Professional Documents
Culture Documents
Internship Report 2010
Internship Report 2010
Internship Report 2010
P REPORT
2010
BERGER PAINTS ,
PAKISTAN
INTERNSHIP REPORT
FOR
BERGER PAINTS PRIVATE LIMITED
28-KM MULTAN ROAD, LAHORE
SUBMITTED BY
MEER SALMAN MUDDASAR
07-CHEM-53
DEDICATION
THIS EFFORT IS DEDICATED TO THE NATION OF
PAKISTAN; COMPRISING FLOOD VICTIMS
ESPECIALLY, PAKISTAN ARMED FORCES, AND
WELL WISHERS OF MOTHERLAND.
CONTENTS
AUTHORIZATION....................................................................................................................................7
ACKNOWLEDGEMENT...........................................................................................................................8
EXECUTIVE SUMMARY.........................................................................................................................9
HISTORY OF ORGANISATION.............................................................................................................10
MISSION STATEMENT..........................................................................................................................14
ORGANIZATIONAL CHART.................................................................................................................15
DEPARTMENTS COVERED IN REPORT.............................................................................................16
PAINT.......................................................................................................................................................18
BERGER PRODUCTS & COSTUMERS.................................................................................................24
ENVIRONMENT AND HEALTH SAFETY............................................................................................29
TECHNICAL / QUALITY CONTROL....................................................................................................33
MACHINE ROOM...................................................................................................................................35
RESINS.....................................................................................................................................................38
IS THERE NEED OF IMPROVEMENT???.............................................................................................47
POWDER COATING...............................................................................................................................49
POWDER COATING LABORATORY...................................................................................................55
PRINTING INK........................................................................................................................................57
BERDEX AND INDUSTRIAL CHEMICALS.........................................................................................87
A TOTAL SOLUTION COMPANY.........................................................................................................87
MAINTENANCE ENGINEERING DEPARTMENT...............................................................................94
PRODUCTION DEPARTMENT..............................................................................................................96
AUTOMOBILE PRODUCTION..............................................................................................................99
CONCLUSIONS.....................................................................................................................................103
AUTHORIZATION
ACKNOWLEDGEMENT
A summer project is a golden opportunity for learning and self
development. I consider myself very lucky and honored to have so
many wonderful people lead me through in completion of this
internship and report.
My grateful thanks to all of the TECHNICALS, ENGINEERS
AND OPERATORS who in spite of being extraordinary busy with
their duties, took time out to bear, guide me and keep me on the
correct path. I don`t know where would I have been without them. A
humble “thank you” to all of them.
MR.WAQAS ASHRAF , HR Department monitored my progress
and arranged all facilities to make my life easier. I choose this
moment to acknowledge his contribution gratefully.
I would like to thanks MR.SHAHID NAVEED,OUR WORTHY
CHAIRMAN (CHEMICAL ENGINEERING DEPARTMENT) for
his effort and help provided me to get such an excellent opportunity.
I would like to thanks OFFICERS MESS STAFF for such a
delicious meal they provided.
Last but not the least there were so many who shared valuable
information that helped me in the successful completion of this
internship.
EXECUTIVE SUMMARY
HISTORY OF ORGANISATION
1932. The opening of Sydney Harbour Bridge was a proud moment for Berger.
Berger had supplied 60,000 gallons of paint to protect the bridge steelwork, thus
providing work for many hundreds during the Great Depression.
In 1974, 51.4% of Australians chose Advance Australia Fair as the national anthem
to supersede God Save the Queen. In the same year, the company changed its name
from Lewis Berger & Sons to Berger Paints.
In September 1988 Berger Paints was acquired by Dulux Australia. This provided
a sound base for the future by giving Berger access to the very best worldwide
resources for research, technology and marketing.
In the 1990's Berger was relaunched in Australia with the 'Made with People in
Mind' proposition, reflecting Berger's deliberate consideration of the human
sensitivities when painting.
2003 Berger revisits its famous 'Keeps on keeping on' proposition and continues to
deliver honest results.
For 88 years it's been said that Berger 'Keeps on keeping on', so now, backed by
this history, you can look forward to a future of continued reliability and trust.
paint industry. This collaboration has enabled BERGER to develop automotive and
industrial paints conforming to exacting international standards.
BERGER Paints has also built up technical collaboration for decorative paints with
BERGER Crown of Akzo Nobel UK.
With its Head Office at Karachi, BERGER PAINTS PAKISTAN has regional
offices at Lahore and Islamabad as well as a wide network of distributors/
dealers and sales personnel at all major urban centers of the country.
BERGER paints launched its second paint manufacturing facility in 2006 located
in Lahore, this is a state-of-the-art plant geared to incorporate the latest
technologies to produce paints and coatings for a variety of applications.
MISSION STATEMENT
EHS
TECHNICAL/QUALITY CONTROL
RESIN/PVA
POWDER COATING
DECORATIVE PRODUCTION
MAINTENANCE ENGINEERING
PAINT
FROM A LAYMAN POINT OF VIEW IT IS SIMPLE A “ COATING MATERIAL”
TECHNICALLY DEFINED AS
“Paint is any liquid, liquefiable, or mastic composition which after application to
a substrate in a thin layer is converted to an opaque solid film”
COMPONENTS OF PAINTS:
PIGMENT
BINDER
SOLVENT
ADDITIVE
Pigment
Binder or vehicle
The binder, commonly referred to as the vehicle, is the actual film forming
component of paint. It is the only component that must be present; other
components listed below are included optionally, depending on the desired
properties of the cured film.
The binder imparts adhesion, binds the pigments together, and strongly influences
such properties as gloss potential, exterior durability, flexibility, and toughness.
Note that drying and curing are two different processes. Drying generally refers
to evaporation of the solvent or thinner whereas curing refers to
polymerization of the binder. The term "vehicle" is industrial jargon which is
used inconsistently, sometimes to refer to the solvent and sometimes to refer to the
binder. Depending on chemistry and composition, any particular paint may
undergo either, or both processes. Thus, there are paints that dry only, those that
dry then cure, and those that do not depend on drying for curing.
