Professional Documents
Culture Documents
Is 10117 2000
Is 10117 2000
Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
1 +, 1 +
01 ' 5
Jawaharlal Nehru
! $ ' +-
Satyanarayan Gangaram Pitroda
! > 0 B
BharthariNtiatakam
Is 10117:2000
( Reaffirmed 2006 )
Indian Standard
CODE OF PRACTICE FOR PASSIVATION OF
STAINLESS STEEL ARTICLES, INDUSTRIAL
EQUIPMENTS AND COMPONENTS
INCLUDING PIPELINES
(First Revision)
~ BIS 2000
BUREAU
OF
INDIAN
STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
Decetnber
2000
Price Group 2
FORE WORD
This Indian Standard (First Revision) was adopted by the Bureau of Indian Standards, after the drafl finalized
by the Corrosion Protection Sectio]lal Committee had been approved by the Metallurgical Engineering
Division Council.
The stainless steel articles including industrial hardware owe their resistance to corrosion to the formation of
a protective oxide film on its surface, Passivation treatment is normally employed for enhancing the formation
of the protective film on the surface, by immersion in an oxidizing acid solution. This standard has been
prepared for specifying the process details for the passivation treatment and methods for testing the passivated
surfaces. This pretreatment is generally applied to stainless steel surgical instruments, cutlery, tubes and
various other industrial equipments and hardware.
In this revision the scope of the standard has been widened to include industrial equipments including
pipelines. This revision of the standard incorporates soak cleaning and mechanical descaling as additional
methods for surface preparation.The recommended passivation treatments for different stainless steels have
been detailed in this version of the standard. While ferroxqd test and high humidity test have been included as
(csts for resistance to corrosion, the potential-time measurement has been introduced to con.tlrm passivation
of the surface.
With the above changes the specification has been made much detailed and user friendly.
IS 10117:2000
Indian Standard
CODE OF PRACTICE FOR PASSIVATION OF
STAINLESS STEEL ARTICLES, INDUSTRIAL
EQUIPMENTS ANI) COMPONENTS
INCLUDING PIPELINES
(First Revision )
1
SCOPE
OF CHEMICALS
IS 10117:2000
3.5 Mechanical
4.3 Passivation
Descaling
fime
24 hours
65C
800C
Stainless Steel
500fJ
25C
35*C
TREATMENT
of Free Machining
Temperature
15 hours
8 hours
4 hours
2 % hours
4.2 Passivation
Steel Tanks
4 PASSIVATION
of Stainless
at 50-60C.
to Corrosion
IS 10117:2000
94 wt percent
3 wt percent
3 wt percent
1000 cm3
20 cm3
30 gm
AND TESTING
Condition
Sutution, Volume
Percentage
All thx-machining
alloys and 400 series
containing less than
H*So,,
Temperature
Time
Minutes
65-80
5-45
20-80
5-30
20-60
5-30
8-11 percent
HN03 ,
15-25 percent
plus HF.
1-8 percent
HN03 ,
10-15 percent
plus HF
I-1.5 percent
16% cllromium
NOTES
1 The table is applicable to the equivalent cast grades of wrought alloys also.
2
3
Shorter time duration and lower temperatures are for low a[loy stainless steels.
.4tkr pickling and water rinse, an aqueous caustic permanganate solution containing NaOH 10 wW. and KMnOq 4 wt% at 70-80C for
5-60 minutes may be used for final dip to remove the smut.koot followed by thorough water rinsing and drykrg.
IS 10117:2000
Table2
Passivation
Steels
Gratle
Surface
Paasivatlon
Condition
Treatment
N(J.
A
ii)
Non-Free
MachiningGrades
200and300
series , 400 series
Precipitation hardening and
maraging alloys with > 16 O/OCr
HN03 + 2-6W%.
20-40 VOI?40
N~Cr2072H20
at 50-70C for
30-60 min
20-50
iii)
20-50 VO1YO
HN03 at 45 to 50C for
20-30 minor at 20-40C for 60 min
iv)
20-25 VOIVO
HN03 + 2-6 WWOC fbr
N~Cr2072H20
at 50-55C for
15-30 minor at 20-40C for 30-60 min
HN03 +
20-50 VO]YO
2-6wt% Na2Cr207 2H20 at 25.50C
for 25-40 min
i)
Free Machining
Grades
or
1-2 Vol% HN03 +
1-5 wV. N~Crz07 2H20 at 50-70C
10 min
ii)
40-60vow.HN03+
2-6 WP?4.
N~Cr,O,
for 20-30 &
-
2H,0 at 50-70C
-
BIS is a statutory institution established under the Bureau of lndian Standards Act, 1986 to promote
harmonious development of the activities of standardization, marking and quality certification of goods
and attending to connected matters in the country.
Copyright
BIS has the copyright of all its publications. No part of these publications may be reproduced in any form
without the prior permission in writing of BIS. This does not preclude the free use, in the course of
implementing the standard, of necessary details, such as symbols and sizes, type or grade designations.
Enquiries relating to copyright be addressed to the Director (Publications), BIS.
Review of Indian Standards
Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed
periodically; a standard along with amendments is reaffirmed when such review indicates that no changes are
needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards
should ascertain that they are in possession of the latest amendments or edition by referring to the latest issue of
BIS Catalogue and Standards: Monthly Additions.
This Indian Standard has been developed from Doc : No. MTD 24 (4217).
Amendments
Amend No.
Date of Issue
Text Affected
Telegrams : Manaksanstha
(Common to all offices)
Telephone
Regional Offices :
Central
Eastern
3237617
{ 3233841
3378499,3378561
{ 3378626,3379120
Northern
603843
{ 602025
Southern
r23502 16,2350442
2351519,2352315
Western
Branches
8329295,8327858
8327891,8327892
{