Thermomechanical Analysis of A Ceramic Cooker 10.1007 - s11668-013-9699-9

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Thermomechanical Analysis of a Ceramic

Cooker

Michael D.Hayes & David L.Ahearn

Journal of Failure Analysis and


Prevention

ISSN 1547-7029

J Fail. Anal. and Preven.


DOI 10.1007/s11668-013-9699-9

1 23
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1 23
Author's personal copy
J Fail. Anal. and Preven.
DOI 10.1007/s11668-013-9699-9

FEATURE

Thermomechanical Analysis of a Ceramic Cooker


Michael D. Hayes David L. Ahearn

Submitted: 26 February 2013


ASM International 2013

Abstract This article highlights the use of experimental lifting the ceramic top. Apparently, the hinge design was
methods in determining operating conditions for a con- modified after the purchase of the subject cooker, but the
sumer product. The research was prompted by the reason for the change is unknown. The cooker had been
investigation of a house fire in which it was determined that installed on a wooden table built by the homeowner.
the fire originated at a ceramic cooker/grill on the home- Examination of the cooker revealed that the top was off at
owners deck. The cause of the fire is believed to be the the time of the fire, and the bottom air vent was closed. A
escape of hot gases from the cooker through a crack in the crack was also found in the lower base of the cooker,
lower portion of the cooker, which pyrolized the wood adjacent to the hinges at the rear of the cooker (Fig. 1). The
table on which the cooker rested. The source of the crack is manufacturer claims operating temperatures in excess of
unknown, but one hypothesis inferred that the hinge design 700 F.
was defective because it applied concentrated loads to the Cold smoke testing on the subject cooker after the
ceramic material at the hinge attachment points. This study incident (Figs. 2, 3) demonstrated that the crack had fully
examines the stress/strains that are experienced by the grown through the thickness of the ceramic wall, and thus,
ceramic material of the cooker during normal operation at a pathway for hot exhaust gas travel to the combustible
elevated temperature and abnormal operation, including wood table existed. Examination of the fracture surfaces
abuse and improper functioning of the hinge. The experi- revealed discoloration, indicating that the crack had existed
mental methods and analysis techniques used to perform even before the fire. Hot gases inside the cooker during use
the measurements are detailed. would cause the pressure inside the cooker to rise above the
pressure outside the cooker, causing the hot gases to flow
Keywords Ceramics  Cracking  Mechanical testing through the crack and heat the wood table. Furthermore,
the geometry of the table would allow the hot gases to
escape through the crack to approach the internal temper-
Background ature of the cooker.
The cause of cracking is unknown. Possible explana-
The authors firm was hired to investigate the cause of a tions include porosity in the ceramic material (Fig. 4) and/
fire at a home. The details of the fire investigation are not or excessive stresses developing in service due to product
presented, but the origin of the fire was found to be a design, or operating factors such as thermal shock, which
ceramic cooker/cooker on the rear deck adjacent to the this material is specifically designed to resist. In particular,
house. The cooker was an oval shaped, two-piece design it was discovered that the table geometry, as built by the
with a hinged lid. The hinge was spring loaded to assist in owner, was such that the hinge would strike the table when
the lid was fully opened. This impact with the table could
potentially introduce unusual loads upon the cooker, such
M. D. Hayes (&)  D. L. Ahearn
as torsion or local bending. The hinge assembly for this
Engineering Systems Inc, 6230 Regency Parkway,
Norcross, GA 30071, USA particular cooker consists of metal bands that are tightened
e-mail: mdhayes@esi-atl.com around the rim portion of both the top and bottom sections.

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Fig. 3 Close-up of smoke transmission through cracks during smoke


test

Fig. 1 Subject cooker with hinge locations indicated by arrows (top),


close-up of crack at one hinge (bottom)

Fig. 4 Porosity in ceramic material near the crack location

The purpose of the study described herein was to


investigate the effect of the loads introduced by the hinge
design in conjunction with the installation geometry on the
stresses/strains imparted to the ceramic material. A cooker
with the original hinge design was not available for testing,
and so a new, exemplar cooker with the newer hinge design
was tested. In addition, the stresses/strains resulting from
thermal expansion of the material (and constraint by the
hinge bands, for example) were characterized.
Fig. 2 Hinge detail on subject cooker (photo taken during smoke
testing)

Material Analysis
The bands are connected to the spring-loaded hinge
through a series of clinch studs (Fig. 2). Therefore, any To first understand the mechanical properties of the
local loading on the hinge could result in concentrated unknown ceramic material, a sample of the subject cooker
forces or moments acting on the ceramic material. It is material was analyzed using semiquantitative x-ray dif-
noted that the hinge design apparently had been changed fraction (XRD). The results, shown in Table 1, indicate a
some time after the owner purchased his cooker. The rea- multiphase ceramic of Cordierite and Mullite with Cordi-
son for the change is unknown. erite comprising over 50% of the material. These phases

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Table 1 XRD results


Phase ID Chemical Formula Estimated wt.%

Cordierite Mg2Al3.96Si5.04O18 11.1


Cordierite Mg2(Al4Si5O18) 39.6
Mullite Al4.44Si1.56O9.78 33.4
Hydrogen magnesium H(Mg2(SiO4))8 May not be present or
silicate could not be measured
Amorphous phase  16.0

Fig. 6 Strain gage and thermocouple installations near the 11:00


position

band, on the band, on the table near the circular cutout, on


the top and bottom sides of the cooker, inside the cooker on
the top of the cooking grate, and on the inside of the base
opposite the steel band. All gages were connected to a sig-
nal-conditioning and data-acquisition system via a high-
temperature-insulated wire for real-time recording of strains
and temperatures.
Fig. 5 Strain gage and thermocouple installations near the 9:00 A number of loading scenarios (initially performed at
position room temperature and then later at elevated temperature)
were considered, including the following:
characteristically have low coefficients of thermal
1. Installation of hinge attachment band.
expansion (0.781.4 9 106 in/in/F and 2.52.9 9
2. Normal, slow opening and closing of the lid.
106 in/in/F, respectively), providing good resistance to
3. Tightening of the hinge attachment band using the
thermal shock. They also provide good mechanical proper-
5/1600 carriage bolt (to 125 in-lbs).
ties [1]. Typical properties for Cordierite are Youngs
4. Quick opening and closing of the lid.
Modulus = 20,000 ksi, bend strength = 35.5 ksi, and
5. Dropping the lid from the fully open position.
fracture toughness = 2.1 ksiHin.
By zeroing out the strain gages before step 1, the strains
induced in the base ceramic by tightening the carriage bolt
Mechanical Analysis on the hinge could be determined.
The table assembly instructions specify the use of a
Cooker Testing concrete stepping stone (paver) between the base of the
cooker and the lower shelf, presumably to insulate the table
In order to establish the stress or strain on the material during from the cooker. The preceding experiments were per-
various operation scenarios, the cooker was instrumented formed with the paver in place (proper setup) and then
with strain gages and thermocouples at a number of loca- repeated without the paver (improper setup) to allow the
tions around the circumference of the cooker on the left, rear hinge mechanism to impact the table. During testing with
quarter of the cooker (from the users perspective). The this modified setup, a twisting load was also introduced
strain gages, type WK-03-250BG-350 from Vishay Micro- through the handle while opening and closing.
Measurements were positioned on the smooth outer lip or
flange of the bottom piece (base) and on the steel hinge
attachment band between the 9:00 and 12:00 locations, as Results
shown in Figs. 5 and 6. A high-temperature adhesive was
utilized to provide survivability up to approximately 500 F. During testing at room temperature, it was found that the
Thermocouples were also mounted at a number of locations, act of attaching the hinge hardware introduced only 46
including the outer and inner surfaces of the base near the microstrains on the ceramic base, and tightening to the

