Correlation Test PM Cems and Reference Method Test Data

CORRELATION TEST PM CEMS AND REFERENCE METHOD TEST DATA
PM CEMS PM concentration Facility: Plant A

response mg/acm Location: Anytown, USA
Run x y Emission Unit: Boiler No. 2
1 Test Dates: Apr - May 2002
2
3 Value Units
4 Emission limit: 20 mg/acm
5
6
10
11
PM Concentration
12
13
14
15 12
16
17 10
19
20 8
21
22
6
23
24
4
0
0 2 4 6 8 10 12
PM CEMS Response
355270027.xls Test Data Page 1 of 29

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PS-11 Correlation Test

Calculation Spreadsheet
Version 2-6 10/25/04

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CALCULATIONS FOR LINEAR CORRELATION
Facility: Plant A Emission Unit: Boiler No. 2

Location: Anytown, USA Test Dates: Apr - May 2002
PM CEMS PM concentration
response mg/acm CALCULATED STATISTICAL PARAMETERS
Run x y (xi-x~)2 (yi-y~)2 (xi-x~)(yi-y~) y^ (yî-yi)2
355270027.xls Linear Calcs Page 4 of 29

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Run x y (xi-x )
~ 2
(yi-y~)2 (xi-x~)(yi-y~) y^ (yî-yi)2

05/18/2017
Run x y (xi-x )
~ 2
(yi-y~)2 (xi-x~)(yi-y~) y^ (yî-yi)2
Sum - - - - 0.00 -
Mean #DIV/0! #DIV/0! y^ at mean x = #DIV/0!

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RESULTS OF LINEAR CORRELATION

Correlation equation: y= #DIV/0! + #DIV/0! x

Variable Equation Value
n Number of data points = 0 Summary of Acceptance Criteria for PS-11
x ~ x~ = 1/n*(Sum of (xi)) = #DIV/0! Criterion Actual Allowable Acceptable?
Sxx Sxx = Sum((xi-x~)^2) = 0 Correlation coefficient #DIV/0! > 0.85 #DIV/0!
y ~ y~ = 1/n*(Sum of (yi)) = #DIV/0! Confidence interval #N/A < 10% #N/A
Syy Syy = Sum((yi-y~)^2) = 0 Tolerance interval #N/A < 25% #N/A
Sxy Sxy = Sum((xi-x~)(yi-y~)) = 0.0 * Indicates correlation coefficient is undefined.
b0 b0 = y~-b1x~ = #DIV/0!
PM C o n c e n tr atio n
b1 b1 = Sxy/Sxx = #DIV/0!
SL SL = SQRT(1/(n-2)(Sum(yi^-yi)^2)) = 0.000
f (x) =
y^mean y^ at mean x value = #DIV/0! Plot of Linear Regression Line
tf tf from table = #N/A 12
CI CI = tf*SL*SQRT(1/n) = #N/A 10
EL Emission Limit = 20.0 8
CI% CI% =CI/EL*100% = #N/A 6
n' n' = n = 0 4
vf vf from table = #N/A 2
un' un' from table = #N/A 0

0 2 4 6 8 10 12
kT kt = un'*vf = #N/A PM CEM S Re s pons e
TI TI = kt*SL = #N/A
TI% TI% = TI/EL*100% = #N/A
Sy Sy = SQRT(Syy/(n-1)) = 0.000 PS-11 Correlation Test
r2 r2 = 1-(SL^2/Sy^2) = #DIV/0! Calculation Spreadsheet
r r = SQRT((1-SL^2/Sy^2)) = #DIV/0! Version 2-6 10/25/04
* Indicates correlation coefficient is undefined.
355270027.xls Linear Summary 05/18/2017

CALCULATIONS FOR POLYNOMIAL CORRELATION

Run x y x2 x3 x4 xy x2y y^ (y^-y)2 delta (yi-y~)2 CI
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355270027.xls Polynomial Calcs
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Sum - - - - - - - - 0.00
Minimum> 0.0000 #N/A

Version 2-6 10/25/04
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RESULTS OF POLYNOMIAL CORRELATION

