Ammonia and Carbon Dioxide in Water on

Rtx-Volatile Amine
Peaks
1.
2.
3.
4.

tR (min)

Nitrogen
Carbon dioxide
Ammonia
Water

4.51
4.83
5.10
6.05

2
3

Time (min)
GC_PC1232
Column
Sample
Injection
Inj. Vol.:

Rtx-Volatile Amine, 60 m, 0.32 mm ID

(cat.# 18078)
See notes

500 L headspace-syringe split

(split ratio 10:1)
Liner:
4 mm Sky single taper w/wool
(cat.# 23303.1)
Inj. Temp.:
200 C
Headspace-Syringe
Split Vent Flow
Rate:
15.8 mL/min
Oven
Oven Temp.:
45 C (hold 10 min)

Carrier Gas
Linear Velocity:
Dead Time:
Detector
Make-up Gas
Flow Rate:
Make-up Gas
Type:
Data Rate:
Sensitivity Mode:
Instrument
Notes

He, constant linear velocity

22 cm/sec, 101 psi, 696.4 kPa @ 45 C
4.54 min @ 45 C
TCD @ 200 C
12 mL/min
He
5 Hz
He/H2
Agilent/HP6890 GC
500 L of ammonia hydroxide and 400 L of
carbon dioxide were bubbled into a 510%
solution of aqueous ammonium hydroxide
(ammonia cleaner).

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