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Characteristics and Origin of Abnormally High Porosity Zones in Buried Paleogene Clastic Reservoirs in The Shengtuo Area, Dongying Sag, East China
Characteristics and Origin of Abnormally High Porosity Zones in Buried Paleogene Clastic Reservoirs in The Shengtuo Area, Dongying Sag, East China
Characteristics and Origin of Abnormally High Porosity Zones in Buried Paleogene Clastic Reservoirs in The Shengtuo Area, Dongying Sag, East China
(2014)11:346-362
DOI 10.1007/s12182-014-0349-y
Abstract: There are three abnormally high porosity zones developed in buried Paleogene nearshore
subaqueous fan and sublacustrine fan clastic reservoirs at 2,800-3,200 m, 3,250-3,700 m and 3,900-
4,400 m, respectively, within the Shengtuo area of the Dongying Sag. Here the porosity of reservoirs
buried deeper than 4,000 m can still be greater than 20%. Investigation of these three abnormally high
porosity (AHP) zones in the 3rd to 4thPHPEHURIWKH3DOHRJHQH6KDKHMLH)RUPDWLRQLQWKH6KHQJWXRDUHD
ZDVFDUULHGRXWZLWKXWLOL]DWLRQRIFRUHREVHUYDWLRQWKLQVHFWLRQLGHQWL¿FDWLRQ6(0REVHUYDWLRQLPDJH
analysis, core physical property testing and other technical methods. The results show that, the AHP
]RQHVLQPDQGPDUHYLVLEOHSRUHVSULPDU\$+3]RQHVGRPLQDWHGE\VLJQL¿FDQW
primary intergranular pores (more than 50% of the total porosity), while secondary pores and micropores
in authigenic clays may develop in some reservoirs. AHP reservoirs in the AHP zone of 3,900-4,400 m
are dominated by micropores in matrix, visible pores are mainly grain dissolution pores but with low
absolute content (< 1%), so this zone belongs to the micropores primary AHP zone. The genesis of the
three AHP zones was studied to distinguish between porosity enhancement and porosity preservation.
Our research shows that, in deeply buried clastic reservoirs in the Shengtuo area, mineral dissolution
occurred in a relatively closed diagenetic system with high temperature and high salinity. Reservoir rocks
underwent extensive feldspar dissolution, while detrital carbonate grains and carbonate cements show
QRHYLGHQFHRIH[WHQVLYHGLVVROXWLRQ$OWKRXJKVLJQL¿FDQWIHOGVSDUGLVVROXWLRQSRUHVGHYHORSHGIHOGVSDU
dissolution enhanced porosity only a little due to the precipitation of almost isovolumetric dissolution
products in the nearby primary intergranular pores in forms of authigenic clays and quartz cements. Net
enhanced porosity originating from feldspar dissolution is generally less than 0.25%. Thus, the subsurface
dissolution has little impact on the mid-deep buried high porosity reservoirs. Reservoirs in braided
channels of middle fans in sublacustrine fans and reservoirs in the middle-front of fan bodies of nearshore
VXEDTXHRXVIDQVSURYLGHWKHEDVLVIRUWKHGHYHORSPHQWRI$+3]RQHV7KHVKDOORZGHYHORSPHQWRIÀXLG
overpressure and early hydrocarbon emplacement have effectively retarded compaction and carbonate
FHPHQWDWLRQVRWKDWWKHKLJKSRURVLW\LQWKHVXSHU¿FLDOOD\HUVLVSUHVHUYHGLQWKHPLGGHHSOD\HUV7KHVH
are the main controlling factors in the development of AHP zones.
Key words: Dongying Sag, Shengtuo area, abnormally high porosity zone, pores, genesis
exceed the maximum porosity of the typical sandstone the secondary AHP zone (the relative percentage content of
VXESRSXODWLRQ:LWKLQVSLUDWLRQIURPWKLVGH¿QLWLRQ0HQJHW secondary pores in reservoirs is more than 50%) (Cao et al,
DOGH¿QHGWKH$+3]RQHDVWKHUHVHUYRLUGHYHORSPHQW 2013). Also, exploration ideas and methods should differ
zone with porosities higher than the maximum porosity between these types of AHP zones.
of clastic rocks that develop in normal sedimentary and The mid-deep clastic reservoirs (>2,500 m) in the
diagenetic environments. The concept of an AHP zone Shengtuo area of the northern steep slope zone in the
emphasizes only the abnormally high level of reservoir Dongying Sag developed three AHP zones at 2,800-3,200
porosity regardless of the pore types. In addition, Chinese m, 3,250-3,700 m and 3,700-4,400 m, respectively. Great
scholars also referred to the AHP zone as the secondary pore success has been achieved in oil-gas exploration in Es4-Es3z
development zone, secondary pore zone, (abnormal) pore VXEWOH UHVHUYRLUV LQ UHFHQW \HDUV )RU H[DPSOH:HOO7
development zone, secondary pore development section, Well T76, Well T710, Well T719 and Well T764 all obtained
etc., of which, the secondary pore development zone has high yields in the Es4-Es3x formations. However, there is still
been used widely (Yuan and Wang, 2001; Zhu et al, 2006; much debate on pore types and genesis of the AHP reservoirs.
