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Varian GC 450 Pre Installation Requirements English PDF
Varian GC 450 Pre Installation Requirements English PDF
Herculesweg 8
4330 EA Middelburg
The Netherlands
450-GC
Pre-Installation Requirements
The information provided here will help you prepare a suitable installation site for
your 450-GC.
The Varian 450-GC has been designed to operate reliably under carefully controlled
environmental conditions. It is your responsibility to provide a suitable location, power source,
and operating environment. Operating or maintaining a system in operational conditions outside
of the power and operating environment limits described below could cause failures of many
types. The repair of such failures is specifically excluded from the Warranty and Service contract
conditions.
All phases of the installation site preparation must conform to local safety,
electrical, and building codes. These codes take precedence over any
recommendations in these instructions, and compliance to them is the
responsibility of the customer.
Table of Contents
COMPLETE THE CHECKLIST ........................................................................................................................ 3
POWER REQUIREMENTS............................................................................................................................... 4
ENVIRONMENTAL REQUIREMENTS............................................................................................................. 6
TEMPERATURE/HUMIDITY ................................................................................................................................. 6
PARTICULATE MATTER ..................................................................................................................................... 6
VIBRATION ....................................................................................................................................................... 6
EXHAUST SYSTEM ............................................................................................................................................ 6
GAS REQUIREMENTS..................................................................................................................................... 7
FUEL AND CARRIER GASES............................................................................................................................... 7
RECOMMENDED GAS CLEAN FILTERS................................................................................................................. 8
PROPER HANDLING OF GAS CYLINDERS .......................................................................................................... 10
REGULATOR INSTALLATION ............................................................................................................................. 10
GAS CONNECTIONS ........................................................................................................................................ 10
GAS LINES ..................................................................................................................................................... 11
GAS FILTERS ................................................................................................................................................. 11
NETWORK REQUIREMENTS........................................................................................................................ 12
INSPECTION................................................................................................................................................... 13
UNPACKING AND INSTALLATION .............................................................................................................. 14
SPARE PARTS............................................................................................................................................... 14
PREVENTIVE MAINTENANCE ...................................................................................................................... 14
Tables
Table 1 Physical Dimensions of the 450-GC System Components.................................................................. 4
Table 2 Instrument Gas Requirements ............................................................................................................ 7
Table 3 Operating Gases .................................................................................................................................. 9
Table 4 Gas Line Fittings ................................................................................................................................ 10
Table 5 Stainless Steel and Copper Tubing ................................................................................................... 11
Table 6 Tubing Closures ................................................................................................................................. 11
Varian, Inc.
Page 2 of 14
The shipping cartons were examined for damage and if damaged, the conditions were
reported
If Varian is performing the installation, the system operator is available during the
installation
Requirements
Principal installation area is in compliance with all relevant safety regulations
Entrance to the lab is at least 91.5 cm (36 in.) wide
Sufficient bench space is available for all components
Bench can support system weight
Specified electrical supply and power outlets installed
Lab temperature maintained between10 and 40 C (50 and 104 F)
Relative humidity maintained between 5 and 95% RH
Laboratory is free of excessive particulate matter
System bench is free from vibrations
Exhaust system is suitable
Carrier gas, regulator, and gas lines are installed.
Detector gas, regulator, and gas lines are installed.
Appropriate gas filters are on site
If the GC will be connected to the company network, the required materials are on site
Varian, Inc.
Page 3 of 14
Height
Width
Depth
Weight
Instrument
in.
cm
in.
cm
in.
cm
lb.
kg
450-GC
21
53
26
66
22
56
90
41
16
41
23
18
46
20
32
83
37
97
15
39
24
10
Quma QHSS-40
16
40
12
29.5
23
60
58
26
Chromatography Workstation
(computer with monitor, approximate values)
17
43
17
43
21
53
35
16
Power Requirements
A separate circuit is required for each 450-GC. The mating socket must have adequate
amperage capacity and a reliable ground.
Note: 120V and 101V GCs are designed for single phase operation only.
A measured GROUND to NEUTRAL potential of greater than 3 volts ac or dc indicates
grounding problems that may need correction before connecting an instrument to the power
source. Any power source suspected of having noise problems should be evaluated with a
recording type power line monitor prior to being used for operating instruments.
Each 450-GC requires a clean 50 or 60 Hz power source capable of providing up to:
101 Vac 10%, 50 or 60 Hz 2%, 25 Amps, 2.5 Kilowatts
120 Vac 10%, 60 Hz 2%, 20 Amps, 2.4 Kilowatts
230 Vac 10%, 50 Hz 2%, 10 Amps, 2.3 Kilowatts
Installation Category: II (per Standard IEC664)
Power supply interruptions/Dips conform to EN61000-4-11: 1994
Voltage drop of 40% maximum, in a timeframe of 20 msec is allowed.
If your local area is subject to power fluctuations or power interruptions, a
power conditioning device or an uninterruptible power supply (UPS) must be
installed.
Varian, Inc.
Page 4 of 14
In 230V, 50 Hz countries, the 450-GC is supplied with a standard molded power cord with an
IEC60320 Hot connector. This connector plugs into the receptacle on the rear of the GC as
shown in Figure 1. This power cord can be replaced to suit local power requirements.
Receptacle located on rear of GC.
10 Amp, 230 Vac Nominal, 50 Hz
Line 2
(blue)
Line 1
(brown)
Ground (green/yellow)
Line 2
(blue)
Line 1 (brown)
Ground
(green/yellow)
Power cords for North America and other 120V, 60 Hz applications are terminated in a 3-prong
plug that requires a matching 120 Vac receptacle as shown in Figure 2. Power cords for 101V, 60
Hz countries require the receptacle shown in Figure 3. Replacement or substitution of the power
plug requires strict compliance with power cord color coding as shown in Figures 2 and 3.
CAUTION
This instrument is designed for
single phase operation ONLY.
Line
Neutral
Neutral
(light blue or white)
Hot (brown or black)
Ground
Neutral
Line
CAUTION
This instrument is designed for
single phase operation ONLY.
Ground
Operation of a 450-GC near the low limit of the permissible line voltage will increase the time
required for thermal zones to reach their final setpoint temperature, and may adversely reduce
the maximum usable ramp rate for programmable thermal zones.
Care must be taken to ensure that sources of radio frequency interference (RFI) and
electromagnetic interference (EMI) are not placed on the same power line, or share the same
ground plane, since this can degrade the performance of the GC. Equipment such as motors,
solenoids, fluorescent light fixtures, and radio communication transmitters should be isolated
from the instrument and connecting cables as much as possible.
Varian, Inc.
Page 5 of 14
Environmental Requirements
You are responsible for providing an acceptable operating environment. Attention paid to the
operating environment will ensure the continued peak performance of your 450-GC.
The 450-GC is intended for indoor use and certified for operation up to an altitude of 2000 meter.
Protect your GC from corrosive chemicals or gases and from direct venting of air conditioners,
heaters, furnaces or fans.
Calculate heat dissipation using the following formula:
Watts x 3.4129 = BTU/hr
Actual dissipation will depend on method parameters and instrument configuration.
Pollution Degree: 2 (per Standard IEC664)
Temperature/Humidity
The optimal operating temperature range for the GC is between 10 to 40 C (50 and 104 F).
The acceptable storage temperature is between -20 to 65 C (-4 and 149 F).
Hot air vented from the GC column oven may contribute to room heating and to the resulting air
conditioning load. Ducting the GC column oven air out of the lab should reduce this heating
effect.
The relative humidity (RH) of the operating environment must be between 5 - 95 %, with no
condensation. Operating the GC at very low humidity will result in the accumulation and
discharge of static electricity which shortens the life of electronic components. Operating the
system at high humidity will produce condensation and result in short circuits.
