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Practica de Viscosidad-1
Practica de Viscosidad-1
Viscosity.
Ostwald Viscosimeter
and Falling-Ball Methods.
RE FERENCES :
PURPOSE:
62
63
Experi ment 5
f;SCUSSION:
mobile
is a familiar one'' Lessn';i'L?r,,...r,
The general concept of. viscosity
H
:? iI u''i Il
3" I ',i? " :" : i:l? t ^?3:*B: "
1 iiu$",l.:=[**#ndx*1ir*fl;l::""'-'
;;-e-ostward Procedure :
il;ilHi"
(r)
A-bulb, 2 ml =- n r4pt
30 cm B - coPi llorY " 8v,[
C - glos rod io
Provide ri glditY pressure on the
in which p is the hydrostatic
tr'" "t'=itv) ' t isof the
i)
\
liquid (p,opoti;;";i-; tft" radius
time of flow lt-totds'- r i" the capillary'
'
\
theabsoluteviscositycanbecalculated,theusualprocedurels.-:
minetheviscosityrelativeto-"referenc"-=.,=t.nceataSelec."e]--:
ture.Thisi=-li*.dthe'"Iti,"viscosit}.tr{aterat25oCis:S.':''
,-,="a ." the reference liquid'
Toobtaintherefative.viscosityof-asubstanceatagiven--=:-;
ft""ti* temperature a:-*
f flow at thatwater
it is necessary to measure
same.1"l*" of in a in the sa::=
if*I;;-;l;; for the
-iir,." *.-pi.==,tt or'liq"id viscosime--::
corresponding :
cosimerer ar 2;;a: i;";;;-a"''=itv' nd since the terr:'s t::--
rhe rype used'i=-proportionjl it. follows
iot.noi'i-"ia= equation:
'
and !. in eguarion- (rl are .rr
"*" ny-tr'e foltowing
ratio of the viscosrties i"'iii'"
nt dttt
rt2 =
ry;
rf substance 2 is-the
i unitv' rhen :"f?:"::i.li:i:3'
nI 1".:^"t,t\";:*":lo}'=ffi:i:ii[i:x^j?=tflq^Frt,'-1
;i;;-;;" equation Q) tc : :::;
: :
""r".
lli"hE.:i:t,t:T";"i:"15'i? #l''Iin!?l';;;-'; i ive t tr'e vis c -
"t
of water at 25"C'
Oncetherefativeviscosityisknown'theabsoluteviscosityca: tr'" substance b'' :
calcutared v *rrliptyl:g^t;:';riiv-"i;"=itv*i
ii=."=ity of water at 25"c'
iiq"i='
Theostwaldprocedure.isnotsuitableforthedeterminationa".-,': + p'ocedure o:=-:
viscosity of hishrv -t'19
*?9;;";;iv "isto's '
rhis consists ir' :-:
used for such rqu-ias is tr,'?iii"n-otrr'*i"'- densirv to rall ---:
minins the tim';;;;"-.lv-;;.';-;i.uir-u.rr'"i"x""*',
i"'i;";;;;""iiq"i and in the lisu:-: '
a fixed disrance in. "orro,ii'o?
viscositY we wish to measure '
is quite. wrLrr tlvuv;;iit than the radius o: --:
nreci3l-*l:n-T:*":::il'"'"i3i"?nl'?I13;
quite- precrse
rhe method is
The
iie ":=:.:
iarrins
-rh; reference
.o" Iiquid ::-:
iix##t;:l1H"i::'.il::: !? ? -Ll;-;;;;.,"
cused by rhe ,=;ri;--.1tio,',lr;-;rii.r.v"'ll iyt"'it' or castor oiI ma'{=:
of course, i..rl=l'ra',"r-f.,igh..i"cosity-'
reference substance'
;;-;;iractrv viscosity bi- --
of relative
The formula used for the
determination
f af f-ini-ball method
follows:
n1 (ds - dr) tr (i
nz (ds - d2) L2
there-
rot ' good resultsmethod
fheeffectoftemperaturechangeonviscosityispronounced,the
*itrr- a"*j.traue -incr"t=t ' '
viscosity a".rIr"ir.,g ;[;;""a tr'"=ii'ar vicosimeter
rore, both tn"=?iiii":rrra constant temperature'
must be carrred ut at Relative viscosity is
viscosity i= t13 poise'
The absolute unit 9f- i= mt'"iv a ratio'
not expressed ii-"'v-"it' "i;;;-it
CHEMICALS:
APPARATUS AND
stoP watch; tube
baths ;'"Lr,"i
constant-temperature or serected
Ostwald viscosimeter; s-7)
t=t""niiure La:'I'methanol
;' caliPeri iron
for f alling-nuii-iir'a
ri-qui"'''-'---i'''' -stual"Jitl-
bearinss ; ";;;;;,
liquid ort"o tilip=i t'=tor oit; glyceror'
supports
:
EXPERI MENTAL PROCEDURE
i :
I
rt' i: ""ttssary
' tto-tr'tt'-t tr't \ I
ments using-*"ir'''of
to use . "o't'*E":ti:;i \ I I ..i
I rr""." substance ' \ l-.:X-H'fJ
Fal l'i nq-Bal I Method
shown in Figure P;.duY'e 5-2'
-'
Note tha! the tube
300 mT'rons and 32
5-2 is approxrmirv two markings on the Falling-bal1 v:iscosimeter'
mm in diameter':*-T
66 Laboratory flanua I
UTILIZATION OF DATA:
and y = *I .-ZlO.l
viscosity of glyc=::-
use this information to calculate Lhe absolute grlmI
of- O'950 may be used ::
at 35oc. For castor oil the value ?35oC =
thecalculationofitsviscosityatthrstemperaEure.
,/