Final Report: Proficiency Testing (PT) Program On Tensile Tests For Glove (2015)

Final Report
ProficiencyTesting
Proficiency Testing(PT)
(PT)Program
Programon
onTensile
Tensile
Testsfor
Tests forGlove
Glove
(2015)
(2015)
Analyzed and Prepared

By
Accreditation & Certification (A&C)
Quality and Technical Services Division
Malaysian Rubber Board
Grateful thanks to staff of the Publication and Library Unit for their assistance in preparing this
final report.
1
CONTENTS
Page
Contents 2
1. Introduction……………………………………………………… 4
2. Features of the Program………………………………………. 4
3. Participating Laboratories……………………………………... 5
4. Materials………………………………………………………… 6
5. Test method……………………………………………………. 6
6. Data analysis…………………………………………………… 7
7. Statistical statement and definitions…………………………. 8
8. Outlier rejection 10
9. Flagging inconsistent results 11
10. Summary of Analysis

Table 1: Summary of flagged data obtained from
participating laboratories……………………………………… 12-13
11. Total Solids Content (TSC) (% weight)……………………… 14-18
Dry Rubber content (DRC) (%
12. 19-23
weight)..................................
13. Alkalinity (NH3) (% weight)……………………………………. 24-28
14. Volatile Fatty Acid (VFA No.)…………………………………. 29-33
15. Mechanical Stability Time (MST) (seconds)………………… 34-38
16. Nitrogen content……………………………………………….. 39-41
2
ProficiencyTesting
Proficiency Testing(PT)
(PT)Program
ProgramononTensile
TensileTests
Testsfor
forGlove
Glove
(2015)
(2015)
1. INTRODUCTION
This report summarizes the results of the Proficiency Testing (PT) Program organized
by MRB in October 2015, for the analysis on Tensile Tests for Glove. The purpose of the
program is to provide means of objectively assessing the precision of the testing
procedure in terms of its repeatability within the laboratory (S r) and reproducibility in
between the laboratories (SR).
The program is conducted annually for quality improvement as required in the MS

ISO/IEC 17025 and ISO 9001, in order to meet the stringent physical requirements and
product guarantee. In order to provide participating laboratories opportunity to assess
their testing performances and efficiencies. This is especially important for purposes of
continual improvement in the quality of test measurements as well as for product
guarantee. Participants of the program can make full use of the results obtained to
demonstrate, to certification and accreditation bodies, comparability and traceability of
their testing performance.
In this program, results obtained were presented in such a way that rouge data or
outliers were either “H” or “k” flagged and treated accordingly. The treated data can be
used to generate precision statement of each of the testing procedures.
A web-based system of “e-Precision” which is produced in house by Malaysian Rubber

Board was used to compute the within-laboratory and between-laboratory measurement
variability.
3
2. FEATURES OF THE PROGRAM
A total of 22 laboratories known for conducting on Tensile Tests for Glove were
participated in the program.
Participants’ confidentiality are assured by identifying each participant by a unique code

number known only to the laboratory concerned and the coordinator of PT program.
Participants were requested to perform the test according to their copy of the
‘Instruction to Participants” and to record their results on the accompanying ‘Result
Sheet”, both which were distributed to the participants together with the samples.
Programme software of ASTM E 691-92 (Practice for conducting an interlaboratory

study to determine the precision of a test methods) was used to compute the within-
laboratory and between-laboratory measurement variability.
Parameters that are used in the scope of this programme are:

 Number of laboratories participating;
 Number of materials;
 Number of replications.
Six laboratories, four materials, and two replications are the minimum parameters stated
in ASTM E 691. The more the better is a general rule for the number of laboratories and
materials, while two or at most three replications are normally sufficient.
3. Aims of the study
The aims of the study are as follows:
 To identify those laboratories disagreeing in a statistical sense, from the majority,

so that, their results can be the subject of further consideration;
4
 To give laboratories feedback on their performance relative to the consensus
results;
 To give laboratories sufficient data to enable them to identify and correct
techniques and calibrations that needed correction;
 To maintain international confidence in the results from all the laboratories;
 To get an estimate of the precision of test method such as repeatability and
reproducibility measurements.
Generally, the analysis of results can be used to suggest possible causes for deviations
from consensus results. These needed to be analysed by examining the equipment, the
test methods, the operators and the results.
Those laboratories wishing to compare the performance of their results with the
consensus may find convenient to start as follows:

Read the main report;

Examine the summary of results and calculation work sheets of each material
and test;
 Examine the h and k values of each test and;
Examine the h and k plot by laboratory of each test
4. PARTICIPATING LABORATORIES
The participating laboratories are as follows:
1. Ansell NP Sdn Bhd.
2. Bonric Sdn Bhd
3. Cardinal Health Malaysia
4. Central Medicare Sdn. Bhd.
5. Encompass Medical Supplies Sdn Bhd
6. G-TACR Sg.Buloh Lembaga Getah Malaysia
7. GX Corporation Sdn Bhd (Plant 2)
8. Hartalega NGC Sdn Bhd
5
9. Hartalega Sdn Bhd
10. Latexx Manufacturing Sdn.Bhd.
11. Molnlycke Health Care KK QA Physical Lab
12. Molnlycke Health Care Sdn Bhd (Batang Kali)
13. Molnlycke Health Care Sdn Bhd R&D Physical Lab
14. N.S Uni-Glove Sdn Bhd
15. Perusahaan Getah Asas Sdn. Bhd.
16. Platinium Glove Industries Sdn Bhd
17. Revertex (M) Sdn Bhd.
18. Riverstone Resources Sdn Bhd (Taiping)
19. Sigma Glove Industries Sdn Bhd
20. Smart Glove Corporation Sdn Bhd
21. Wear Safe(Malaysia) Sdn Bhd
22. WRP Asia Pacific Sdn Bhd
The list is arranged at random according to test data received. A code number
identifies the laboratory and the number above is not the same as the code
number of the laboratory taking part.
5. MATERIALS AND SAMPLE PREPARATION
Two different gloves are used in this study, that is, Glove A (Powdered free examination
glove) and Glove B (powdered examination glove). Two gloves and six cut dumbbells
from each material were supplied to participating laboratory. The participated lab then
prepared and cut another three dumbbells from the two gloves supplied.
6
6. Test method
The ASTM D3578-05 test method is used as the main reference. Ageing is carried in
accordance with the requirements specified in ASTM D3578, that is, 166±2 h at 70°C.
The tests are as follows:
(i) Unaged tensile properties:

Tensile strength;
Force at break,
Elongation at break.
(ii) Aged tensile properties:

Tensile strength;
Force at break,
Elongation at break;
(iii) Unaged tensile properties on dumbbells cut by LGM:

Tensile strength;
Force at break,
(iv) Aged tensile properties on dumbbells cut by LGM:

Tensile strength;
Force at break,
7
7. Equipment particulars
Type of equipment
Laboratory Die Thickness Tensile Oven

Cutter gauge machine
MRB – Instron 5564 Die C Mitutoyo Instron 5564 Binder
MRB – Zwick Die C Mitutoyo Zwick Binder
MRB – Testometric 2 Die C Mitutoyo Tensometric Binder
GMP Medicare Die C Mitutoyo Instron Memmert
Supermax Die C Mitutoyo LLOYD LRX Memmert
MIM Technical Lab. Die C - - -
Regent Hospital Products Die C Mitutoyo Instron 4301 Memmert

(Batang Kali)
Regent Hospital Products Die C Mitutoyo Instron 5564 Memmert

(Kuala Ketil, Kedah)
Regent Hospital Products Die C Sylvac Instron 5564 Memmert

(Kulim, Kedah)
Hartalega Die C Mitutoyo Instron 3345 Model ZRD 7140
8. TEST METHOD AND SCHEDULE
In this program, participants were asked to perform their testing according to the test
methods and dates as shown in the following list.
8
Test Ageing in the oven Date of testing
Sample
Method (70±2° C, 7 days) Set A Set B
Set A Set B
In Out In Out
Aged 28/10/2015 29/10/2015
ASTM
20/10/2015 27/10/2015 21/10/2015 28/10/2015
D3578
Unaged - 21/10/2015 22/10/2015
Each test parameter was carried out in duplicate for both samples A and B on two
different days respectively.
9. DATA ANALYSIS
New computer software is used for performing the calculations and producing the tables
and graphs associated with the standard practice of ASTM E691-99: Standard Practice
for Conducting an Interlaboratory Study to Determine the Precision of a Test Method.
The software called “e-Precision” is a web-based system produced in-house by the
Malaysian Rubber Board (MRB) for analyzing data obtained from the Proficiency
Testing (PT) or round robin program. Being green, versatile and user-friendly, the
system is not only able to provide the precision values obtained from the PT program in
terms of repeatability (r) and reproducibility (R); it is also capable of treating outliers
data which is a plus point as other commercially available software fails to offer. The
treated values are used to establish a precision statement which is an essential element
in any national and/or international standards.
10. STATISTICAL STATEMENT and DEFINITIONS
(a) Cell statistics:
(i) Cell average,
9
Where = the average of individual test results in one cell,
x = the individual test results in one cell, and
n = the number of test results in one cell.
(ii) Cell standard deviation,
(iii) Average of the cell average,
Where = the average of the cell averages for one material, and
p = the number of laboratories in the proficiency testing.
(iv) Cell deviation,
(v) Standard deviation of the cell average,
(b) Precision statistics
(i) Repeatability standard deviation,
(ii) Reproducibility standard deviation,
(c) Consistency statistics, h and k value
The derivation of the equations for calculating critical values of h and k are given
below:
(i)
10
where h = Consistency statistics between laboratory.
The closer this value to zero, the better is the reproducibility.
(ii) k = s / sr
where k = Consistency statistics within the laboratory.
Critical values for h and k

The appropriate critical value for h and k (calculated at the 0.5% Significance level as
taken from ASTM E691-99) is shown in the table:
Critical Values of h and k at the 0.5% Significance Level
Critical values of k
Critical
Number of replicates, n
value p
of h 2 3 4 5 6 7 8 9 10
11
1.15 3 1.72 1.67 1.61 1.56 1.52 1.49 1.47 1.44 1.42
1.49 4 1.95 1.82 1.73 1.66 1.60 1.56 1.53 1.50 1.47
1.74 5 2.11 1.92 1.79 1.71 1.65 1.60 1.56 1.53 1.50
1.92 6 2.22 1.98 1.84 1.75 1.68 1.63 1.59 1.55 1.52
2.05 7 2.30 2.03 1.87 1.77 1.70 1.65 1.60 1.57 1.54
2.15 8 2.36 2.06 1.90 1.79 1.72 1.66 1.62 1.58 1.55
2.23 9 2.41 2.09 1.92 1.81 1.73 1.67 1.62 1.59 1.56
2.29 10 2.45 2.11 1.93 1.82 1.74 1.68 1.63 1.59 1.56
2.34 11 2.49 2.13 1.94 1.83 1.75 1.69 1.64 1.60 1.57
2.38 12 2.51 2.14 1.96 1.84 1.76 1.69 1.64 1.60 1.57
2.41 13 2.54 2.15 1.96 1.84 1.76 1.70 1.65 1.61 1.58
2.44 14 2.56 2.16 1.97 1.85 1.77 1.70 1.65 1.61 1.58
2.47 15 2.57 2.17 1.98 1.86 1.77 1.71 1.66 1.62 1.58
2.49 16 2.59 2.18 1.98 1.86 1.77 1.71 1.66 1.62 1.58
2.51 17 2.60 2.19 1.99 1.86 1.78 1.71 1.66 1.62 1.59
2.53 18 2.61 2.20 1.99 1.87 1.78 1.72 1.66 1.62 1.59
2.54 19 2.62 2.20 2.00 1.87 1.78 1.72 1.67 1.62 1.59
2.56 20 2.63 2.21 2.00 1.87 1.79 1.72 1.67 1.63 1.59
Where p= number of laboratories
The critical value for h depends on the number of laboratories participating and the
critical value for k depends on both number of laboratories and number of replicates.
The above critical values are calculated from Student’s t and the F-ratio.
8. OUTLIER REJECTION
Outliers are test results that deviate so much from the bulk of the data. They are
considered to be irreconcilable with remainder of the data. If outliers are present, outlier
12
rejection techniques are used to eliminate the indicated data values. Reanalysis is
conducted on the adjusted database. This analysis yields the statistical parameters that
are then used to calculate the precision parameters, that is h and k-values. The outlier
is treated and the treated results are attached in the report.
9. FLAGGING INCONSISTENT RESULTS
Some results may be flagged either h or k or both. Laboratory flagged with either h or k
or both has exceeded the limit of what the other labs has determined. The labs are
advised to take further steps to check their test methods and/or test equipment.
SUMMARY OF
13
ANALYSIS
Table 1: Summary of Flagged Data Obtained from Participating Laboratories
Laboratories having Laboratories having

Type of tests poor reproducibility poor repeatability
(“H” flagged) (“K” flagged)
Aged tensile properties
Tensile strength
Force at break
Elongation at break
Unaged tensile properties
Tensile strength
Force at break
Elongation at break
Aged tensile properties on dumbbells

cut by LGM:
Tensile strength;
Force at break
Elongation at break
Unaged tensile properties on dumbbells

cut by LGM:
14
Tensile strength;
Force at break
Elongation at break
15
GROUP 1
16
SUMMARY OF TENSILE STRENGTH (GLOVE)
AGED
Flagged Flagged
Lab Code Test Result x` s d h k
'H' 'K'
Day 1 Day 1 Day 1 Day 2 Day 2 Day 2

