19.

383
45.771

pikno kosong
pikno + air
berat labu kosong
berat sterofom
pikno kosong + metanol

air
metanol

289.35
36.06

40.212

Kalibrasi Refraktometer
volume
metanol

air
0
1
2
3
4
5
6
7
8
9
10

indeks bias
N
1.32
10
1.321
9
1.328
8
1.33
7
1.333
6
1.334
5
1.335
4
1.331
3
1.329
2
1.329
1
1.324
0

Refluks total (metanol:air= 50:50)

waktu
temperatur (C)
t(menit)
Td
Tw
60
4
60
8
60
12
59
16
58
20
60
24
60
28
60
32
60
36
40
60

densitas
air
0.9971
0.9971
0.9971
0.9971
0.9971
0.9971
0.9971
0.9971
0.9971
0.9971
0.9971

temperatur (K)
Td
86
86
86
86
85
86
86
86
86
86

333
333
333
332
331
333
333
333
333
333

Refluks total ( metanol : air = 30:70)

waktu
t(menit)

temperatur (C)
Td
4
62

temperatur (K)
Td

Tw
80

335

8
12
16
20
24
28
32
36
40

65
65
65
65
65
65
65
65
65

79
79
80
80
80
80
80
80
80

338
338
338
338
338
338
338
338
338

Refluk Parsial (metanol : air = 50:50)

waktu
t(menit)

temperatur (C)
Td
4
8
12
16
20
24
28
32
36
40

temperatur (K)
Td

Tw
60
60
60
60
60
60
60
60
60
60

82
82
82
82
82
82
82
82
82
82

333
333
333
333
333
333
333
333
333
333

Refluk Parsial (metanol:air=30:70)

waktu
t(menit)

temperatur (C)
Td
4
60
8
60
12
60
16
60
20
60
24
60
28
60
32
60
36
60
40
60

temperatur (K)
Td

Tw
77
77
77
77
77
77
77
77
77
77

333
333
333
333
333
333
333
333
333
333

waktu
t(menit)

waktu
t(menit)

temperatur (C)
Td
4
62
8
62
12
62
16
61
20
61
24
61
28
61
32
61
36
61
40
61

temperatur (C)
Td
4
61
8
61
12
60
16
60
20
60
24
60
28
60
32
60
36
60
40
60
44
60

temperatur (K)
Td

Tw
77
77
77
77
77
77
77
77
77
77

335
335
335
334
334
334
334
334
334
334

temperatur (K)
Td

Tw
78
78
78
79
79
79
79
79
79
79
79

334
334
333
333
333
333
333
333
333
333
333

26.388
20.829

0.7870
0.7870
0.7870
0.7870
0.7870
0.7870
0.7870
0.7870
0.7870
0.7870
0.7870

Tw

A
B
C

mol
air

metanol

Tw

AIR

fraksi metanol
metanol
X metanol
0.0000
0.2459
0.0554
0.2214
0.1108
0.1968
0.1662
0.1722
0.2216
0.1476
0.2770
0.1230
0.3324
0.0984
0.3878
0.0738
0.4431
0.0492
0.4985
0.0246
0.5539
0.0000

Indeks bias
Nd
1.32
359
1.312
359
1.32
359
1.32
359
1.32
358
1.32
359
1.32
359
1.32
359
1.32
359
359
1.32

Indeks bias
Nd
353
1.32

16.5362
3985.44
-38.9974

1.0000
0.7998
0.6398
0.5088
0.3998
0.3075
0.2284
0.1599
0.0999
0.0470
0.0000

Trata-rata
(C)

Nw
1.329
1.329
1.33
1.32
1.32
1.32
1.32
1.32
1.32
1.32

(K)
73
73
73
72.5
71.5
73
73
73
73
73

Trata-rata
(C)

Nw
1.334

346
346
346
345.5
344.5
346
346
346
346
346

(K)
71

344

352
352
353
353
353
353
353
353
353

1.32
1.32
1.32
1.32
1.32
1.32
1.32
1.32
1.32

Indeks bias
Nd

Tw
355
355
355
355
355
355
355
355
355
355

Tw

1.334
1.333
1.333
1.333
1.333
1.333
1.333
1.333
1.333

Indeks bias
Nd
350
1.32
350
1.32
350
1.32
350
1.32
350
1.32
350
1.32
350
1.32
1.32
350
1.32
350
1.32
350