Paints that cure by oxidative cross linking are generally single package coatings
that when applied, the exposure to oxygen in the air starts a process that cross links
and polymerizes the binder component. Classic alkyd enamels would fall into this
category. Oxidative cure coatings are catalyzed by metal complex driers such
as cobalt naphthenate.
Paints that cure by catalyzed polymerization are generally two package coatings
that polymerize by way of a chemical reaction initiated by mixing resin and
hardener, and which cure by forming a hard plastic structure. Depending on
composition they may need to dry first, by evaporation of solvent. Classic two
package epoxies or polyurethanes would fall into this category.
Solvent
The main purposes of the solvent are to adjust the curing properties
and viscosity of the paint. It is volatile and does not become part of the paint film.
It also controls flow and application properties, and affects the stability of the paint
while in liquid state. Its main function is as the carrier for the non volatile
components. In order to spread heavier oils (i.e. linseed) as in oil-based interior
house paint, a thinner oil is required. These volatile substances impart their
properties temporarily—once the solvent has evaporated or disintegrated, the
remaining paint is fixed to the surface.
Water is the main diluent for water-borne paints.
Solvent-borne, also called oil-based, paints can have various combinations of
solvents as the diluent, including aliphatics , aromatics ,alcohols, ketones
and white spirit. These include organic solvents such as petroleum
distillate, esters, glycol ethers, and the like. Sometimes volatile low-molecular
weight synthetic resins also serve as diluents. Such solvents are used when water
resistance, grease resistance, or similar properties are desired.
Additives
Besides the three main categories of ingredients, paint can have a wide variety of
miscellaneous additives, which are usually added in very small amounts and yet
give a very significant effect on the product. Some examples include additives to
modify surface tension, improve flow properties, improve the finished appearance,
increase wet edge, improve pigment stability, impart antifreeze properties, control
foaming, control skinning, etc. Other types of additives include catalysts,
thickeners, stabilizers, emulsifiers, texturisers, adhesion promoters, UV stabilizers,
flatteners (de-glossing agents), biocides to fight bacterial growth, and the like.
Additives normally do not significantly alter the percentages of individual
components in a formulation.
Container Div.
Orders (Tins)
Production Filling
Planning (1 day)
Tanks Pots
(Large Batch) (Small Batch)
Store Ink Jet
(Raw Material) Printing
NOTE: The daily deviations are also reported to all the departments as any
new extra or out of ordinary orders are placed.
QUALITY CHECK (Q.C): the quality of the product is checked in all terms
and respects including colour, shine, bonding, base material, drying
procedures, drying time etc.
FILING: The Orders for the filling packs or tins are given at the time when
production Schedule is made, so by the time manufacturing is completed the
empty packs and tins are ready and available from the supplier.
NOTE: Filing of Industrial Products of 2000 – 5000 litres takes one day.
And filling of Decorative products of 2000 – 8000 litres a day.
PRINTING: Ink Jet printing is used to print each tin or packets. A single
packet or tin takes 1 min for printing.
STORING: all the finished goods after packing and printing are stored in the
warehouse which is situated within the premises of Berger Pakistan S.I.T.E.
WATER BASE
• PLASTIC EMULSION
• ECONOMY EMULSION
OIL BASE
• BERGER ELEGANT
• BERGER ENAMEL
2 AUTOMOTIVE PAINTS
3 POWDER PAINTS
7 PRINTING INKS
CARS ASSEMBLERS
• HONDA.
• TOYOTA.
• CHEVROLET JOY.
• REVO.
COMMERCIAL VEHICLES
• ZABARDAST, TRUCK.
• MASTER TRUCK.
• STAR TRUCK.
• KALASH PICK-UP.
• HINO BUSES.
MOTORCYCLES:
• HONDA.
• YAMAHA.
• SUZUKI.
• 25 CHINESE BRANDS.
TRACTORS:
FIAT TRACTORS.
SUNIVERSAL TRACTORS.
SINGER.
PHILIPS.
SIEMENS.
PAK FAN.
PSO.
PBS.
CALTEX.
KSB PUMPS.
NATIONAL REFINERY.
POWDER PAINTS:
• MOTORWAY.
• KOHAT TUNNEL.
• DHA, KARACHI.
• SHAHBAZ AIRFIELD.
• BAHRIA TOWN.
SPECIALIZED PAINTS FOR ARMY, NAVY, AIR FORCE, SHIPYARD AND FISH
HARBOUR.
UNIT # 01
1. Environmental
Environment
Occupational Health and Safety
Community Health and Safety
After fire incident of BERGER in 2008, think tanks are looking to accommodate
EHS at there maximum , so that further incidents can be made avoided. So far
people in EHS are focusing in following aspects.
FIRE: If fire ignites there are fire points where quick response team defined for each department from workers
that are trained, have to get there and launch fire extinguishing plan, as decided.
ADDICTION TO FUMES: Paint have a very strong relations with volatility ; since almost chemicals are
found fuming and INHALATION of chemicals produce addict people those feels suffocations if they don’t inhale
these chemicals regularly. So department is found showing keen interest in rectifying this problem.
SKIN PROBLEMS AND IRRITATION: Few chemicals including caustic soda used for cleaning ,
cause skin problems and irritation among people ; causing itching , and irritations.
SLIPPAGE: due to leakage of chemical , and lubricants ; there are slippage problems in plant sites that may
cause serious accidents by chance. EHS is trying to point out these sort of imperfections and rectify them.
EYE CONTACT: If contact is made with the eyes, then hold your eyes open and flood them with luke warm
water for at least 5 minutes and then immediately consult a doctor.
IF SWALLOWED: Do not induce vomiting. Drink plenty of water and seek immediate medical help.
UNIT # 02
E Extenders
P Pigments
R Resins
O Oils
X,Y,Z Chemicals
H Dryers
C Cellulose
W Wax
S Solvents
MACHINE ROOM
Machine room is a sort of pilot plant where R & D work is carried out.
