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Organic Syllabus 2
Organic Syllabus 2
Organic Syllabus 2
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GENERAL INFORMATION
MATERIALS
ATTENDANCE POLICIES
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worksheet and answer all post-lab questions; and (d) turn in your lab
report, which is based upon the lab work you performed this term as you
enter the lab at the next scheduled lab, which is usually the following
week.
You are allowed to attend only the laboratory section in which you are
registered. If you are absent from one of the scheduled experiments, you
are not allowed to make it up in a different section as you are not
permitted to attend a lab section in which you are not registered.
A student who misses a lab for a University approved reason (e.g. illness,
religious observance, participation in another University sanctioned activity,
death in the family, court appearance or jury duty, military duty, etc.) may
make up a grade for that lab by taking a make-up exam at the scheduled
time, as described on the ELMS page.
If a student knows s/he will miss a lab for religious observance, a
University sponsored activity, etc. it is his/her responsibility to notify
his/her TA BEFORE the absence, and to apply for the make-up exam.
If the University closes for inclement weather, or the department cancels a lab
for some reason, failure to perform that lab will not count against students
absence limit and they will not be required to take a make-up exam to
earn credit for it; rather, the missing grade will be replaced with an average
of the other lab grades. Students will be responsible for the material of
the missed exercise on any exams that are given.
IMPORTANT DATES
LABORATORY PREPARATION
To adequately prepare for each lab, you should read the background
material from the textbook prior to coming to the lab.
You will also write out a brief/bulleted procedure for the experiment that
you will be performing so that you dont have to hunt through the text for
what to do next. A copy of this pre-lab will be handed into your TA at
the beginning of the associated lab. It will be worth 2 points towards
your experiment grade.
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You will be given a brief, one question written pre-lab quiz at the
beginning of each lab period. This quiz will be worth 1 point towards your
experiment grade.
At the beginning of the day, after taking the quiz, your TA will give a brief
lecture pointing out experimental, waste, and safety considerations.
PRE-LAB QUIZZES
COURSE GRADES
The grade for each of the labs will be based upon the pre-lab quiz (both
electronic and in-lab), written lab report, and the post-lab questions. Each
lab is worth a total of 30 points (this includes the online quiz)with the
exception of the NMR workshop, which is worth 40 points, and the
unknown lab, which is worth 25 points. NO laboratory grade will be
dropped.
There will be one 20 point syllabus quiz that must be completed within
the first two weeks of the semester.
There will be one mid-term and one final exam, each of which is worth 75
points.
There will be a practical during the second to last full week of the
semester that is worth 50 points.
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The final course grade in CHEM 242 will be based upon the following:
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Once a lab report has been submitted to the teaching assistant, the
report cannot be returned to the student for further reconsideration,
reevaluation, or any sort of alteration. If a student removes his or her lab
report after turning it in, the student will receive a grade of incomplete
[No Grade for purposes of calculating final course grades] for that lab.
The student will not be allowed to sign up for and/or take that labs
makeup exam, that lab will count as one of the three
missed/uncompleted labs that a student is allowed and still remain in the
course, and the student will be referred to the Office of Student Conduct
as this is considering cheating since working on a report after it is
submitted is unauthorized.
If a student is absent from lab on the day that a lab report is due, that
student is required to turn the late lab report at the following lab period
s/he attends.
The graded lab report will only be returned to the individual who
submitted it.
If a lab cannot meet for any reason beyond the students control [for
example, the university closes due to snow], the lab report originally due
that day must be turned in with the aforementioned absentee/late lab
report policy (i.e. at the next lab period that the student attends). If the
university closes after the scheduled start time of the lab, you are still
required to have turned in your lab report due that day as you entered
the lab.
All students are required to write each of their lab reports individually
based upon lab work actually performed this semester. You should treat
the writing of a lab report, including the answering of the post-lab
questions, as a take-home examination.
Graded lab reports will be returned to the students at the next lab after
they were submitted.
