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    S-26 IC Application Note No.: Title: Speciation of Phosphate and Phosphite

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    salvaleuven
    This document summarizes an ion chromatography method for separating and detecting fluoride, chloride, nitrite, bromide, nitrate, phosphate, phosphite, sulfate, and tetrafluoroborate ions using a Metrosep Anion Dual 2 column with 2 mmol/L sodium hydrogencarbonate and 1.3 mmol/L sodium carbonate eluent containing 12% acetone. The method uses chemical suppression with a 50 mmol/L sulfuric acid regenerant and is able to resolve phosphate and phosphite peaks within 20 minutes.

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    S-26 IC Application Note No.: Title: Speciation of Phosphate and Phosphite

    Uploaded by

    salvaleuven
    6 views1 page
    This document summarizes an ion chromatography method for separating and detecting fluoride, chloride, nitrite, bromide, nitrate, phosphate, phosphite, sulfate, and tetrafluoroborate ions using a Metrosep Anion Dual 2 column with 2 mmol/L sodium hydrogencarbonate and 1.3 mmol/L sodium carbonate eluent containing 12% acetone. The method uses chemical suppression with a 50 mmol/L sulfuric acid regenerant and is able to resolve phosphate and phosphite peaks within 20 minutes.

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    Speciation of phosphate and phosphite

    Original Title

    696003_AN-s026

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    This document summarizes an ion chromatography method for separating and detecting fluoride, chloride, nitrite, bromide, nitrate, phosphate, phosphite, sulfate, and tetrafluoroborate ions using a Metrosep Anion Dual 2 column with 2 mmol/L sodium hydrogencarbonate and 1.3 mmol/L sodium carbonate eluent containing 12% acetone. The method uses chemical suppression with a 50 mmol/L sulfuric acid regenerant and is able to resolve phosphate and phosphite peaks within 20 minutes.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    6 views1 page

    S-26 IC Application Note No.: Title: Speciation of Phosphate and Phosphite

    Uploaded by

    salvaleuven
    This document summarizes an ion chromatography method for separating and detecting fluoride, chloride, nitrite, bromide, nitrate, phosphate, phosphite, sulfate, and tetrafluoroborate ions using a Metrosep Anion Dual 2 column with 2 mmol/L sodium hydrogencarbonate and 1.3 mmol/L sodium carbonate eluent containing 12% acetone. The method uses chemical suppression with a 50 mmol/L sulfuric acid regenerant and is able to resolve phosphate and phosphite peaks within 20 minutes.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    of 1

    IC Application Note No.

    S-26
    Title: Speciation of phosphate and phosphite

    Summary: Separation of fluoride, chloride, nitrite, bromide, nitrate,


    phosphate, phosphite, sulfate and tetrafluoroborate using
    anion chromatography with conductivity detection after
    chemical suppression.

    Sample: Standard
    Sample Preparation:

    Column: 6.1006.100 Metrosep Anion Dual 2


    Eluent: 2 mmol/L sodium hydrogencarbonate,
    1.3 mmol/L sodium carbonate, 12% acetone
    Suppressor: Metrohm Suppressor Module (MSM, 50 mmol/L H2SO4)
    Flow: 0.8 mL/min
    Injection Volume: 20 L

    fluoride

    chloride 1 S/cm

    nitrate
    bromide

    sulfate
    nitrite
    phosphite fluoroborate
    phosphate

    5 10 15 20 min

    Results: F- Cl-, NO2- Br-, NO3-, HPO42-, HPO32-, SO42-, BF4-


    mg/L mg/L mg/L
    2 5 10

    S-26/2

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