NERACA MASSA

Basis 100 kg C3H5Cl

C3H5Cl = 98.5% x 100 = 98.5 kg/jam
H2O = 1.5% x 100 = 1.5 kg/jam

C3H5Cl masuk reaktor

C3H5Cl = (98.5 kg/jam) / (76.5 kg/kmol) = 1.2875817 kmol/jam
H2O = (1.5 kg/jam) / (18 kg/kmol) = 0.08333333 kmol/jam

NaOH masuk reaktor = 1.2875817 kmol/jam 1.26183007 73.8170588

NaOH berlebih 20% = 1.54509804 kmol/jam
Massa NaOH 61.8039216 kg/jam
Air dari NaOH 556.23529412 kg/jam 30.9019608 kmol/jam

REAKTOR
Konversi x=0.98 Reaksi :
masuk keluar C3H5Cl
Komp. BM
kmol/jam kg/jam kmol/jam kg/jam
C3H5Cl 76.5 1.2875816993 98.5 0.02575163 1.97
NaOH 40 1.5450980392 61.8039216 0.28326797 11.330719
C3H5OH 58 0 0 1.26183007 73.1861438
NaCl 58.5 0 0 1.26183007 73.8170588
H2O 18 30.985294118 557.735294 30.9852941 557.735294
Jumlah 33.817973856 718.039216 33.8179739 718.039216

NETRALIZER
masuk keluar Reaksi :
Komp. BM
kmol/jam kg/jam kmol/jam kg/jam NaOH
C3H5Cl 76.5 0.025751634 1.97 0.02575163 1.97
NaOH 40 0.2832679739 11.330719 0 0
C3H5OH 58 1.2618300654 73.1861438 1.26183007 73.1861438
NaCl 58.5 1.2618300654 73.8170588 1.54509804 90.3882353
H2O 18 32.15150932 578.727168 32.4347773 583.825991
HCl 36.5 0.2832679739 10.339281 0 0
Jumlah 33.817973856 749.37037 35.267457 749.37037

STRIPPER
Masuk keluar(hasil atas) keluar(hasil bawah)
Komp. BM
kmol/jam kg/jam kmol/jam kg/jam kmol/jam kg/jam
C3H5Cl 76.5 0.025751634 1.97 0.02575163 1.97 0 0
C3H5OH(lk) 58 1.2618300654 73.1861438 1.24921176 72.4542824 0.0126183 0.73186144
NaCl 58.5 1.5450980392 90.3882353 0 0 1.54509804 90.3882353
H2O(hk) 18 32.434777294 583.825991 0.32434777 5.83825991 32.1104295 577.987731
Jumlah 35.267457032 749.37037 1.59931117 80.2625423 33.6681459 669.107828
Diinginkan C3H5OH 99%
Diinginkan H2O 1%

MENARA DESTILASI 1
Masuk keluar(hasil atas) keluar(hasil bawah)
Komp. BM
kmol/jam kg/jam kmol/jam kg/jam kmol/jam kg/jam
C3H5Cl(lk) 76.5 0.025751634 1.97 0.02536536 1.94045 0.00038627 0.02955
C3H5OH(hk) 58 1.2492117647 72.4542824 0.01873818 1.08681424 1.23047359 71.3674681
H2O 18 0.3243477729 5.83825991 0 0 0.32434777 5.83825991
Jumlah 1.5993111716 80.2625423 0.04410354 3.02726424 1.55520764 77.235278
Diinginkan C3H5Cl 98.5%
Diinginkan C3H5OH 1.5%

MENARA DESTILASI 2
Masuk keluar(hasil atas) keluar(hasil bawah)
Komp. BM
kmol/jam kg/jam kmol/jam kg/jam kmol/jam kg/jam
C3H5Cl 76.5 0.0003862745 0.02955 0.00038627 0.02955 0 0
C3H5OH(lk) 58 1.2304735882 71.3674681 1.21816885 70.6537934 0.01230474 0.71367468
H2O(hk) 18 0.3243477729 5.83825991 0.00324348 0.0583826 0.3211043 5.77987731
Jumlah 1.5552076357 77.235278 1.2217986 70.741726 0.33340903 6.49355199
Diinginkan C3H5OH 99%
Diinginkan H2O 1%
UMPAN SEGAR TANGKI 3 RECYCLE DARI MD 1
Umpan Segar Tangki 3 Recycle
Komponen BM Komponen BM
kmol/jam kg/jam kmol/jam
C3H5Cl 76.5 1.2622163399 96.55955 C3H5Cl 76.5 0.02536536
H2O 18 0.0192215686 0.34598824 C3H5OH 58 0.01873818
Jumlah 1.2814379085 96.9055382 Jumlah 0.04410354

MIXER
massa NaOH 61.8039216 kg/jam
massa H2O 556.235294 kg/jam
H2O dari NaOh dengan kadar 48% 66.9542484 kg/jam 3.71968046 kmol/jam
H2O yang ditambahkan 489.281046 kg/jam 27.1822803 kmol/jam