If you feel that your lab report was not properly graded for some reason,
consult your lab TA first your lab TA is allowed to perform regrades in
accordance with the regulations below. If your lab TA cannot or will not
resolve the problem to your satisfaction, you can submit the report to Dr.
Friedman for a regrade. If you submit a lab report for a regrade, you
must follow and be aware of these guidelines.
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#1. You must submit the original lab report within one week after having
it returned to you. Any lab reports submitted after this one-week time
period will not be re-graded.
#2. Only lab reports and post-lab questions written totally in ink may be
considered for a regrade. A lab report and lab questions written totally or
in part [even the smallest part] in pencil may not be accepted for a
regrade. If a lab report is written in pencil then overwritten in ink [in part
or totally] it is not eligible to be regraded.
#3. If any part of a lab report and/or its associated post-lab questions is
obscured by using white out or any one of its equivalents, that lab report
will not be regraded under any circumstances.
#4. You must submit the lab report, the corresponding lab notebook data
sheet(s), the respective pre-lab quiz, and the post-lab question
responses.
#5. You must attach a separate sheet of paper stating what you believe
to be the problem with the original grading of the lab report and why you
want it re-graded. If you write on the original graded report, it will not
be regraded.
#6. Dr. Friedman or your TA may opt to regrade the entire lab report,
including the post-lab questions.
#7. As the result of a regrade, the score on the lab report can remain
unchanged from the original score, or it can increase or it can decrease
with respect to the original score.
#8. Lab regrades are final. There will be no regrades of a regraded lab
report.
MATH ERRORS
If there is a discrepancy between the overall grade for a lab and the
grades for the individual components [the pre-lab quiz, notebook pages,
report sheet, and the post-lab questions], bring this to the attention of
your lab TA or Dr. Friedman. You are expected to bring these math errors
to our attention within one week after the graded lab report is returned.
In these cases, the report will not be regraded but the grade recorded will
be corrected to reflect the correct actual score.
Students are required to have the following items to be admitted to the lab
at check-in and for each subsequent lab session:
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A bound laboratory notebook, with alternating carbon-copy tear out
pages; carbon paper if it is not provided with the laboratory notebook
A combination lock stamped CHEM to secure your lab drawer; they are
available at the University Book Center. No other type of lock is
permitted any other type of lock may be cut off your drawer. You will
be held financially responsible for the contents of the drawer while the
drawer remains unlocked.
Acceptable safety goggles
A lab coat
Shoes that cover the tops of the feet; sandals and open-toed shoes are
unacceptable; high heels are strongly discouraged.
Four (4) Chemistry Department breakage cards, which are available at
the cash registers at the University Book Center
A ball-point pen
A calculator
A brief pre-lab. This should be written in your lab notebook using carbon
copy paper prior to coming to lab. You will hand this in prior to doing the
days experiment.
LAB SAFETY
During the check-in process, students are expected to sign and submit a
Safety Contract and Policies and Procedures document (both on ELMS)
indicating that they have read, understood, and agree to follow the safety
rules and policies for the course.
All students must wear safety goggles or approved safety glasses any
time any student is either working on the experiment or cleaning up.
Wearing safety goggles means that the goggles are worn over the eyes or
over glasses. Wearing goggles does not mean on the forehead or on
top of the head or dangling from the neck.
If a student is observed even once not wearing his or her goggles over
the eyes, that student may be dismissed from the lab, even during the
first lab of the semester.
Students must wear their lab coat while in the laboratory performing
experiments.
Students must wear appropriate shoes in the laboratory. Sandals and
open-toed shoes are unacceptable; high heels are strongly discouraged.
Any act of unsafe behavior, including failure to wear safety goggles
whenever anyone is working in the lab, may result in dismissal from the
lab.
Students dismissed from the lab for safety violations or disruptive
behavior will not be eligible to take the make-up exam and can earn no
credit for that lab.
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In any case, dismissal from the lab counts toward the limit of three
missed and/or uncompleted labs.