Liu et al, 2009; Wang, 2010). Some scholars considered the Previous studies suggested that, the deep buried Paleogene
relative content of secondary pores in the reservoirs (Wang clastic reservoirs in the Shengtuo area consist mainly of
and Shao, 1999; Wang, 2010), for example, Wang (2010) secondary pores, and subsurface dissolution is the main
VXPPDUL]HGVWXGLHVRIWKH&KLQHVHVFKRODUVDQGGH¿QHGWKH controlling factor of these AHP zones (Zhong et al, 2003; Zhu
secondary pore development zone as a zone where reservoirs et al, 2006; Yuan et al, 2007; Gao et al, 2008). Among them,
with high porosity (higher than the ĭcutoff) developed, based on Zhong et al (2003) and Zhu et al (2006) proposed that the
the introduction of effective reservoir porosity cutoff (ĭcutoff), reservoirs consist mainly of intergranular dissolution pores,
and where the percentage of secondary pores in reservoirs is and significant dissolution of carbonate cements is critical
more than 50%. However, without considering the content to the AHP zones. However, Yuan et al (2007) and Gao et al
of secondary pores in reservoirs, some scholars subjectively (2008) argued that the dissolution of carbonate cements is
GH¿QHGWKHFRQFHQWUDWHGGHYHORSPHQW]RQHRI$+3UHVHUYRLUV not obvious, and significant feldspar pores contribute more
with secondary pores as the secondary pore development WRWKHVH$+3]RQHV*HRORJLFDOIDFWRUVEHQH¿FLDOWRSULPDU\
zone (Zhong et al, 2003; Xiao et al, 2003; Liu and Zhu, 2006; SRUHSUHVHUYDWLRQVXFKDVÀXLGRYHUSUHVVXUHDQGK\GURFDUERQ
Zhu et al, 2007; Zhang et al, 2011). emplacement occur commonly in the Shengtuo area (Zhang
Publications suggest that both geological processes et al, 2009; Wang, 2010; Sun, 2010). However, the AHP
beneficial to porosity preservation (e.g. (1) the shallow zones were identified as secondary AHP zones (secondary
GHYHORSPHQWRIÀXLGRYHUSUHVVXUHDQGFKORULWHFRDWVDQG pore development zones) by previous studies (Zhong et al,
early hydrocarbon emplacement) and processes beneficial 2003; Zhu et al, 2006; Yuan et al, 2007; Gao et al, 2008),
to porosity enhancement (mineral dissolution) can be the which is questionable. Using core observation, thin section
important controlling factors to the development of mid- identification, SEM analysis, image analysis, rock physical
deep AHP reservoirs (Ehrenberg, 1993; Warren and Pulham, property tests, fluid inclusion analysis, statistical analysis
2001; Luo et al, 2002; Bloch et al, 2002; Marchand et al, and other techniques, on the basis of the distribution of AHP
2002; Zhong et al, 2003; Zhu et al, 2004; 2006; Zhang et al, zones in the Shengtuo area, we studied the pore types and the
2007; Yu et al, 2008; Peng et al, 2009; Zhong et al, 2008; genesis of these AHP zones.
Taylor et al, 2010; Meng et al, 2010; Wang, 2010; Jin et
al, 2011; Chen et al, 2011; Zhu et al, 2012). Even recently, 2 Geological background
most Chinese scholars still thought that burial dissolution of
minerals (particularly mesogenenic dissolution) is the main The Dongying Sag is a sub-tectonic unit lying in the
controlling factor of the mid-deep AHP zones (Zhang et al, southeastern part of the Jiyang Depression of the Bohai Bay
2003; Zhu et al, 2004; Yuan et al, 2007; Zhu et al, 2006; Yu %DVLQ (DVW &KLQD )LJ D ,W LV D 0HVR]RLF&HQR]RLF
et al, 2008; Zhong et al, 2008; Zhu et al, 2012). In recent half graben rift-downwarped lacustrine basin, developed on
years, many foreign scholars and some Chinese scholars Paleozoic bedrock paleotopography (Yuan et al, 2007). The
began to accentuate the importance of geological processes Dongying Sag, which is located west of the Qingtuozi Salient,
beneficial to porosity preservation (e.g. fluid overpressure, north of the Luxi Uplift and Guangrao Salient, east of the
hydrocarbon emplacement and chlorite coats), and rethought Linfanjia and Gaoqing Salient, south of the Chenjiazhuang-
the importance of secondary pores (Bloch et al, 2002; Taylor Binxian Salient. It covers an area of 5,850 km2 with an east-
et al, 2010; Berger et al, 2009; Marchand et al, 2002; Higgs ZHVWD[LVRINPDQGDQRUWKVRXWKD[LVRINP,QSUR¿OH
et al, 2007; Jin et al, 2011; Ehrenberg et al, 2012; Yuan et the Dongying Sag is a half graben with a faulted northern
DOE:KHQJHRORJLFDOSURFHVVHVEHQH¿FLDOWRSRURVLW\ margin and a gentle southern margin. In plan, the Dongying
preservation serve as main controlling factors, AHP reservoirs sag is further subdivided into secondary structural units, such
consist mainly of primary pores; while when the secondary as the northern steep slope zone, middle uplift belt, trough
dissolution is the main controlling factor, the AHP reservoirs zones of the Lijin, Minfeng, Niuzhuang and Boxing subsags,
consist mainly of secondary pores (Bloch et al, 2002; Meng et DQGWKHVRXWKHUQJHQWOHVORSH]RQH=KDQJHWDO)LJ
al, 2006; 2010). Thus, we suggested dividing the AHP zones 1(b)).
into two types: the primary AHP zone (the relative percentage The Shengtuo area is located in the middle part of the
content of primary pores in reservoirs is more than 50%) and northern steep slope zone of the Dongying sag, with the
348 Pet.Sci.(2014)11:346-362
ft
0 10 20km
pli
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40°
Beijing Yanshan
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han U
Bohai Bay
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38°
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lift
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Up
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Northern zone
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racture
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Paleogene Paleogene
area overlap zone
Luxi Uplift
Study Major Paleogene
area fault denuded zone
Fig. 1 (a) Tectonic setting of the Dongying Sag in the Jiyang Depression ( ) of the Bohai Bay Basin, East China.
Other depressions in the Bohai Bay Basin are Jizhong Depression ( ), Huanghua Depression (II), Bozhong Depression
(IV), Liaohe Depression (V) and Dongpu Depression (VI) (After Liu et al, 2012). (b) Structural map of the Dongying
Sag. The area in the green line is the study area (After Zhang et al, 2006).
Chenjiazhuang Salient to the north, the central faulted in the Shengtuo area, the quartz content is 5%-63% with
anticlinal zone to the south, the Lijin subsag to the southwest an average of 32%, the feldspar content is 4%-74% with an
and the Minfeng subsag to the southeast, with an exploration average of 37% and the detritus content is 3%-88% with an
area of 230 km 2 *DR HW DO )LJ E7KH EDVLQ average of 30%. The reservoir rocks consist mainly of lithic
controlling boundary Chennan fault and the secondary Tuo- DUNRVH DQG IHOGVSDWKLF OLWKLF VDQGVWRQHV )LJ 2Q WKH
Sheng-Yong sub fracture system, jointly controlled the whole, detrital grains are moderately to poorly sorted, with
terrace tectonic style in the Shengtuo area, and had important sub-angular or sub-rounded shapes. Grain contacts are mainly
LQIOXHQFHRQVHGLPHQWVDQGUHVHUYRLUV)LJ'XULQJWKH point contact and point-line contact.
early period of Es4x, the Tuo-Sheng-Yong sub fracture system
had not yet begun to develop, and nearshore subaqueous 3.2 Diagenesis features
IDQVGHSRVLWHG)URPWKHODWHSHULRGRI(V4x to the period of According to the new diagenetic stage division standard
Es3z, the Tuo-Sheng-Yong sub fracture system developed and of clastic reservoirs in China’s oil and gas industry (Standard
formed the terrace. The nearshore subaqueous fans deposited No. SY/T5477-2003), the Paleogene Es4-Es3z reservoirs at
on the terrace that was constrained by the Chennan fault and depths of 1,500-4,500 m in the Shengtuo area are mainly in
Tuo-Sheng-Yong sub fracture system, and sublacustrine fans the eogenetic and mesogenetic stages. Among them, 1,500-
deposited in the subsag that was close to the Tuo-Sheng- 2,200 m belongs to the eogenetic stage A period, 2,200-3,000
<RQJ VXE IUDFWXUH V\VWHP $Q )LJ &RQWUROOHG m belongs to the B period of the eogenetic stage, 3,000-3,500
by the tectonic setting, the formation fluid pressure in the m belongs to the A1 sub-period of the mesogenetic stage,
Shengtuo area has apparent zoning. Normal and weak fluid and 3,500-4,500 m belongs to the mesogenetic stage A2 sub-
overpressure developed mainly in the nearshore subaqueous period (Table 1). The major diagenetic events in the reservoir
fans, and medium-strong overpressure with the pressure rocks include compaction, carbonate cements (mainly calcite,
FRHI¿FLHQWRIGHYHORSHGLQWKHVXEODFXVWULQHIDQV*DR dolomite, ferroan calcite and ankerite), quartz cements,
et al, 2008; An, 2010). feldspar dissolution, quartz dissolution, authigenetic clays
NDROLQLWHDQGLOOLWHDQGLOOLWL]DWLRQRINDROLQLWH)LJ)LJ
3 Petrography and diagenesis 5). Using textural evidence of precipitation and dissolution
of minerals and the homogenization temperatures (Th) of
3.1 Petrography
fluid inclusions, the epigenetic sequence was determined
The data show that in the mid-deep Paleogene reservoirs as follows: 1) compaction, early carbonate cementation
Pet.Sci.(2014)11:346-362 349
Depth, m
N
Depth, m
0 2 4km SP RT SP RT
Lithologic ȍ.m Lithologic ȍ.m
mv mv
column column
Chenjiazhuang Salient 10 100 -10 90 0 80 0 20
T105
Chennan Fault T175 T75
T137 T116
3150
2000
T104
T174
T127 T145 T123
T131 Tg2 T122 T125 T129
T160 T121
T82 T126 120 T128
T24 T156
3200
2050
T170 T158
T112
T81
T167 T17
134 T714
T164
3250
2100
T713 T76 T732
T764
T166 T766 T761
T717 T71 T7
T746 T765
T742 T153
T715
3300
2150
T718
60
Well site Normal Contour line Root of fan body Middle-front of fan body Fan edge subfacies Sublacustrine Deep lake Middle Gritstone Fine Fine sandstone Sand- Mudstone
/well number fault of sand content in subaqueous fan in subaqueous fan in subaqueous fan fan facies conglomerate conglomerate conglomerate
Fig. 2 (a) Distribution map of nearshore subaqueous fans and sublacustrine fans in Es4sLQWKH6KHQJWXRDUHDPRGL¿HGIURP$Q
2010). (b) Depositional sequence of sublacustrine fans and deep lake facies. (c) Depositional sequence of nearshore subaqueous fans
20
80 4 Distribution of porosity intervals and
zones
Lithic Feldspathic
Feldsarenite feldsarenite litharenite Litharenite 100
0
100 80 60 40 20 0 3RURVLW\LQWHUYDODQG]RQHFODVVL¿FDWLRQVFKHPH
Feldspar, % Rock fragment, %
Core porosities of Paleogene Es4-Es 3z reservoirs were
Fig. 3 Ternary plot showing composition of Paleogene Es4-Es reservoirs 3
z
XVHGWRSORWWKHSRURVLW\GHSWKSUR¿OH,QWKHSRURVLW\GHSWK
in the Shengtuo area, the Dongying Sag (using sandstone classification profile, normal porosity development depth intervals, AHP
VFKHPHRI)RONHWDO development depth intervals, and AHP zones, high porosity
zones, low porosity zones in different depth intervals were
)LJFGIHOGVSDUGLVVROXWLRQTXDUW]FHPHQWDWLRQ identified with the constraints of three curves, namely, the
DXWKLJHQLF NDROLQLWH SUHFLSLWDWLRQ )LJ F TXDUW] normal evolution curve of average porosity, the normal
GLVVROXWLRQODWHFDUERQDWHFHPHQWDWLRQ)LJJIHOGVSDU evolution curve of maximum porosity and the porosity
GLVVROXWLRQ TXDUW] FHPHQWDWLRQ )LJ J LOOLWL]DWLRQ RI HQYHORSHFXUYH,QWKHSRURVLW\GHSWKSUR¿OHWKH]RQHVZKHUH
NDROLQLWHDQGDXWKLJHQLFLOOLWHSUHFLSLWDWLRQ)LJHI reservoirs with porosities that deviated from the normal
The compaction was mainly mechanical compaction, evolution curve of maximum porosity to higher values is
and pressure dissolution was weak. The dissolution mainly recognized as AHP zones; the zones where reservoirs with
LQFOXGHV IHOGVSDU GLVVROXWLRQ )LJ F H J )LJ F porosities that deviated from the normal evolution curve of
(e)), a little dissolution of aluminosilicate detrital grains maximum porosity to lower values but deviated from normal
DQGTXDUW]JUDLQV'HWULWDOFDUERQDWHJUDLQV)LJEH evolution curve of average porosity to higher values is
IDQGFDUERQDWHFHPHQWV)LJFKVKRZQRHYLGHQFH recognized as high porosity zones; the zones where reservoirs
of significant dissolution. Carbonate cements represent the with porosities that deviated from normal evolution curve of
PRVWDEXQGDQWSRUH¿OOLQJFHPHQWV)LJZLWKDPD[LPXP average porosity to lower values is recognized as low porosity
FRQWHQWXSWR)LJDQGDQDYHUDJHFRQWHQWRI zones. In the porosity-depth profile, the depth interval
350 Pet.Sci.(2014)11:346-362
Table 1 Diagenetic stages and main characteristics of the Es4-Es3z reservoirs in the Shengtuo area, the Dongying Sag
Temperature, °C
Diagenetic Authigenic cements in sandstones Dissolution
Compaction
Organic matter
stage %S
Depth, m
Contact Pore
Carbonate
cements
Feldspar
Feldspar
cements
Quartz
cements
in
Quartz
Debris
Relative Maturity I/S K I I/S Ch type type
Stage Period R o, % yield
Organic
acids
Oil Immature Primary
A CO2 65 Point dominant
2200 100
Eodiagenesis
0.35
65
40
3000 120 0.5
30 Line
Low point, Primary
A1 mature ĉ Point secondary
20 line
3500 35 0.7
Mesodiagenesis
Point
Ċ Primary
Mature line,
A2 20 secondary
Line
with AHP zones is recognized as the AHP development Comparison between calculated mudstone fluid pressure
depth interval and the depth interval without AHP zones and measured adjacent sandstone fluid pressure shows
is recognized as the normal porosity development depth that the difference is always less than 5%. As well, the oil-
interval. bearing properties of more than 8,000 reservoir samples
with core porosity data were analyzed with core-logging
4.2 Normal evolution curve of maximum (average) PDWHULDOV6HFRQGE\UHMHFWLQJWKHSRURVLWLHVUHODWLQJWRÀXLG
porosity overpressure and/or high-level oil saturation (oil immersion,
The normal evolution curve of maximum porosity oil saturated and oil rich) from the porosity database, one
in clastic reservoirs refers to the evolution curve of the SRURVLW\GHSWKSUR¿OHZDVSORWWHGXVLQJUHVHUYRLUSRURVLWLHV
maximum porosity evolving with the burial depth in with normal pressure and low level oil content (oil-free, oil
reservoirs that did not experience abnormal geological trace, fluorescence and oil patches). The normal evolution
processes in favor of porosity enhancement and porosity curve of maximum porosity in Es 4-Es 3z reservoirs in the
preservation during deep burial. It can be determined by northern steep slope zone in the Dongying Sag was then
connecting the maximum porosity at different depths with determined through the smooth connection of maximum
a smooth curve in the porosity-depth profile. Among these SRURVLWLHVDWGLIIHUHQWGHSWKVLQVXFKDSRURVLW\GHSWKSUR¿OH
abnormal geological processes, the process in favor of )LJ$VHDUO\JUDLQFRDWLQJFKORULWHZDVQRWGHYHORSHG
porosity enhancement is the dissolution of unstable minerals and reservoirs with significant dissolution also have
(e.g. feldspars and carbonate minerals), while the processes relatively good oiliness, the rejection of porosities relating
in favor of porosity preservation consist mainly of fluid to fluid overpressure and/or high-level oil saturation from
overpressure, early hydrocarbon emplacement, and grain porosity database promises the elimination of the influence
coats. Thus, the normal evolution curve of maximum porosity of abnormal geological processes (fluid overpressure,
almost follows the compaction curve. hydrocarbon emplacement, grain coats and rims, and
In order to determine the distribution of AHP zones in dissolution) on porosities in the Shengtuo area.
WKH 6KHQJWXR DUHD ZH GLG WKH IROORZLQJ ZRUN )LUVW ZLWK The normal evolution curve of average porosity in clastic
WKHFRQVWUDLQWVRIWKHPHDVXUHGIRUPDWLRQÀXLGSUHVVXUHWKH reservoirs refers to the evolution curve of the average porosity
formation fluid pressure of over 300 wells in the northern evolving with the burial depth in reservoirs that did not
steep slope zone in the Dongying Sag was calculated by experience abnormal geological processes in favor of porosity
the equivalent-depth method with acoustic logging data. enhancement and porosity preservation during deep burial. On
Pet.Sci.(2014)11:346-362 351
Qa
FD
Qa
Qa
FD
Qa
FD FD
200ȝP 200ȝP
(a) Well T165, 3236.08 m (-) (b) Well T145, 2018.3 m (-)
FD K
K
FD
FD
FD
FD
FD
Qa
K
K
FD
100ȝP 25ȝP
(c) Well T714, 2841.3 m (-) (d) Well T714, 2841.3 m (-)
Qa
Qa
FD
I
I Qa
FD
100ȝP 100ȝP
(e) Well T720, 3671.1 m (-) (f) Well T720, 3671.1 m (-)
An
FD
An
Qa
the basis of the normal evolution curve of maximum porosity 4.3 Porosity intervals and zones
in clastic reservoirs, the normal average porosity of different With the constraints of the three curves, 3,880 core
depth intervals can be calculated using reservoir porosities porosities in the Shengtuo area show one normal porosity
with normal pressure and low oil-bearing saturation. Then development depth interval at depth of 1,300-2,800 m and
in the porosity-depth profile, the normal evolution curve of three AHP development depth intervals developed vertically
average porosity in clastic reservoirs can be determined by in Es4-Es3z reservoirs in the Shengtuo area. The three AHP
connecting the average porosities at different depths with a development depth intervals are at 2,800-3,200 m, 3,250-
VPRRWKFXUYH)LJ 3,700 m, 3,900-4,400 m respectively, and three AHP zones
352 Pet.Sci.(2014)11:346-362
Cc
Cc
Cc Cd
Cc
Cc
FD
F F
As
(c) Well T73, 3371.25 m (-) 50ȝP (d) Well T73, 3371.25 m (+)
50ȝP
Cc Cc
Cd Cd
FD FD
(e) Well T720, 3535.0 m (-) 200ȝP (f) Well T720, 3535.0 m (+) 200ȝP
D D
Qa-Ċ
An An
Qa-ĉ
FD
(g) Well T720, 3535.0 m (+) 25ȝP (h) Well T724, 4169.8 m, SEM
5/11/2006 HFW WD Mag 20.0μm
Fig. 5 Photomicrographs showing diagenetic features related to carbonate cements in Paleogene Es4-Es3z
reservoirs in the Shengtuo area, the Dongying Sag. (a) Carbonate cement filled most pores, (b) Carbonate
detrital grain and the carbonate overgrowths, (c), (d) Intact early carbonate cement cladding and extensive
GLVVROYHGIHOGVSDUIHOGVSDUGLVVROXWLRQSRUHVSDUWLDOO\¿OOHGZLWKDVSKDOWHI,QWDFWFDUERQDWHGHWULWDOJUDLQV
and early carbonate cement cladding, extensively dissolved feldspars, (g) Two stages of quartz overgrowths,
intact ankerite wrapped in Qa-II, (h) Euhedral ankerite cements. (a, b, g): thin sections; (c-f) red epoxy resin–
LPSUHJQDWHGWKLQVHFWLRQ&F&DUERQDWHFHPHQWV&G'HWULWDOFDUERQDWHJUDLQ)')HOGVSDUGLVVROXWLRQSRUHV
As: Asphalt; An: Ankerite; Qa: Quartz overgrowths
Core porosity, % Kaolinite, wt% Illite, wt% Illite/Smectite, wt% %Smectite in I/S Chlorite, wt% Carbonate cements, wt%
0 10 20 30 40 50 0 20 40 60 80 0 20 40 60 80 0 20 40 60 80 0 20 40 60 80 0 20 40 60 80 0 10 20 30 40 50
1.0 1.0
Es3z
Es3x
Es4s
Es4x
1.5 1.5
Normal
porosity
development
2.0 interval 2.0
Normal evolution
curve of
average porosity
2.5 2.5
Depth, km
Porosity Depth, km
envelope
curve
Abnormally
high porosity
3.0 Anomalously development 3.0
high porosity intervalĉ
zoneĉ
Abnormally
high porosity
3.5 Anomalously development 3.5
high porosity intervalĊ
zoneĊ
Fig. 6 Vertical distribution of core porosities, clays and carbonate cements in Paleogene Es4-Es3z
reservoirs in the Shengtuo area, the Dongying Sag
the abnormally high porosities 23%. In the AHP development PDLQO\GLVWULEXWHGLQ)LJ7KHORZSRURVLWLHV
interval III (3,900-4,400 m), the histogram of porosities account for 1%, the high porosities 9%, and the abnormally
distribution shows positive skewness, and the porosities are high porosities 90%.
30 30 30
2800-3200 m 3250-3700 m 3900-4400 m
25 Sample No.: 1203 25 Sample No.: 1105 25 Sample No.: 88
Frequency, %
Frequency, %
Frequency, %
20 20 20
15 15 15
10 10 10
5 5 5
0 0 0
0 4 8 12 16 20 24 28 0 4 8 12 16 20 24 28 0 4 8 12 16 20 24 28
Porosity, % Porosity, % Porosity, %
Fig. 7 Histograms of porosities in different AHP development depth intervals in the Shengtuo area, the Dongying Sag
2.0 2.0
Normal
porosity
development
interval
Normal evolution
curve of
2.5 2.5 average porosity
Porosity
envelope
curve
Depth, km
Depth, km
Abnormally
Primary high porosity
3.0 3.0 abnormally
development
high porosity intervalĉ
zoneĉ
Abnormally
Primary high porosity
3.5 3.5 abnormally development
high porosity intervalĊ
zoneĊ
Fig. 8 Core plug porosity, secondary surface porosity, percentage of secondary surface porosity in total surface porosity and
percentage of primary surface porosity in total surface porosity in Paleogene Es4-Es3z reservoirs in the Shengtuo area, Dongying
6DJ)RUHDFKFRUHSRURVLW\VDPSOHWKHUHDUHPDWFKHGWKLQVHFWLRQDQGUHGHSR[\UHVLQ±LPSUHJQDWHGWKLQVHFWLRQ
Anomalously high porosity sandstones High porosity sandstones Low porosity sandstones
porosity development interval Ⅰ
(2800m-3200m) Abnormally high
B-1
(d) 200ȝP B-2
(e) 100ȝP B-3
(f) 100ȝP
Tuo720, 3671.1 m, ĭ=14.2%; Tuo73, 3371.25 m, ĭ=10.2%; Tuo73, 3368.4 m, ĭ=3.5%;
primary pores (-) mainly primary pores (-) debris secondary pores (-)
porosity development interval Ⅲ
(3900-4400m) Abnormally high
Fig. 9 Photomicrographs showing pores of Paleogene Es4-Es3z reservoirs with different porosity levels in different AHP development
intervals. (a-g, i): red epoxy resin–impregnated thin section
Pet.Sci.(2014)11:346-362 355
50 50 50
DPP :HOO7P (b) PP Well T720,P, (c) PP Well T764,P,
ĭ=22.3%, k P' ĭ=19.0%,k P' ĭ=14.4%,k P'
40 Well T126,P, 40 Well T76,P, 40 Well T764,P,
Percentage, %
Percentage, %
Percentage, %
ĭ=16.6%,k P' ĭ=12.9%,k P' ĭ=6.1%,k P'
Well T167,P, Well T73,P, Well 764,P,
30 ĭ=4.6%,k P' 30 ĭ=3.5%,k P' 30 ĭ=1.8%,k P'
20 20 20
10 10 10
0 0 0
1030
16.0
25.0
40.0
63.0
0.16
0.25
0.40
1.63
1.00
2.60
4.50
6.00
0.000
0.006
0.010
0.016
0.025
0.040
0.63
0.10
4.50
6.00
1030
16.0
25.0
40.0
63.0
.0
0.10
0.16
0.25
0.40
1.63
1.00
2.60
40.0
63.0
.0
0.000
0.006
0.010
0.016
0.025
0.040
0.63
1.63
1.00
2.60
4.50
6.00
1030
16.0
25.0
0.000
0.006
0.010
0.016
0.025
0.040
0.63
0.10
0.16
0.25
0.40
.0
0
0
0
0.
0.
0.
Fig. 10 Pore-throat radius distribution of Paleogene Es4-Es3z reservoirs with different porosity levels in
different AHP development intervals
Fluid pressure, MPa Fluid pressure coefficient R o, % Temperature, °C CO2 in natural gas, %
0 10 20 30 40 50 60 0.6 0.8 1.0 1.2 1.4 1.6 1.8 0 0.5 1.0 1.5 0 50 100 150 0 5 10 15 20
1.0
0.35 0.7 1.3
1.5
2.0
2.5 B sub-stage
Depth, km
of eogenesis
3.0
Early-A sub-stage
of mesogenesis
3.5
Late-A sub-stage
of mesogenesis
Hydrostatic pressure
4.0
4.5
(Ro) is 0.35%-0.70% in the diagenetic stage from period B authigenic kaolinite and quartz overgrowths with red epoxy
of the eogenetic stage to sub-period A1 of the mesogenetic UHVLQ±LPSUHJQDWHGWKLQVHFWLRQV)LJVKRZVWKDWZLWKRXW
stage. Thermal evolution of organic matter can generate calibration of kaolinite micropores, the difference between the
large amounts of organic acids and CO2 )LJ 7KHVH contents of feldspar pores and byproducts is generally below 0.
acidic fluids expelled into reservoirs from source rocks He and Nan (2004) found authigenic kaolinite microporosity
by compaction and overpressure related to hydrocarbon to be 25%-50%. With an average value of 37%, we made the
generation and clay dehydration should be the most likely correction of kaolinite content. Then, the difference between
source of acids for stage-I feldspar leaching. The stage-II contents of feldspar pores and byproducts was generally less
feldspar dissolution mainly occurred at 160 °C to 180 °C. WKDQDQGXVXDOO\YHU\FORVHWR)LJ7UDQVIHU
When the temperature exceeded 160 °C, the degradation of of the dissolution byproducts out of the sandstones may take
organic matter in source rocks generated CO2. Meanwhile, place during dissipation of overpressure, resulting in some
the organic acid generated earlier experienced intense enhanced porosity. However, the data demonstrate that, in a
decarboxylation, and its concentration decreased sharply. UHODWLYHO\FORVHGV\VWHPVLJQL¿FDQWIHOGVSDUSRUHVH[LVWEXW
CO 2 generated in these processes diffused into the pore the feldspar dissolution has little impact on porosity. The main
water and released H+, which controlled the pH and provided function of feldspar dissolution is converting primary pores
acidic fluids for the stage II feldspar leaching (Surdam et into isovolumetric feldspar secondary pores and micropores
al, 1989). CO 2 detected in the fluid inclusions in quartz in authigenic clays.
overgrowths also suggests the formation of these cements in In relatively closed diagenetic systems, the feldspar
the presence of CO2 (Chen et al, 2010). In addition, in the oil- dissolution products cannot be effectively removed from the
gas reservoirs below 4,000 m, the low CO2 content indicates sandstones. Precipitation occurs in forms of authigenic clay
the consumption of CO2E\IHOGVSDUGLVVROXWLRQ)LJ minerals (kaolinite and illite) and quartz cements in situ, and
6.1.2 Little porosity enhancement from feldspar the maximum enhanced porosity by dissolution of one unit
dissolution volume of K-feldspar, albite and anorthite is 13%, 7% and
Whether feldspar dissolution can effectively increase 4%, respectively (Giles and de Boer, 1990). The maximum
the reservoir porosity depends on whether the dissolution amount of feldspar pores in reservoirs in the Shengtuo area
byproducts can be removed from the dissolution area. The is about 3%, then, the maximum enhanced porosity due to
feldspar dissolution in Es 4-Es 3z reservoirs occurred in a feldspar dissolution (suppose all are K-feldspars) is just 0.4%
relatively closed diagenetic system with high temperature and (3%×13%=0.4%), which is in consistent with the statistical
salinity. We can also determine this from microscopy, which data.
shows that if the feldspar dissolution is weak, the dissolution 6.1.3 Little dissolution of carbonate minerals
byproducts are less; if feldspar dissolution is abundant, the Based on the negative relationship between core porosity
dissolution byproducts are abundant. To objectively evaluate and the amount of carbonate cements, Zhong et al (2003),
the impact of feldspar dissolution on reservoir porosities, Zhu et al (2007) and Zhang et al (2007) argued that the low
using interactive image analysis techniques, quantitative content of carbonate cements in the high porosity reservoirs
statistics were collected for the contents of feldspar pores, LQWKH6KHQJWXRDUHDRULJLQDWHGIURPVLJQL¿FDQWGLVVROXWLRQRI
Pet.Sci.(2014)11:346-362 357
Es4s
Es3x
Es3z
Es3s
Stratigraphy Es4x Es2 Es1 Ed Ng Nm Q
0 20 ņ
40 ņ
1 60 ņ
Burial and thermal history
80 ņ
Depth, km
2 100 ņ
120 ņ
3 140 ņ
160 ņ
4
Well Tuo-764
160 ņ
1.8
Pressure increasing stage Pressure stable Pressure decreasing Pressure increasing stage due to
1.6 due to low compaction stage with stage with hydrocarbon generation with
Pressure evolution and oil
charging history in Es3x-Ex3z
with rapid subsidence slow subsidence tectonic uplift relative rapid subsidence
Pressure coefficient
1.4
1.2
1.8 Normal pressure Pressure increasing stage Stable pressure Pressure decreasing Pressure increasing stage due to
stage with rapid due to low compaction stage with stage with hydrocarbon generation with
1.6 subsidence with rapid subsidence slow subsidence tectonic uplift relative rapid subsidence
and hydrocarbon
Pressure evolution and oil
charging history in Es4
generation
Pressure coefficient
1.4
1.2
Fig. 12 Burial and thermal history, fluid pressure evolution history and hydrocarbon charging history of
VXEODFXVWULQHIDQVLQWKH6KHQJWXRDUHD'DWDRIK\GURFDUERQFKDUJLQJKLVWRU\DQGÀXLGSUHVVXUHHYROXWLRQKLVWRU\
from Cai et al (2009) and Sun (2010))
2.1
2.3
Depth, km
2.5
2.7
2.9
3.1
3.3
A, %: Difference between feldspar pore content and dissolution byproducts;
B, %: Difference between feldspar pore content and 62.5% of kaolinite content and quartz overgrowth content
Fig. 13 Amount of feldspar pores, dissolution products, and their differences in Es4-Es3z reservoirs
buffer system, the carbonate minerals tend to be precipitated 5) The calculation of Meshri (1986) shows that at 25 °C
rather than to be corroded, but the feldspars tend to be leached DQGEDUWKH*LEEVIUHHHQHUJ\ǻG) for leaching of anorthite
(Surdam et al, 1989). and K-feldspar by acetic acid to form kaolinite is –36.9 kJ/
2) Thick gypsum and salt layers and carbonate layers PRODQG±N-PRODQGǻG of the reaction between calcite
exist in the Palaeogene Es4 )RUPDWLRQ DQG VXJJHVW D KLJK and acetic acid is +11.20 kJ/mol. Meanwhile, as temperature
salinity and strong alkalinity of the sedimentary water (Wang, DQG SUHVVXUH LQFUHDVHǻG of reaction between organic
6DOLQLW\GDWDRIÀXLGLQFOXVLRQVLQTXDUW]RYHUJURZWKV acid and feldspars decreases (Huang et al, 2009b), while as
LQGLFDWHWKHOHDFKLQJRIIHOGVSDUVE\DFLGLFÀXLGVZLWKKLJK temperature increases, the solubility of carbonate minerals
salinity (Table 2). The modern pore water in reservoirs has decreases sharply. Therefore, in a relatively closed diagenetic
high salinity, and the concentration of Ca2+ and Mg2+ is high environment with high temperature, the organic acids tend to
)LJ+LJKVDOLQLW\DQGKLJKFRQFHQWUDWLRQRI&D2+ and dissolve feldspars rather than carbonate minerals.
Mg2+ probably inhibit carbonate dissolution, and promote its
precipitation due to the common-ion effect. 6.2 Geological processes in favor of porosity
3) The main source rocks in the Dongying Sag contain preservation
high percentage of carbonate minerals (up to 50%), feldspars
6.2.1 Sedimentary facies
DQGRWKHUXQVWDEOHPLQHUDOV4LDQHWDO)LQHXQVWDEOH
minerals with high specific surface area in source rocks Statistical data show that sedimentary facies in the
UHDFWHG¿UVWZLWKWKHRUJDQLFDFLGVWKDWZHUHUHOHDVHGGXULQJ Shengtuo area have significant influence on the reservoir
thermal evolution of organic matter due to their proximity porosity. On the whole, porosities of sublacustrine fan
(Giles and Marshall, 1986). In addition, the initial salinity of reservoirs are higher than those of nearshore subaqueous
SRUHZDWHUZDVKLJKVRÀXLGH[SHOOHGIURPVRXUFHURFNVLQWR fans, which might be related to the fluid overpressure in
reservoirs would be rich in various ions. As the fluid with VXEODFXVWULQH IDQV )RU H[DPSOH LQ$+3 GHYHORSPHQW
high salinity and weak acidity entered into the reservoirs, its intervals I and II, reservoirs in sublacustrine fans have an
acidity decreased further, in such condition, the carbonate average porosity of 15.03% and 10.72%, while the average
minerals tended to be precipitated, rather than be dissolved porosity of reservoirs in nearshore subaqueous fans is
(Zeng, 2001). just 10.43% and 6.43% (Table 3). In sublacustrine fans,
4) The study by Song and Huang (1990) shows that porosities of reservoirs in braided channels in the mid-fan
carbonate minerals may precipitate at a pH between 5 and are the best, followed by porosities of main channels inner-
6, although most scholars argued that carbonate minerals fan, and porosities of outer fan and inter-channels in mid-
begin to precipitate when pH exceeds 8.4. In addition, the fan are the worst. In nearshore subaqueous fans, porosities of
calculation results by Huang et al (2009a) show that, for reservoirs in middle-front of fan body are the best, porosities
carbonate dissolution in deep buried reservoirs (>3,000 m), of reservoirs in root of fan body and fan edge are worse (Table
the pH of fluid should be lower than 5. However, CaCl2- 3).
type pore water with high salinity of the relatively stagnant 6.2.2 Fluid overpressure
environment in the Shengtuo area is generally weakly acidic The fluid pressure in the Es4 formation experienced five
ZLWKS+EHWZHHQDQG)LJZKLFKLVQRWIDYRUDEOHIRU stages: 1) normal pressure stage with rapid subsidence at 49-
carbonate dissolution in deep burial. 40 Ma, 2) pressure increase stage due to low compaction with
Pet.Sci.(2014)11:346-362 359
pH K+ & Na+, mg/L Ca2+, mg/L Mg2+, mg/L Clí, mg/L SO 42í, mg/L HCO3í , mg/L Total salinity, mg/L Water type
6.0 7.0 1000 100000 100 10000 10 1000 1000 100000 100 1000 100 10000 1000 100000 CaCl2 NaHCO3 MgCl2
1.5
2.0
2.5
Depth, km
3.0
3.5
Es3s
Es3z
Es3x
Es4s
Es4x
4.0
Min, %
M 1.0
1. 1.0 2.6 1.9 1.4 3.5 1.4 1.7 1.8 1.0 1.8 1.4 1.0 1.4 2.9
Abnormally
high porosity Max, % 22.0 19.2 22.0 23.6 29.5 19.7 29.5 21.1 19.9 27.0 19.9 29.5 26.9 23.8 29.5
development Ave, % 10.43 7.46 12.92 6.62 15.03 10.33 17.70 8.34 9.02 11.20 11.62 15.39 10.22 11.35 16.55
interval ĉ
Sample No. 516 50 302 164 873 78 595 27 173 426 294 669 363 425 601
Min, % 0.7 0.7 1.8 2.9 1.1 1.5 1.6 1.2 1.1 0.7 1.1 1.2 0.7 1.3 1.5
Abnormally
high porosity Max, % 20.9 8.8 20.9 20.9 32.9 28.1 32.9 16.8 19.9 11.4 22.1 32.9 22.1 28.1 32.9
development Ave, % 6.43 3.57 8.60 11.06 10.72 9.66 12.55 6.89 7.16 5.27 10.18 11.92 6.44 10.02 13.63
interval Ċ
Sample No. 171 71 70 30 793 166 451 93 83 142 544 278 345 293 326
rapid subsidence and hydrocarbon generation at 40-31.9 Ma, development at 35-24.6 Ma. Moderate-strong overpressure
3) stable pressure stage with slow subsidence at 31.9-24.6 EHJDQWRGHYHORSDIWHUDERXW0D)LJ&DLHWDO
Ma, 4) pressure decrease stage with tectonic uplifting at 24.6- :KHQÀXLGRYHUSUHVVXUHEHJDQWRGHYHORSWKHEXULDOGHSWKV
14 Ma and 5) pressure increase stage due to hydrocarbon of sublacustrine fan reservoirs in Es3 and Es 4 are always
JHQHUDWLRQZLWKUHODWLYHO\UDSLGVXEVLGHQFHDW0D)LJ shallower than 2,200 m. The shallow development of fluid
12) (Zhang et al, 2009; Sun, 2010). overpressure retarded compaction during deeper burial and
Before 13 Ma, fluid pressure in sublacustrine fans in pores in reservoirs were preserved to greater depths.
Es 3 was generally normal, but with weak overpressure Data in Table 3 show that as fluid overpressure
360 Pet.Sci.(2014)11:346-362
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