Varian recommends that your laboratory be equipped with a temperature/humidity monitor. This
will ensure that your laboratory is always in conformance with temperature and humidity
specifications.
Particulate Matter
Take necessary precautions to minimize particulates in the laboratory environment. A layer of
dust on the electronic components could act as an insulating blanket, and reduce heat transfer to
the surrounding air.
Vibration
Ensure that lab benches are free from vibrations, e.g., those caused by equipment in adjoining
locations.
Exhaust System
It is your responsibility to provide an adequate exhaust system. Consult local regulations for the
proper method of exhausting the fumes from your system.
Varian, Inc.
Page 6 of 14
Do not exceed MAXIMUM inlet pressures listed on the rear panel of the instrument.
Gas Requirements
Fuel and Carrier Gases
Table 2 lists the gases commonly used with GC detectors. Table 3 lists gases that may be
required for other GC purposes. Refer to Table 4 for regulator and gas line fittings.
Table 2 Instrument Gas Requirements
Detector
TCD
FID
Gas
Purity
99.999
H2
99.999
He, N2, Ar
H2
99.999
Air
0 grade
He, N2
99.999
H2
99.999
He, N2, Ar
99.999
H2
99.999
Air
0 grade
He, N2
99.999
He, N2, Ar
99.999
H2
99.999
Air
0 grade
Detector Gas:
ECD
Detector Gas:
Makeup Gas:
PFPD
Maximum *
Gas Inlet Pressure
Makeup Gas:
TSD
Typical
Gas Inlet Pressure
Injector
Carrier Gas Type
Detector Gas:
Makeup Gas:
N/A
* High pressure applications requires inlet pressure between 80-160 psig / 5.5 10 Bar
He, N2, Ar can ONLY be used as carriergas
Obtain gases for chromatographic use from a supplier who is aware of your
requirements. An analysis of selected impurities is used to determine the purity
rating for a given gas. If your supplier does not establish purity based on an
analysis of appropriate chromatographic contaminants, a purity rating of
99.999% may not be suitable for GC use. A quality supplier of gas and the
regular use of filters will minimize system contamination problems.
Varian, Inc.
Page 7 of 14
Detector
Carrier Gas
Moisture Filter
Oxygen Filter
Column
TCD
Makeup Gas: He, N2, Ar
Reference
Channel
H2
TCD
Detector
Carrier Gas
Moisture Filter
Oxygen Filter
Column
FID
Detector Gas: H2
Air
Hydrogen
Make-Up
Gas
Charcoal Filter
FID
Air
Charcoal Filter
Detector
Carrier Gas
Moisture Filter
Make-Up Gas
Charcoal Filter
Oxygen Filter
Column
FID
Detector Gas: H2
Air
Makeup Gas: He, N2
Hydrogen
Charcoal Filter
FID
Air
Charcoal Filter
Carrier Gas
Moisture Filter
Oxygen Filter
Nitrogen
Moisture Filter
Oxygen Filter
Detector
Column
ECD
Detector Gas: N2 , Ar/CH4
Make-Up
Gas
Purge Gas
ECD
Varian, Inc.
Page 8 of 14
Detector
Carrier Gas
TSD
Moisture Filter
Oxygen Filter
Column
Detector Gas: H2
Make-Up
Gas
Air
Hydrogen
Charcoal Filter
TSD
Charcoal Filter
Carrier Gas
Moisture Filter
Make-Up Gas
Charcoal Filter
Detector
TSD
Detector Gas: H2
Oxygen Filter
Column
Air
Hydrogen
Charcoal Filter
TSD
Charcoal Filter
Carrier Gas
Moisture Filter
Hydrogen
Charcoal Filter
Detector
Oxygen Filter
Column
PFPD
Detector Gas: H2
Flame
Air
Makeup Gas: N/A
PFPD
Air
Charcoal Filter
Flame 2
Purpose
Recommended Gas
Inlet Pressure
Valve Actuators
Air
60 psig
4.1 bar
Subambient (LCO2*)
LCO2*
850-1000 psig
58.5 68.8 bar
Subambient LN2
LN2
20-50 psig
1.4 3.4 bar
Varian, Inc.