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specified torque reduced the strain to approximately 0


microstrains (i.e., induced compression on the ceramic).
Hard opening and closing or twisting at room temperature
increased the strain up to approximately 100 microstrains.
Removing the paver had a negligible effect, increasing the
strain to 104 microstrains.
Next, the experiment (without paver) was repeated for a
hot cooker. After zeroing the strain gages and starting the
data-acquisition program, a 9-pound bag of Kingsford
Original charcoal briquettes was poured into the base and
lit. The lid was closed, and the top and bottom vents were
left completely open to maximize airflow. Strains and
temperatures were monitored as the cooker heated up to a
maximum temperature of 690 F, according to the built-in Fig. 7 Raw, uncorrected strains and temperatures versus time
measured during the CTE experiment
lid thermometer. According to the thermocouple mea-
surements, the temperature was as high as 1,450 F at the
grate (just above the fire) and on the inside of the cooker,
just below the lip of the base. The outside of the base at the
same location reached 450 F.
Once a steady-state temperature profile was reached
(approximately one hour), the opening/closing, dropping,
and twisting steps above were repeated. The cooker vents
were then closed and left to cool naturally. Data were
recorded for approximately 8 min until the outer temper-
ature had dropped to approximately 200 F, and then the
test was concluded.

CTE Measurements

The data obtained in the cooker testing provided strain Fig. 8 Corrected strains and temperature versus time measured
measurements as a function of thermal history. These during the CTE experiment
readings include not only the mechanical strain induced by
the introduction of external stresses (e.g., band tightening,
opening/closing, etc.), but also thermal strains due to the The strain gages were chosen to have similar coefficient
thermal expansion of the material. In the absence of con- of thermal expansion (CTE) as the Cordierite/Mullite
straints, a part or component that is allowed to expand ceramic. However, owing to the thermal sensitivity of the
freely will experience no additional stress as a result of material comprising the gage, the strain gages will produce
thermal expansion. However, if some type of constraint is a temperature-induced apparent strain. This apparent
introduced to limit the thermal expansion, a stress will be strain depends on both the gage and the substrate material.
generated. Thus, the thermal expansion strains must be It can be estimated using the data provided by the gage
known and subtracted from the total strains to isolate pure manufacturer, but direct measurement is preferred [3].
mechanical strains. The presence of constraints must also Therefore, a control sample of titanium silicate with a CTE
be assessed, as they could introduce additional stresses. equal to 0.0 was also gaged and placed in the oven adjacent
To this end, an experiment was devised to measure the to the ceramic test sample to directly measure the tem-
CTE of the subject cooker material, following the approach perature-induced apparent strain. This strain was then
outlined in the American Society for Testing and Materials, subtracted from the measured strain on the ceramic test
Standard Test Method for Linear Expansion of Metals, sample at every measurement increment (Fig. 8). (Note
ASTM Standard No. B95-39 [2]. A piece of material taken that both samples were free of constraint except for friction
from the subject cooker was instrumented with two strain with the oven rack; a sheet of Teflon was placed between
gages and a thermocouple. The sample was then heated in a the samples and the oven rack to minimize friction.)
commercial oven to a temperature of over 450 F through The results indicated an artificial, temperature-induced
several heating and soak steps over a period of 8 h apparent strain of approximately 1,000 microstrains
(Fig. 7). (1,000 9 106 in/in) at 450 F (see Fig. 9)not an

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Fig. 9 Temperature-induced apparent strain versus temperature


