V. Pengolahan Data: Ethanol Ethanol+aquades

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V.

PENGOLAHAN DATA
A. Tabel Kurva Kalibrasi
Ethanol

Aquades

Ethanol

(ml)

(ml)

(mol)

5.00
4.50
3.95
3.42
2.89
2.37
1.84
1.31
0.74
0

0
0.50
1.05
1.58
2.10
2.63
3.16
3.68
4.12
5.00

0.086
0.077
0.068
0.058
0.049
0.04
0.031
0.022
0.013
0

Aquades
(mol)
0
0.028
0.058
0.088
0.12
0.15
0.176
0.204
0.23
0.28

Contoh Perhitungan Fraksi Mol Etanol


5 ml etanol dan 0 ml air.

Massa etanol = x v
= 0,789 x 5 = 3,945 gr

Massa air
=xv
= 1 x 0 = 0 gr

Mol etanol
= gr / Mr
= 3,945 / 46,07 = 0,086 mol

Mol air

= gr / Mr
= 0 / 18 = 0 mol

n aseton
n aseton n kloroform

X etanol

=
0,086
1
0,086 0

Xethanol
ethanol
ethanol+ aquades
1
0.73
0.54
0.397
0.29
0.21
0.15
0.097
0.053
0

Indeks
Bias
1.365
1.361
1.358
1.354
1.352
1.350
1.348
1.346
1.340
1.330

Kurva Kalibrasi
1.37
1.36

f(x) = 0.03x + 1.34


R = 0.81

1.35
Indeks Bias 1.34
1.33

Linear ()

1.32
1.31
0

0.2

0.4

0.6

0.8

1.2

Fraksi Mol Etanol

B. DATA PENGAMATAN
Preheater
Waktu
(Menit)
0
7
14

Indeks
Distilat
1.364
1.363
1.361

Bias
Residu
1.339
1.335
1.335

Dari Kurva Kalibrasi


XD
XW
0.86
0.05
0.82
0.029
0.75
0.029

21

1.358

1.334

0.64

0.021

28

1.358

1.333

0.64

0.019

35

1.357

1.333

0.61

0.019

42

1.357

1.333

0.61

0.019

49

1.355

1.332

0.53

0.011

56

1.355

1.331

0.53

0.009

Reboiler
Waktu
(Menit)
0
7
14

Indeks
Distilat
1.359
1.347
1.346

Bias
Residu
1.335
1.335
1.334

Dari Kurva Kalibrasi


XD
XW
0.61
0.029
0.124
0.029
0.095
0.021

21

1.342

1.334

0.07

0.021

28

1.342

1.333

0.07

0.019

Preheater
Xd Xw

1
Xd Xw

0.81
0.79
0.72
0.62
0.62
0.59
0.59
0.52
0.52

1.23
1.26
1.39
1.61
1.61
1.69
1.69
1.92
1.92

2.5
2

f(x) = -0.47 ln(x) - 0.24


R = 0.91

1.5

Logarithmic ()

1
0.5
0
0

0.01

0.02

0.03

Reboiler
Xd Xw

1
Xd Xw

0.581
0.095
0.074
0.049
0.051

1.72
10.53
13.51
20.41
19.61

0.04

0.05

0.06

25
20

f(x) = -32.63 ln(x) - 109.36


R = 0.73

15
Logarithmic ()

10
5
0
0.02

0.02

0.02

0.02

0.03

0.03

0.03

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