Variable Equation Value Correlation equation: y= #DIV/0! + #DIV/0! x + #DIV/0! x2

n Number of data points = 0
S1 S1 = Sum (xi) = 0 Summary of Acceptance Criteria for PS-11
S2 S2 = Sum (xi2) = 0 Criterion Actual Allowable Acceptable?
S3 S3 = Sum (xi3) = 0 Correlation coefficient #DIV/0! > 0.85 #DIV/0!
S4 S4 = Sum (xi4) = 0 Confidence interval #N/A < 10% #N/A
S5 S5 = Sum (yi) = 0 Tolerance interval #DIV/0! < 25% #DIV/0!
S6 S6 = Sum (xiyi) = 0 * Indicates correlation coefficient is undefined.
S7 S7 = Sum (xi2yi) = 0
det A det A = nS2S4-S2S2S2+S1S3S2-S3S3n+S2S1S3-S4S1S1 = 0.000E+00 Check for Correlation Curve Minimum/Maximum
b0 b0 = (S5S2S4+S1S3S7+S2S6S3-S7S2S2-S3S3S5-S4S6S1)/det A = #DIV/0! Correlation curve minimum point #DIV/0!
b1 b1 = (nS6S4+S5S3S2+S2S1S7-S2S6S2-S7S3n-S4S1S5)/det A = #DIV/0! Minimum allowable x value #DIV/0!
b2 b2 = (nS2S7+S1S6S2+S5S1S3-S2S2S5-S3S6n-S7S1S1)/det A = #DIV/0! Is correlation curve minimum < minimum x value? #DIV/0!
Sp Sp = Sqrt((1/(n-3)Sum of (y^-Y)2) = 0.000 Correlation curve maximum point #DIV/0!
D D = n(S2S4-S32)+S1(S3S2-S1S4)+S2(S1S3-S22) = 0.000E+00 Extrapolation limit for x (125% of maximum x value) #DIV/0!
C0 C0 = (S2S4-S32)/D = #DIV/0! Is correlation curve maximum > extrapolation limit? #DIV/0!
C1 C1 = (S3S2-S1S4)/D = #DIV/0!
P M Conce ntra tion

C2 C2 = (S1S3-S22)/D = #DIV/0!
C3 C3 = (nS4-S22)/D = #DIV/0! f(x) =
C4 C4 = (S1S2-nS3)/D = #DIV/0! Plot of Polynomial Regression Curve
C5 C5 = (nS2-S12)/D = #DIV/0!
12
tf tf from table = #N/A
CI CI = tf*Sp *sqrt(delta-min) = #N/A 8

CI% CI% = CI/EL*100= #N/A
6
vf vf from table = #N/A
un' un' from table = #DIV/0! 4
n' n' = 1/delta = #DIV/0! 2
kT kt = un'*vf = #DIV/0!
0
TI TI = kt*sp = #DIV/0!
0 2 4 6 8 10 12
TI% TI% = TI/EL *100% = #DIV/0!
y~ y~ = 1/n*(Sum of (yi)) = #DIV/0! PM CEMS Response
Sy Sy = sqrt(Sum of ( yi-y~)^2/(n-1) = 0.00

r2 r2 = 1-(Sp^2/Sy^2) = #DIV/0!
r r = sqrt((1-Sp^2/Sy^2)) = #DIV/0!
Max-min? b2 > 0? #DIV/0! PS-11 Correlation Test
xmax-min y = -b1/2b2 = #DIV/0! Calculation Spreadsheet
1.25xmax 0.00 Version 2-6 10/25/04
355270027.xls Polynomial Summary 05/18/2017

CALCULATIONS FOR LOGARITHMIC CORRELATION

PM CEMS response PM concentration

Measured Transformed mg/acm CALCULATED STATISTICAL PARAMETERS
Run x x' = ln (x) y (xi'-x'~)2 (yi-y~)2 (x'i-x'~)(yi-y~) y^ (yî-yi)2
Page 13 of 29
355270027.xls Logarithmic Calcs
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Sum - - - - 0.000 0.000