Fig. 11 Strains (and temperature) versus time during heating of the
cooker

Fig. 10 Corrected thermal strains used to calculate CTE

insignificant amount. Subtracting this response from the


ceramic sample data yielded the real strain versus tem- Fig. 12 Strains (and temperature) versus time during operation of the
perature response. The corrected (actual) strain at each cooker
temperature level was then plotted as a function of tem-
perature, as shown in Fig. 10. The curves obtained at the were then corrected to eliminate temperature-induced
two gages have different slopes and are slightly non-linear. apparent strain. The resulting strain versus time curves are
Fitting the curves with linear fits provides CTE estimates of shown in Figs. 11 and 12 for the ceramic during heating
1.4 and 0.88 9 106 in/in/F. The variation between the and operation at the maximum temperature. (Note that the
two gage locations is likely due to the material inhomo- red thermocouple (TCO, channel 0) curve corre-
geneity of this multiphase composite. The average value sponds to temperature on the right-hand vertical axis. As
was 1.14 9 106 in/in/F. Referring back to the handbook shown in Fig. 12, the temperature only rose to about 6 F
data, this information confirms the observation of high when the lid was opened.) The data indicate maximum
Cordierite content, as determined through XRD. readings on the cooker at the 9:00 location, which is closest
to the left-side hinge attachment point. However, the
Data Analysis maximum value was only about 400 microstrains with
small fluctuations up to 430 microstrains during opening
Using the thermally induced apparent strain curves and closing. Furthermore, the free expansion thermal strain
obtained above, the data acquired during the cooker testing is estimated to be between 394 and 633 (average = 513)

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microstrains at 450 F. Assuming no constraint to limit free with external temperatures on the cooker exceeding
expansion, this means that the mechanical strain was no more 450 F. At these temperatures, special strain gages, adhe-
than 200 microstrains (or 81 microstrains, using the average sives, and conductor cable are required. In addition, the
CTE). This is similar to the maximum value obtained during resulting strain values must be adjusted to compensate for
the room temperature testing: 104 microstrains. artificial or apparent strains resulting from the thermal
During heating, the gaged steel band expanded to characteristics of the gages themselves.
approximately 3,000 microstrains at 450 F, indicating a The analysis performed as part of this investigation was
CTE of approximately 7.9 9 106 in/in/F, which is in the prompted by the observation that a crack in the ceramic
typical range for steel. Thus, the steel band also expands cooker could have allowed hot gases to escape over time
relatively freely and likely relaxes the clamping stress on and pyrolize the wood table. This crack was associated
the ceramic, thereby allowing the ceramic to also expand with the attachment point for the steel hinge band on the
relatively freely. The result is that heating the cooker has lower portion of the cooker. However, a detailed experi-
little or no effect on the stress in the ceramic with the mental analysis of the stresses/strains acting on the ceramic
exception of relieving some of the compressive stress material during normal and abnormal operation of an
exerted by the band when tightened during installation. exemplar cooker with an updated hinge design did not
While the subject ceramic material was not tested to reveal any appreciable values. Furthermore, the stresses/
provide mechanical strength data, the Engineered Materials strains appeared to be unaffected by the key variables of
Handbook data suggest a strain to failure of at least 773 installation, adjustment, and operation, thereby suggesting
microstrains for a pure Cordierite phase, and the Mullite that cracks would not have occurred under normal cir-
phase may contribute even greater strength to the com- cumstances. It is possible that the original hinge design did,
posite. Thus, the factor of safety on ultimate strength for in fact, overstress the ceramic material, but this hypothesis
this design is estimated to be very high (773/104 = 7.4), has not been proven.
and the propensity for self-initiated cracking of the ceramic
is considered to be very low for the conditions of normal
use (and even some abnormal use). References

1. ASM International: Engineering Materials Handbook, vol. 4:


Summary Ceramics and Glasses, ASM International (1991)
2. Vishay Micro-Measurements Tech Note TN-513-1, Measurement
of Thermal Expansion Coefficient Using Strain Gages (2010)
This article highlights the use of experimental methods in 3. Vishay Micro-Measurements Tech Note TN-513-1, Technical
determining operating conditions for a consumer product. Note TN-504-1, Strain Gage Thermal Output and Gage Factor
In this case, the operating conditions were fairly extreme Variation with Temperature (2007)

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