The Department has instituted a formal three strikes policy, with the goal
of strictly enforcing rules regarding wearing personal protective equipment
(goggles/safety glasses, lab coats, pants, close toed shoes) during labs. Any
member of the Department of Chemistry and Biochemistry (Dr. Friedman,
any TA, any faculty member or stockroom personnel) are permitted to
record violations of rules relating to safety attire, which will count as
strikes.
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Safety rules must be followed from the moment that your TA tells you that
the lab activity is underway until you exit the lab (not until you finish your
experiment).
Please note that in all lab courses offered by the department, more than
three absences, for any reason (including dismissal from lab), results in a
grade of F for the course.
For most circumstances for missing a laboratory, you are allowed to apply
for and take the lab make-up exam for the lab that you missed. For
example, if you are absent from lab due to illness or for a religious
observance, you would be allowed to apply for the respective laboratory
makeup exam.
The laboratory makeup exam is NOT a substitute for the in-class
participation of conducting and performing the actual experiment, but
ONLY provides a grade for the excused absence. The makeup exams do
not take the place of or replace the missed lab; the missed lab still counts
toward the three that you are allowed to miss and still pass the course.
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In general, if you physically perform a laboratory, you are not allowed to
take the makeup exam for that particular lab.
Each lab makeup exam is worth the value of the respective missed lab.
If you do miss a lab, you need to apply to take the lab makeup exam. To
apply to take a lab make-up exam, go to the following link:
http://portal.chem.umd.edu/undergradoffice/. The link is also available
by going the ELMS page and clicking the Pages button in the left menu.
The lab make-up exams are given on Friday morning in CHM1402 from
7:15 7:45 a.m. You will have a maximum of 30 minutes to work the lab
make-up exams. Should you come to a lab makeup exam after the 7:15
a.m. start time you will have until 7:45 a.m. to complete the exam. If you
have signed up to take a lab make-up exam and do not take it [i.e. you
are a No Show], you will receive a grade of incomplete (i.e. zero) for
that lab. There are no make-ups for lab make-up exams.
NOTE: If you are in an SEF section, you will take your make-up exam
on Wednesday evening (prior to the Friday listed in the make-up exam
schedule). Contact Dr. Friedman via e-mail at the beginning of the week
of the make-up exam to arrange details.
Sign up for the make-up exams is as follows: You will normally have until
11:55 p.m. on the Monday of the week after the week after the lab you
miss to sign up for the make-up exam for the missed lab; put another
way, this refers to the second Monday after the last week that a lab is
done. For example, if you miss the lab during the week of February 6-10,
you have until 11:55 p.m. on February 20 to sign up for that make-up
exam.
Each lab make-up exam is closed-book. You are not permitted to use
your laboratory manual, laboratory notebook, lecture text, notes, etc. to
work a lab make-up exam. You are permitted and encouraged to bring a
calculator. You may not use a cell phone as a calculator.
CONTENT the content for the lab make-up exams will be similar to the
content of the pre-lab quizzes, the lab reports themselves, and the post-
lab questions. The questions can address any aspect of the lab you
missed: the equipment used to perform the experimental work,
calculations you would have performed to write the lab report or answer
the post-lab questions, the experimental techniques used in the lab,
underlying chemistry and theory, mechanisms, and reagents involved in
the experimental work [solvents, drying agents, catalysts, reactants, test
reagents, and products]; this is not an all-inclusive list.
You are strongly encouraged to bring a calculator to any and all lab
make-up examinations. If you do not bring a calculator to a lab make-up
exam, you will have to work any and all quantitative problems without
one. If you bring a calculator to a lab makeup exam and if it should
become non-functional for any reason, you will have to work any and all
quantitative problems without one.
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You are strongly advised to bring more than one functional writing
instrument to any and all laboratory makeup exams. If you bring a
writing instrument to a lab makeup exam and it becomes non-functional
for any reason, you will have to make do with the non-functional writing
instruments.
Cell phones All cell phones must be turned off during a lab makeup
exam. You may not use a cell phone as a calculator during a lab makeup
exam.
Proctors the proctor(s) are there to hand out the makeup exams and
then collect the completed lab makeup exams. The proctors will not
provide calculators, writing instruments, erasers, or scratch paper, etc. to
anyone taking a laboratory makeup exam.
NOTE: All students who are have previously submitted ADS
accommodations must make those needs known at that time you apply to
take a lab make-up examination via e-mail to Dr. Friedman.
The material covered in lab is fair game for inclusion on the mid-term
and/or final exam despite the fact that you may have taken a make-up
exam for one or more labs.
NOTE: You are responsible for the online 3-point quiz for all labs that
have them (everything except for the NMR assignment and the unknown
identity lab). Lab make-up exams will be out of 27 for all labs with an
online quiz.
CHECKOUT
Once you have checked into a laboratory section, you must check out
when you leave (i.e. drop the course, change sections, or complete the
course at the end of the semester). If you change sections or drop the
lab before the drop/add date, you must check out of your original drawer
as soon as possible so a new student can use that drawer. If you drop the
lab after the drop/add date, you may check out at any time during the
semester at the regular lab time, but sooner is preferred. All students
completing the course must check out during check-out week at your
regular lab time.
If you have checked into a laboratory section but fail to check out, your
TA will check you out and any expenses for missing, damaged, or
excessively dirty glassware or equipment will be charged to your student
account.
EXAMS
You will be given two written, 75-point exams during the semester. One
of these exams is the final exam. If you require ADS accommodations,
you must make your request known before the mid-term is given. The
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exams will be multiple choice and short answer examinations that
may/will cover any or all experiments [pre-lab quizzes, lab reports, post-
lab questions, techniques, equipment, etc.] done up to that point in time.
ADS accommodations must be presented to Dr. Friedman. Failure to
discuss ADS accommodations with only your TA and not with Dr.
Friedman will result in you not receiving accommodations.
The exams will consist of multiple choice and short answer questions
involving providing numerical values (e.g. masses, moles) or structures.
The final exam will occur on December 13th and will be a fifty minute
exam. The time and location of the final exam will be communicated via
ELMS by Dr. Friedman and will be posted on ELMS when they are known.
There is also a lab practical that will be administered during the week of
November 27th. Information regarding content/format will be
posted/announced during the semester.
Only university-excused absences will be accepted for missed exams.
Proper documentation is expected. As exams qualify as major grading
events (University policy V-1.00(G)), self-signed notes from the Health
Center page will not be accepted as documentation for an excused
absence. You must contact me within 24 hours of the missed exam.
Failure to meet these requirements will result in a ZERO for the missed
exam.
If any student needs ADS accommodation, you must bring your written
documentation to Dr. Friedman as early as possible in the semester.
Dr. Friedman will discuss appropriate accommodations with you and will
notify your TA of any accommodations that need to be made.
Discussing and presenting your ADS accommodations to only your TA will
result in you not receiving accommodations for exams. To receive ADS
accommodations on exams, you must meet with Dr. Friedman in person
as close to the beginning of the semester as possible.
Should you need accommodations for a lab makeup exam, indicate your
accommodations when filling out the online form and follow up by e-
mailing Dr. Friedman.
Accessability and Disability Service contact information is as follows:
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TA OFFICE HOURS
Students are expected to sign the Honor Pledge, which appears on each
lab report, as well as on each exam. Any evidence of academic
dishonesty found by a TA or grader and reported to Dr. Friedman will be
pursued by the Department: examples include, but are not limited to (a)
fabrication of data (defined by the Code of Academic Integrity as
intentional and unauthorized falsification or invention of any
informationin an academic exercise); (b) use of data other than that
submitted to the TA; (c) unauthorized collusion with others including, but
not limited to, communal calculation of experimental results and copying
of pre-lab and post-lab exercises from another student; (d) plagiarism.
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What is permissible:
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