Graph 13 (Corner se edge ka sample) ko sample 2 krdo or graph 14(center wala) ko sample 3

Graph 013:
From the DSC-TGA of the sample from the top corner, the heat flow rate was found to be -0.65(W/g) at
temperature 56.66oC which is close to the Thermal conductivity of pure paraffin. This was due to
inhomogeneous distribution of nano-magnetite at the corners, to compensate shrinkage.
Graph 014:
The heat flow rate from the DSC-TGA curve of sample from the center portion, was found to be -1.25
(W/g). The transition temperature also increased to 60.70 oC as compared to pure paraffin and sample 2.