Trata-rata
(C)

Nw
1.32
1.32
1.32
1.32
1.32
1.321
1.321
1.321
1.321
1.321

72
72
72.5
72.5
72.5
72.5
72.5
72.5
72.5

1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33

(K)
71
71
71
71
71
71
71
71
71
71

Trata-rata
(C)

Nw
1.331
1.331
1.331
1.331
1.331
1.331
1.331
1.331
1.331
1.331

345
345
345.5
345.5
345.5
345.5
345.5
345.5
345.5

344
344
344
344
344
344
344
344
344
344

(K)
68.5
68.5
68.5
68.5
68.5
68.5
68.5
68.5
68.5
68.5

341.5
341.5
341.5
341.5
341.5
341.5
341.5
341.5
341.5
341.5

Tw

Tw

Indeks bias
Nd
1.32
350
1.32
350
1.32
350
1.32
350
1.32
350
350
1.32
350
1.32
350
1.32
350
1.32
350
1.32

Indeks bias
Nd
1.315
351
1.315
351
1.317
351
1.317
352
1.317
352
1.318
352
1.318
352
1.32
352
1.32
352
352
1.32
352
1.32

Trata-rata
(C)

Nw
1.329
1.329
1.329
1.329
1.329
1.329
1.329
1.329
1.329
1.329

(K)
69.5
69.5
69.5
69
69
69
69
69
69
69

Trata-rata
(C)

Nw
1.331
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33
1.33

342.5
342.5
342.5
342
342
342
342
342
342
342

(K)
69.5
69.5
69
69.5
69.5
69.5
69.5
69.5
69.5
69.5
69.5

342.5
342.5
342
342.5
342.5
342.5
342.5
342.5
342.5
342.5
342.5

METANOL

16.494
3598.39
-35.225
i
n
d
e
k
s
b
i
a
s

0.1

0.2

0.3

0.4

0.5
X metanol

Ln Pa
(metanol)

Pa
4.9152
4.9152
4.9152
4.8966
4.8591
4.9152
4.9152
4.9152
4.9152
4.9152

Ln Pa
(metanol)

Ln Pb
(air)

136.3517
136.3517
136.3517
133.8311
128.9055
136.3517
136.3517
136.3517
136.3517
136.3517

Pa
4.8402 126.4996

Pb
3.5544
3.5544
3.5544
3.5332
3.4907
3.5544
3.5544
3.5544
3.5544
3.5544

Ln Pb
(air)

Alpha

34.9675571342
34.9675571342
34.9675571342
34.2348255956
32.808279625
34.9675571342
34.9675571342
34.9675571342
34.9675571342
34.9675571342

Pb
3.4693 32.1140939156

3.8994
3.8994
3.8994
3.9092
3.9291
3.8994
3.8994
3.8994
3.8994
3.8994
3.9033

Alpha
3.9391

4.8779
4.8779
4.8966
4.8966
4.8966
4.8966
4.8966
4.8966
4.8966

Ln Pa
(metanol)

131.3492
131.3492
133.8311
133.8311
133.8311
133.8311
133.8311
133.8311
133.8311

Pa
4.8402
4.8402
4.8402
4.8402
4.8402
4.8402
4.8402
4.8402
4.8402
4.8402

Ln Pa
(metanol)

Ln Pb
(air)

126.4996
126.4996
126.4996
126.4996
126.4996
126.4996
126.4996
126.4996
126.4996
126.4996

Pa
4.7451
4.7451
4.7451
4.7451
4.7451
4.7451
4.7451
4.7451
4.7451
4.7451

3.5120
3.5120
3.5332
3.5332
3.5332
3.5332
3.5332
3.5332
3.5332

115.0209
115.0209
115.0209
115.0209
115.0209
115.0209
115.0209
115.0209
115.0209
115.0209

33.5151286262
33.5151286262
34.2348255956
34.2348255956
34.2348255956
34.2348255956
34.2348255956
34.2348255956
34.2348255956

Pb
3.4693
3.4693
3.4693
3.4693
3.4693
3.4693
3.4693
3.4693
3.4693
3.4693

Ln Pb
(air)

Alpha

32.1140939156
32.1140939156
32.1140939156
32.1140939156
32.1140939156
32.1140939156
32.1140939156
32.1140939156
32.1140939156
32.1140939156