Page 9 of 14
Never move a cylinder with a regulator installed. Make sure safety cap is in place over valve
when transporting cylinder.
Always use cylinder condition labels to show whether tank is FULL, IN USE, or EMPTY.
Always leave at least 100 psig (6.9 bar) residual gas in a depleted cylinder. Always store in
empty tank storage area with tank valve closed. Empty cylinders should be clearly marked as
such and dated.
Regulator Installation
Carrier gases must have a two-stage regulator having a 0 to 100 psig (6.9 bar) low-pressure
stage.
The inlet pressure for He is normally 80 psig (5.5 bar).
Pressure inlet must be 30 psig (2 Bar) higher then the Column Head Pressure.
Gas Connections
All instrument gases connect to 1/8-inch Swagelok fittings on the rear of the instrument. (The
exception is liquid nitrogen, which requires 1/4-inch fittings.) All fittings are labeled for specific
gases with provision for auxiliaries and cryogenic coolant supplies.
Table 4 lists the part numbers of hardware that may be required to connect gases to the
instrument.
Table 4 Gas Line Fittings
Description
Part Number
Pressure Regulator
57-000180-00
Specify connector:
CGA 350 Connector (H2 or Ar/CH4)
16-000207-00
16-000197-00
16-000196-00
28-207304-00
28-202012-00
28-694205-00
28-694027-01
28-694028-01
1/8" nut
28-694029-00
03-918326-00
88-189610-00
*For use on pipe fittings ONLY. Never use Teflon tape on Swagelok fittings.
A 1/8-inch line with brass fittings (such as Copper Carrier Gas Kit, P/N 02-000034-00) is required
to connect the carrier gas supply cylinder to the instrument bulkhead fitting. However, additional
tubing may be required to connect the GC to the required gas supplies.
Varian, Inc.
Page 10 of 14
Gas Lines
Table 5 Stainless Steel and Copper Tubing
Stainless Steel
Copper
OD, in.
ID, in.
Length, ft (m)
Part Number
1/16
0.046
10 (3)
37-000241-02
1/16
0.046
50 (15)
37-000241-01
1/8
0.093
50 (15)
37-000119-01
1/8
0.065
25 (7.6)
03-918326-00
1/4
0.190
50 (15)
37-000146-00*
Note: Fully annealed and specially heat-cleaned copper tubing is recommended for ease of
plumbing. This tubing will usually appear discolored due to the heat-cleaning process.
*Not heat cleaned
Use these plastic closures to keep metal tubing interiors clean during storage.
Table 6 Tubing Closures
Part Number
1/16
28-996023-00
1/8
28-995806-00
1/4
28-995808-00
Gas Filters
Carrier gas filters should be installed to further clean high purity gases, reduce detector noise,
and protect the chromatography system from potential contamination. Carrier gas filters should
be installed where the indicator is visible. The following filters are recommended for GC systems
(see Table 2 for filter kit part numbers):
Table 7 Gas Filters / Filter Bases
Filter
Description
Removes water vapor from carrier gas
Installed between gas tank and GC inlet
Molecular sieve
Filter should be changed when indicator shows filter is
spent
Removes oxygen from carrier gas
Installed between moisture filter and GC inlet
Recommended with capillary columns
Required for ECD
Filter should be changed when indicator shows filter is
spent
Removes organic contaminants from detector gas
Installed between gas tank and GC inlet
Activated charcoal
Filter should be changed at the same time as other
filters
Snap-on cartridge design
No flushing of gas lines required
Pre-Installation Requirements 450-GC
Part Number
CP17971
CP17970
CP17972
CP7988
Page 11 of 14
CP738407
CP736520
IMPORTANT NOTE: Filters are used to remove small amounts of contaminants from high purity
gases. They are not capable of removing all of the contaminants from low purity gases. The
purity specifications listed in Table 2 are minimum acceptable values.
Description
392594491
Filter Kit He/N2 for carrier gas (moisture and oxygen filter, duoplate, 1 m copper tubing)
392594492
Filter Kit H2/Air for supply gas (charcoal filter, baseplate, 1 m copper tubing)
CP17974
CP17975
CP17976
Varian Gas Clean GC/MS filter kit (incl. 1 connecting unit 1/8 and 2 GC/MS filters)
CP17977
Varian Gas Clean GC/MS filter kit (incl. 1 connecting unit 1/4 and 2 GC/MS filters)
Varian Gas Clean GC/MS filter installation kit (incl. CP17976 1 mtr copper tubing, 2 nuts and 2 ferrules
1/8)
Filter Kit for Service Engineers (incl. 1 Moisture, 1 Oxygen, 2-Base Unit 1/8", Leaflets Filters general and
GC/MS-Filter)
CP17978
CP28204
CP736530
Varian Gas Clean filter kit (connecting unit for 4 filters, incl. 4 filters (1/8 tube))
CP738408
CP7995
Varian Gas Clean filter kit (connecting unit for 4 filters, incl. 4 filters (1/4 tube))
Network Requirements
To connect your 450-GC to a company network, you will need to provide a RJ45 connection to
the back panel of the 450-GC. In addition, the company network must allow TCP/IP
communications to be routed across it from the 450-GC to the Workstation.
The PC network card must be a type 100 MB or higher and needs to be configured like this.
The use of 100 MB/s switches or higher is mandatory to connect the 450-GC to the customer
network, use of hubs is prohibited.
In case a 450-GC and a CP-3800 need to be installed on a customer network, connect Galaxie
and the 450-GC(s) direct to the 100 MB/s switch. The coaxial hub, where the 3800 is connected
to, can be connected with a RJ-45 cabel to the Switch.
Any hardware, adapters, cables, configuration and setup work required to convert from the
company network wiring type to RJ45 wiring will need to be provided by you or your network
administrator.
Varian, Inc.
Page 12 of 14
Inspection
When your 450-GC arrives, carefully inspect the exterior of the shipping cartons for evidence of
any damage that might have occurred during shipment. Inspect the cartons for the following:
Water stains
Cuts, punctures, or deep indentations
Crushed corners or excessively abraded edges
If one or more of the above conditions are evident on any of the shipping cartons, report the
conditions to the carrier at time of receipt.
Systems are shipped either FOB Varian or FOB Destination. The manner of shipment
determines who has responsibility for filing a claim against the carrier if the system is damaged in
transit. Most systems are shipped FOB Varian, and in this instance any damages incurred in
shipment are the responsibility of the purchaser and the carrier. Contact Varian Service for
assistance with claims filing and billing for repairs if necessary. If the system is shipped FOB
Destination, contact Varian Order Processing who will file a claim against the carrier. Note,
however, that Varian will not accept liability for damage if you receive obviously damaged
materials but do not make note of the damage on the receiving documents.
If none of the conditions listed above are evident after inspecting the shipping carton, place the
shipping container on the floor near the installation site. Before proceeding, you should make
sure that the site to be used for installation has the required power and meets the space
requirements described in these instructions.
Varian, Inc.
Page 13 of 14
Spare Parts
The 450-GC User Manual provides a list of replacement parts for routine operation.
Preventive Maintenance
Please note that it is essential that you perform regular preventive maintenance on your GC. By
performing this maintenance, you will increase the life of the system, increase system uptime,
and enjoy optimum system performance. Please refer to the Maintenance section of the 450-GC
User Manual for details.
Varian, Inc.
Page 14 of 14