Room contains HSD (high speed dispersers) ,and iterators that are used for
pigment size reduction, and to produce mixing as well; here is a detail of all
equipments;
UNIT # 03
RESINS
Resin is a natural or synthetic compound which begins in a highly viscous state
and hardens with treatment. Typically, resin is soluble in alcohol, but not in water.
There are a number of different classes of resin, depending on
exact chemical composition and potential uses. There are numerous applications
for resins, ranging from art to polymer production, and many consumers interact
with products which contain resin on a daily basis.
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BASIC CHEMISTRY
CONDENSATION POLYMERISATION OIL BASED (ALKYD RESIN)
ADDITION POLYMERISATION
CO-POLYMERISATION WATER BASED
ADDITION POLYMERIZATION
CO POLYMERIZATION
FIRED HEATER
REACTOR TANK
PROCESS
Set heater put 500Kg water in it along with chemical A 6 bags (6*25) at 70 0C; with
this addition heat jumps to 82-83 0C, and keep in hold for 2 hours. put monomer on
above tank using air diaphragm pump to pump monomer ingredients into tank so
that It may not catch fire. Chemical B added on kettle reactor tank and first stage is
started. STAGE ONE; Catalyst C is added gradually in small amount and hang on
till all of the catalyst is added. After 5 min hold, start STAGE TWO , monomer
takes 4-4.5 hours to completely added to tank while heat jumps to 90 0C. start
cooling and add chemical D,E,F in formulated amount. This is the finished GLUE ,
which is filtered and packed in pouch of 0.5, 1 Kg size.
Alkyd coatings are typically sold in three classes; Long, Medium, and Short. These
terms represent the relative fraction of drying oil component in the resin. Long oil
alkyds have a high percentage of drying oil content and are generally sold as
medium duty coatings for the consumer market. Medium oil alkyds have less
drying oil and have a higher percentage of large molecular weight polyester
backbone. They dry slower and are employed as high gloss coatings and wood
finishes. At the bottom end are short oil alkyds where the percentage of drying oil
is very low in relation to the base polyester polymer or backbone chain. These
coatings will not air dry or harden unless heated. Short oil alkyds are employed as
baking enamels for finished metal products.
Because the major components of an alkyd coating, i.e. fatty acids and triglyceride
oils, are derived from low cost renewable resources this has kept the cost of alkyd
coatings very low despite ever increasing cost of petroleum which is the
predominant raw material source of most other coatings such
as vinyls, acrylics, epoxies, and polyurethanes. Typical sources of drying oils for
alkyd coatings are sunflower oil , safflower oil, walnut oil, soybean oil, fish
oil, corn oil, and tall oil (resinous oil by-product from pulp and paper
manufacturing).
Unit contains kettle reactors along with condenser and monomer tank , and
separate vertical condenser. Except a kettle that is used for research purpose with
capacity 700-800 Kg is provided with separate catalyst tank, all other tanks don’t
not require catalyst tank and all the ingredients are poured directly into the tank.
Reaction temperature is 280 0C to carry out reaction, and to carry out reaction at
such an elevated temperature e series of 3 fired heaters are available that uses
thermal oil as an heating media. Few words on thermal oil are as follow, under.
Thermal oils are available in a wide range of specifications to suit the needs of
various processes. Currently available thermal oils have a maximum temperature
limit of around 400 °C. There are thermal oils that are in use in cryogenic fields up
to -100 °C
Thermal oil heaters functionally are similar to steam boilers. The combustion
chamber that burns fuel oil, bio fuel, coal or any other fuel with all necessary
safety devices is the same. Since there is, no evaporation the oil passes through
simple heater coils placed in the radiant or convection zones. The oil pumped
through these coils heats up and flows to the process heat exchanger. The cooler oil
returns to a tank and then back to the pump. An expansion tank takes care of the
thermal expansion. The tanks have provisions to
prevent the oxidation and vaporization of the oil.
In this time of energy crisis , world is facing a real hawk of energy, but oil based
resin plant play a game show of energy wastage.
Cooled water that is used to cool kettles reactor containing internal jackets
coil release cooling media in form of steam mean at temperature nearby 100-
110 0C. it is found that this stream from kettle is directly wasted.
Stack tower was found releasing flue gases at temperature about 100 0C. If it
is paid attention this energy can be made useful, and plays an important role
in reducing the energy consumptions of plant.
Since plant contains burners running on natural gas; and heating thermal oil
as heating media. Its found that valves joining headers that contains rubber
gas kits, but thermal oil from burner is almost at 280 0C causing rubber made
gaskits to melt and produce slippage and loss in strength of thermal oil, since
highly flammable chemicals producing dense volatile vapors are observed
around, that are waiting for flash of fire. So it is advised to immediately take
action in rectifying the risk of catching fire and setting life of workers to
high risk.
In resins water based section packing of berlith glue is carried out using
pneumatic machine, and it is found that machine was causing mis weight
age. Its filling section was injection random weight jet of glue in pouch and
remarkable difference in weight of bag pouch was observed, that should be
rectified to maintain standards of BERGER.
UNIT # 04
POWDER COATING
WHAT IS POWDER COATING + BRIEF HISTORY…
Powder coating is the technique of applying dry paint to a part. The final cured
coating is the same as a 2-pack wet paint. In normal wet painting such as house
paints, the solids are in suspension in a liquid carrier, which must evaporate before
the solid paint coating is produced.
In powder coating, the powdered paint may be applied by either of two techniques.
The item is lowered into a fluidised bed of the powder, which may or may
not be electrostatically charged, or
The powdered paint is electrostatically charged and sprayed onto the part.
The part is then placed in an oven and the powder particles melt and coalesce to
form a continuous film.
There are two main types of powder available to the surface finisher:
Aluminum coating
M-S
Pak Fans
Geysers
PEL
GFC fan
Royal fan
Pak fan
PRODUCT RANGE;
For the production of all of the above range the procedure of process is same, as
quoted below.
ELECTROSTATIC CHARGING;
Powdery material is filled in electrostatic gun and sprayed over charged metal
sheet. Afterward it is heated to 200 0C till melted , taking 10-15 min, powder
coated metal sheet is ready.
PRODUCTION UNIT
LABORATORY
PRODUCTION UNIT;
Unit consists of 6 regular extruding machines three AVMz and 4 mixers. Material to
be produced in ; is charged in mixers, which are actually mixer tumblers , a tumble of
mixer charged is moved into extruder feeding duct. A screw driven motor moves
powdery charge in extruder ,. Where two rollers provided with internal cooling coils
are used to cool down the charge , making paste type material to solid. Before getting
into rollers , material had to pass through heating coils, which melts down material
turning into paste. It contains three different tooth screw rollers. Material comes out of
rollers as plain sheet form heated due to screws and provide heat. Over conveyer
where chilled water via convectional cools metal surface , reduces temperature of
sheet further. Conveyor leads material into crusher (toothed) running at opposite pace,
making chips out of it.
Since material undergo screwing , its temperature enhances that tends to melt material
and cooling produce material in chips form.
System is made vacuum via centrifugal blower running at its anti chips are lifted
manually , which are transported from extruder to crushed via ho cart. Material is
taken upward and passed through a cyclone , where classification into three categories
take place, Coarse , fine , standard.
Fines are passed up (since light) and filtered via provided filter arrangement , and
stored. Coarse are separated from bottom side end of cyclone. Particles of required
size passes test of passing through sieve of required , size. product is collected and
bagged.
NOTE; A product 326-MATT was reversed by costumer during my stay over unit.
Since it was not weight properly as mentioned . 35 Kg out of total was missing,
this was because a temporary sort of seal packing used here.
Humidity control is necessary , since its excess cause powder to deposit or form
lump. So , its temperature is controlled , so that gave control floor temperature.
Aerosols or Al2O3 is added along charge in ACM, cause moisture absorbent and
remove water out.
MOISTURE METER
REFLECTO METER
CONICAL MANDREL
SPRAY BOOTH
HEATER
COFFEE GRINDER
UNIT # 05
PRINTING INK
Printing is widely used in our society to pass on information and to decorate
objects. This has resulted in printing being used on many different surfaces ranging
from aluminum cans and plastic bottles through to paper. Different inks have been
developed for use in these different situations.
Printing ink was invented by the Chinese about 300 years later. They used a
mixture of colored earth, soot and plant matter for pigments, again mixed with
gums for binder. By 1440, when Johannes Guttenberg invented the first printing
press with moveable type, ink was made of soot bound either linseed oil or varnish
similar materials to those used for black inks today. Coloured inks were introduced
in 1772 and drying agents were first used in the nineteenth century.
1) Liquids
2) Pastes
These types are further classified into subclasses according to the printing process.
The composition of printing ink and its physical properties are determined greatly
by the nature of the printing process used to transfer an image from the printing
surface to substrate.
1) Letterpress
2) Flexography
3) Gravure
4) Offset
5) Screen Printing
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Flexography:
DESCRIPTION
Flexography is a printing process which utilizes a flexible relief plate that can be
adhered to a printing cylinder. It can be used for printing on almost any type of
substrate including plastic, metallic films, cellophane, and paper. It is widely used
for printing on the non-porous substrates required for various types of food
packaging. It is also well suited for printing large areas of solid color.
APPLICATIONS
PRINTING PROCESS:
The relief plate used for flexography is made of molded rubber or photopolymer
materials with the image areas raised above the non-image areas of the plate.
of ink to the plate. The number of cells per linear inch can vary according to the
type of print job and the quality required.
The name "anilox" is derived from the ink that was used for the process until the
1950's. Anilox ink was manufactured with "aniline" dyes which, in the 1950's,
were discovered to be health hazards, so pigment based inks were developed and
have been used ever since. The ink carrying roller has continued to be called the
"anilox roller" even though the aniline dye inks are no longer used for flexography.
The current inks are very fluid and dry rapidly and are most often water based.
Gravure:
APPLICATIONS
There are also many specialty items that are created with rotogravure including gift
wrap, wallpaper, plastic laminates, printed upholstery, imitation wood grain
finishes, and vinyl flooring. Many of the specialty items are printed on very wide
presses. Some of them, such as those that print patterns on floor coverings, are up
to 150 inches wide.
A gravure sheet-fed process is used for smaller runs for such items as limited
edition prints and other artwork, photographic books, high denomination postage
stamps, stock certificates, and some advertising pieces.
PRINTING PROCESS
chromium begins to wear, it is removed from the cylinder and a new coating is
applied.
During the printing process, the gravure cylinder revolves in an ink fountain where
it is coated with a very fluid ink. A stainless steel blade (doctor blade) clears the
ink from the unwanted areas, leaving the ink in the depressions of the cylinder. The
substrate passes between the gravure cylinder and an impression cylinder covered
in rubber. The substrate passes between the two cylinders and the ink from the
cells is deposited onto the substrate.
Besides being very thin and fluid, the ink colors used with process color
applications differ in hue than the inks used with other processes. Instead of the
usual cyan, magenta, yellow, and black used with offset lithography, blue, red,
yellow, and black are used. Standards have been established by the Gravure
Association of America for the correct ink types and colors that should be used for
different types of substrates and printing applications.
1. Weighting Balance
Pots are used as a storage tank during the production of ink. All the raw material is
added to the pot which leaves the pot only when the product is formed whether it is
varnish or ink.
Mixing is applied to the process to reduce the degree of Non-uniformity and make
viscosity of the raw material constant throughout the solvent. Mechanical agitation
is used for mixing of suspended in liquid. High speed disperser (HSD) is being
used for this purpose.
Construction:
MIXING MECHANISM
As the solution formed is of low viscosity the bulk flow pattern in mixing vessel
is turbulent. Fluid undergoes shear when one area of fluid travels with a different
velocity relative to an adjacent area. The velocity, or tip speed of the fluid at the
outside diameter of the rotor will be higher than the velocity at the centre of the
rotor, and it is this that creates shear.
The inertia imparted by the liquid by the rotating impeller is
sufficient to cause the liquid to circulate throughout the vessel and return to the
impeller. Turbulent eddy diffusion takes place throughout the vessel but is
maximum in the vicinity of the impeller. Eddy diffusion is inherently much faster
than molecular diffusion and consequently turbulent mixing occurs much more
rapidly than laminar mixing. Ultimately homogenization at the molecular level
depends on the molecular diffusion which takes place more rapidly in low viscous
liquids.
FLOW PATTERN:
The impeller creates an axial flow which is upward. Circulation pattern like these
are useful in avoiding dead zone.
TIME OF MIXING
High shear mixers are used in industry to produce standard mixtures of ingredients
that do not naturally mix. When the total fluid is composed of two or more liquids,
the final result is an emulsion.
To achieve a standard mix, the technique of equilibrium mixing is used. A target
characteristic is identified, such that once the mixed product has acquired that
characteristic, it will not change significantly thereafter, no matter how long the
product is processed. For dispersions, this is the equilibrium particle size. For
emulsions, it is the equilibrium droplet size. The amount of mixing required to
achieve equilibrium mixing is measured in tank turnover - the number of times the
volume of material must pass through the high shear zone.
DYNA MILL:
Dyna Mill is a type of ball mill and consists of following parts
1. Grinding Cylinder
2. Water Jacket
3. Air filtration
4. Mechanical Seal lubrication feed tank
5. Grinding medium
6. Agitator disc
Grinding Cylinder:
Dyna mill consist of a hollow cylinder, partially filled with balls, with is at
horizontal axis. The material to be fed is in through a hollow trunnion at one end
and the product leaves through a similar trunnion at one end and the product leaves
through a small trunnion at the other end. The outlet is normally covered with a
coarse screen to prevent the escape of the balls.
Agitator disc:
Agitator disc are used for agitation of the feed. Six agitator disc are
used for this purpose which rotate due to the movement of the shaft and the
material is agitated.
Water jacket:
Grinding chamber is manufactured with a water space around the
areas that will receive most heat. This is known as water jacket. The water jacket
surrounds the cylinders of the machine, the grinding chamber, and the cooling
copper coil in the Mechanical seal lubrication tank.
The inlet of cooling water is located at the bottom of the grinding cylinder and the
outlet at the top. The cooling water has the important task of cooling the grinding
chamber, where the water jacket surrounds the grinding chamber will indirectly
cooling the grinding material, and reduce the wear inside the grinding chamber due
to heating. Water is taken from the chiller which is circulated through the water
jacket and is later returned to the chiller about 800-1500 liter per hour water is
circulated through the water jacket with a pressure of 6 kg/s.
Air Filter :( Compressed air lubrication)
Air to be used for centrifugal pump which is used for the pumping of
paste is filtered first by passing it through compressed air lubrication solution to
remove any dust particles that may the machine and disturb our product.
Rising Circulation tank for Mechanical Seal Lubrication Fluid Tank:(Main
shaft sealing)
Mechanical Seal Lubrication tank contains the lubricating oil which is used for the
cooing of the seal. The shaft seal of the mill has one set lubricating Mechanical
seal and Lip seal. The lubricating liquid is circulated at the flow rate of 10-30
Liters/Hour. When machine runs the circulation fluid begins to flow through the
machine sealing system. Lubricating oil perform two-fold duties of lubricating and
cooling. Types of lubricating oil being used are
For water based: Mixture of water and Glycol
For Solvent base: Butyl Cellusolve
For Oil Base: Mineral oil
The lubricating liquid is liable to a slight discoloration from the product being
grounded and it must be replaced at regular intervals.
GRINDING MEDIA:
To prevent heavy wearing at inner surfaces of the cylinder and
better performance of the grinding output, suitable grinding media and ratio of
grinding beads must be carefully applied. 60-65 kilograms of Chrome Steel balls
are being used. Grinding element must be topped at the ratio of 1.5 kg for every
200 hours.
Cleaning:
For solvent based grinding:
After completion of the each grinding, pump in some resins into the
grinding chamber for cleaning out as much as possible the retaining color pastes.
Subsequently, pump in some solvent to clean thoroughly the left over paste and let
the cleaning pumping solvents discharge from the front cover discharge valve.
For water oil base grinding:
After completion of each grinding, pump in some oil
or water thoroughly the left over color paste.
Reason for use of Dyna Mill:
Dyna mill is used for further grinding of the pigments
and resin so that we reach our particle size standard that is 2-3 miacro meter.
RAW MATERIALS:
1) Pigments
2) Binders
3) Solvents
4) Additives
Solvents:
Solvents are used to keep the ink liquid form when it is applied to the printing plate
or cylinder until it has been transferred to the surface to be printed. At this point
the solvent must separate from the body of the ink to allow the image to dry and
bind to the surface.
Printing processes like gravure and flexography processes require a solvent that
evaporates rapidly. These use volatile solvents (i.e. those with boiling point below
120 C) .Ink formulators and printers select solvents based on
Resin system
Press speed
Cost
Toxicity of solvent
Classification of Solvents:
All Solvents can be classified into two types based upon their ability to dissolve a
polymer and resin.
a) Active
b) Latent
c) Diluents
a) Active
b) Latent:
c) Diluents:
Diluents are non solvent but are added to reduce the viscosity of the ink
RESINS:
Resins commonly referred to as vehicle is the substance in the
ink mixture which carries the pigment and binds it to the printed surface. The
vehicle must have the ability to be in liquid form during the printing process, but
dry rapidly when it reaches the printing surface.
Selection of binder is purely dependent on the substrate on
which the printing ink will eventually be used. We use about 20-25 percent resin
in a batch of ink. The most commonly used resins are listed below
Cellulose derivatives
Acrylics
Ketones
Alkydes
Formaldehydes
Phenolics
Pigments:
Pigments are insoluble and are applied not as solutions but as finely ground solid
particles mixed with a liquid. In general, the same pigments are employed in oil
and water based paints, printing inks, and plastics. Pigments may be organic or
inorganic.
The majorities of inorganic pigments are brighter and last longer than organic ones.
Organic pigments made from natural sources have been used for centuries, but
most pigments used today are either inorganic or synthetic organic ones. Synthetic
organic pigments are derived from coal tar and other petrochemicals. Inorganic
pigments are made by chemical reactions – notably oxidation- or are found
naturally as earths.
Inorganic pigments include white opaque pigments used to provide opacity and to
lighten other colours. The most important member of this class is titanium dioxide.
White extender pigments are added to paints to lower their cost or to improve their
properties. This class includes calcium carbonate, calcium sulfate, and china clays.
Carbon black is used to give black colour to printing ink.
ADDITIVES:
Additives produce a specific property not obtainable through a resin alone. Many
different types of additives are used to alter the final properties of the ink. The
most common types of additives used are
Types Function
Plasticiser Enhances the flexibility of the
printed ink
Wax Promotes rub resistance
Drier Catalyses the oxidation
reaction of inks which dry by
oxidation
Chelating agent Increase the viscosity of the
ink(aluminium chelate) and
promotes adhesion( titanium
chelate)
Antioxidant Delays the onset of oxidation
polymerization
Deformer Reduce the water tension in
water based inks, meaning that
Semi Finish
Finish
Semi Finish:
In Semi finish steps we make different products that may or may not
be used in a particular ink. These products are
1. Varnish
2. Pastes
Varnishes:
Varnish is a clear liquid that solidifies as a thin film. It binds the pigment to the
printed surface, provides the printability of ink and wets the pigment particles.
Varnish produced are simple resin solutions and do not need a high temperature to
effect a reaction.
MANUFACTURING PROCESS OF VARNISHES:
They are manufactured by breaking up the resin particles and dissolving them in a
solvent by using HSD (High speed disperser) Manufacturing Process of Varnishes
can be divided into two parts
1. Weighting of raw materials
2. Dispersion using HSD
Solvents are weighed on the weighting balance. The fluid volume is about 66
percent of the final batch. Rest of the material is added during mixing taking place
in “HSD”
Types of Varnishes:
Different kinds of varnish are produced by adding different types of resins in it.
Resins are responsible of carrying the pigment and binding it to the printing
surface. As there are different kind of printing surfaces like plastic and paper, A
single resin will not be able to bind the pigment to all printing surface so we add
different resins according to the substrate resulting in different kinds of varnishes.
1. Pastes:
Pastes are semi finish form of inks which are processed further to produce different
kinds of inks. There are four pastes currently being made
Yellow
Magenta
Cyan
Black
Solvents and varnishes are weighed on the weighting balanc.The fluid volume is
about 66 percent of the final batch. Rest of the material is added during mixing
taking place in “HSD”
HSD” is used to break down dry agglomerates (Pigmets) into a liquid vehicle thus
producing a uniform, stable dispersion with the finest particle size possible. The
blade creates a vortex that pull in the contents of the vessel to the blade sharp
edges, the blade surface then tear apart solids thereby reducing their size and at the
same time dispersing them among liquids. A revolving propeller traces a perfect
helix in the fluid.
“HSD” batch is started at a fairly low level, or volume, of fluid and no dry
product. The fluid volume is 66% of the final batch. The low speed produces a
deep vortex that the dry powder ingredients can be added into if we add the entire
ingredient vortex will not form. Dry ingredients are added after vortex is formed.
After all the ingredients have been added HSD is run at a maximum speed for the
time specified in batch paper. HSD is stopped only when Pigments are completely
dissolved and required viscosity is achieved.
Types of Pastes:
Pastes can be divided into different types on the basis of two factors
Varnish used determines the Substrate on which ink can be used and pigment
that we will use determines the colour that we will get thus by variation of these
two factors we get different kinds of pastes.
Production of ink
Before discussing the Manufacturing process of ink let us first discuss the basis
of production of different kinds of inks.
When white light hits an object, some of the light is absorbed and the
remainder reflected. The colour of the reflected light is the colour that we
perceive as the colour of the object, thus a leaf appears green because it absorbs
all colours except green. Printing is usually done using four different colours of
ink: cyan, magenta, yellow and black. The subtractive colours are chosen
because by 'overprinting' these inks, all other colours can be formed. For
example, red is produced by overprinting yellow and magenta, as the yellow
absorbs the blue light (because yellow is the emission of red and green light)
and magenta absorbs the green light, leaving behind pure red light. Black ink is
used because although in theory cyan, magenta and yellow should add together
to give black, in practice they usually give brown.
Pastes of different colors are added into the pot according to the ratio provided in
batch paper. These different pastes are selected on the basis of Young and
Helmholtz theory which on mixing give us our desired colour.
Raw materials are mixed together using a mixer. Revolution time is around 10 to
20 minutes which give us our required color of ink.
Post-Production:
1. Filtration of ink
2. Packing of ink
1. Filtration of ink:
2. Ink is filtered using a 200 mesh cloth on the filtration machine.
Mesh cloth is vibrated from time to time using a motor which shake the
whole frame of filtration machine.
3. Packing of ink:
After ink is filtered it is packed in 25 kg cans and delivered to
the customer.
4. Posting of batch paper:
After a particular batch is produced it bath paper is
posted i-e the information of that batch along with the values of the Quality
control is entered into the computer system.
QUALITY CONTROL
To ensure quality of ink every bath that is produced is checked in the lab.
Following Test are performed to test the quality of Printing ink.
1. Viscosity Test
2. Shade Test
3. Nail Test
4. Tape Test
5. Particle Size Test
6. Rubbing Test
1. Viscosity Test:
Equipment used:
No 2 Zahn Cup
Din cup
The time taken by ink to completely drain out of the cup is called “efflux time”.
Conversion
One can convert efflux time to kinematic viscosity by using an equation for each
cup specification number, where t is the efflux time and ν is the kinematic viscosity
in centistokes.
Din cup:
It is a simple gravity based device that permits the timed flow of liquid
from an orifice that is located at the bottom of the cup. It is used for water based
ink having low viscosity. In ideal conditions flow rate is equal to that of the
kinematic viscosity.
Viscosity Calculations:
Shade Test:
Shade Test is used to check the shade of the batch with the standard.
For this purpose two types of equipment are being used
Print coater
Control Coater
Print Coater:
Print Coater has gravues in it. This equipment is used to match the shade of
Gravure ink.
Control Coater:
Control Coater is used to match the shade of the flexo based ink
Process:
Two tiny dots one from batch and one from standard are taken. Viscosity of batch
is matched to that of the standard before taking shade. Two dots one from ink and
other from our standard are taken. A print of ink on the substrate (The surface on
which the ink is to be applied) is taken after applying two dots on the machine one
from batch produced and other from our standard. These two are then compared if
the shade is light more pigments are added in our batch to strengthnize its color. If
its sharp more solvent is added.
Nail Test:
Nail Test is used to find the adhesion of the ink to the substrate. After ink has dried
we try to starch the ink with the help of nails, if the ink is scratched it means that
ink has not properly attached to the surface. We add more resin to the ink to
increase its adhesion strength.
Tape Test:
Tape test also used to find the adhesion of the ink to the surface. Sometimes ink
passes the Tape test but fail nail test. In Tape test after ink has dried a tape is
attached to the substrate and removed with full strength if ink is removed along the
surface of the tape it fails the test. We add resin to increase the strength of the ink
Tack Test:
Tack test is used to find the stickness of the ink. In some printing process printing
material is rolled in the form of rolls after printing. This Stickness is high ink will
join two sheets of rolls together resulting in loss of printing material.
Rubbing Test:
Rubbing test is performed to check the rub resistance of ink against another ink or
surface to check how much ink is removed when two surfaces are rub against one
another.
New resin and Pigment are supplied by the supplier along the literature for lab
testing.
Resin Testing:
Following test are performed to check the suitability of Resin for a particular ink.
1. Viscosity
2. Tack Test
3. Gloss
4. Stability
5. Physical Appearance
Viscosity Test:
Viscosity of manufactured varnish is compared to that of the standard. If the
viscosity is high or very low then given resin is rejected because high viscosity
means that our shade will show low strength because we will need more solvent
addition and low viscosity means that we will have to add more resin resulting in
the increase of the manufacturing cost.
Tack Test:
Tack test is used to find the stickiness of produced varnish. Tack test is performed
manually using fingers to compare it to that of our standard varnish tackiness. If
Gloss Test:
Gloss of produced ink is compared to that of our standard if the gloss is less than
the standard then the given resin is not rejected but we will need to reduce the
quantity of wax.
Stability:
Varnish is checked after some days to check if any chemical reactions have taken
place or not if chemical reaction has occurred then the resin is rejected.
Physical Appearance:
Physical Appearance of produced varnish is checked after some days if varnish has
changed colors and has become opaque while it was transparent before than the
resin is rejected.
Pigment Testing:
Ink or paste is made by using the new pigment in the hymeter. After ink is
produced following test are performed to check the suitability of the pigment.
Shade Test:
Shade test is performed as defined to before. Shade is then compared if
shades are same then pigment is passed.
BERGER VR PRODUCTS;
LOW FLASH
1)VITON
2)NITRO
3)DURA
Jet black
8/18 LKA blue
002 black
U-26 suzuki white
T/C solid
Acid catt matt lacq
Wood lacq
T/C sanding sealer (mark) / NC sanding sealer (industry)
BUXLY PRODUCTS
BERGER THINNER
HONDA THINNER
TYPES OF LACQ.
Wood lacq
Acid catt matt lacq for high quality.
UNIT OPERATIONS;
Ball mill produces N/C grey petty for resin grind which are solid coarse.
Z shaped mixer N/C + ball mill gives produces paste grey putty used as
surface filler in denting.
UNIT # 06
There are number of products produced as per name of berdex, that are basically
industrial chemicals. These include moisture absorbent paints, whether resistant,
floor coatings, tile fillers and variety of products that produces.
Accelerators, Retarders
Water reducers,
Super plasticizers,
Integral Water proofing
Air entraining admixtures,
Anti-washout agents, etc.
2. Protection Systems
As globalization has assumed the central role and the world has become a global
village, ensuring cost effectiveness has become inevitable for any business entity
to sustain the cut throat competition prevalent all over. The corrosion control
product of BERDEX has been industries’ partner in protective systems for a long
time. As the leader in the market in terms of technology, polymer linings, coatings
and flooring systems. It has made a significant contribution in reducing costs and
assuring a smooth performance with a long operating life of the asset.
Some of the unique polymer formulations produced at BERDEX are:
Flake reinforced linings/coatings
Monolithic lining and flooring systems
Sanitary floor toppings
Static-dissipating floors
that can withstand internal and external water pressure in concrete structures.
Cement based coatings take care of water seepage as well as cracking due to
extreme temperatures. These provide excellent water resistance, considerable
flexibility and elongation of concrete. Ideally suited for new buildings as well as
repair of old structures, it ensures, resistance to ultra violet radiation, anti
carbonation and chemical resistant coating, thermal insulation and weatherproof
protective coating.
4. Precision Grouts
A high quality, properly placed grout is essential to the stability and operating life
of heavy machinery. It must maintain precise machine alignment in the face of
many destabilizing forces.
5. Concrete Repair
Need of repair is inevitable in concrete structures. Causes of concrete
deteriorations are physical, chemical, thermal & biological. Solutions offered
by BERDEX for concrete related issues include, patching mortars, polymer-
modified mortars and concrete, epoxy mortars and concrete, surface sealers, free
flowing, non-shrink, helps in rapid installation and gains high strength resistant to
acids and alkalis. It is also capable of transmitting high stresses & is capable of
withstanding repetitive dynamic loading. It ensures high compression, flexural and
tensile strength, Bonds monolithically with base concrete.
6. Flooring Systems
BERDEX develops and applies various flooring solutions that are customizable as
per the requirements. They are self balancing epoxy and resin based floorings.
It is Ideal for Industrial plants, Pharmaceuticals, Food, Beverage Plants,
Automobile workshops, Hospital etc.
7. Epoxy Floors:
Epoxy is one of the most commonly used flooring solutions in industrial concerns.
Epoxy flooring is attractive and seamless that leaves no crevices where dirt and
bacteria can dwell in, hence hygienic standards are maintained. Epoxy flooring
solution is Abrasion resistant, non-tainting, and non-dusting bearing a hard
wearing floor finish.
PRODUCT RANGE
BER FLEX
IWP is liquid water proofing admixture which can be used in concrete and cement
mortar. It reduces water demand and also improves impermeability of concrete.
BERTEX MORTAR
Multi-component, heavy duty epoxy resin based screed system designed to provide
continuous protection and repair solution to concrete floors in medium to heavy
duty situations.
BER TOP
BER HARDFLOOR
BER ACRYL
BER SHIELD
Hygienic self leveling epoxy resin flooring for medium duty load conditions.
BER LASTIC
Hydrate type flexible water proofing material based on special synthetic resin
dispersion and a blend of selected cements mixed with well graded sand, and high
performance polymer.
BER POLYCURE W
Wax based concrete curing compound which when applied on concrete forms a
seamless film, and prevent evaporation of water from capillaries of concrete.
SBR is styrene butadiene rubber copolymer which has been specifically designed
for use with cement composition. It is used to form water and vapor resistant bond
coating.
BER PROOF WP
Liquid integral water proofing compound for cement mortar and concrete.
BER PLAST
High grade retarding water reducer based on high grade modified naphthalene
sulphate, specifically formulated with combination of resin.
UNIT # 07
Electrical maintenance
Mechanical maintenance
Civil works
General maintenance
Preventive maintenance
Breakdown maintenance
Over see new projects + keep plant in
running condition
UNIT # 08
PRODUCTION DEPARTMENT
OIL BASED
CHARGING SECTION; to feed charge it is required that pigment should
have a specified size range so that it may not lost its characteristics, to do
so , no of size reduction mills are available including;
For oil based production unit, binder hold tanks are installed, so it is pumped
directly into overhead tank 3 in no from where it can be poured into mills by
gravity through pumping system. Since powdery material is involved , so
proper duct emission system is installed in both water and oil based sections.
WALL PUTTY
As far as mixing operation is concerned in chemical engineering , where it is
asserted that for perfect mixing , mixer should operate in tank along
diameter in all dimensions, so that dead areas may not form. Wall putty
contains a mixer centralized that can change angle of orientation, also a
thresher to remove sticky viscous material that may stick along wal, with
different RPMz . Jansoline wall putty is made from it and used for weather
resistant coating and long life exterior , reliable coating.
UNIT # 09
AUTOMOBILE PRODUCTION
There are no of classifications that can be made to describe this class.
For all the automobile paints need stoving as to melt paint and create a film over
newly made metal automobile.
Sand mill
itertors
AREA DIVISION;
Mixing area;
Cold mixing plain operation to convert semi finish product to finished, color
matching and properties are adjusted by adding stainer, while pigment in powder
form is charged already while forming base in chagrining area. In mixing section
where stainer is added , only shade is provided.
Packing area;
Auto section deals with high flammable and fire catching volatile vaporos
chemicals. So if humidity and temperature is not maintained, there are sure
chances of catching fire, here minimum limit of humidity (relative) is 65%, while a
regular cycle process (humidifier) is located that keep air in circulation and
removes volatiled air and replaced with fresh air.
Road marking produced here is in liquid form and can be applied over foot paths,
road pavements , etc while that produce in berdex is in powder form , that is
applied by melting powder , and film is applied over flat surface. As far as inclined
or tall surface is concerned , it is impossible to apply this melt , using melt heater
machine over there, so liquid road marking is produced over in automobile
production unit as well.
COMPARISON
PRE-TREATMENT
Chemicals produced are made dust , rust ,and oil free before primer / under coat is
applied.
Zinc phosphate , chemical produces used for bonding paint and surface.
rinsing
passivation (solution to
maintain phosphating)
acid
value control (reduces if
high/ increase if low)
CONCLUSIONS
It was a good experience spending 28 days in berger. Being a chemical engineer,
it’s a new tactic to stay in a process where batch process is carried out. In
engineering courses it is steady continuous process that is considered, therefore
this experience definitely provide a newer mind set.
In this time of energy crisis , world is facing a real hawk of energy, but oil based resin plant play
a game show of energy wastage.
Cooled water that is used to cool kettles reactor containing internal jackets coil release
cooling media in form of steam mean at temperature nearby 100-110 0C. it is found that
this stream from kettle is directly wasted.
Stack tower was found releasing flue gases at temperature about 100 0C. If it is paid
attention this energy can be made useful, and plays an important role in reducing the
energy consumptions of plant.
Since plant contains burners running on natural gas; and heating thermal oil as heating
media. Its found that valves joining headers that contains rubber gas kits, but thermal oil
from burner is almost at 280 0C causing rubber made gaskits to melt and produce slippage
and loss in strength of thermal oil, since highly flammable chemicals producing dense
volatile vapors are observed around, that are waiting for flash of fire. So it is advised to
immediately take action in rectifying the risk of catching fire and setting life of workers
to high risk.
In resins water based section packing of berlith glue is carried out using pneumatic
machine, and it is found that machine was causing mis weight age. Its filling section was
injection random weight jet of glue in pouch and remarkable difference in weight of bag
pouch was observed, that should be rectified to maintain standards of BERGER.