Masuk keluar
Komponen BM
kmol/jam kg/jam kmol/jam kg/jam
NaOH 40 1.5450980392 61.8039216 1.54509804 61.8039216
H2O 18 3.7196804648 66.9542484 30.9019608 556.235294
H2O yang ditambahkan 27.18228032 489.281046 0 0
jumlah 32.447058824 618.039216 32.4470588 618.039216
 Faktor 25000*1000/330/24

NaOH >>> C3H5OH NaCl

HCl >>> NaCl H2O

Recycle
kg/jam
1.94045
1.0868144
3.0272644
NERACA MASSA
Basis 100 kmol C5H4O2
C5H4O2 = 95% x 100 = 95 kmol/jam Basis
H2O = 5% x 100 = 5 kmol/jam

C5H4O2 masuk reaktor

CHO542 = 19.78043 kmol/jam
H2O = 1.041075 kmol/jam

H2 masuk raktor
H2 4.118581191 kmol/jam
H2 berlebih 20.59290596 kmol/jam
CH4 dari H2 0.20592906 kmol/jam

Reaktor
Konversi x=0,9969
masuk keluar
Komp. BM
kmol/jam kg/jam kmol/jam kg/jam
C5h4o2 96 19.780425 1898.9208 0.061319 5.886654
H2 2 20.59290596 41.1858 0.8738 1.747601
c5h6o2 98 0 0.0000 19.71911 1932.472
ch4 16 0.20592906 3.2949 0.205929 3.294865
h20 18 1.041075 18.7394 1.041075 18.73935
Jumlah 41.62033502 1962.1408 21.90123 1962.141

FDS
masuk keluar atas keluar bawah
Komp BM kmol/jam kg/jam kmol/jam kg/jam kmol/jam kg/jam
C5h4o2 96 0.061319317 5.88665448 0 0 0.061319 5.886654
H2 2 0.873800274 1.7476005488 0.8738 1.747601 0 0
c5h6o2 98 19.71910568 1932.47235689 0 0 19.71911 1932.472
ch4 16 0.20592906 3.2948649531 0.205929 3.294865 0 0
h20 18 1.041075 18.73935 0 0 1.041075 18.73935
Jumlah 21.90122933 1962.14082687 1.079729 5.042466 20.8215 1957.098

MD1
MENARA DESTILASI 1
Masuk keluar(hasil atas) keluar(hasil bawah)
Komponen BM
kmol/jam kg/jam kmol/jam kg/jam kmol/jam kg/jam
H2O 18 1.041075 18.73935 1.041075 18.73935 0 0
c5h4o2 96 0.061319317 5.88665448 0.060093 5.768921 0.001226 0.117733
c5h6o2 98 19.71910568 1932.47235689 0.394382 38.64945 19.32472 1893.823
Jumlah 20.8215 1957.09836137 1.49555 63.15772 19.32595 1893.941
Diinginkan C5h6o2 98%
Diinginkan c5h4o2 2%
 faktor
0.999999

1962.141
1957.098
 H2 9 10
H2 1 1

11
5
11

3 3 3
4

2
2

konversi 0.9969 Faktor 1.9988626819

Basis 1000 kg

komponen 1 2 3 4 5
H2 24.4830 0.0000 98.9583 79.2280 79.2280
CH4 0.2473 0.0000 4.1226 4.1226 4.1226
H2O 0.0000 50.0000 50.0000 50.0000 0.0000
C5H4O2 0.0000 950.0000 950.0000 2.9450 0.0000
C5H6O2 0.0000 0.0000 0.0000 966.7853 0.0000
Total 24.7303 1000.0000 1103.0809 1103.0809 83.3506
-3.8858E-16

komponen 1 2 3 4 5
H2 48.9382 0.0000 197.8041 158.3659 158.3659
CH4 0.4943 0.0000 8.2405 8.2405 8.2405
H2O 0.0000 99.9431 99.9431 99.9431 0.0000
C5H4O2 0.0000 1898.9195 1898.9195 5.8867 0.0000
C5H6O2 0.0000 0.0000 0.0000 1932.4711 0.0000
Total 49.4325 1998.8627 2204.9073 2204.9073 166.6064
NM OVERALL = Min = Mout
2048.2952 = 2048.2952
 9

3 4

6 7 8 9 10 (Purging) 11 BM
0.0000 0.0000 0.0000 74.4753 4.7527 98.9583 2
0.0000 0.0000 0.0000 3.8753 0.2473 4.1226 16
50.0000 0.0000 50.0000 0.0000 0.0000 0.0000 18
2.9450 0.0589 2.8861 0.0000 0.0000 0.0000 96
966.7853 947.4496 19.3357 0.0000 0.0000 0.0000 98
1019.7303 947.5085 72.2218 78.3506 5.0000 103.0809

6 7 8 9 10 11 BM
0.0000 0.0000 0.0000 148.8659 9.5000 197.8041 2
0.0000 0.0000 0.0000 7.7461 0.4943 8.2405 16
99.9431 0.0000 99.9431 0.0000 0.0000 0.0000 18
5.8867 0.1177 5.7689 0.0000 0.0000 0.0000 96
1932.4711 1893.8217 38.6494 0.0000 0.0000 0.0000 98
2038.3009 1893.9394 144.3615 156.6121 9.9943 206.0446