Lake Charles Methanol, LLC Internal

Lake Charles Methanol Project copy

Document ID JYH 25-Jun-2015 08:57
5000 STPD grade AA Methanol Unit S-06030 P53002-E _D
Job no. Doc. no. Rev.
Page Item no.
2nd Feed effluent exchanger 1 of 5
09-E-0002 1/2

Process specification
for
09-E-0002 1/2
2nd Feed effluent exchanger

Revision Description Date Made By Chd. By Appd. By

_A For Check 20-May-2015 PTRH / /
_B For Review 1-Jun-2015 PTRH / /
_C For Check 18-Jun-2015 PTRH / /
_D For Re-Review 18-Jun-2015 PTRH / /
Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
 Lake Charles Methanol, LLC Internal
Lake Charles Methanol Project copy
Document ID JYH 25-Jun-2015 08:57
5000 STPD grade AA Methanol Unit S-06030 P53002-E _D
Job no. Doc. no. Rev.
Page Item no.
2nd Feed effluent exchanger 2 of 5
09-E-0002 1/2

Datasheet for Shell and Tube Heat Exchanger

Design case SOR Design case
TEMA type DET Special Calculated surface area per unit 37431 ft
Duty 189.17 MM BTU/h Installed surface area per unit 39165 ft
MTD 44 F Shells per unit 2 parallel
Corrected MTD 44 F

Performance of one unit

Description Shell Side Tube Side Units
Fluids Reactor feed Reactor effluent
Quantity: total 844035 884142 lb/h
liquid 139960 lb/h
gas 844035 844035 884142 744182 lb/h
Operating temperature 123 410 455 240 F
Operating pressure 1156 1121 psig
Pressure drop, max. allowable/calculated 1) / 5 / 5 psi
Liquid: molecular weight 30.2 lb/lbmol
density 43.26 lb/ft
viscosity 0.199 cP
specific heat capacity 0.83 BTU/lb/F
thermal conductivity 0.112 BTU/ft/h/F
boiling temperature F
Gas: molecular weight 9.25 9.25 12.19 10.97 lb/lbmol
density 1.67 1.12 1.38 1.62 lb/ft
viscosity 0.016 0.022 0.021 0.018 cP
specific heat capacity 0.78 0.78 0.68 0.71 BTU/lb/F
thermal conductivity 0.074 0.095 0.083 0.074 BTU/ft/h/F
dew point 276 F
Fouling resistance 0.0005 0.001 fthF/BTU
Film coefficient, refers to outside surface 332 284 BTU/ft/h/F
Heat transfer coefficients (clean/dirty) 139 / 115 BTU/ft/h/F
Mean metal temperature 293 313 F

Construction of one shell

Mechanical design temperature (min/max) 14 / 490 14 / 540 F
Mechanical design pressure (min/max) 2) / 1440 / 1440 psig
Test pressure psig
Number of passes per shell 1 1
Corrosion allowance 0 0 in
Design H2 partial pressure 1150 1150 psia
Insulation purpose Hot Hot
Design mean metal temperature F
Construction
Shell inner diameter (ID) 66 in Baffle type Disc and doughnut
Kettle inner diameter in Baffle cut orientation
No. of tubes 4400 Baffle spacing 17 in
Effective tube length 408 in Front end baffle spacing 17 in
Tube outer diameter (OD) 0.5 in Rear end baffle spacing 17 in
Tube inner diameter (ID) 0.37 in Outer baffle cut (of shell ID) 90 %
Tube pitch 0.813 in Inner baffle cut (of shell ID) 54 %
Tube pitch pattern Triangular Free outer baffle hole area 4.51 ft
Shell orientation Vertical Free inner baffle hole area 4.46 ft
Construction code ASME Sec. VIII Drain notch area in
Stress relieving According to code Tubes in outer baffle window
TEMA Class TEMA Class R Impingement plate (shell inlets) 3) Yes

Materials
Shell 4) SS304L Baffles/tube supports SS304
Tubes SS304L Front end head SS304L
Tubesheet SS304L Rear end head SS304L

Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
 Lake Charles Methanol, LLC Internal
Lake Charles Methanol Project copy
Document ID JYH 25-Jun-2015 08:57
5000 STPD grade AA Methanol Unit S-06030 P53002-E _D
Job no. Doc. no. Rev.
Page Item no.
2nd Feed effluent exchanger 3 of 5
09-E-0002 1/2

Nozzles and Connections

Ref. No. Size Description Nozzle Device
A1 1 20" Tube inlet
A2-3 2 14" Shell inlet
B1 1 20" Tube outlet
B2-3 2 14" Shell outlet

Remarks
1 Pressure loss in shell side nozzles included.
2 Design differential pressure shell/tube side: 140 psi.
3 Ring chamber impingement protection at shell side inlet and outlet.
4 Alternatively heads and shell in 1Cr Mo clad with SS304L.
5 Tubes shall be strength welded into tubesheet. Grooves shall be omitted.

L2 DC1 C2 ptrh 1854493

Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
 Lake Charles Methanol, LLC Internal
Lake Charles Methanol Project copy
Document ID JYH 25-Jun-2015 08:57
5000 STPD grade AA Methanol Unit S-06030 P53002-E _D
Job no. Doc. no. Rev.
Page Item no.
2nd Feed effluent exchanger 4 of 5
09-E-0002 1/2

Heating / Cooling Table

Tube side
Liquid heat Liquid thermal
Temperature Gas fraction Duty profile Liquid density Liquid viscosity capacity conductivity Surface tension
F wt % MM BTU/h lb/ft cP BTU/lb/F BTU/ft/h/F dyn/cm
240 84.17 0 43.26 0.199 0.83 0.112 14
251 87.98 -10.51 42.91 0.190 0.85 0.112 13
260 91.98 -21.02 42.59 0.182 0.86 0.112 13
269 96.15 -31.53 42.32 0.176 0.88 0.113 12
276 100.00 -40.96
315 100.00 -52.55
350 100.00 -63.06
385 100.00 -73.57
420 100.00 -84.08
455 100.00 -94.59

Gas heat Gas thermal

Temperature Gas fraction Duty profile Gas density Gas viscosity capacity conductivity
F wt % MM BTU/h lb/ft cP BTU/lb/F BTU/ft/h/F
240 84.17 0 1.62 0.018 0.71 0.074
251 87.98 -10.51 1.64 0.018 0.70 0.074
260 91.98 -21.02 1.67 0.018 0.69 0.073
269 96.15 -31.53 1.70 0.018 0.68 0.072
276 100.00 -40.96 1.73 0.018 0.68 0.071
315 100.00 -52.55 1.64 0.019 0.68 0.074
350 100.00 -63.06 1.56 0.019 0.68 0.076
385 100.00 -73.57 1.50 0.020 0.68 0.078
420 100.00 -84.08 1.44 0.021 0.68 0.081
455 100.00 -94.59 1.38 0.021 0.68 0.083

Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS