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    B (D) 6.96 C (D) 6.57: de La Paz, Joshua Lab 301 GSI: Sarah Klass Expt. C-Crossed Aldol 1H NMR

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    musicman314
    The document is an NMR spectroscopy report. It contains a 1H NMR spectrum with peaks labeled A, B, and C. Peak A is a multiplet at 7.40 ppm. Peak B is a doublet at 6.96 ppm. Peak C is a doublet at 6.57 ppm. The solvent used was chloroform-d.

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    B (D) 6.96 C (D) 6.57: de La Paz, Joshua Lab 301 GSI: Sarah Klass Expt. C-Crossed Aldol 1H NMR

    Uploaded by

    musicman314
    6 views3 pages
    The document is an NMR spectroscopy report. It contains a 1H NMR spectrum with peaks labeled A, B, and C. Peak A is a multiplet at 7.40 ppm. Peak B is a doublet at 6.96 ppm. Peak C is a doublet at 6.57 ppm. The solvent used was chloroform-d.

    Original Description:

    An NMR sample

    Original Title

    Processed Aldol 20170207

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    The document is an NMR spectroscopy report. It contains a 1H NMR spectrum with peaks labeled A, B, and C. Peak A is a multiplet at 7.40 ppm. Peak B is a doublet at 6.96 ppm. Peak C is a doublet at 6.57 ppm. The solvent used was chloroform-d.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    6 views3 pages

    B (D) 6.96 C (D) 6.57: de La Paz, Joshua Lab 301 GSI: Sarah Klass Expt. C-Crossed Aldol 1H NMR

    Uploaded by

    musicman314
    The document is an NMR spectroscopy report. It contains a 1H NMR spectrum with peaks labeled A, B, and C. Peak A is a multiplet at 7.40 ppm. Peak B is a doublet at 6.96 ppm. Peak C is a doublet at 6.57 ppm. The solvent used was chloroform-d.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    of 3

    2.

    32 EtOAc
    7.25 CDCl3

    1.28 EtOH
    1.24 EtOH
    1.64 H2O

    0.00 TMS
    1.26 C6
    1.22 C6
    de la Paz, Joshua

    6.97
    6.95
    6.90
    6.59
    6.54
    1100000

    7.50
    7.48
    7.44
    7.39
    7.37
    7.34
    7.31
    7.02
    Lab 301
    GSI: Sarah Klass
    Expt. C- Crossed Aldol 1H NMR

    B (d) 1000000
    6.96 1H NMR (300 MHz, Chloroform-d) 7.63 7.27 (m, 60H), 6.96 (d, J =
    7.9 Hz, 21H), 6.57 (d, J = 15.2 Hz, 10H).
    A (m) C (d) 900000
    7.40 6.57
    800000

    700000

    600000

    500000

    400000

    300000

    200000

    100000

    0
    60.05

    20.60

    10.09

    0.06

    1.00
    0.08
    0.11
    0.19
    0.07
    9.5 9.0 8.5 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 -0.5
    f1 (ppm)
    7.25 CDCl3

    6.97
    6.95

    6.90

    6.59

    6.54
    7.50
    7.48
    7.44
    7.39
    7.37
    7.34
    7.31

    7.02
    1100000

    1000000
    A (m) B (d) C (d)
    7.40 6.96 6.57
    900000

    800000

    700000

    600000

    500000

    400000

    300000

    200000

    100000

    0
    60.05

    20.60

    10.09
    7.8 7.7 7.6 7.5 7.4 7.3 7.2 7.1 7.0 6.9 6.8 6.7 6.6 6.5 6.4 6.3
    f1 (ppm)
    76.62 CDCl3
    77.47 CDCl3
    77.05 CDCl3
    5500000

    162.33

    143.05
    141.64
    141.48

    136.16

    129.19
    129.05
    128.87
    127.28
    127.02
    de la Paz, Joshua
    C- Crossed Aldol 13C NMR
    5000000

    4500000

    129.19
    129.05
    128.87

    127.28
    127.02
    4000000

    3500000

    3000000

    2500000

    131 130 129 128 127 126 125 2000000


    f1 (ppm)

    1500000

    1000000

    500000

    170 165 160 155 150 145 140 135 130 125 120 115 110 105 100 95 90 85 80 75 70
    f1 (ppm)

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