G17 23.683 0.739 -0.296 -0.145 0.71
24.2 22.6 23.1 24.6 24 23.6

G29 24.167 0.753 0.188 0.092 0.72
25 24 24 23 25 24

G15 25.098 1.123 1.119 0.550 1.08
25.6 26.28 24.86 23.6 24.04 26.21

G04 26.455 0.616 2.476 1.217 0.59
26.93 25.5 27.03 26.93 26.03 26.31

G13 22.370 0.776 -1.609 -0.791 0.75
21.78 21.25 22.31 22.68 22.75 23.45

G30 23.405 2.638 -0.574 -0.282 2.53 K
26.23 24.58 24.5 24.79 20.98 19.35

G11 24.740 0.619 0.761 0.374 0.59
24.07 25.09 25.53 24.4 24.13 25.22

G19 26.300 0.934 2.321 1.141 0.9
25.6 27.8 26.2 26.7 25.1 26.4

G06 26.717 0.711 2.738 1.346 0.68
27.4 26.7 27 26.2 25.6 27.4

G05 17.950 1.498 -6.029 -2.964 1.44 H
17.2 20.9 17.9 17.2 17.7 16.8

G02 22.950 0.558 -1.029 -0.506 0.54
22.6 23.7 23.3 23.3 22.3 22.5
17
G21 22.668 0.761 -1.311 -0.644 0.73
23.56 23.5 22.39 22.31 21.57 22.68

G33 23.050 0.695 -0.929 -0.457 0.67
23.2 22.9 22.1 24.2 23.2 22.7

G31 25.009 0.432 1.030 0.506 0.42
24.362 25.255 24.753 24.996 25.055 25.631

G27 25.098 0.673 1.119 0.550 0.65
25.09 23.92 25.93 25.34 24.91 25.4

G24 24.043 0.529 0.064 0.032 0.51
24.32 24.2 24.67 23.7 24.2 23.17

G09 23.940 1.350 -0.039 -0.019 1.3
22.41 22.9 24.59 23.13 24.64 25.97
cell = test result of a laboratory Average of cell averages, x" = 23.979

x' = cell average Standard deviation of cell averages, sx' = 2.034
s = cell standard deviation Repeatability standard deviation, sr = 1.0413
d = cell deviation = x' - x'' Reproducibility standard deviation, sR = 2.2452
h = d/s(x') Repeatability, r = 2.947
k = s/sr Reproducibility, R = 6.3538
18
TREATED VALUE/VALUES
Flagged
Lab Code Test Result x` s d h k Flagged 'K'
'H'

G17 23.683 0.739 -0.673 -0.512 0.71
24.2 22.6 23.1 24.6 24 23.6

G29 24.167 0.753 -0.189 -0.144 0.72
25 24 24 23 25 24

G15 25.098 1.123 0.742 0.566 1.08
25.6 26.28 24.86 23.6 24.04 26.21

G04 26.455 0.616 2.099 1.599 0.59
26.93 25.5 27.03 26.93 26.03 26.31

G13 22.370 0.776 -1.986 -1.513 0.75
21.78 21.25 22.31 22.68 22.75 23.45

G30 23.405 0.847 -0.951 -0.724 1
26.23 24.58 24.5 24.79 20.98 19.35

G11 24.740 0.619 0.384 0.293 0.59
24.07 25.09 25.53 24.4 24.13 25.22

G19 26.300 0.934 1.944 1.481 0.9
25.6 27.8 26.2 26.7 25.1 26.4

G06 26.717 0.711 2.361 1.798 0.68
27.4 26.7 27 26.2 25.6 27.4

G05 24.356 1.498 0.000 0.000 1.44
17.2 20.9 17.9 17.2 17.7 16.8

G02 22.950 0.558 -1.406 -1.071 0.54
22.6 23.7 23.3 23.3 22.3 22.5

G21 22.668 0.761 -1.688 -1.286 0.73
23.56 23.5 22.39 22.31 21.57 22.68

G33 23.050 0.695 -1.306 -0.995 0.67
23.2 22.9 22.1 24.2 23.2 22.7
19
G31 25.009 0.432 0.653 0.497 0.42
24.362 25.255 24.753 24.996 25.055 25.631

G27 25.098 0.673 0.742 0.566 0.65
25.09 23.92 25.93 25.34 24.91 25.4

G24 24.043 0.529 -0.313 -0.238 0.51
24.32 24.2 24.67 23.7 24.2 23.17

G09 23.940 1.350 -0.416 -0.317 1.3
22.41 22.9 24.59 23.13 24.64 25.97

20
K & H VALUE GRAPH- TENSILE STRENGTH (GLOVE)
AGED
21
SUMMARY OF FORCE AT BREAK (GLOVE)
AGED
Flagged Flagged
'H' 'K'

G17 16.367 0.592 -0.059 -0.045 0.88
16.9 15.8 16.3 17.2 16.3 15.7

G29 16.467 0.524 0.041 0.031 0.78
17.1 16.7 16.5 16 16.8 15.7

G15 17.383 0.739 0.958 0.730 1.1
17.1 17.9 17.5 16.5 16.8 18.5

G04 18.073 0.606 1.648 1.256 0.9
18.23 17.14 18.73 18.67 17.69 17.98

G13 15.678 0.521 -0.747 -0.570 0.77
15.81 15.18 15.35 15.52 16.65 15.56

G30 15.957 1.232 -0.469 -0.357 1.83 K
17.31 16.55 16.17 16.68 15.1 13.93

G11 17.025 0.602 0.600 0.457 0.89
17.21 17.4 17.61 16.25 16.28 17.4

G19 18.083 0.818 1.658 1.264 1.21
17.9 18.9 18 19.2 17.3 17.2

G06 17.917 0.601 1.491 1.137 0.89
17.9 17.3 17.4 18.3 17.7 18.9

G05 12.417 0.880 -4.009 -3.056 1.3 H
11.9 14.2 12.1 12.2 12 12.1

G02 15.567 0.509 -0.859 -0.655 0.75
15.2 15.4 15.5 15.9 15 16.4

G21 16.167 0.456 -0.259 -0.197 0.68
16.81 16.6 16.12 16.06 15.72 15.69
22
G33 15.750 0.327 -0.675 -0.515 0.48
15.9 15.9 15.2 16 16 15.5

G31 16.790 0.261 0.365 0.278 0.39
16.757 16.635 16.434 17.215 16.85 16.849

G27 16.135 0.627 -0.290 -0.221 0.93
16.56 15.78 17.11 15.7 16.24 15.42

G24 16.897 0.384 0.471 0.359 0.57
16.78 17.28 17.47 16.61 16.7 16.54

G09 16.562 1.027 0.136 0.104 1.52
15.68 15.19 16.66 16.46 17.84 17.54

23
Lab Code Test Result x` s d h k Flagged 'H' Flagged 'K'

G17 16.367 0.592 -0.309 -0.383 0.88
16.9 15.8 16.3 17.2 16.3 15.7

G29 16.467 0.524 -0.209 -0.259 0.78
17.1 16.7 16.5 16 16.8 15.7

G15 17.383 0.739 0.707 0.875 1.1
17.1 17.9 17.5 16.5 16.8 18.5

G04 18.073 0.606 1.397 1.728 0.9
18.23 17.14 18.73 18.67 17.69 17.98

G13 15.678 0.521 -0.998 -1.234 0.77
15.81 15.18 15.35 15.52 16.65 15.56

G30 15.957 0.623 -0.719 -0.890 1
17.31 16.55 16.17 16.68 15.1 13.93

G11 17.025 0.602 0.349 0.432 0.89
17.21 17.4 17.61 16.25 16.28 17.4

G19 18.083 0.818 1.407 1.740 1.21
17.9 18.9 18 19.2 17.3 17.2

G06 17.917 0.601 1.241 1.534 0.89
17.9 17.3 17.4 18.3 17.7 18.9

G05 16.676 0.880 0.000 0.000 1.3
11.9 14.2 12.1 12.2 12 12.1

G02 15.567 0.509 -1.109 -1.372 0.75
15.2 15.4 15.5 15.9 15 16.4

G21 16.167 0.456 -0.509 -0.630 0.68
16.81 16.6 16.12 16.06 15.72 15.69

G33 15.750 0.327 -0.926 -1.145 0.48
15.9 15.9 15.2 16 16 15.5
24
Day 2
Day 1 Day 1 Day 1 Day 2 Day 2
G31 16.790 0.261 0.114 0.141 0.39
16.757 16.635 16.434 17.215 16.849
16.85

G27 16.135 0.627 -0.541 -0.669 0.93
16.56 15.78 17.11 15.7 16.24 15.42

G24 16.897 0.384 0.221 0.273 0.57
16.78 17.28 17.47 16.61 16.7 16.54

G09 16.562 1.027 -0.114 -0.141 1.52
15.68 15.19 16.66 16.46 17.84 17.54

25
K & H VALUE GRAPH- FORCE AT BREAK (GLOVE)
AGED
26
SUMMARY OF ELONGATION AT BREAK (GLOVE)
AGED

G17 777.833 17.440 -4.751 -0.105 0.78
768 752 770 794 797 786

G29 835.167 36.723 52.583 1.163 1.64
806 786 825 845 865 884

G15 876.667 12.754 94.083 2.081 0.57
868 888 888 860 868 888

G04 773.333 16.330 -9.251 -0.205 0.73
780 740 780 780 780 780

G13 870.000 20.000 87.416 1.933 0.89
880 880 880 830 870 880

G30 750.000 37.417 -32.584 -0.721 1.67
800 780 760 740 720 700
Day 1 Day 1
Day 1 Day 2 Day 2 Day 2
G11 708.887 15.380 -73.697 -1.630 0.69
695.34 707.97 707.75 714.06
692.7 735.5

G19 795.833 16.376 13.249 0.293 0.73
786 806 786 825 786 786

G06 792.667 16.330 10.083 0.223 0.73
806 786 766 786 806 806

G05 730.000 14.114 -52.584 -1.163 0.63
729 750 742 711 721 727

G02 740.167 10.108 -42.417 -0.938 0.45
745 749 749 732 724 742

G21 768.667 5.888 -13.917 -0.308 0.26
772 772 764 768 760 776

G33 773.333 10.328 -9.251 -0.205 0.46
760 780 780 780 780 760
27
Day 1 Day 1
G31 804.710 22.693 22.126 0.489 1.01
802.32 827.94 809.62 794.88
766.9 826.6

G27 770.000 51.769 -12.584 -0.278 2.31 K
720 740 720 780 820 840

G24 750.000 10.954 -32.584 -0.721 0.49
740 740 760 760 760 740

G09 786.667 10.328 4.083 0.090 0.46
780 800 800 780 780 780

28
Flagged Flagged
'H' 'K'

G17 777.833 17.440 -4.751 -0.105 0.78
768 752 770 794 797 786

G29 835.167 36.723 52.583 1.163 1.64
806 786 825 845 865 884

G15 876.667 12.754 94.083 2.081 0.57
868 888 888 860 868 888

G04 773.333 16.330 -9.251 -0.205 0.73
780 740 780 780 780 780

G13 870.000 20.000 87.416 1.933 0.89
880 880 880 830 870 880

G30 750.000 37.417 -32.584 -0.721 1.67
800 780 760 740 720 700
Day 1 Day 1
G11 708.887 15.380 -73.697 -1.630 0.69
695.34 707.97 707.75 714.06
692.7 735.5

G19 795.833 16.376 13.249 0.293 0.73
786 806 786 825 786 786

G06 792.667 16.330 10.083 0.223 0.73
806 786 766 786 806 806

G05 730.000 14.114 -52.584 -1.163 0.63
729 750 742 711 721 727

G02 740.167 10.108 -42.417 -0.938 0.45
745 749 749 732 724 742

G21 768.667 5.888 -13.917 -0.308 0.26
772 772 764 768 760 776

G33 773.333 10.328 -9.251 -0.205 0.46
760 780 780 780 780 760
29
Day 1 Day 1
G31 804.710 22.693 22.126 0.489 1.01
802.32 827.94 809.62 794.88
766.9 826.6

G27 770.000 19.101 -12.584 -0.278 1
720 740 720 780 820 840

G24 750.000 10.954 -32.584 -0.721 0.49
740 740 760 760 760 740

G09 786.667 10.328 4.083 0.090 0.46
780 800 800 780 780 780

30
K & H VALUE GRAPH- ELONGATION AT BREAK (GLOVE)
AGED
31
UNAGED
Flagged Flagged
'H' 'K'

G17 24.350 0.432 -0.903 -0.507 0.41
25.2 24.3 24.3 24.2 24.1 24

G29 24.667 1.966 -0.586 -0.329 1.84 K
24 25 28 25 22 24

G15 25.660 0.957 0.407 0.229 0.9
25.71 27.42 25.74 24.92 24.72 25.45

G04 26.878 1.295 1.625 0.913 1.21
25.54 25.79 26.12 28.87 27.2 27.75

G13 24.063 0.756 -1.190 -0.668 0.71
24.57 23.04 23.19 24.24 24.57 24.77

G30 25.205 1.145 -0.048 -0.027 1.07
25.57 25.71 26.81 23.98 23.77 25.39

G11 25.745 0.723 0.492 0.276 0.68
25.41 25.93 24.57 26.01 26.75 25.8

G19 26.550 0.802 1.297 0.729 0.75
26.6 26.9 26.3 27.4 25.1 27

G06 26.000 0.961 0.747 0.420 0.9
25.4 24.6 25.7 26.6 27.3 26.4

G05 19.750 1.725 -5.503 -3.091 1.62 H
20.4 19.9 17.9 22.3 17.7 20.3

G02 24.183 0.861 -1.070 -0.601 0.81
23.1 24.7 23.1 25 24.8 24.4

G21 25.223 1.139 -0.030 -0.017 1.07
24.72 24.41 25.96 24.97 27.16 24.12
32
G33 24.800 0.510 -0.453 -0.255 0.48
25.2 24.5 24.3 25.6 24.4 24.8

G31 27.676 0.958 2.423 1.361 0.9
29.378 28.096 27.598 27.036 26.737 27.211

G27 27.523 0.948 2.270 1.275 0.89
26.99 27.23 29.32 26.83 27.82 26.95

G24 25.658 0.801 0.405 0.228 0.75
25.39 24.3 26.39 26.29 25.39 26.19

G09 25.370 1.000 0.117 0.066 0.94
25.09 25.46 26.44 26.42 25.04 23.77

33

G17 24.350 0.432 -1.247 -1.159 0.41
25.2 24.3 24.3 24.2 24.1 24

G29 24.667 0.984 -0.930 -0.865 1
24 25 28 25 22 24

G15 25.660 0.957 0.063 0.059 0.9
25.71 27.42 25.74 24.92 24.72 25.45

G04 26.878 1.295 1.281 1.191 1.21
25.54 25.79 26.12 28.87 27.2 27.75

G13 24.063 0.756 -1.534 -1.425 0.71
24.57 23.04 23.19 24.24 24.57 24.77

G30 25.205 1.145 -0.392 -0.364 1.07
25.57 25.71 26.81 23.98 23.77 25.39

G11 25.745 0.723 0.148 0.138 0.68
25.41 25.93 24.57 26.01 26.75 25.8

G19 26.550 0.802 0.953 0.886 0.75
26.6 26.9 26.3 27.4 25.1 27

G06 26.000 0.961 0.403 0.374 0.9
25.4 24.6 25.7 26.6 27.3 26.4

G05 25.597 1.725 0.000 0.000 1.62
20.4 19.9 17.9 22.3 17.7 20.3

G02 24.183 0.861 -1.414 -1.314 0.81
23.1 24.7 23.1 25 24.8 24.4

G21 25.223 1.139 -0.374 -0.347 1.07
24.72 24.41 25.96 24.97 27.16 24.12

G33 24.800 0.510 -0.797 -0.741 0.48
25.2 24.5 24.3 25.6 24.4 24.8
34
G31 27.676 0.958 2.079 1.932 0.9
29.378 28.096 27.598 27.036 26.737 27.211

G27 27.523 0.948 1.926 1.790 0.89
26.99 27.23 29.32 26.83 27.82 26.95

G24 25.658 0.801 0.061 0.057 0.75
25.39 24.3 26.39 26.29 25.39 26.19

G09 25.370 1.000 -0.227 -0.211 0.94
25.09 25.46 26.44 26.42 25.04 23.77

35
UNAGED
36
UNAGED
Flagged Flagged
'H' 'K'

G17 16.733 0.273 -0.585 -0.444 0.41
16.8 17.2 16.4 16.8 16.6 16.6

G29 16.983 1.068 -0.335 -0.254 1.6
16.1 17.5 18.4 17.2 15.4 17.3

G15 17.250 0.596 -0.068 -0.052 0.89
18.2 17.6 17.3 16.6 16.7 17.1

G04 18.288 0.353 0.970 0.737 0.53
17.73 18.11 18.18 18.71 18.47 18.53

G13 17.123 0.477 -0.195 -0.148 0.71
17.34 16.59 16.68 17.81 16.9 17.42

G30 17.638 0.908 0.320 0.243 1.36
18.41 18.15 18.05 16.71 16.27 18.24

G11 18.105 0.474 0.787 0.597 0.71
17.53 18.67 18.42 17.9 18.46 17.65

G19 18.567 0.398 1.248 0.948 0.6
18.7 18.5 18.1 19.2 18.2 18.7

G06 18.400 0.837 1.082 0.821 1.25
17.8 17.6 18 19.9 18.4 18.7

G05 12.950 0.758 -4.368 -3.317 1.13 H
13.2 12.9 12.1 14.3 12.5 12.7

G02 16.150 0.804 -1.168 -0.887 1.2
15.2 17 15.4 15.7 16.8 16.8

G21 17.293 0.698 -0.025 -0.019 1.04
16.58 16.43 17.59 17.91 18.12 17.13
37
G33 16.967 0.266 -0.352 -0.267 0.4
16.6 16.9 16.9 17.4 17.1 16.9

G31 17.404 0.474 0.086 0.065 0.71
18.056 16.973 17.036 17.8 16.972 17.589

G27 18.290 1.068 0.972 0.738 1.6
17.08 17.97 19.37 17.71 19.83 17.78

G24 18.202 0.538 0.883 0.671 0.8
17.98 17.78 19.1 18.58 17.7 18.07

G09 18.065 0.584 0.747 0.567 0.87
17.25 18.23 18.72 18.33 18.42 17.44

38
Flagged Flagged
'H' 'K'

G17 16.733 0.273 -0.858 -1.255 0.41
16.8 17.2 16.4 16.8 16.6 16.6

G29 16.983 1.068 -0.608 -0.889 1.6
16.1 17.5 18.4 17.2 15.4 17.3

G15 17.250 0.596 -0.341 -0.499 0.89
18.2 17.6 17.3 16.6 16.7 17.1

G04 18.288 0.353 0.697 1.020 0.53
17.73 18.11 18.18 18.71 18.47 18.53

G13 17.123 0.477 -0.468 -0.685 0.71
17.34 16.59 16.68 17.81 16.9 17.42

G30 17.638 0.908 0.047 0.069 1.36
18.41 18.15 18.05 16.71 16.27 18.24

G11 18.105 0.474 0.514 0.752 0.71
17.53 18.67 18.42 17.9 18.46 17.65

G19 18.567 0.398 0.975 1.427 0.6
18.7 18.5 18.1 19.2 18.2 18.7

G06 18.400 0.837 0.809 1.183 1.25
17.8 17.6 18 19.9 18.4 18.7

G05 17.591 0.758 0.000 0.000 1.13
13.2 12.9 12.1 14.3 12.5 12.7

G02 16.150 0.804 -1.441 -2.109 1.2
15.2 17 15.4 15.7 16.8 16.8

G21 17.293 0.698 -0.298 -0.436 1.04
16.58 16.43 17.59 17.91 18.12 17.13

G33 16.967 0.266 -0.625 -0.914 0.4
16.6 16.9 16.9 17.4 17.1 16.9
39
Day 2
G31 17.404 0.474 -0.187 -0.273 0.71
18.056 16.973 17.036 16.972 17.589
17.8

G27 18.290 1.068 0.699 1.022 1.6
17.08 17.97 19.37 17.71 19.83 17.78

G24 18.202 0.538 0.610 0.893 0.8
17.98 17.78 19.1 18.58 17.7 18.07

G09 18.065 0.584 0.474 0.693 0.87
17.25 18.23 18.72 18.33 18.42 17.44

40
UNAGED
41
UNAGED
Flagged Flagged
'H' 'K'

G17 768.000 10.040 -16.080 -0.440 0.92
782 773 761 775 757 760

G29 802.667 8.165 18.587 0.509 0.75
806 806 786 806 806 806

G15 904.000 13.145 119.920 3.283 1.21 H
920 888 896 900 920 900

G04 780.000 0.000 -4.080 -0.112 0
780 780 780 780 780 780

G13 808.333 9.832 24.254 0.664 0.9
810 800 820 820 800 800

G30 760.000 0.000 -24.080 -0.659 0
760 760 760 760 760 760
Day 1
G11 775.990 13.585 -8.090 -0.221 1.25
800.56 775.67 764.67 765.96 767.98
781.1

G19 799.167 16.005 15.087 0.413 1.47
825 806 806 786 786 786

G06 799.333 10.328 15.254 0.418 0.95
806 806 786 786 806 806

G05 741.667 15.161 -42.413 -1.161 1.39
744 751 720 733 738 764

G02 742.000 10.198 -42.080 -1.152 0.94
740 753 746 723 745 745

G21 767.000 6.164 -17.080 -0.468 0.57
760 768 772 764 776 762
42
G33 793.333 10.328 9.254 0.253 0.95
800 800 800 800 780 780

G31 781.200 7.202 -2.880 -0.079 0.66
785.89 773.27 790.38 775.05 786.42 776.19

G27 766.667 16.330 -17.413 -0.477 1.5
740 760 780 780 760 780

G24 770.000 10.954 -14.080 -0.385 1
760 780 780 780 760 760

G09 770.000 10.954 -14.080 -0.385 1
780 760 780 780 760 760

43
Flagged Flagged
'H' 'K'

G17 768.000 10.040 -8.585 -0.441 0.92
782 773 761 775 757 760

G29 802.667 8.165 26.082 1.339 0.75
806 806 786 806 806 806

G15 776.585 13.145 0.000 0.000 1.21
920 888 896 900 920 900

G04 780.000 0.000 3.415 0.175 0
780 780 780 780 780 780

G13 808.333 9.832 31.749 1.630 0.9
810 800 820 820 800 800

G30 760.000 0.000 -16.585 -0.851 0
760 760 760 760 760 760
Day 1
G11 775.990 13.585 -0.595 -0.031 1.25
800.56 775.67 764.67 765.96 767.98
781.1

G19 799.167 16.005 22.582 1.159 1.47
825 806 806 786 786 786

G06 799.333 10.328 22.749 1.168 0.95
806 806 786 786 806 806

G05 741.667 15.161 -34.918 -1.793 1.39
744 751 720 733 738 764

G02 742.000 10.198 -34.585 -1.776 0.94
740 753 746 723 745 745

G21 767.000 6.164 -9.585 -0.492 0.57
760 768 772 764 776 762

G33 793.333 10.328 16.749 0.860 0.95
800 800 800 800 780 780
44
G31 781.200 7.202 4.615 0.237 0.66
785.89 773.27 790.38 775.05 786.42 776.19

G27 766.667 16.330 -9.918 -0.509 1.5
740 760 780 780 760 780

G24 770.000 10.954 -6.585 -0.338 1
760 780 780 780 760 760

G09 770.000 10.954 -6.585 -0.338 1
780 760 780 780 760 760

45
UNAGED
46
SUMMARY OF TENSILE STRENGTH (DUMBBELS)
AGED
Flagged Flagged
'H' 'K'

G17 22.867 0.852 0.119 0.073 0.71
21.6 23.2 22.5 24.2 22.9 22.8

G29 23.167 1.329 0.419 0.258 1.1
21 25 23 23 23 24

G15 22.455 1.140 -0.293 -0.180 0.94
24.03 23.61 21.08 21.73 21.96 22.32

G04 24.100 0.829 1.352 0.833 0.69
24.63 23.77 23.48 25.15 22.96 24.61

G13 21.272 0.563 -1.476 -0.910 0.47
21.64 20.85 20.67 21.92 20.78 21.77

G30 20.188 2.905 -2.559 -1.577 2.41 K
23.24 22.83 22.37 17.57 17.07 18.05

G11 22.147 0.382 -0.601 -0.370 0.32
22.75 21.7 22.05 21.81 22.23 22.34

G19 24.200 0.901 1.452 0.895 0.75
24.9 24.7 25.1 24.3 22.9 23.3

G06 24.267 0.680 1.519 0.936 0.56
25.3 24.6 23.8 24.6 23.5 23.8

G05 18.867 1.572 -3.881 -2.391 1.3
19.8 20.2 15.9 18.7 19.8 18.8

G02 24.983 0.794 2.236 1.377 0.66
24 24.9 24.5 26.2 24.7 25.6

G21 21.068 1.425 -1.679 -1.035 1.18
22.1 19.94 19.07 22.04 22.69 20.57
47
G33 23.067 0.599 0.319 0.196 0.5
22.1 23 22.9 23.8 23 23.6

G31 24.051 1.209 1.303 0.803 1
22.898 22.752 23.548 24.252 25.749 25.105

G27 23.838 1.058 1.091 0.672 0.88
25.46 23.47 23.84 24.55 23.3 22.41

G24 23.553 0.767 0.806 0.496 0.64
22.23 23.46 23.76 23.52 23.75 24.6

G09 22.623 1.205 -0.124 -0.077 1
23.28 21.54 20.78 22.9 23.93 23.31

48
Lab Flagged Flagged

Test Result x` s d h k
Code 'H' 'K'
G17 22.867 0.852 0.119 0.073 0.71
21.6 23.2 22.5 24.2 22.9 22.8