Version 2-6 10/25/04
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RESULTS OF LOGARITHMIC CORRELATION

Correlation equation: y= #DIV/0! + #DIV/0! Ln(x)

x' ~ x'~ = 1/n*(Sum of (x'i)) = #DIV/0! Criterion Actual Allowable Acceptable?
Sx'x' Sx'x' = Sum((x'i-x'~)^2) = 0.00 Correlation coefficient #DIV/0! > 0.85 #DIV/0!
y ~ y~ = 1/n*(Sum of (yi)) = #DIV/0! Confidence interval #N/A < 10% #N/A
Syy Syy = Sum((yi-y~)^2) = 0 Tolerance interval #N/A < 25% #N/A
Sx'y Sx'y = Sum((x'i-x'~)(yi-y~)) = 0.0 * Indicates correlation coefficient is undefined.
b0 b0 = y~-b1x'~ = #DIV/0!
PM C o n ce n tr atio n
b1 b1 = Sx'y/Sx'x' = #DIV/0!
SL SL = SQRT(1/(n-2)(Sum(yi^-yi)^2)) = 0.000 f (x) = NaN ln(x)
y^mean y^ at mean x value = #DIV/0! Plot of Logar ithm ic Re gr e s s ion Curve

CI CI = tf*SL*SQRT(1/n) = #N/A 10
CI% CI% =CI/EL*100% = #N/A 6
n' n' = n = 0 4
un' un' from table = #N/A 0
0 2 4PM CEM S Re
6 s pons e 8 10 12
kT kt = un'*vf = #N/A
TI TI = kt*SL = #N/A
TI% TI% = TI/EL*100% = #N/A
Sy Sy = SQRT(Syy/(n-1)) = 0.000 PS-11 Correlation Test
r2 r2 = 1-(SL^2/Sy^2) = #DIV/0! Calculation Spreadsheet
r r = SQRT((1-SL^2/Sy^2)) = #DIV/0! Version 2-6 10/25/04
355270027.xls Logarithmic Summary 05/18/2017

CALCULATIONS FOR EXPONENTIAL CORRELATION

PM concentration
PM CEMS mg/acm
response Measured Transformed CALCULATED STATISTICAL PARAMETERS
Run x y y' = Ln(y) (xi-x~)2 (y'i-y'~)2 (xi-x~)(y'i-y'~) y'^ (y'î-y'i)2
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355270027.xls Exponential Calcs
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PM concentration
PM CEMS mg/acm
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PM concentration
PM CEMS mg/acm
Sum - - - - 0.000 -
Mean #DIV/0! #DIV/0! #DIV/0! y^ at mean x = #DIV/0!

Version 2-6 10/25/04
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RESULTS OF EXPONENTIAL CORRELATION

Correlation equation: y = #DIV/0! e ### x

x~ x~ = 1/n*(Sum of (xi)) = #DIV/0! Criterion Actual Allowable Acceptable?
Sxx Sxx = Sum((xi-x~)^2) = 0.0 Correlation coefficient #DIV/0! > 0.85 ###
y'~ y'~ = 1/n*(Sum of (y'i)) = #DIV/0! Confidence interval #DIV/0! < 10% ###
Sy'y' Sy'y' = Sum((y'i-y'~)^2) = 0.00 Tolerance interval #DIV/0! < 25% ###
Sxy' Sxy' = Sum((xi-x~)(y'i-y'~)) = 0.00 * Indicates correlation coefficient is undefined.
b0' b0' = y'~-b1x~ = #DIV/0!
b0 b0 = e^b0' = #DIV/0! f(x) = NaN exp( NaN x )
PM Concentration
b1 b1 = Sxy'/Sxx = #DIV/0! Plot of Exponential Regression Curve
SL SL = SQRT(1/(n-2)(Sum(y'i^-y'i)^2)) = 0.000 12
y'^mean y'^ at mean x value = #DIV/0!
CI' CI' = tf*SL*SQRT(1/n) = #N/A

