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Self Prop 1701011 She Dam Kor
Self Prop 1701011 She Dam Kor
Self Prop 1701011 She Dam Kor
AbstractMagnesium ferrite (MgFe2O4) was prepared by simple low-cost oxalate coprecipitation method
and characterized by XRD and SEM. The X-ray analysis confirmed the formation of a single-phase cubic
spinel structure. The product revealed a non-uniform morphology and some certain extent of agglomeration.
Crystallite size, texture coefficient, dislocation density, hopping length, and mechanical properties of the
product are also reported.
Keywords: oxalate co-precipitation method, sintering, magnesium ferrite MgFe2O4 texture coefficients, dis-
location density, strain
DOI: 10.3103/S1061386217010113
75
76 SHEDAM et al.
Intensity
1400
1300
+
(311)
1200
900
20 30 40 50 60 70 5 m
5.000
Angle (2theta)
XRD SEM
Furnace
Magnetic stirrer
Dried Powder
D = 0.9 .
(hkl) and lattice parameter (a) were calculated as
shown below and collected in Table 1. cos
(311)
1200
LA = a 3 , LB = a 2
(440) 4 4
1100 (422)
(220) (400) (511) The results are presented in Table 2.
1000
2.5
2.0
TC(hkl)
1.5
TC
1.0
0.5
0
220 311 400 422 511 440
TC(hkl) 0.518 0.279 1.549 2.198 0.744 0.710
(a) 50 m (b) 1 m
Table 2. Lattice constant, strain, volume, crystallite size, dislocation density, and hopping lengths of magnesium ferrite
Hopping length,
a, V, 3 D, nm D, m 2
LA LB
place because they experience a permanent magnetic 9. Rane, K.S., Verenkar, V.M.S., and Sawant, P.Y.,
moment proportional to their volume [24, 25]. Dielectric behavior of MgFe2O4 prepared from chemi-
cally beneficiated iron ore rejects, Bull. Mater. Sci.,
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4. CONCLUSIONS BF02704930
10. Liu, Y.L., Liu, Z.M., Yang, Y., Yang, H.F., Shen, G.L.,
Synthesized nano-crystalline MgFe2O4 is single and Yu, R.Q., Simple synthesis of MgFe2O4 nanoparti-
phase and has a cubic spinel structure (lattice constant cles as gas sensing materials, Sens. Actuators B, 2005,
a = 8.31826 , crystallite size D = 35.10 nm) with pref- vol. 107, no. 2, pp. 600604. doi 10.1016/j.snb.
erential orientation of grains along the (422) plane. 2004.11.026
11. Candeia, R.A., Souza, M.A.F., Bernardi, M.I.B.,
Maestrelli, S.C., Santos, I.M.G., Souza, A.G., and
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