G29 23.167 1.329 0.419 0.258 1.1
21 25 23 23 23 24

G15 22.455 1.140 -0.293-0.180 0.94
24.03 23.61 21.08 21.73 21.96 22.32

G04 24.100 0.829 1.352 0.833 0.69
24.63 23.77 23.48 25.15 22.96 24.61

G13 21.272 0.563 -1.476-0.910 0.47
21.64 20.85 20.67 21.92 20.78 21.77

G30 20.188 1.010 -2.559-1.577 1
23.24 22.83 22.37 17.57 17.07 18.05

G11 22.147 0.382 -0.601-0.370 0.32
22.75 21.7 22.05 21.81 22.23 22.34

G19 24.200 0.901 1.452 0.895 0.75
24.9 24.7 25.1 24.3 22.9 23.3

G06 24.267 0.680 1.519 0.936 0.56
25.3 24.6 23.8 24.6 23.5 23.8

G05 18.867 1.572 -3.881-2.391 1.3
19.8 20.2 15.9 18.7 19.8 18.8

G02 24.983 0.794 2.236 1.377 0.66
24 24.9 24.5 26.2 24.7 25.6

G21 21.068 1.425 -1.679-1.035 1.18
22.1 19.94 19.07 22.04 22.69 20.57

G33 23.067 0.599 0.319 0.196 0.5
22.1 23 22.9 23.8 23 23.6
49
G31 24.051 1.209 1.303 0.803 1
22.898 22.752 23.548 24.252 25.749 25.105

G27 23.838 1.058 1.091 0.672 0.88
25.46 23.47 23.84 24.55 23.3 22.41

G24 23.553 0.767 0.806 0.496 0.64
22.23 23.46 23.76 23.52 23.75 24.6

G09 22.623 1.205 -0.124-0.077 1
23.28 21.54 20.78 22.9 23.93 23.31

50
K & H VALUE GRAPH- F TENSILE STRENGTH (DUMBBELS)
AGED
51
SUMMARY OF FORCE AT BREAK (DUMBBELL)
AGED
Flagged Flagged
'H' 'K'

G17 16.167 0.622 0.646 0.719 0.79
15.2 16.3 16 17.1 16.4 16

G29 15.933 0.946 0.412 0.459 1.21
14.5 17.1 16.6 16 15.2 16.2

G15 15.400 0.959 -0.121 -0.134 1.22
17.3 15.4 14.9 14.7 15.1 15

G04 16.210 0.579 0.689 0.767 0.74
16.17 15.93 16.28 17.2 15.43 16.25

G13 15.248 0.530 -0.273 -0.303 0.68
15.17 15.2 14.35 15.88 15.21 15.68

G30 13.712 1.717 -1.809 -2.013 2.19 K
15.44 15.07 15.16 11.6 12.04 12.96

G11 15.232 0.380 -0.289 -0.322 0.49
15.01 14.73 15.22 15.16 15.85 15.42

G19 16.583 0.349 1.062 1.182 0.45
16.9 16.9 16.9 16.3 16.2 16.3

G06 15.650 0.524 0.129 0.144 0.67
16.3 15.8 15.7 15.8 15.6 14.7

G05 13.300 0.465 -2.221 -2.471 0.59
13.5 13.8 13.8 13.1 12.8 12.8

G02 16.400 1.135 0.879 0.978 1.45
15.4 16.5 14.7 17.7 17 17.1

G21 14.913 0.332 -0.608 -0.676 0.42
14.67 14.96 14.52 15.46 15.07 14.8

G33 15.733 0.427 0.212 0.236 0.55
15.2 15.2 15.8 16.1 16 16.1
52
G31 15.406 0.638 -0.115 -0.127 0.81
15.166 14.562 14.929 15.544 16.169 16.068

G27 15.627 0.897 0.106 0.118 1.14
16.8 15.49 15.74 16.21 15.38 14.14

G24 16.545 0.646 1.024 1.140 0.83
15.43 16.56 16.5 16.48 16.92 17.38

G09 15.795 0.833 0.274 0.305 1.06
16.37 14.7 15.29 15.48 17.05 15.88

53
Flagged Flagged
'H' 'K'
G17 16.167 0.622 0.646 0.719 0.79
15.2 16.3 16 17.1 16.4 16

G29 15.933 0.946 0.412 0.459 1.21
14.5 17.1 16.6 16 15.2 16.2

G15 15.400 0.959 -0.121 -0.134 1.22
17.3 15.4 14.9 14.7 15.1 15

G04 16.210 0.579 0.689 0.767 0.74
16.17 15.93 16.28 17.2 15.43 16.25

G13 15.248 0.530 -0.273 -0.303 0.68
15.17 15.2 14.35 15.88 15.21 15.68

G30 13.712 0.684 -1.809 -2.013 1
15.44 15.07 15.16 11.6 12.04 12.96

G11 15.232 0.380 -0.289 -0.322 0.49
15.01 14.73 15.22 15.16 15.85 15.42

G19 16.583 0.349 1.062 1.182 0.45
16.9 16.9 16.9 16.3 16.2 16.3

G06 15.650 0.524 0.129 0.144 0.67
16.3 15.8 15.7 15.8 15.6 14.7

G05 13.300 0.465 -2.221 -2.471 0.59
13.5 13.8 13.8 13.1 12.8 12.8

G02 16.400 1.135 0.879 0.978 1.45
15.4 16.5 14.7 17.7 17 17.1

G21 14.913 0.332 -0.608 -0.676 0.42
14.67 14.96 14.52 15.46 15.07 14.8

G33 15.733 0.427 0.212 0.236 0.55
15.2 15.2 15.8 16.1 16 16.1
54
G31 15.406 0.638 -0.115 -0.127 0.81
15.166 14.562 14.929 15.544 16.169 16.068

G27 15.627 0.897 0.106 0.118 1.14
16.8 15.49 15.74 16.21 15.38 14.14

G24 16.545 0.646 1.024 1.140 0.83
15.43 16.56 16.5 16.48 16.92 17.38

G09 15.795 0.833 0.274 0.305 1.06
16.37 14.7 15.29 15.48 17.05 15.88

55
K & H VALUE GRAPH- FORCE AT BREAK (DUMBBELL)
AGED
56
SUMMARY OF ELONGATION AT BREAK (DUMBBELLS)
AGED
Flagged Flagged
'H' 'K'

G17 767.000 6.419 -3.412 -0.074 0.29
761 765 759 774 774 769

G29 808.833 44.079 38.421 0.831 2 K
766 806 746 845 845 845

G15 852.000 13.387 81.588 1.765 0.61
868 860 864 840 840 840

G04 753.333 20.656 -17.079 -0.370 0.94
740 740 740 780 740 780

G13 868.333 22.286 97.921 2.119 1.01
880 880 900 850 860 840

G30 730.000 41.473 -40.412 -0.874 1.88 K
780 760 760 680 700 700

G11 673.693 10.926 -96.719 -2.093 0.5
679.3 689.86 674.91 662.72 660.27 675.1

G19 756.167 20.692 -14.245 -0.308 0.94
786 766 766 746 727 746

G06 766.167 21.545 -4.245 -0.092 0.98
786 766 766 766 786 727

G05 734.450 9.937 -35.962 -0.778 0.45
731 724 725 740.7 750 736

G02 752.167 12.624 -18.245 -0.395 0.57
748 768 766 746 735 750

G21 749.333 6.532 -21.079 -0.456 0.3
748 748 740 760 748 752
57
G33 786.667 10.328 16.255 0.352 0.47
800 780 780 780 780 800

G31 815.530 8.998 45.118 0.976 0.41
830.7 818.09 808.39 806.47 810.65 818.88

G27 766.667 37.238 -3.745 -0.081 1.69
740 740 720 800 800 800

G24 746.667 10.328 -23.745 -0.514 0.47
740 760 740 740 760 740

G09 770.000 20.976 -0.412 -0.009 0.95
800 780 780 760 760 740

58
Flagged Flagged
'H' 'K'
Day 2
G17 767.000 6.419 -3.412 -0.074 0.29
769
761 765 759 774 774

G29 808.833 19.839 38.421 0.831 1
766 806 746 845 845 845

G15 852.000 13.387 81.588 1.765 0.61
868 860 864 840 840 840

G04 753.333 20.656 -17.079 -0.370 0.94
740 740 740 780 740 780

G13 868.333 22.286 97.921 2.119 1.01
880 880 900 850 860 840

G30 730.000 17.626 -40.412 -0.874 1
780 760 760 680 700 700
Day 1 Day 2
G11 673.693 10.926 -96.719 -2.093 0.5
689.86 674.91 662.72 660.27
679.3 675.1

G19 756.167 20.692 -14.245 -0.308 0.94
786 766 766 746 727 746

G06 766.167 21.545 -4.245 -0.092 0.98
786 766 766 766 786 727

G05 734.450 9.937 -35.962 -0.778 0.45
731 724 725 740.7 750 736

G02 752.167 12.624 -18.245 -0.395 0.57
748 768 766 746 735 750

G21 749.333 6.532 -21.079 -0.456 0.3
748 748 740 760 748 752
59
G33 786.667 10.328 16.255 0.352 0.47
800 780 780 780 780 800
Day
G31 1 815.530 8.998 45.118 0.976 0.41
818.09 808.39 806.47 810.65 818.88
830.7

G27 766.667 37.238 -3.745 -0.081 1.69
740 740 720 800 800 800

G24 746.667 10.328 -23.745 -0.514 0.47
740 760 740 740 760 740

G09 770.000 20.976 -0.412 -0.009 0.95
800 780 780 760 760 740

60
K & H VALUE GRAPH- ELONGATION AT BREAK (DUMBBELLS)
AGED
61
SUMMARY OF TENSILE STRENGTH (DUMBBELLS)
UNAGED

G17 24.567 0.234 0.248 0.141 0.28
24.1 24.7 24.7 24.6 24.6 24.7

G29 23.000 1.095 -1.319 -0.752 1.3
23 23 25 22 22 23

G15 23.960 0.695 -0.359 -0.204 0.82
24.78 23.21 23.13 23.99 23.99 24.66

G04 25.947 0.529 1.628 0.928 0.63
25.29 26.27 26.16 26.16 26.52 25.28

G13 23.538 0.771 -0.780 -0.445 0.91
23.96 24.49 23.85 23.72 22.52 22.69

G30 24.465 1.191 0.146 0.083 1.41
23.49 25.98 24.52 24.78 25.3 22.72

G11 23.097 0.571 -1.222 -0.697 0.68
22.84 22.85 24.08 22.93 23.42 22.46

G19 25.383 0.806 1.065 0.607 0.95
26.1 24.6 25.9 24.9 24.5 26.3

G06 24.433 0.557 0.115 0.065 0.66
24 24 23.9 25.3 24.7 24.7

G05 19.050 1.494 -5.269 -3.004 1.77 H
19.5 18.9 18.2 17.3 18.7 21.7

G02 24.783 1.102 0.465 0.265 1.3
23.3 25.4 23.6 25.7 25.9 24.8

G21 23.532 0.524 -0.787 -0.449 0.62
24.2 22.92 23.56 23.29 24.1 23.12
62
G33 25.150 0.288 0.831 0.474 0.34
25.2 24.7 25.3 25.4 24.9 25.4
Day 2
G31 27.249 0.718 2.930 1.670 0.85
26.252 26.876 27.472 27.405 28.408
27.08

G27 25.830 0.824 1.511 0.862 0.98
25.72 24.45 26.03 27.02 25.79 25.97

G24 25.392 0.797 1.073 0.612 0.94
24.17 25.49 25.07 25.12 26.15 26.35

G09 24.042 1.091 -0.277 -0.158 1.29
24.68 24.85 23.78 22.41 25.28 23.25

63
Flagged Flagged
'H' 'K'
Day 2
G17 24.567 0.234 -0.081 -0.073 0.28
24.7
24.1 24.7 24.7 24.6 24.6

G29 23.000 1.095 -1.648 -1.484 1.3
23 23 25 22 22 23

G15 23.960 0.695 -0.688 -0.619 0.82
24.78 23.21 23.13 23.99 23.99 24.66

G04 25.947 0.529 1.299 1.169 0.63
25.29 26.27 26.16 26.16 26.52 25.28

G13 23.538 0.771 -1.110 -0.999 0.91
23.96 24.49 23.85 23.72 22.52 22.69

G30 24.465 1.191 -0.183 -0.165 1.41
23.49 25.98 24.52 24.78 25.3 22.72

G11 23.097 0.571 -1.551 -1.397 0.68
22.84 22.85 24.08 22.93 23.42 22.46

G19 25.383 0.806 0.735 0.662 0.95
26.1 24.6 25.9 24.9 24.5 26.3

G06 24.433 0.557 -0.215 -0.193 0.66
24 24 23.9 25.3 24.7 24.7

G05 24.648 1.494 0.000 0.000 1.77
19.5 18.9 18.2 17.3 18.7 21.7

G02 24.783 1.102 0.135 0.122 1.3
23.3 25.4 23.6 25.7 25.9 24.8

G21 23.532 0.524 -1.116 -1.005 0.62
24.2 22.92 23.56 23.29 24.1 23.12
64
G33 25.150 0.288 0.502 0.452 0.34
25.2 24.7 25.3 25.4 24.9 25.4
Day
G31 2 27.249 0.718 2.601 2.342 0.85
26.252 26.876 27.472 27.405 28.408
27.08

G27 25.830 0.824 1.182 1.064 0.98
25.72 24.45 26.03 27.02 25.79 25.97

G24 25.392 0.797 0.744 0.670 0.94
24.17 25.49 25.07 25.12 26.15 26.35

G09 24.042 1.091 -0.606 -0.546 1.29
24.68 24.85 23.78 22.41 25.28 23.25

65
K & H VALUE GRAPH- TENSILE STRENGTH (DUMBBELLS)
UNAGED
66
SUMMARY OF FORCE AT BREAK (DUMBBELLS)
UNAGED
Flagged Flagged
'H' 'K'

G17 17.083 0.431 0.435 0.379 0.72
16.4 16.8 17.4 17.1 17.6 17.2

G29 15.817 0.833 -0.832 -0.725 1.39
15.2 16.3 17.3 15.4 15.5 15.2

G15 16.300 0.537 -0.348 -0.303 0.89
16.8 15.6 15.8 16.7 16.1 16.8

G04 17.340 0.303 0.692 0.603 0.5
16.84 17.49 17.27 17.43 17.26 17.75

G13 16.613 0.697 -0.035 -0.030 1.16
17.16 17.32 16.99 16.68 15.91 15.62

G30 16.812 0.739 0.163 0.142 1.23
16.89 17.15 17.65 16.42 17.21 15.55

G11 16.125 0.452 -0.523 -0.456 0.75
16.11 15.76 16.99 15.82 16.16 15.91

G19 17.700 0.502 1.052 0.917 0.83
17.9 17 18.5 17.5 17.5 17.8

G06 16.917 0.392 0.268 0.234 0.65
17.2 16.8 16.2 17 17.3 17

G05 12.767 0.712 -3.882 -3.383 1.18 H
13.2 12.6 12.6 12.5 11.8 13.9

G02 16.667 0.841 0.018 0.016 1.4
16.1 17.5 15.3 17 17.4 16.7

G21 16.868 0.531 0.220 0.192 0.88
17.43 16.5 16.45 16.77 17.63 16.43
G33 17.133 0.314 0.485 0.423 0.52

67
17.1 16.8 16.8 17.5 17.1 17.5

G31 17.608 0.390 0.960 0.837 0.65
17.388 17.039 17.548 17.66 17.833 18.182

G27 16.455 0.429 -0.193 -0.168 0.71
16.95 15.86 16.84 16.64 16.34 16.1

G24 17.975 0.563 1.327 1.156 0.94
17.22 18.01 17.56 17.83 18.61 18.62

G09 16.840 0.999 0.192 0.167 1.66
17.05 18.33 16.56 15.29 17.25 16.56

68
Flagged Flagged
'H' 'K'
Day 2
G17 17.083 0.431 0.193 0.342 0.72
17.2
16.4 16.8 17.4 17.1 17.6

G29 15.817 0.833 -1.074 -1.910 1.39
15.2 16.3 17.3 15.4 15.5 15.2

G15 16.300 0.537 -0.591 -1.051 0.89
16.8 15.6 15.8 16.7 16.1 16.8

G04 17.340 0.303 0.449 0.799 0.5
16.84 17.49 17.27 17.43 17.26 17.75

G13 16.613 0.697 -0.277 -0.493 1.16
17.16 17.32 16.99 16.68 15.91 15.62

G30 16.812 0.739 -0.079 -0.141 1.23
16.89 17.15 17.65 16.42 17.21 15.55

G11 16.125 0.452 -0.766 -1.362 0.75
16.11 15.76 16.99 15.82 16.16 15.91

G19 17.700 0.502 0.809 1.439 0.83
17.9 17 18.5 17.5 17.5 17.8

G06 16.917 0.392 0.026 0.046 0.65
17.2 16.8 16.2 17 17.3 17

G05 16.891 0.712 0.000 0.000 1.18
13.2 12.6 12.6 12.5 11.8 13.9

G02 16.667 0.841 -0.224 -0.399 1.4
16.1 17.5 15.3 17 17.4 16.7

G21 16.868 0.531 -0.023 -0.040 0.88
17.43 16.5 16.45 16.77 17.63 16.43
69
G33 17.133 0.314 0.243 0.431 0.52
17.1 16.8 16.8 17.5 17.1 17.5
Day
G31 2 17.608 0.390 0.718 1.276 0.65
17.388 17.039 17.548 17.833 18.182
17.66

G27 16.455 0.429 -0.436 -0.775 0.71
16.95 15.86 16.84 16.64 16.34 16.1

G24 17.975 0.563 1.084 1.928 0.94
17.22 18.01 17.56 17.83 18.61 18.62

G09 16.840 0.999 -0.051 -0.090 1.66
17.05 18.33 16.56 15.29 17.25 16.56

70
K & H VALUE GRAPH- FORCE AT BREAK (DUMBBELLS)
UNAGED
71
UNAGED
Flagged Flagged
'H' 'K'

G17 762.833 6.178 -10.527 -0.332 0.51
757 764 771 755 762 768

G29 782.667 8.165 9.306 0.294 0.67
786 766 786 786 786 786

G15 879.333 11.147 105.973 3.342 0.91 H
880 880 868 872 900 876

G04 766.667 20.656 -6.694 -0.211 1.69
780 780 780 780 740 740

G13 800.000 6.325 26.639 0.840 0.52
800 790 800 810 800 800

G30 753.333 10.328 -20.027 -0.632 0.85
760 760 760 740 760 740

G11 755.513 10.842 -17.847 -0.563 0.89
759.87 764.98 769.21 744.11 743.48 751.43

G19 776.000 16.733 2.639 0.083 1.37
766 746 786 786 786 786

G06 769.333 8.165 -4.027 -0.127 0.67
766 766 786 766 766 766

G05 740.483 17.005 -32.877 -1.037 1.39
757 724 758.9 730 751 722

G02 740.167 4.708 -33.194 -1.047 0.39
743 746 735 744 737 736

G21 754.000 6.066 -19.361 -0.611 0.5
764 756 748 756 752 748
72
G33 790.000 16.733 16.639 0.525 1.37
800 800 800 760 780 800

G31 780.133 12.097 6.773 0.214 0.99
770.71 767.73 790.5 797.69 771.85 782.32

G27 763.333 8.165 -10.027 -0.316 0.67
760 760 760 760 780 760

G24 760.000 17.889 -13.361 -0.421 1.47
780 780 760 740 740 760

G09 773.333 10.328 -0.027 -0.001 0.85
780 780 760 760 780 780

73
Flagged Flagged
'H' 'K'
G17 762.833 6.178 -3.904 -0.242 0.51
757 764 771 755 762 768

G29 782.667 8.165 15.929 0.989 0.67
786 766 786 786 786 786

G15 766.737 11.147 0.000 0.000 0.91
880 880 868 872 900 876

G04 766.667 20.656 -0.071 -0.004 1.69
780 780 780 780 740 740

G13 800.000 6.325 33.263 2.065 0.52
800 790 800 810 800 800
Day 1 Day 1 Day 1 Day 2 Day 2 Day 2 -

G30 753.333 10.328 -0.832 0.85
760 760 760 740 760 740 13.404
G11 755.513 10.842 -0.697 0.89
759.87 764.98 769.21 744.11 743.48 751.43 11.224
G19 776.000 16.733 9.263 0.575 1.37
766 746 786 786 786 786

G06 769.333 8.165 2.596 0.161 0.67
766 766 786 766 766 766

G05 740.483 17.005 -1.630 1.39
757 724 758.9 730 751 722 26.254
G02 740.167 4.708 -1.649 0.39
743 746 735 744 737 736 26.571
G21 754.000 6.066 -0.791 0.5
764 756 748 756 752 748 12.737
G33 790.000 16.733 23.263 1.444 1.37
800 800 800 760 780 800
74
Day 1
G31 780.133 12.097 13.396 0.832 0.99
770.71 767.73 797.69 771.85 782.32
790.5

G27 763.333 8.165 -3.404 -0.211 0.67
760 760 760 760 780 760

G24 760.000 17.889 -6.737 -0.418 1.47
780 780 760 740 740 760

G09 773.333 10.328 6.596 0.409 0.85
780 780 760 760 780 780

75
UNAGED
76
GROUP 2
77
AGED
Flagged Flagged
'H' 'K'

G03 21.898 1.564 -2.039 -1.078 1.16
19.43 23.25 23.37 20.93 22.92 21.49

G08 19.622 3.424 -4.316 -2.281 2.55 K
23.15 23.98 20.55 16.82 16.18 17.05

G10 25.864 1.173 1.927 1.019 0.87
24.697 24.409 26.01 27.506 26.693 25.87

G12 24.147 0.804 0.209 0.111 0.6
23.97 23.34 24.7 25.05 24.72 23.1

G14 26.325 0.900 2.388 1.262 0.67
27.59 26.02 26.98 26.25 24.95 26.16

G16 24.765 1.732 0.828 0.438 1.29
26.97 26.14 25.22 24.11 24.05 22.1

G18 24.413 0.393 0.476 0.252 0.29
24.24 24 24.1 24.43 25.06 24.65

G20 24.000 0.632 0.063 0.033 0.47
25 24 24 23 24 24

G23 24.110 0.799 0.173 0.091 0.59
24.03 24.37 24.03 24.72 22.64 24.87

G25 25.888 0.496 1.951 1.031 0.37
25.55 26.25 25.47 26.15 26.56 25.35

G32 24.833 0.929 0.896 0.474 0.69
25.6 25.3 24.6 24.1 23.5 25.9

G26 24.198 0.668 0.261 0.138 0.5
23.62 24.97 23.3 24.17 24.9 24.23
78
G35 24.833 0.408 0.896 0.474 0.3
25 25 25 24 25 25

G07 25.290 0.975 1.353 0.715 0.73
24.93 25.76 25.21 26.06 26.21 23.57

G28 21.778 1.607 -2.159 -1.141 1.2
21.9 19.38 20.93 24.09 21.57 22.8

G22 20.500 1.915 -3.437 -1.817 1.43
22.7 20.4 22.2 20.9 19.3 17.5

G01 24.468 0.760 0.531 0.281 0.57
23.87 23.71 24.3 24.67 24.42 25.84

79
Lab Flagged Flagged

Code 'H' 'K'

G03 21.898 1.564 -2.039 -1.078 1.16
19.43 23.25 23.37 20.93 22.92 21.49

G08 19.622 1.089 -4.316 -2.281 1
23.15 23.98 20.55 16.82 16.18 17.05

G10 25.864 1.173 1.927 1.019 0.87
24.697 24.409 26.01 27.506 26.693 25.87

G12 24.147 0.804 0.209 0.111 0.6
23.97 23.34 24.7 25.05 24.72 23.1

G14 26.325 0.900 2.388 1.262 0.67
27.59 26.02 26.98 26.25 24.95 26.16

G16 24.765 1.732 0.828 0.438 1.29
26.97 26.14 25.22 24.11 24.05 22.1

G18 24.413 0.393 0.476 0.252 0.29
24.24 24 24.1 24.43 25.06 24.65

G20 24.000 0.632 0.063 0.033 0.47
25 24 24 23 24 24

G23 24.110 0.799 0.173 0.091 0.59
24.03 24.37 24.03 24.72 22.64 24.87

G25 25.888 0.496 1.951 1.031 0.37
25.55 26.25 25.47 26.15 26.56 25.35

G32 24.833 0.929 0.896 0.474 0.69
25.6 25.3 24.6 24.1 23.5 25.9

G26 24.198 0.668 0.261 0.138 0.5
23.62 24.97 23.3 24.17 24.9 24.23
80
G35 24.833 0.408 0.896 0.474 0.3
25 25 25 24 25 25

G07 25.290 0.975 1.353 0.715 0.73
24.93 25.76 25.21 26.06 26.21 23.57

G28 21.778 1.607 -2.159 -1.141 1.2
21.9 19.38 20.93 24.09 21.57 22.8

G22 20.500 1.915 -3.437 -1.817 1.43
22.7 20.4 22.2 20.9 19.3 17.5

G01 24.468 0.760 0.531 0.281 0.57
23.87 23.71 24.3 24.67 24.42 25.84

81
AGED
82
AGED
Flagged Flagged
'H' 'K'

G01 17.340 0.602 0.927 0.805 0.65
17.04 16.88 17.35 17.46 16.85 18.46

G03 15.680 0.977 -0.733 -0.637 1.05
14.07 16.41 16.63 15.1 16.31 15.56

G07 16.850 0.628 0.437 0.380 0.68
16.9 17 17.7 17.1 16.6 15.8

G08 13.682 2.170 -2.731 -2.372 2.34 K
16.56 15.44 14.77 11.94 11.59 11.79

G10 16.931 0.804 0.518 0.450 0.87
16.726 16.011 16.331 18.112 17.673 16.734

G14 18.168 0.786 1.755 1.525 0.85
19.56 17.86 18.3 18.04 17.16 18.09

G16 17.215 1.189 0.802 0.697 1.28
18.94 17.42 17.55 17.36 16.72 15.3

G18 17.315 0.562 0.902 0.783 0.61
17.45 17.56 17.49 16.27 17.92 17.2

G20 16.833 0.720 0.420 0.365 0.78
17.6 17.3 17.5 16 16.5 16.1

G22 14.233 0.812 -2.180 -1.893 0.87
15.2 13.3 15 14.4 14.2 13.3

G23 16.725 0.782 0.312 0.271 0.84
16.56 15.29 17.15 17.44 16.66 17.25

G25 17.087 0.329 0.674 0.585 0.35
16.86 17.33 16.81 17.26 17.53 16.73

G28 15.698 1.139 -0.715 -0.621 1.23
15.46 13.85 15.02 16.63 16.59 16.64
83
G32 16.633 0.700 0.220 0.191 0.75
17 16.9 17.2 15.6 15.9 17.2

G26 15.318 0.423 -1.095 -0.951 0.46
14.95 15.81 14.75 15.3 15.76 15.34

G35 16.683 0.838 0.270 0.235 0.9
17.3 17.6 16.9 15.7 15.6 17

G12 16.628 0.826 0.215 0.187 0.89
15.82 15.84 16.45 18.03 17 16.63

84
Lab Flagged Flagged

Code 'H' 'K'
G01 17.340 0.602 0.927 0.805 0.65
17.04 16.88 17.35 17.46 16.85 18.46

G03 15.680 0.977 -0.733-0.637 1.05
14.07 16.41 16.63 15.1 16.31 15.56

G07 16.850 0.628 0.437 0.380 0.68
16.9 17 17.7 17.1 16.6 15.8

G08 13.682 0.789 -2.731-2.372 1
16.56 15.44 14.77 11.94 11.59 11.79

G10 16.931 0.804 0.518 0.450 0.87
16.726 16.011 16.331 18.112 17.673 16.734

G14 18.168 0.786 1.755 1.525 0.85
19.56 17.86 18.3 18.04 17.16 18.09

G16 17.215 1.189 0.802 0.697 1.28
18.94 17.42 17.55 17.36 16.72 15.3

G18 17.315 0.562 0.902 0.783 0.61
17.45 17.56 17.49 16.27 17.92 17.2

G20 16.833 0.720 0.420 0.365 0.78
17.6 17.3 17.5 16 16.5 16.1

G22 14.233 0.812 -2.180-1.893 0.87
15.2 13.3 15 14.4 14.2 13.3

G23 16.725 0.782 0.312 0.271 0.84
16.56 15.29 17.15 17.44 16.66 17.25

G25 17.087 0.329 0.674 0.585 0.35
16.86 17.33 16.81 17.26 17.53 16.73

G28 15.698 1.139 -0.715-0.621 1.23
15.46 13.85 15.02 16.63 16.59 16.64
85
G32 16.633 0.700 0.220 0.191 0.75
17 16.9 17.2 15.6 15.9 17.2

G26 15.318 0.423 -1.095-0.951 0.46
14.95 15.81 14.75 15.3 15.76 15.34

G35 16.683 0.838 0.270 0.235 0.9
17.3 17.6 16.9 15.7 15.6 17

G12 16.628 0.826 0.215 0.187 0.89
15.82 15.84 16.45 18.03 17 16.63

86
AGED
87
AGED
Flagged Flagged
'H' 'K'

G01 753.333 10.328 -41.450 -0.949 0.51
740 740 760 760 760 760

G03 841.667 11.690 46.884 1.074 0.58
830 860 850 840 840 830

G07 882.000 20.823 87.217 1.998 1.03
900 900 900 868 872 852

G08 727.167 40.534 -67.616 -1.549 2 K
764 779 743 706 685 686

G10 805.208 9.152 10.425 0.239 0.45
801.44 822.6 796.38 801.44 806.87 802.52

G12 753.333 10.328 -41.450 -0.949 0.51
740 760 760 760 760 740

G14 766.667 20.656 -28.116 -0.644 1.02
780 740 780 780 740 780

G16 773.333 45.019 -21.450 -0.491 2.22 K
800 820 820 740 740 720

G18 762.438 17.132 -32.345 -0.741 0.85
751.41 761.93 741.2 785.82 779.46 754.81

G20 838.500 20.335 43.717 1.001 1
845 825 806 845 865 845

G22 755.667 11.928 -39.116 -0.896 0.59
773 744 766 755 743 753

G23 776.667 15.055 -18.116 -0.415 0.74
780 780 780 800 760 760

G25 826.667 10.328 31.884 0.730 0.51
840 820 840 820 820 820
88
G26 780.833 7.360 -13.950 -0.320 0.36
775 790 770 780 785 785

G28 853.333 19.664 58.550 1.341 0.97
860 850 880 860 820 850

G32 779.333 10.328 -15.450 -0.354 0.51
786 786 786 766 766 786

G35 835.167 16.376 40.384 0.925 0.81
825 845 806 845 845 845

89
Flagged Flagged
'H' 'K'
Day 2
G01 753.333 10.328 -41.450 -0.949 0.51
760
740 740 760 760 760

G03 841.667 11.690 46.884 1.074 0.58
830 860 850 840 840 830

G07 882.000 20.823 87.217 1.998 1.03
900 900 900 868 872 852

G08 727.167 18.233 -67.616 -1.549 1
764 779 743 706 685 686
Day
G10 1 805.208 9.152 10.425 0.239 0.45
801.44 796.38 801.44 806.87 802.52
822.6

G12 753.333 10.328 -41.450 -0.949 0.51
740 760 760 760 760 740

G14 766.667 20.656 -28.116 -0.644 1.02
780 740 780 780 740 780

G16 773.333 15.051 -21.450 -0.491 1
800 820 820 740 740 720
Day
G18 1 762.438 17.132 -32.345 -0.741 0.85
751.41 761.93 785.82 779.46 754.81
741.2

G20 838.500 20.335 43.717 1.001 1
845 825 806 845 865 845

G22 755.667 11.928 -39.116 -0.896 0.59
773 744 766 755 743 753

G23 776.667 15.055 -18.116 -0.415 0.74
780 780 780 800 760 760

G25 826.667 10.328 31.884 0.730 0.51
840 820 840 820 820 820
90
G26 780.833 7.360 -13.950 -0.320 0.36
775 790 770 780 785 785

G28 853.333 19.664 58.550 1.341 0.97
860 850 880 860 820 850

G32 779.333 10.328 -15.450 -0.354 0.51
786 786 786 766 766 786

G35 835.167 16.376 40.384 0.925 0.81
825 845 806 845 845 845

91
AGED
92
UNAGED
Flagged Flagged
'H' 'K'

G01 25.920 0.771 0.366 0.192 0.64
25.12 25 26.58 26.74 26.46 25.62

G03 23.450 0.628 -2.104 -1.106 0.52
23.73 24.26 22.81 22.7 23.93 23.27

G07 26.042 0.827 0.487 0.256 0.69
26.13 25.56 26.76 26.79 24.63 26.38

G08 22.415 2.332 -3.139 -1.650 1.94 K
19.87 24.23 25.37 20.54 20.64 23.84

G10 28.671 0.890 3.116 1.638 0.74
28.211 28.839 27.09 29.201 29.486 29.197

G12 25.420 2.013 -0.134 -0.071 1.68
27.14 26.54 27.7 24.89 22.98 23.27

G14 28.058 0.993 2.504 1.316 0.83
27.71 26.6 27.62 29.18 28.07 29.17

G16 27.142 0.965 1.587 0.834 0.8
28.86 26.78 27.44 26.36 26.21 27.2

G18 26.832 1.011 1.277 0.671 0.84
26.05 26.39 25.44 27.49 27.91 27.71

G20 25.833 1.169 0.279 0.147 0.97
26 27 27 25 24 26

G22 21.900 1.343 -3.654 -1.921 1.12
22.5 21.2 21.3 20.5 24.3 21.6

G23 23.767 1.562 -1.788 -0.940 1.3
24.65 25.35 24.91 23.35 21.09 23.25
93
G25 27.592 0.760 2.037 1.071 0.63
27.39 26.9 28.36 26.66 27.7 28.54

G26 25.127 1.226 -0.428 -0.225 1.02
23.85 25.86 27.04 24.82 25.31 23.88

G28 24.240 0.830 -1.314 -0.691 0.69
24.71 23.31 23.28 25.27 24.82 24.05

G32 26.017 0.884 0.462 0.243 0.74
25.9 26.5 24.7 25.4 27.2 26.4

G35 26.000 0.632 0.446 0.234 0.53
26 26 27 26 26 25

94
Lab Flagged Flagged

Code 'H' 'K'
Day 2
G01 18.317 0.487 0.865 0.733 0.64
17.88
17.64 18.19 18.66 18.73 18.8

G03 16.917 0.504 -0.535 -0.453 0.66
17.03 17.8 16.65 16.57 17.05 16.4

G07 17.717 0.581 0.265 0.225 0.77
17.4 17.8 18.2 18 16.7 18.2

G08 15.933 0.683 -1.518 -1.285 1
14.35 17.02 17.86 14.87 14.53 16.97
Day
G10 2 17.671 0.714 0.219 0.186 0.94
17.383 17.954 16.529 18.699 17.638
17.82

G12 17.068 1.172 -0.383 -0.324 1.55
16.29 18.01 18.28 17.92 16.55 15.36

G14 19.188 0.582 1.737 1.471 0.77
18.66 18.68 19.05 18.91 19.87 19.96

G16 18.640 0.558 1.189 1.007 0.74
19.57 18.27 18.78 18.52 17.93 18.77

G18 18.607 0.599 1.155 0.978 0.79
18.48 18.6 17.54 18.69 19.09 19.24

G20 17.333 0.622 -0.118 -0.100 0.82
17.5 17.9 17.8 16.6 16.5 17.7

G22 14.617 0.866 -2.835 -2.400 1.14
15.9 14 13.8 14.3 15.5 14.2

G23 17.037 0.733 -0.415 -0.351 0.97
17.35 17.74 17.64 17.25 16.17 16.07
95
G25 18.760 0.465 1.309 1.108 0.61
19.26 18.11 19.16 18.91 18.29 18.83

G26 15.907 0.776 -1.545 -1.308 1.02
15.1 16.37 17.12 15.71 16.02 15.12

G28 17.077 0.647 -0.375 -0.317 0.85
17.28 16.64 16.35 18.13 17.36 16.7

G32 17.967 0.838 0.515 0.437 1.1
17.9 18.1 16.8 17.7 19.4 17.9

G35 17.917 0.366 0.465 0.394 0.48
18.1 18.3 18.2 17.8 17.8 17.3

96
UNAGED
97
UNAGED
Flagged Flagged
'H' 'K'

G01 18.317 0.487 0.865 0.733 0.64
17.64 18.19 18.66 18.73 18.8 17.88

G03 16.917 0.504 -0.535 -0.453 0.66
17.03 17.8 16.65 16.57 17.05 16.4

G07 17.717 0.581 0.265 0.225 0.77
17.4 17.8 18.2 18 16.7 18.2

G08 15.933 1.521 -1.518 -1.285 2.01 K
14.35 17.02 17.86 14.87 14.53 16.97

G10 17.671 0.714 0.219 0.186 0.94
17.383 17.954 16.529 18.699 17.82 17.638

G12 17.068 1.172 -0.383 -0.324 1.55
16.29 18.01 18.28 17.92 16.55 15.36

G14 19.188 0.582 1.737 1.471 0.77
18.66 18.68 19.05 18.91 19.87 19.96

G16 18.640 0.558 1.189 1.007 0.74
19.57 18.27 18.78 18.52 17.93 18.77

G18 18.607 0.599 1.155 0.978 0.79
18.48 18.6 17.54 18.69 19.09 19.24

G20 17.333 0.622 -0.118 -0.100 0.82
17.5 17.9 17.8 16.6 16.5 17.7

G22 14.617 0.866 -2.835 -2.400 1.14
15.9 14 13.8 14.3 15.5 14.2

G23 17.037 0.733 -0.415 -0.351 0.97
17.35 17.74 17.64 17.25 16.17 16.07

G25 18.760 0.465 1.309 1.108 0.61
19.26 18.11 19.16 18.91 18.29 18.83
98
G26 15.907 0.776 -1.545 -1.308 1.02
15.1 16.37 17.12 15.71 16.02 15.12

G28 17.077 0.647 -0.375 -0.317 0.85
17.28 16.64 16.35 18.13 17.36 16.7

G32 17.967 0.838 0.515 0.437 1.1
17.9 18.1 16.8 17.7 19.4 17.9

G35 17.917 0.366 0.465 0.394 0.48
18.1 18.3 18.2 17.8 17.8 17.3

99
Lab Flagged Flagged

Code 'H' 'K'
Day 2
G01 18.317 0.487 0.865 0.733 0.64
17.88
17.64 18.19 18.66 18.73 18.8

G03 16.917 0.504 -0.535 -0.453 0.66
17.03 17.8 16.65 16.57 17.05 16.4

G07 17.717 0.581 0.265 0.225 0.77
17.4 17.8 18.2 18 16.7 18.2

G08 15.933 0.683 -1.518 -1.285 1
14.35 17.02 17.86 14.87 14.53 16.97
Day
G10 2 17.671 0.714 0.219 0.186 0.94
17.383 17.954 16.529 18.699 17.638
17.82

G12 17.068 1.172 -0.383 -0.324 1.55
16.29 18.01 18.28 17.92 16.55 15.36

G14 19.188 0.582 1.737 1.471 0.77
18.66 18.68 19.05 18.91 19.87 19.96

G16 18.640 0.558 1.189 1.007 0.74
19.57 18.27 18.78 18.52 17.93 18.77

G18 18.607 0.599 1.155 0.978 0.79
18.48 18.6 17.54 18.69 19.09 19.24

G20 17.333 0.622 -0.118 -0.100 0.82
17.5 17.9 17.8 16.6 16.5 17.7

G22 14.617 0.866 -2.835 -2.400 1.14
15.9 14 13.8 14.3 15.5 14.2

G23 17.037 0.733 -0.415 -0.351 0.97
17.35 17.74 17.64 17.25 16.17 16.07
100
G25 18.760 0.465 1.309 1.108 0.61
19.26 18.11 19.16 18.91 18.29 18.83