LCL' LCL' = y~' - CI' #DIV/0! 8
UCL' UCL' = y~' + CI' #DIV/0!
CI CI = (eÛCL' - e^LCL')/2 #DIV/0! 6
EL Emission Limit = 20.0
CI% CI% =CI/EL*100% = #DIV/0! 4
n' n' = n = 0
un' un' from table = #N/A
kT kT = un'*vf = 0
#N/A
0 2 4 6 8 10 12
TI' TI' = kt*SL = #N/A PM CEMS Response
LTL' LTL' = y~' - TI' #DIV/0!
UTL' UTL' = y~' + TI' #DIV/0!
TI TI = (eÛTL' - e^LTL')/2 #DIV/0!
TI% TI% = TI/EL*100% = #DIV/0!
Sy' Sy' = SQRT(Sy'y'/(n-1)) = 0.000 PS-11 Correlation Test
r2 r2 = 1-(SL^2/Sy'^2) = #DIV/0! Calculation Spreadsheet
r r = SQRT((1-SL^2/Sy'^2)) = #DIV/0! Version 2-6 ###
355270027.xls Exponential Summary 05/18/2017

CALCULATIONS FOR POWER CORRELATION

PM concentration
PM CEMS response mg/acm
Measured Transformed Measured Transformed CALCULATED STATISTICAL PARAMETERS
Run x x' = Ln(x) y y' = Ln(y) (x'i-x'~)2 (y'i-y'~)2 (x'i-x'~)(y'i-y'~) y'^ (y'I^-y'i)2
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355270027.xls Power Calcs
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PM concentration
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PM concentration
Sum - - 0.00 - 0.000 -


Version 2-6 10/25/04
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RESULTS OF POWER CORRELATION

Correlation equation: y = #DIV/0! x #DIV/0!

x'~ x'~ = 1/n*(Sum of (x'i)) = #DIV/0! Criterion Actual Allowable Acceptable?
Sx'x' Sx'x' = Sum((x'i-x'~)^2) = 0.00 Correlation coefficient #DIV/0! > 0.85 #DIV/0!
y'~ y'~ = 1/n*(Sum of (y'i)) = #DIV/0! Confidence interval #DIV/0! < 10% #DIV/0!
Sy'y' Sy'y' = Sum((y'i-y'~)^2) = 0.00 Tolerance interval #DIV/0! < 25% #DIV/0!
Sx'y' Sx'y' = Sum((x'i-x'~)(y'i-y'~)) = 0.00 * Indicates correlation coefficient is undefined.
b0' b0' = y'~-b1x~ = #DIV/0!
b0 b0 = e^b0' = #DIV/0!
b1 b1 = Sx'y'/Sx'x' = #DIV/0! f(x) = NaN x^NaN
PM Concentration
SL SL = SQRT(1/(n-2)(Sum(y'i^-y'i)^2)) = 0.000 Plot of Power Function Regression Curve
y'^mean y'^ at mean x value = #DIV/0!
12
tf tf from table = #N/A
CI' CI = tf*SL*SQRT(1/n) = #N/A 10
LCL' LCL' = y~' - CI' #DIV/0!
UCL' UCL' = y~' + CI' #DIV/0! 8
CI CI = (eÛCL' - e^LCL')/2 #DIV/0!
CI% CI% =CI/EL*100% = #DIV/0!
n' n' = n = 0 4
vf vf from table = #N/A
un' un' from table = 2
#N/A
kT kT = un'*vf = #N/A 0
TI' TI' = kTSL = #N/A 0 2 4 6 8 10 12
LTL' LTL' = y~' - TI' #DIV/0! PM CEMS Response
UTL' UTL' = y~' + TI' #DIV/0!
TI TI = (eÛTL' - e^LTL')/2 #DIV/0!
TI% TI% = TI/EL*100% = #DIV/0!
Sy' Sy' = SQRT(Sy'y'/(n-1)) =0.000 PS-11 Correlation Test
r2 r2 = 1-(SL^2/Sy'^2) = #DIV/0! Calculation Spreadsheet
r r = SQRT((1-SL^2/Sy'^2)) = #DIV/0! Version 2-6 10/25/04
355270027.xls Power Summary 05/18/2017

