novAA 350

Operator:

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28/06/2016 12:38
Laboratory:
SAA

SAA

Method Parameters Technique: Flame

Name:
Created:
Comment:

(Method is not saved)

28/12/1800 0:00

Version:
Operator:

Lines
Line

Elem. Wavel.
[nm]
Cu
324.8

Cu324

Optic. mode Lamp

Current
[mA]
2

Single-beam HCL

Boost
[mA]
-

Slit [nm]
1.4

Meas time. PMT [V]

[s]
3.0
300

Evaluation/Background correction
Line
Cu324

Background
no background

Int.mode AZDK
Mean
off

Smooth
on

D2 cur. [mA] HC/BC rat.

-

Flame Parameters
Type:
Burner type:
Line

C2H2/air
50 mm
C2H2/air
[L/h]
50

Cu324

Ox. control:
Burner angle:

off
0 deg

Nebulizer rate:

0 mL/min

Burner height
[mm]
6

Sample Transport
Autosampler:
Dilution if conc.
exceeded:
Injection switch:
Wash:

Yes
none

Delay time:

10 s

No
after sample

Wash time:

15 s

std. cal.

Std. prep.:

manual

Mixing cup cycles: 1

Calibration
Method:

Calibration Curve Parameters

Line
Calib.func.. Intercept
Cu324
linear
calculate
Calibration table

Weighting
none

No.

Type

Pos

Rec

1
2
3
4
5

Cal-Zero
Cal-Std
Cal-Std
Cal-Std
Cal-Std

1
2
3
4
5

Check
none

Unit
mg/L

Cu
[mg/L]
0
5
10
15
20

Statistics Parameters
Statistics:
Repl./sample:
ASpect LS 1.3.2.0

Mean stat.
3

CI calc.:
absolute
Repl./calib.sample:
3

Confidence level:
Repl./QC:

95.4%
3
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novAA 350
Operator:

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28/06/2016 12:38
Laboratory:
SAA

SAA

Pre-runs:

Grubbs test:

off

QCS Parameters
No entries exist

QCC Parameters
RSD/RR% check:

ASpect LS 1.3.2.0

Calib. check:

Recal. check:

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novAA 350
Operator:

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28/06/2016 12:38
Laboratory:
SAA

SAA

Results
Results file:
Instrument:

C:\Use...\BC-021-SAA-16-0054-5-dx200.tps
novAA 350
Technique:
#AA101217199

Comment:
Line
Autozero

Mean
default(1)

Cu324
Cal-Zero1

default(1)

Cu324
Conc.1
Abs

0
0.00022

SD

RSD[%]

Flame

CI

Unit
Date:
Date:

Rem.
28/06/2016 12:28
28/06/2016 12:28

mg/L
0.00016

70.6

Single values (Abs.): #1: 0.00024 #2: 0.00038 #3: 0.00006 (SEV: 204V)
Cal-Zero1 Cu324
0.004
Abs.

0.003
0.002
0.001
0.000
0

Time [s]

Cal-Std1

default(1)

Cu324
Conc.1
Abs

5
0.06136

Date:

28/06/2016 12:29

mg/L
0.00040

0.7

Single values (Abs.): #1: 0.06166 #2: 0.06151 #3: 0.06090 (SEV: 204V)
Cal-Std1 Cu324

Abs.

0.06
0.04
0.02
0.00
0

Time [s]

Cal-Std2

default(1)

Cu324
Conc.1
Abs

10
0.12885

Date:

28/06/2016 12:30

mg/L
0.00033

0.3

Abs.

Single values (Abs.): #1: 0.12901 #2: 0.12907 #3: 0.12848 (SEV: 204V)
0.150
0.125
0.100
0.075
0.050
0.025
0.000
0

Cal-Std2 Cu324

Time [s]

Cal-Std3

default(1)

Cu324
Conc.1
Abs

15
0.19894

Date:

28/06/2016 12:31

mg/L
0.00124

0.6

Single values (Abs.): #1: 0.20025 #2: 0.19778 #3: 0.19879 (SEV: 204V)
Cal-Std3 Cu324
0.20
Abs.

0.15
0.10
0.05
0.00
0

Time [s]

ASpect LS 1.3.2.0

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novAA 350
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28/06/2016 12:38
Laboratory:
SAA

SAA

Line
Cal-Std4

Mean
default(1)

Cu324
Conc.1
Abs

20
0.27218

SD

RSD[%]

CI

Unit
Date:

Rem.
28/06/2016 12:32

mg/L
0.00151

0.6

Abs.

Single values (Abs.): #1: 0.27382 #2: 0.27190 #3: 0.27083 (SEV: 204V)
0.30
0.25
0.20
0.15
0.10
0.05
0.00
0

Cal-Std4 Cu324

Time [s]

Compute calib.

Cu324

Date:

28/06/2016 12:32

Cu324
R(adj.): 0.997734888 Slope: 0.01363 Abs./mg/L Char.conc.: 0.31988 mg/L/1%A
Method SD: 0.30739 y=a+bx
a=-.0039889 b=0.0136299
mg/L
Cu324
4
0.25

Abs.

0.20

0.15
2
0.10
1

0.05
0.00

Z
0

10
Conc. [mg/L]

15

20

Autozero

default(1)

Date:

28/06/2016 12:33

Cu324
H 13 D20X

default(1)

Date:

28/06/2016 12:33

Pre-DF: 1
Cu324
Conc.1
Conc.2
Abs

Wt.[g]:
13.63
13.63
0.18179

Vol.[mL]: 100
0.1648
0.1648
0.00225

AS-DF: 1.0

1.2
1.2
1.2

0.6803
0.6803

Blank corr.:

off

mg/L
mg/L

Single values (Abs.): #1: 0.18425 #2: 0.17985 #3: 0.18127 (SEV: 204V)
0.20

H 13 D20X Cu324

Abs.

0.15
0.10
0.05
0.00
0

Time [s]

ASpect LS 1.3.2.0

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Laboratory:
SAA

SAA

Line
H 14 D20X

Mean
default(1)

Pre-DF: 1
Cu324
Conc.1
Conc.2
Abs

Wt.[g]:
13.96
13.96
0.18629

SD

RSD[%]
Vol.[mL]: 100

0.0359
0.0359
0.00049

CI
AS-DF: 1.0

0.3
0.3
0.3

0.6878
0.6878

Unit
Date:

Rem.

Blank corr.:

28/06/2016 12:34
off

mg/L
mg/L

Single values (Abs.): #1: 0.18575 #2: 0.18644 #3: 0.18670 (SEV: 204V)
H 14 D20X Cu324

0.20

Abs.

0.15
0.10
0.05
0.00
0

Time [s]

H 15 D20X

default(1)

Pre-DF: 1
Cu324
Conc.1
Conc.2
Abs

Wt.[g]:
0.6844
0.6844
0.00534

Date:
Vol.[mL]: 100
0.0064
0.0064
0.00009

AS-DF: 1.0

0.9
0.9
1.6

0.8739
0.8739

Blank corr.:

28/06/2016 12:35
off

mg/L
mg/L

Single values (Abs.): #1: 0.00544 #2: 0.00527 #3: 0.00531 (SEV: 204V)
0.006

H 15 D20X Cu324

Abs.

0.004
0.002
0.000
0

Time [s]

H 16 D20X

default(1)

Pre-DF: 1
Cu324
Conc.1
Conc.2
Abs

Wt.[g]:
10.14
10.14
0.13424

Date:
Vol.[mL]: 100
0.0062
0.0062
0.00008

AS-DF: 1.0

0.1
0.1
0.1

0.6395
0.6395

Blank corr.:

28/06/2016 12:36
off

mg/L
mg/L

Abs.

Single values (Abs.): #1: 0.13434 #2: 0.13419 #3: 0.13420 (SEV: 204V)
0.150
0.125
0.100
0.075
0.050
0.025
0.000
0

H 16 D20X Cu324

Time [s]

ASpect LS 1.3.2.0

Analytik Jena

novAA 350
Operator:

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28/06/2016 12:38
Laboratory:
SAA

SAA

Line
H 17 D20X

Mean
default(1)

Pre-DF: 1
Cu324
Conc.1
Conc.2
Abs

Wt.[g]:
11.36
11.36
0.15084

SD

RSD[%]
Vol.[mL]: 100

0.0452
0.0452
0.00062

CI
AS-DF: 1.0

0.4
0.4
0.4

0.6453
0.6453

Unit
Date:

Rem.

Blank corr.:

28/06/2016 12:37
off

mg/L
mg/L

Abs.

Single values (Abs.): #1: 0.15016 #2: 0.15098 #3: 0.15137 (SEV: 204V)
0.175
0.150
0.125
0.100
0.075
0.050
0.025
0.000
0

H 17 D20X Cu324

Time [s]

ASpect LS 1.3.2.0

Analytik Jena