G26 15.907 0.776 -1.545 -1.308 1.02
15.1 16.37 17.12 15.71 16.02 15.12

G28 17.077 0.647 -0.375 -0.317 0.85
17.28 16.64 16.35 18.13 17.36 16.7

G32 17.967 0.838 0.515 0.437 1.1
17.9 18.1 16.8 17.7 19.4 17.9

G35 17.917 0.366 0.465 0.394 0.48
18.1 18.3 18.2 17.8 17.8 17.3

101
UNAGED
102
UNAGED
Flagged Flagged
'H' 'K'

G01 773.333 10.328 -14.906 -0.389 0.73
780 780 780 760 780 760

G03 788.333 11.690 0.094 0.002 0.83
800 770 790 790 780 800

G07 908.000 26.046 119.760 3.127 1.85 H K
940 888 896 940 880 904

G08 742.500 23.805 -45.740 -1.194 1.69
722 779 761 722 725 746

G10 760.502 5.053 -27.738 -0.724 0.36
759.83 764.34 754.68 761.37 755.22 767.57

G12 760.000 0.000 -28.240 -0.737 0
760 760 760 760 760 760

G14 780.000 0.000 -8.240 -0.215 0
780 780 780 780 780 780

G16 760.000 0.000 -28.240 -0.737 0
760 760 760 760 760 760

G18 783.072 8.580 -5.168 -0.135 0.61
776.5 794.93 772.12 782.24 790.93 781.71

G20 818.833 15.842 30.594 0.799 1.13
806 825 825 806 806 845

G22 754.333 14.292 -33.906 -0.885 1.02
761 747 729 757 765 767

G23 770.000 20.976 -18.240 -0.476 1.49
760 740 760 800 780 780

G25 790.000 10.954 1.760 0.046 0.78
800 780 780 800 800 780
103
G26 798.333 17.512 10.094 0.264 1.24
820 805 790 810 795 770

G28 801.667 4.082 13.427 0.351 0.29
810 800 800 800 800 800

G32 782.667 15.055 -5.573 -0.146 1.07
766 786 766 786 786 806

G35 828.500 14.748 40.260 1.051 1.05
845 845 825 825 825 806

104
Lab Flagged Flagged

Code 'H' 'K'
G01 773.333 10.328 -7.421 -0.327 0.73
780 780 780 760 780 760

G03 788.333 11.690 7.579 0.334 0.83
800 770 790 790 780 800

G07 780.755 12.971 0.000 0.000 1
940 888 896 940 880 904

G08 742.500 23.805 -1.686 1.69
722 779 761 722 725 746 38.255
G10 760.502 5.053 -0.893 0.36
759.83 764.34 754.68 761.37 755.22 767.57 20.253
G12 760.000 0.000 -0.915 0
760 760 760 760 760 760 20.755
G14 780.000 0.000 -0.755 -0.033 0
780 780 780 780 780 780

G16 760.000 0.000 -0.915 0
760 760 760 760 760 760 20.755
Day 1
G18 783.072 8.580 2.317 0.102 0.61
794.93 772.12 782.24 790.93 781.71
776.5

G20 818.833 15.842 38.079 1.679 1.13
806 825 825 806 806 845

G22 754.333 14.292 -1.165 1.02
761 747 729 757 765 767 26.421
G23 770.000 20.976 -0.474 1.49
760 740 760 800 780 780 10.755
105
G25 790.000 10.954 9.245 0.408 0.78
800 780 780 800 800 780

G26 798.333 17.512 17.579 0.775 1.24
820 805 790 810 795 770

G28 801.667 4.082 20.912 0.922 0.29
810 800 800 800 800 800

G32 782.667 15.055 1.912 0.084 1.07
766 786 766 786 786 806

G35 828.500 14.748 47.745 2.105 1.05
845 845 825 825 825 806

106
UNAGED
107
SUMMARY OF TENSILE STRENGTH (DUMBBELS)
AGED
Flagged Flagged
'H' 'K'

G01 23.490 0.488 0.426 0.381 0.41
23.76 23.04 23.69 23.25 24.23 22.97

G07 23.190 0.785 0.126 0.113 0.65
22.32 22.88 22.83 24.6 23.03 23.48

G08 22.062 2.222 -1.002 -0.895 1.85 K
23.07 23.45 23.25 22.08 22.89 17.63

G10 24.228 1.432 1.164 1.039 1.19
23.563 25.778 22.427 23.197 24.426 25.976

G12 20.485 2.024 -2.579 -2.303 1.69
21.93 23.37 18.53 21.4 18.89 18.79

G14 24.283 1.175 1.220 1.089 0.98
23.98 25.22 23.64 22.44 24.76 25.66

G16 24.547 1.631 1.483 1.324 1.36
23.27 23.85 27.48 23.01 24.99 24.68

G20 23.167 0.753 0.103 0.092 0.63
24 22 24 23 23 23

G22 22.167 1.261 -0.897 -0.801 1.05
22.5 20.2 21.1 23.1 23.5 22.6

G23 23.480 0.786 0.416 0.372 0.66
22.67 23.57 22.64 24.2 23.25 24.55

G25 24.053 1.157 0.990 0.884 0.97
24.97 23.86 22.16 23.85 25.53 23.95

G28 21.585 1.203 -1.479 -1.320 1
21.27 21.33 19.96 23.67 21.84 21.44

G35 23.333 0.516 0.270 0.241 0.43
24 23 23 23 24 23
108
G26 22.980 0.897 -0.084 -0.075 0.75
23.09 24.29 23.24 23.33 21.81 22.12

G03 21.625 1.081 -1.439 -1.285 0.9
21.22 20.11 20.91 22.1 23.1 22.31

G18 23.860 0.703 0.796 0.711 0.59
22.68 23.83 23.73 23.82 24.78 24.32

G32 23.550 0.404 0.486 0.434 0.34
23.6 23.7 22.8 24 23.7 23.5

109
Lab Flagged Flagged

Code 'H' 'K'
G01 23.490 0.488 0.426 0.381 0.41
23.76 23.04 23.69 23.25 24.23 22.97

G07 23.190 0.785 0.126 0.113 0.65
22.32 22.88 22.83 24.6 23.03 23.48

G08 22.062 1.104 -1.002-0.895 1
23.07 23.45 23.25 22.08 22.89 17.63

G10 24.228 1.432 1.164 1.039 1.19
23.563 25.778 22.427 23.197 24.426 25.976

G12 20.485 2.024 -2.579-2.303 1.69
21.93 23.37 18.53 21.4 18.89 18.79

G14 24.283 1.175 1.220 1.089 0.98
23.98 25.22 23.64 22.44 24.76 25.66

G16 24.547 1.631 1.483 1.324 1.36
23.27 23.85 27.48 23.01 24.99 24.68

G20 23.167 0.753 0.103 0.092 0.63
24 22 24 23 23 23

G22 22.167 1.261 -0.897-0.801 1.05
22.5 20.2 21.1 23.1 23.5 22.6

G23 23.480 0.786 0.416 0.372 0.66
22.67 23.57 22.64 24.2 23.25 24.55

G25 24.053 1.157 0.990 0.884 0.97
24.97 23.86 22.16 23.85 25.53 23.95

G28 21.585 1.203 -1.479-1.320 1
21.27 21.33 19.96 23.67 21.84 21.44

G35 23.333 0.516 0.270 0.241 0.43
24 23 23 23 24 23
110
G26 22.980 0.897 -0.084-0.075 0.75
23.09 24.29 23.24 23.33 21.81 22.12

G03 21.625 1.081 -1.439-1.285 0.9
21.22 20.11 20.91 22.1 23.1 22.31

G18 23.860 0.703 0.796 0.711 0.59
22.68 23.83 23.73 23.82 24.78 24.32

G32 23.550 0.404 0.486 0.434 0.34
23.6 23.7 22.8 24 23.7 23.5

111
K & H VALUE GRAPH- TENSILE STRENGTH (DUMBBELS)
AGED
112
SUMMARY OF FORCE AT BREAK (DUMBBELL)
AGED
Flagged Flagged
'H' 'K'

G01 16.525 0.450 0.616 1.080 0.37
16.93 16.14 16.59 16.42 17.12 15.95

G03 15.263 0.386 -0.646 -1.133 0.31
15.25 14.68 15.07 15.21 15.62 15.75

G07 15.600 0.465 -0.309 -0.542 0.38
15.1 16 16.3 15.5 15.2 15.5

G08 15.537 1.739 -0.373 -0.654 1.42
16.56 17.01 16.59 14.82 15.89 12.35

G10 16.092 0.884 0.183 0.321 0.72
15.61 16.618 14.625 16.487 16.076 17.137

G12 15.942 3.894 0.032 0.057 3.17 K
14.47 16.83 23.23 15.41 13.31 12.4

G14 16.372 0.542 0.462 0.811 0.44
16.14 16.95 16.08 15.55 16.87 16.64

G16 16.850 1.398 0.941 1.650 1.14
16.19 16.17 18.63 14.77 17.54 17.8

G18 16.605 0.807 0.696 1.220 0.66
14.97 16.89 16.94 16.94 16.79 17.1

G20 15.767 0.612 -0.143 -0.250 0.5
16 15.2 16.9 15.5 15.5 15.5

G22 15.833 0.602 -0.076 -0.133 0.49
15.1 15.6 15.8 16 15.6 16.9

G23 16.447 0.595 0.537 0.942 0.48
16.46 16.07 15.58 16.66 16.56 17.35

G25 15.877 0.762 -0.033 -0.057 0.62
16.48 15.75 14.63 15.74 16.85 15.81
113
G26 14.548 0.569 -1.361 -2.387 0.46
14.62 15.38 14.71 14.77 13.81 14

G28 15.435 0.913 -0.474 -0.832 0.74
15.15 15.45 14.24 17.06 15.3 15.41

G32 15.600 0.443 -0.309 -0.542 0.36
15.7 15.2 15.6 16.2 15.9 15

G35 16.167 0.432 0.257 0.451 0.35
16.6 15.8 16.4 16.2 16.5 15.5

114
Lab
Test Result x` s d h k Flagged 'H' Flagged 'K'
Code
Day 2
G01 16.525 0.450 0.616 1.080 0.37
15.95
16.93 16.14 16.59 16.42 17.12

G03 15.263 0.386 -0.646 -1.133 0.31
15.25 14.68 15.07 15.21 15.62 15.75

G07 15.600 0.465 -0.309 -0.542 0.38
15.1 16 16.3 15.5 15.2 15.5

G08 15.537 1.739 -0.373 -0.654 1.42
16.56 17.01 16.59 14.82 15.89 12.35
Day
G10 1 16.092 0.884 0.183 0.321 0.72
16.618 14.625 16.487 16.076 17.137
15.61

G12 15.942 0.810 0.032 0.057 1
14.47 16.83 23.23 15.41 13.31 12.4

G14 16.372 0.542 0.462 0.811 0.44
16.14 16.95 16.08 15.55 16.87 16.64

G16 16.850 1.398 0.941 1.650 1.14
16.19 16.17 18.63 14.77 17.54 17.8

G18 16.605 0.807 0.696 1.220 0.66
14.97 16.89 16.94 16.94 16.79 17.1

G20 15.767 0.612 -0.143 -0.250 0.5
16 15.2 16.9 15.5 15.5 15.5

G22 15.833 0.602 -0.076 -0.133 0.49
15.1 15.6 15.8 16 15.6 16.9

G23 16.447 0.595 0.537 0.942 0.48
16.46 16.07 15.58 16.66 16.56 17.35
115
G25 15.877 0.762 -0.033 -0.057 0.62
16.48 15.75 14.63 15.74 16.85 15.81

G26 14.548 0.569 -1.361 -2.387 0.46
14.62 15.38 14.71 14.77 13.81 14

G28 15.435 0.913 -0.474 -0.832 0.74
15.15 15.45 14.24 17.06 15.3 15.41

G32 15.600 0.443 -0.309 -0.542 0.36
15.7 15.2 15.6 16.2 15.9 15

G35 16.167 0.432 0.257 0.451 0.35
16.6 15.8 16.4 16.2 16.5 15.5

116
K & H VALUE GRAPH- FORCE AT BREAK (DUMBBELL)
AGED
117
AGED
Flagged Flagged
'H' 'K'

G01 750.000 10.954 -35.418 -0.728 0.52
760 740 760 740 760 740

G03 863.333 19.664 77.915 1.600 0.94
840 870 880 890 850 850

G07 862.667 15.731 77.249 1.587 0.75
880 868 876 864 848 840

G08 752.000 34.158 -33.418 -0.686 1.63
777 778 774 738 755 690

G10 785.202 15.767 -0.216 -0.004 0.75
770.63 803.6 798.44 781.95 792.63 763.96

G12 720.000 17.889 -65.418 -1.344 0.85
740 740 700 720 720 700

G14 746.667 16.330 -38.751 -0.796 0.78
740 740 740 740 780 740

G16 800.000 43.818 14.582 0.300 2.09 K
840 840 840 760 760 760

G18 711.570 18.780 -73.848 -1.517 0.9
689.27 699.81 703.44 739.36 709.13 728.41

G20 815.667 16.256 30.249 0.621 0.78
806 806 845 806 806 825

G22 755.167 5.845 -30.251 -0.621 0.28
755 744 760 755 758 759

G23 766.667 16.330 -18.751 -0.385 0.78
760 780 740 780 760 780
118
G25 803.333 8.165 17.915 0.368 0.39
800 800 800 800 820 800