SELECTION OF BEST MODEL

Correlation Confidence interval Tolerance interval half Min/max within Does model meet all
Model > 0.85 ? < 10% ? < 25% ?
coefficient (a) half range percentage range percentage allowable range? criteria?
Linear #DIV/0! #DIV/0! #N/A #N/A #N/A #N/A (b) #DIV/0!
Polynomial #DIV/0! #DIV/0! #N/A #N/A #DIV/0! #DIV/0! #DIV/0! #DIV/0!
Logarithmic #DIV/0! #DIV/0! #N/A #N/A #N/A #N/A (b) #DIV/0!
Exponential #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! (b) #DIV/0!
Power #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! (b) #DIV/0!
(a) * indicates correlation coefficient is undefined; model does not satisfy criterion.
(b) Not applicable; criterion applies only to polynomial model.
Best model: #DIV/0!

Version 2-6 10/25/04
355270027.xls Best Model 05/18/2017

PREDICTED PM CONCENTRATIONS

PM CEMs Predicted PM concentrations (y), in units of : mg/acm

response (x) Linear Polynomial Logarithmic Exponential Power
4 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
33 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! PS-11 Correlation Test
34 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Calculation Spreadsheet
35 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Version 2-6 10/25/04
355270027.xls Predicted Values 05/18/2017

VALUES FOR STATISTICAL PARAMETERS
df tf vf un' (75)
3 3.182 2.920 1.266
4 2.776 2.372 1.247
5 2.571 2.089 1.233
6 2.447 1.915 1.223
7 2.365 1.797 1.214
8 2.306 1.711 1.208
9 2.262 1.645 1.203
10 2.228 1.593 1.198
11 2.201 1.551 1.195
12 2.179 1.515 1.192
13 2.160 1.485 1.189
14 2.145 1.460 1.186
15 2.131 1.437 1.184
16 2.120 1.418 1.182
17 2.110 1.400 1.181
18 2.101 1.384 1.179
19 2.093 1.370 1.178
20 2.086 1.358 1.177
21 2.080 1.346 1.175
22 2.074 1.335 1.174
23 2.069 1.326 1.173
24 2.064 1.316 1.172
25 2.060 1.308 1.172
26 2.056 1.300 1.171
27 2.052 1.293 1.170
28 2.048 1.286 1.170
29 2.045 1.280 1.169
30 2.042 1.274 1.168
31 2.040 1.268 1.168
32 2.037 1.263 1.167
33 2.035 1.258 1.167
34 2.032 1.253 1.166
35 2.030 1.248 1.166
36 2.028 1.244 1.165
37 2.026 1.240 1.165
38 2.024 1.236 1.165
39 2.023 1.232 1.164
40 2.021 1.228 1.164
41 2.020 1.225 1.164
42 2.018 1.222 1.163
43 2.017 1.218 1.163
44 2.015 1.215 1.163
45 2.014 1.212 1.163
46 2.013 1.210 1.162
47 2.012 1.207 1.162
48 2.011 1.204 1.162
49 2.010 1.202 1.162
50 2.009 1.199 1.161
51 2.008 1.197 1.161
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355270027.xls Stats Table
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df tf vf un' (75)
52 2.007 1.195 1.161
53 2.006 1.192 1.161
54 2.005 1.190 1.161
55 2.004 1.188 1.160
56 2.003 1.186 1.160
57 2.002 1.184 1.160
58 2.002 1.182 1.160
59 2.001 1.180 1.160
60 2.000 1.179 1.160
61 2.000 1.177 1.159
62 1.999 1.175 1.159
63 1.998 1.174 1.159
64 1.998 1.172 1.159
65 1.997 1.170 1.159
66 1.997 1.169 1.159
67 1.996 1.167 1.159
68 1.995 1.166 1.159
69 1.995 1.165 1.158
70 1.994 1.163 1.158
71 1.994 1.162 1.158
72 1.993 1.160 1.158
73 1.993 1.159 1.158
74 1.993 1.158 1.158
75 1.992 1.157 1.158
76 1.992 1.156 1.158
77 1.991 1.154 1.158
78 1.991 1.153 1.158
79 1.990 1.152 1.157
80 1.990 1.151 1.157
81 1.990 1.150 1.157
82 1.989 1.149 1.157
83 1.989 1.148 1.157
84 1.989 1.147 1.157
85 1.988 1.146 1.157
86 1.988 1.145 1.157
87 1.988 1.144 1.157
88 1.987 1.143 1.157
89 1.987 1.142 1.157
90 1.987 1.141 1.157
91 1.986 1.140 1.157
92 1.986 1.139 1.156
93 1.986 1.138 1.156
94 1.986 1.138 1.156
95 1.985 1.137 1.156
96 1.985 1.136 1.156
97 1.985 1.135 1.156
98 1.984 1.134 1.156
99 1.984 1.134 1.156
100 1.984 1.133 1.156
Page 28 of 29
355270027.xls Stats Table
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Version 2-6
October 25, 2004
355270027.xls Version 05/18/2017