Pb
3.3613
3.3613
3.3613
3.3613
3.3613
3.3613
3.3613
3.3613
3.3613
3.3613

3.9191
3.9191
3.9092
3.9092
3.9092
3.9092
3.9092
3.9092
3.9092
3.9142

28.8267845576
28.8267845576
28.8267845576
28.8267845576
28.8267845576
28.8267845576
28.8267845576
28.8267845576
28.8267845576
28.8267845576

3.9391
3.9391
3.9391
3.9391
3.9391
3.9391
3.9391
3.9391
3.9391
3.9391
3.9391

Alpha
3.9901
3.9901
3.9901
3.9901
3.9901
3.9901
3.9901
3.9901
3.9901
3.9901
3.9901

Ln Pa
(metanol)

Pa
4.7833
4.7833
4.7833
4.7643
4.7643
4.7643
4.7643
4.7643
4.7643
4.7643

119.504
119.504
119.504
117.2447
117.2447
117.2447
117.2447
117.2447
117.2447
117.2447

Ln Pb
(air)

Pb
3.4047
3.4047
3.4047
3.3830
3.3830
3.3830
3.3830
3.3830
3.3830
3.3830

30.1056984381
30.1056984381
30.1056984381
29.4603572808
29.4603572808
29.4603572808
29.4603572808
29.4603572808
29.4603572808
29.4603572808

Alpha
3.9695
3.9695
3.9695
3.9797
3.9797
3.9797
3.9797
3.9797
3.9797
3.9797
3.9767
3.9767

Ln Pa
Pa
Ln Pb
Pb
Alpha
(metanol)
(air)
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7642632222 117.2447 3.3830455386 29.4603572808 3.9797447482
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7833499308 119.504 3.4047144707 30.1056984381 3.9694814146
4.7833499308 119.504 3.4047144707 30.1056984381
3.970507748
3.970507748
3.9705

0.3

0.4

0.5

0.6

0.7

0.8

0.9

X metanol

1.20
1.00

data kesetimbangan
Xa

0.80

Ya
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

0.0000
0.3025
0.4939
0.6259
0.7224
0.7961
0.8541
0.9011
0.9398
0.9723
1.0000

0.60
y metanol
0.40
0.20
0.00
0

xw

1.20
1.00

data kesetimbangan
Xa

Ya
0

0.0000

0.1

-0.20

0.80
0.60
y metanol
0.40

0.2

1.00
0.80

0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

0.3031
0.4946
0.6265
0.7229
0.7965
0.8545
0.9013
0.9400
0.9724
1.0000

0.60
y metanol
0.40
0.20
0.00
0

0.1

0.2

-0.20
x metanol

1.20

data kesetimbangan
Xa

1.00

Ya
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

0.0000
0.3044
0.4962
0.6280
0.7242
0.7975
0.8553
0.9019
0.9403
0.9726
1.0000

0.80
0.60
y metanol
0.40
0.20
0.00
-0.20

0.1

0.2

1.20

data kesetimbangan
Xa

Ya
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

1.00

0.0000
0.3072
0.4994
0.6310
0.7268
0.7996
0.8568
0.9030
0.9410
0.9729
1.0000

0.80
0.60
y metanol
0.40
0.20
0.00
-0.20

X
w

0.1

0.2

Xf

Xd

0.3

-0.20

X
w

data kesetimbangan
Xa

0.1

0.2

Xf

Xd

0.3

1.20

Ya
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

0.0000
0.3064
0.4985
0.6302
0.7261
0.7991
0.8564
0.9027
0.9409
0.9728
1.0000

1.00
0.80
0.60
y metanol
0.40
0.20
0.00
-0.20

0.1

Xf

X
w

data kesetimbangan
Xa

0.2

1.20

Ya
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1

0
0.3061181432
0.4981499138
0.6298553052
0.7258024174
0.7988133103
0.8562342912
0.9025770141
0.9407654209
0.9727776858
1

1.00
0.80
0.60
y metanol
0.40
0.20
0.00
-0.20

X
w

0.1

0.2

Xf

1.20
1.00
0.80
0.60
y metanol
0.40
0.20
0.00
0

0.1

0.2

0.3

0.4

0.5

0.6

-0.20

xw

1.20
1.00
0.80

0.60
y metanol
0.40

x metanol

Xd

0.7

0.8

0.9

1.1

1.00
0.80

0.60
y metanol
0.40
0.20
0.00
0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

