
2,100
2,348
2,348
3,561
3,561
4,697

T
19,616
-1,186
0,878
2,085
1,383
2,555

PRESS = 1015,86
R-Sq(pred) = 0,00%

P
0,000
0,274
0,409
0,076
0,209
0,038

R-Sq(adj) = 43,68%

Analysis of Variance for Filtration Time

Source
Regression
Linear
A

DF
5
2
1

Seq SS
315,60
48,02
31,04

Adj SS
315,60
48,02
31,04

Adj MS
63,119
24,011
31,037

F
2,86
1,09
1,41

P
0,102
0,388
0,274

Hold Values
A 0
B 0
C 0

B
Square
A*A
B*B
Interaction
A*B
Residual Error
Lack-of-Fit
Pure Error
Total

1
2
1
1
1
1
7
3
4
12

16,99
123,58
81,39
42,18
144,00
144,00
154,40
139,60
14,80
470,00

16,99
123,58
95,88
42,18
144,00
144,00
154,40
139,60
14,80

16,985
61,788
95,879
42,184
144,000
144,000
22,058
46,534
3,700

0,77
2,80
4,35
1,91
6,53
6,53

0,409
0,128
0,076
0,209
0,038
0,038

12,58

0,017

Unusual Observations for Filtration Time

Obs
3
9
13

StdOrder
3
9
13

Filtration
Time
53,000
32,000
47,000

Fit
45,839
37,948
52,862

SE Fit
3,713
3,713
3,713

Residual
7,161
-5,948
-5,862

St Resid
2,49 R
-2,07 R
-2,04 R

R denotes an observation with a large standardized residual.

Estimated Regression Coefficients for Filtration Time using data in uncoded
units
Term
Constant
A
B
A*A
B*B
A*B

Coef
41,2000
-1,96967
1,45711
3,71250
2,46250
6,00000

Contour Plot of Filtration Time vs B; A

Filtration
Time
< 40
40 45
45 50
50 55
55 60
60 65
> 65

1,0

0,5

0,0

-0,5

-1,0

-1,0

-0,5

0,0
A

0,5

1,0

Surface Plot of Filtration Time vs B; A

70
60
Filtration Time
50
1

40
0
-1

0
A

-1
1