Correlation Test PM Cems and Reference Method Test Data

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Correlation Test PM Cems and Reference Method Test Data

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CORRELATION TEST PM CEMS AND REFERENCE METHOD TEST DATA

PM CEMS PM concentration Facility: Plant A

355270027.xls Test Data Page 1 of 29

355270027.xls Test Data Page 2 of 29

PS-11 Correlation Test

355270027.xls Test Data Page 3 of 29

Facility: Plant A Emission Unit: Boiler No. 2

355270027.xls Linear Calcs Page 4 of 29

355270027.xls Linear Calcs Page 5 of 29

PS-11 Correlation Test

355270027.xls Linear Calcs Page 6 of 29

Facility: Plant A Emission Unit: Boiler No. 2

Correlation equation: y= #DIV/0! + #DIV/0! x

un' un' from table = #N/A 0

355270027.xls Linear Summary 05/18/2017

Facility: Plant A Emission Unit: Boiler No. 2

PS-11 Correlation Test

Facility: Plant A Emission Unit: Boiler No. 2

Variable Equation Value Correlation equation: y= #DIV/0! + #DIV/0! x + #DIV/0! x2

P M Conce ntra tion

CI CI = tf*Sp *sqrt(delta-min) = #N/A 8

Sy Sy = sqrt(Sum of ( yi-y~)^2/(n-1) = 0.00

355270027.xls Polynomial Summary 05/18/2017

Facility: Plant A Emission Unit: Boiler No. 2

PM CEMS response PM concentration

Sum - - - - 0.000 0.000

PS-11 Correlation Test

Facility: Plant A Emission Unit: Boiler No. 2

Correlation equation: y= #DIV/0! + #DIV/0! Ln(x)

tf tf from table = #N/A 12

355270027.xls Logarithmic Summary 05/18/2017

Facility: Plant A Emission Unit: Boiler No. 2

PS-11 Correlation Test

Facility: Plant A Emission Unit: Boiler No. 2

Correlation equation: y = #DIV/0! e ### x

Variable Equation Value

CI' CI' = tf*SL*SQRT(1/n) = #N/A

355270027.xls Exponential Summary 05/18/2017

Facility: Plant A Emission Unit: Boiler No. 2

Sum - - 0.00 - 0.000 -

PS-11 Correlation Test

Facility: Plant A Emission Unit: Boiler No. 2

Correlation equation: y = #DIV/0! x #DIV/0!

355270027.xls Power Summary 05/18/2017

Facility: Plant A Emission Unit: Boiler No. 2

PS-11 Correlation Test

355270027.xls Best Model 05/18/2017

Facility: Plant A Emission Unit: Boiler No. 2

PM CEMs Predicted PM concentrations (y), in units of : mg/acm

355270027.xls Predicted Values 05/18/2017

355270027.xls Version 05/18/2017

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CI CI = tfSp sqrt(delta-min) = #N/A 8

CI' CI' = tfSLSQRT(1/n) = #N/A