0.5

0.6

0.7

0.8

0.9

1.1

-0.20

X
w

x metanol

Xd

1.20
1.00
0.80

0.60
metanol
0.40
0.20
0.00
-0.20

0.1

0.2

0.3

0.4

x metanol

1.1

Xd

Xw

X
d

1.20
1.00
0.80

0.60
etanol
0.40
0.20
0.00
-0.20

X
w

0.1

0.2

Xf

Xd

0.3

0.4

0.5
x metanol

0.6

0.7

0.8

0.9

1.1

-0.20

X
w

0.1

0.2

Xf

Xd

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1.1

x metanol

1.20
1.00
0.80

0.60
y metanol
0.40
0.20
0.00
-0.20

0.1

0.2

0.3

0.4

x metanol

Xf

X
w

0.5

0.6

0.7

0.8

0.9

1.1

0.7

0.8

0.9

1.1

Xd

1.20
1.00
0.80

0.60
y metanol
0.40
0.20
0.00
-0.20

X
w

0.1

0.2

Xf

0.3

0.4

0.5
x metanol

0.6

Xd

Nd

Nw
1.32

Nd

Xd
1.32

Nw
1.32

Xw
0.63

Xd
1.333

1.0000

Xw
0.4946

0.3998

nd

nw
1.321

1.33
0.5

xf

nd

xd

nw

1.32
1.331
intersep
0.109701
xf
0.3

xw
0.7975

xd

intersept
0.5088

xw
0.3072

0.1599

0.455733

nd

nw
1.32

xd
1.329

xw
0.3064

0.0999

0.3064

nd

nw
1.32

0.0999

xd
xw
1.33 0.902577
0.5088
0.9025

0.5088

indeks bias

Jenis Refluks
Refluks total 50:50
Refluks total 30:70
refluks parsial 6:8
Refluks Parsial 9:5

Jenis Refluks
Refluks total 50:50
Refluks total 30:70
refluks parsial 6 :8
Refluks Parsial 9:5

massa
labu+metanol 50:50
labu+metanol 30:70
labu+metanol 50:50 (6:8)
labu+metanol 30:70 (9:5)

berat sterofom

Nd

Nw

1.32
1.32
1.321
1.32
1.32
1.32

1.32
1.333
1.33
1.331
1.329
1.33

fraksi mol
xw

xd

1.0000
0.3998
0.5088
0.1599

0.63
0.4946
0.7975
0.3072

0.10

0.31

0.5088

0.9025

sebelum

setelah
762.49
674.53
764.59
741.28
752.49
741.84
36.06

740.46
704.34
737.95
699.99
704.46
695.49

fraksi mol
Xd
0.63
0.4946
0.7975
0.3072
0.3064
0.9025

3.90
3.91
3.94
3.99
3.98
3.97

ALPHA
Xw
1.0000
0.3998
0.5088
0.1599
0.0999
0.5088

3.9033
3.9142
3.9391
3.9901
3.9767
3.9705

Jumlah Tahap
Frenske Underwood
Mac Cabe-Thiele
5.07
3.00
1.69
1.00
1.68
1.00
1.66
1.00
1.67
1.00
2.00
3.3398

HETP
Mac Cabe
3.00
1.00
1.00
1.00
1.00
2.00

Xd/(1-Xd)
1.6729
0.9785
3.9391
0.4433
0.4418
9.2564

(1-Xw)/Xw
0.0000
1.5015
0.9652
5.2552
9.0100
0.9654

Log
0.5914
0.5926
0.5954
0.6010
0.5995
0.5988

Y*Z
0.0000
1.4693
3.8022
2.3299
3.9802
8.9362

LOG C
Err:502
0.1671
0.5800
0.3673
0.5999
0.9512

29.03003003

Chart Title
1.34
1.335
1.33
N (indeks bias)

1.325

Column

1.32
1.315
1.31
0

0.2

0.4

0.6
X

0.8

1.2

Nm
5.0724
1.6874
1.6796
1.6639
1.6680
3.3398

Mac Cabe
3
1
1
1
1
2

0.8

Column C

1.2

HETP
0.2760
0.8297
0.8336
0.8414
0.8393
0.4192