Water Layer (%wt) Isopropyl Ether Layer (%wt)

Acetic Acid Water Isopropyl Ether Acetic Acid Water Isopropyl Ether
0 98.8 1.2 0 0.6 99.4
0.69 98.1 1.2 0.18 0.5 99.3
1.41 97.1 1.5 0.37 0.7 98.9
2.89 95.5 1.6 0.79 0.8 98.4
6.42 91.7 1.9 1.93 1 97.1
13.3 84.4 2.3 4.82 1.9 93.3
25.5 71.1 3.4 11.4 3.9 84.7
36.7 58.9 4.4 21.6 6.9 71.5
44.3 45.1 10.6 31.1 10.8 58.1
46.4 37.1 16.5 36.2 15.1 48.7

Isopropyl Ether Layer (Raffinate) Water Layer (Extract)

Acetic Acid Water Isopropyl Ether Acetic Acid Water Isopropyl Ether
0 0.006 0.994 0 0.988 0.012
1.1
0.0018 0.005 0.993 0.0069 0.981 0.012
1
0.0037 0.007 0.989 0.0141 0.971 0.015
0.9
0.0079 0.008 0.984 0.0289 0.8 0.955 0.016

Mass Fraction C (xC, yC)

0.0193 0.01 0.971 0.0642 0.7 0.917 0.019
0.0482 0.019 0.933 0.133 0.6 0.844 0.023
0.114 0.039 0.847 0.255 0.5 0.711 0.034
0.216 0.069 0.715 0.367 0.4 0.589 0.044
0.311 0.108 0.581 0.443 0.3 0.451 0.106
0.362 0.151 0.487 0.464 0.2 0.371 0.165
0.4 0.5 0.1
0.5 0.6 0
0.6 0.7 0 0.1 0.2 0.3 0.4 0.5 0.6 0
0.7 0.8 Mass Fraction A (xA, yA)
0.8 0.9
0.9

Water Layer (Raffinate) Isopropyl Ether Layer (Extract)

Acetic Acid Water Isopropyl Ether Acetic Acid Water Isopropyl Ether
0 0.988 0.012 0 0.006 0.994
0.0069 0.981 0.012 0.0018 0.005 0.993
0.0141 0.971 0.015 0.0037 0.007 0.989
0.0289 0.955 0.016 0.0079 0.008 0.984
0.0642 0.917 0.019 0.0193 0.01 0.971
0.133 0.844 0.023 0.0482 0.019 0.933
0.255 0.711 0.034 0.114 0.039 0.847
0.367 0.589 0.044 0.216 0.069 0.715
0.443 0.451 0.106 0.311 0.108 0.581
0.464 0.371 0.165 0.362 0.151 0.487
 A Acetic Acid
B Isopropyl Ether Raffinate
C Water Extract

1
0.9
0.8
0.7
Water Layer (Extract)

0.6
0.5
0.4
0.3
x 0.2 y
0 0.1 0
0.1 0 0.1
0.2 00.2 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
0.3 0.3 Ether Layer (Raffinate)
0.4 0.4
0.5 0.5
0.6 0.6
0.7 0.7
0.8 0.8
0.9 0.9
1 1.1 1
1
0.4 0.5 0.6 0.7 0.8
0.9 0.9 1
Mass Fraction A (xA, yA) 0.8
Mass Fraction C (xC,yC)

0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
Mass Fraction A (xA,yA)

1
0.9
0.8
0.7
Ether Layer (Extract)

0.6
0.5
0.4
0.3
0.2
0.1
 0.8
0.7

Ether Layer (Extract)

0.6
0.5
0.4
0.3
0.2
0.1
0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
Water Layer (Raffinate)