G26 778.333 13.663 -7.085 -0.146 0.65
780 790 770 755 790 785

G28 866.667 33.267 81.249 1.669 1.59
870 920 880 850 860 820

G32 749.333 8.165 -36.085 -0.741 0.39
746 746 746 766 746 746

G35 825.500 21.361 40.082 0.823 1.02
806 806 806 845 845 845

119
Lab Flagged Flagged

Code 'H' 'K'
G01 750.000 10.954 -35.418 -0.728 0.52
760 740 760 740 760 740

G03 863.333 19.664 77.915 1.600 0.94
840 870 880 890 850 850

G07 862.667 15.731 77.249 1.587 0.75
880 868 876 864 848 840

G08 752.000 34.158 -33.418 -0.686 1.63
777 778 774 738 755 690
Day 1
G10 785.202 15.767 -0.216 -0.004 0.75
770.63 798.44 781.95 792.63 763.96
803.6

G12 720.000 17.889 -65.418 -1.344 0.85
740 740 700 720 720 700

G14 746.667 16.330 -38.751 -0.796 0.78
740 740 740 740 780 740

G16 800.000 18.636 14.582 0.300 1
840 840 840 760 760 760

G18 711.570 18.780 -73.848 -1.517 0.9
689.27 699.81 703.44 739.36 709.13 728.41

G20 815.667 16.256 30.249 0.621 0.78
806 806 845 806 806 825

G22 755.167 5.845 -30.251 -0.621 0.28
755 744 760 755 758 759

G23 766.667 16.330 -18.751 -0.385 0.78
760 780 740 780 760 780
120
G25 803.333 8.165 17.915 0.368 0.39
800 800 800 800 820 800

G26 778.333 13.663 -7.085 -0.146 0.65
780 790 770 755 790 785

G28 866.667 33.267 81.249 1.669 1.59
870 920 880 850 860 820

G32 749.333 8.165 -36.085 -0.741 0.39
746 746 746 766 746 746

G35 825.500 21.361 40.082 0.823 1.02
806 806 806 845 845 845

121
K & H VALUE GRAPH- BREAK (DUMBBELLS)
AGED
122
SUMMARY OF TENSILE STRENGTH (DUMBBELLS)
UNAGED
Flagged Flagged
'H' 'K'

G01 24.540 0.639 0.301 0.199 0.66
25.07 23.65 25.14 23.84 24.85 24.69

G03 22.858 0.767 -1.381 -0.916 0.79
21.59 23.1 23.43 23.72 22.9 22.41

G07 22.482 1.483 -1.758 -1.165 1.53
23.25 20.69 23.25 23.85 23.36 20.49

G08 21.967 1.329 -2.273 -1.507 1.37
22.63 23.35 20.44 23.37 21.41 20.6

G10 27.542 0.782 3.303 2.190 0.8
27.568 27.543 28.911 27.155 27.552 26.525

G12 23.523 0.981 -0.716 -0.475 1.01
24.93 24.17 23.98 22.45 22.69 22.92

G14 26.020 0.889 1.781 1.181 0.91
26.22 26.95 24.38 26.45 26.35 25.77

G16 24.715 0.572 0.476 0.315 0.59
24.9 23.95 24.75 25.21 24.12 25.36

G18 25.817 0.636 1.577 1.046 0.65
25.53 25.38 25.88 26.88 26.13 25.1

G20 24.500 0.548 0.261 0.173 0.56
24 25 25 24 25 24

G22 22.750 1.522 -1.489 -0.988 1.56
24.8 22.6 23.1 20.1 22.7 23.2

G23 23.003 1.396 -1.236 -0.820 1.44
23.83 20.89 24.8 21.91 23.28 23.31

G25 26.248 0.454 2.009 1.332 0.47
26.92 26.5 26.47 25.95 25.73 25.92
123
G26 24.443 0.632 0.204 0.135 0.65
24.55 24.33 25.29 23.39 24.3 24.8

G28 23.662 0.369 -0.578 -0.383 0.38
23.61 24.23 23.41 23.92 23.19 23.61

G32 23.500 1.552 -0.739 -0.490 1.6
24.4 22.4 25.1 21 23.5 24.6

G35 24.500 0.548 0.261 0.173 0.56
25 25 24 24 24 25

124
K & H VALUE GRAPH- TENSILE STRENGTH (DUMBBELLS)
UNAGED
125
SUMMARY OF FORCE AT BREAK (DUMBBELLS)
UNAGED
Flagged Flagged
'H' 'K'

G01 17.415 0.411 0.850 1.079 0.63
17.91 16.85 17.64 16.98 17.52 17.59

G03 16.308 0.337 -0.257 -0.326 0.52
15.64 16.59 16.41 16.39 16.45 16.37

G07 15.567 0.528 -0.999 -1.268 0.81
15.9 14.9 15.5 16.4 15.2 15.5

G08 15.420 0.905 -1.145 -1.455 1.39
15.92 16.07 14.56 16.65 14.74 14.58

G10 17.301 0.401 0.735 0.934 0.62
16.914 17.462 17.98 17.376 17.135 16.937

G12 15.782 0.564 -0.784 -0.995 0.87
15.75 16.75 16.06 15.57 15.17 15.39

G14 17.598 0.681 1.033 1.312 1.05
18.86 17.89 17.11 17.14 17.23 17.36

G16 16.952 0.414 0.386 0.491 0.64
16.75 16.35 17.05 17.24 16.79 17.53

G18 17.853 0.771 1.288 1.636 1.19
17.34 17.06 17.7 18.96 18.65 17.41

G20 16.667 0.497 0.101 0.129 0.76
16 17 17.2 16.4 17.1 16.3

G22 15.850 0.896 -0.715 -0.909 1.38
17.1 16 15.5 14.4 16.3 15.8

G23 16.333 0.924 -0.232 -0.295 1.42
16.27 14.9 17.44 15.78 17.15 16.46

G25 17.440 0.261 0.875 1.111 0.4
17.86 17.49 17.47 17.18 17.5 17.14
126
G26 15.473 0.399 -1.092 -1.387 0.61
15.54 15.4 16.01 14.81 15.38 15.7

G28 16.833 0.228 0.268 0.341 0.35
17.04 16.52 17.09 16.85 16.61 16.89

G32 16.150 1.097 -0.415 -0.527 1.69
16.7 15.3 17.6 14.6 15.9 16.8

G35 16.667 0.841 0.101 0.129 1.29
16.8 17.6 16.7 15.1 16.7 17.1

127
K & H VALUE GRAPH- FORCE AT BREAK (DUMBBELLS)
UNAGED
128
UNAGED
Flagged Flagged
'H' 'K'

G01 760.000 17.889 -17.326 -0.508 1.07
780 740 780 760 760 740

G03 786.667 10.328 9.340 0.274 0.62
770 780 790 790 790 800

G07 886.000 18.889 108.674 3.183 1.13 H
900 896 908 884 868 860

G08 751.833 19.302 -25.493 -0.747 1.16
756 781 752 757 743 722

G10 761.662 15.434 -15.665 -0.459 0.93
776.9 766.4 733.5 759.05 760.81 773.31

G12 753.333 20.656 -23.993 -0.703 1.24
740 760 720 780 760 760

G14 773.333 16.330 -3.993 -0.117 0.98
780 780 780 780 780 740

G16 756.667 15.055 -20.660 -0.605 0.9
760 740 740 760 760 780

G18 747.385 21.943 -29.941 -0.877 1.32
734.55 742.07 737.63 775.64 721.51 772.91

G20 805.833 24.983 28.507 0.835 1.5
766 806 806 806 845 806

G22 746.667 12.628 -30.660 -0.898 0.76
757 752 730 755 755 731

G23 766.667 10.328 -10.660 -0.312 0.62
760 760 760 780 780 760

G25 770.000 10.954 -7.326 -0.215 0.66
780 780 760 760 780 760
129
G26 796.667 6.055 19.340 0.567 0.36
795 790 800 790 805 800

G28 793.333 8.165 16.007 0.469 0.49
790 780 790 800 800 800

G32 756.000 10.954 -21.326 -0.625 0.66
746 746 746 766 766 766

G35 802.500 26.258 25.174 0.737 1.58
806 845 786 766 806 806

130
Lab Flagged Flagged

Code 'H' 'K'
G01 760.000 17.889 -10.534 -0.540 1.07
780 740 780 760 760 740

G03 786.667 10.328 16.132 0.826 0.62
770 780 790 790 790 800

G07 770.534 18.889 0.000 0.000 1.13
900 896 908 884 868 860

G08 751.833 19.302 -18.701 -0.958 1.16
756 781 752 757 743 722
Day 1 Day 1 Day 1

Day 2 Day 2 Day 2
G10 761.662 15.434 -8.872 -0.454 0.93
759.05 760.81 773.31
776.9 766.4 733.5

G12 753.333 20.656 -17.201 -0.881 1.24
740 760 720 780 760 760

G14 773.333 16.330 2.799 0.143 0.98
780 780 780 780 780 740

G16 756.667 15.055 -13.868 -0.710 0.9
760 740 740 760 760 780

G18 747.385 21.943 -23.149 -1.186 1.32
734.55 742.07 737.63 775.64 721.51 772.91

G20 805.833 24.983 35.299 1.808 1.5
766 806 806 806 845 806

G22 746.667 12.628 -23.868 -1.223 0.76
757 752 730 755 755 731

G23 766.667 10.328 -3.868 -0.198 0.62
760 760 760 780 780 760

G25 770.000 10.954 -0.534 -0.027 0.66
780 780 760 760 780 760
131
G26 796.667 6.055 26.132 1.339 0.36
795 790 800 790 805 800

G28 793.333 8.165 22.799 1.168 0.49
790 780 790 800 800 800

G32 756.000 10.954 -14.534 -0.744 0.66
746 746 746 766 766 766

G35 802.500 26.258 31.966 1.637 1.58
806 845 786 766 806 806

132
UNAGED
133
134

Final Report: Proficiency Testing (PT) Program On Tensile Tests For Glove (2015)

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Final Report: Proficiency Testing (PT) Program On Tensile Tests For Glove (2015)

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Final Report

Analyzed and Prepared

2. Features of the Program………………………………………. 4

7. Statistical statement and definitions…………………………. 8

9. Flagging inconsistent results 11

10. Summary of Analysis

14. Volatile Fatty Acid (VFA No.)…………………………………. 29-33

15. Mechanical Stability Time (MST) (seconds)………………… 34-38

16. Nitrogen content……………………………………………….. 39-41

The program is conducted annually for quality improvement as required in the MS

A web-based system of “e-Precision” which is produced in house by Malaysian Rubber

Participants’ confidentiality are assured by identifying each participant by a unique code

Programme software of ASTM E 691-92 (Practice for conducting an interlaboratory

Parameters that are used in the scope of this programme are:

3. Aims of the study

The aims of the study are as follows:

 To identify those laboratories disagreeing in a statistical sense, from the majority,

2. Bonric Sdn Bhd

3. Cardinal Health Malaysia

4. Central Medicare Sdn. Bhd.

5. Encompass Medical Supplies Sdn Bhd

6. G-TACR Sg.Buloh Lembaga Getah Malaysia

7. GX Corporation Sdn Bhd (Plant 2)

8. Hartalega NGC Sdn Bhd

10. Latexx Manufacturing Sdn.Bhd.

11. Molnlycke Health Care KK QA Physical Lab

12. Molnlycke Health Care Sdn Bhd (Batang Kali)

13. Molnlycke Health Care Sdn Bhd R&D Physical Lab

14. N.S Uni-Glove Sdn Bhd

15. Perusahaan Getah Asas Sdn. Bhd.

16. Platinium Glove Industries Sdn Bhd

17. Revertex (M) Sdn Bhd.

18. Riverstone Resources Sdn Bhd (Taiping)

19. Sigma Glove Industries Sdn Bhd

20. Smart Glove Corporation Sdn Bhd

21. Wear Safe(Malaysia) Sdn Bhd

22. WRP Asia Pacific Sdn Bhd

5. MATERIALS AND SAMPLE PREPARATION

(i) Unaged tensile properties:

(ii) Aged tensile properties:

(iii) Unaged tensile properties on dumbbells cut by LGM:

(iv) Aged tensile properties on dumbbells cut by LGM:

Laboratory Die Thickness Tensile Oven

MRB – Instron 5564 Die C Mitutoyo Instron 5564 Binder

MRB – Zwick Die C Mitutoyo Zwick Binder

MRB – Testometric 2 Die C Mitutoyo Tensometric Binder

GMP Medicare Die C Mitutoyo Instron Memmert

Supermax Die C Mitutoyo LLOYD LRX Memmert

MIM Technical Lab. Die C - - -

Regent Hospital Products Die C Mitutoyo Instron 4301 Memmert

Regent Hospital Products Die C Mitutoyo Instron 5564 Memmert

Regent Hospital Products Die C Sylvac Instron 5564 Memmert

Hartalega Die C Mitutoyo Instron 3345 Model ZRD 7140

8. TEST METHOD AND SCHEDULE

Unaged - 21/10/2015 22/10/2015

10. STATISTICAL STATEMENT and DEFINITIONS

(a) Cell statistics: