39.

08

34.58

31.88

30.63

29.74
29.27
29.21
29.16

25.02

24.03

22.66

14.02
Parameter Set:#C13−CPD−QNP−34 (2008.11.19) TS1.3PL8.
NMR System: Bruker Avance DRX 400
Oper. MB/ Registry No.: 5992
User: R. Cioanca
Sample Changer Position:
DU \\Bruker−1−New\D\UTI−FChimInd\RCioanca
Sample name and description: BAO−AZO4 (spectru inregistrat la 55 grade C)
data
USER BAO−AZO4

nmr
NAME c
EXPNO 1
PROCNO 1
Date_ 20090702
Time 17.22
INSTRUM spect
PROBHD 5 mm QNP 1H/29
PULPROG zgpg30
TD 65536
SOLVENT CDCl3
NS 1024
DS 4
SWH 31847.133 Hz
FIDRES 0.485949 Hz
AQ 1.0289652 sec
RG 7298.2
DW 15.700 usec
DE 6.00 usec
TE 328.2 K
D1 1.00000000 sec
d11 0.03000000 sec
DELTA 0.89999998 sec
TD0 1

======== CHANNEL f1 ========

NUC1 13C
P1 8.30 usec
PL1 −4.00 dB
SFO1 100.6254462 MHz

======== CHANNEL f2 ========

CPDPRG2 waltz16
NUC2 1H
PCPD2 80.00 usec
PL2 −5.00 dB
PL12 13.06 dB
PL13 14.00 dB
SFO2 400.1316005 MHz
SI 32768
SF 100.6127556 MHz
WDW EM
SSB 0
LB 1.00 Hz
GB 0
PC 1.40
OFFSET 284.399 ppm
PH_mod pk

40 39 38 37 36 35 34 33 32 31 30 29 28 27 26 25 24 23 22 21 20 19 18 17 16 15 ppm