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MSL Guia de Calibracion Manometros PDF
MSL Guia de Calibracion Manometros PDF
Pressure Gauge
Calibration
Measurement Standards Laboratory of New Zealand • fax: +64 (0)4 931 3003 • e-mail: msl@irl.cri.nz • website: http://msl.irl.cri.nz 1
The gauge reading at each calibration point is meas- There are three main uncertainty components for a
ured for both rising and falling pressure. Rising pressure gauge calibration. These are: uref the reference standard
means starting at zero applied pressure (or the lowest component, ures the gauge resolution component and
pressure point on the gauge) and steadily increasing the urep the gauge repeatability. The standard uncertainty for
pressure until the calibration pressure point is reached. pcorr is given by
Falling pressure means starting at the maximum pres-
sure point on the gauge and then steadily decreasing the
ucorr = uref
2
+ ures
2
+ urep
2
.
pressure to the calibration pressure point. In practice the
pressure applied to the gauge is cycled from the zero (or
the minimum scale point) up to the maximum scale point Here the uncertainty components are combined follow-
and then back to zero. ing section 5 of [2].
On reaching the desired point the pressure is held Finally the expanded uncertainty is calculated using
steady in readiness for taking the gauge reading. The Ucorr = kucorr where k is the coverage factor chosen so
operator must wait until both the applied pressure and that the uncertainty interval has a 95 percent level of
gauge reading have stabilised before recording a read- confidence. The value of k is calculated using the t-
ing. The waiting time will depend on the reference equip- distribution and the effective degrees of freedom of the
ment, the gauge response time and size of the pressure measurement, see Table G.2 in [2]. The effective de-
change from the previous point. Waiting times could be grees of freedom are calculated using the Welch-
as short as a few seconds for low accuracy gauges or as Satterthwaite formula found in section G.4 of [2].
long as several minutes for a high resolution high pres- The calculation of k for a pressure gauge calibrated
sure gauge. The system response time should be de- following this guide can be simplified by choosing to use
termined before starting the calibration. k = 2.2. This approximation will have a maximum error of
The order that the gauge pressure points are applied 9 % as k will be in the range 2.0 to 2.4. This error is
to the gauge can be varied. One method is to calibrate small compared to other sources of error in the ex-
the gauge sequentially by making all the rising pressure panded uncertainty.
readings in increasing order until the maximum pressure
is reached. Then the falling pressure readings are made
in decreasing order stopping after the zero reading is
Components of Uncertainty
taken. In this case one calibration cycles the gauge from This section discusses how the three main uncer-
zero to maximum and back once. tainty components are calculated.
An alternative is chose a pressure point and take
both the rising and falling pressure readings before con- Reference Pressure Uncertainty uref
tinuing on to the next chosen pressure point. In this case
This term is the standard uncertainty of the applied
the applied pressure will start at zero and rise steadily up
pressures and its value can be found in the reference
to the desired pressure where a rising pressure reading
instrument calibration report. A typical uncertainty state-
is taken. Then the pressure is increased to the maximum
ment for a dead weight tester will read:
pressure and decreased back to the pressure point
‘The expanded uncertainty in the pressure that
where the falling pressure reading is recorded. Finally
is generated by the deadweight tester is 0.015 % of
the pressure is reduced to zero.
the calculated pressure or 0.04 kPa, whichever is
The main advantage of this alternative order is the
greater, for pressures in the range 260 kPa to
ease with which repeat measurements can be made,
3000 kPa.’
especially when using a dead weight tester or pressure
The expanded uncertainty was calculated using
balance. The repeat measurements can be made by
a coverage factor k = 2.1 and defines an interval
simply taking the pressure around another calibration
estimated to have a 95% level of confidence.’
cycle without any need to load or unload weights. This
The expanded uncertainty Uref is converted to a
reduces both the time and effort required to make a re-
peat calibration. standard uncertainty by dividing by the coverage factor k
This alternative order has other advantages. It pro- so that uref = Uref k .
vides the opportunity to record a number of zero read- In the example above the standard uncertainty at
ings during the calibration which can be used to assess 2000 kPa will be given by
any drift in the gauge reading. It also allows the pressure
readings to be taken in any order, rather than in a con- 0.015 %
uref (2000 kPa) = × 2000 kPa = 0.14 kPa.
tinuously increasing and decreasing sequence. 2.1
Measurement Standards Laboratory of New Zealand • fax: +64 (0)4 931 3003 • e-mail: msl@irl.cri.nz • website: http://msl.irl.cri.nz 2
For the example shown above, the gauge resolution where N is the number of rising and falling pressure
th
is 0.01 kPa. The resolution of some digital devices can points in a single calibration cycle, pread1,i is the i gauge
change as the pressure increases so the resolution un- pressure reading from the first calibration cycle, pread2,i is
certainty will also change with pressure. Some digital the ith gauge pressure reading from the second calibra-
displays may increment by more than one count, in this tion cycle. and Diff12,i is difference between each reading
case the resolution is equal to the size of the increment. from cycle 1 and 2. The 1 2 term arises as the re-
The resolution of a gauge with an analogue scale is ported corrections are an average of the two cycles. This
calculated as a fraction of the smallest scale interval. calculation is more straightforward than is looks, see the
The scale interval is the smallest pressure interval worked examples below.
marked on the gauge scale.
Worked Examples
The following examples show the details of the un-
certainty calculations for the pressure gauge corrections.
1 ∑( p read1,i − pread2,i )
urep = i =0
Repeatability Uncertainty urep
2 2N
This component is calculated from the difference be-
tween the two calibration cycles. The data is shown in
2
N the table below, where Type is the pressure direction,
1 ∑ (Diff ) 12,i pref the reference pressure, the two sets of gauge read-
= i =0
,
2 2N
Measurement Standards Laboratory of New Zealand • fax: +64 (0)4 931 3003 • e-mail: msl@irl.cri.nz • website: http://msl.irl.cri.nz 3
pref Cycle 1 Cycle 2 Diff1,2 Diff1,22 pcorr
Type pnom/ kPa
/ kPa / kPa / kPa / kPa / kPa2
Rise / kPa Fall / kPa
Rise 1000.2 1020 1040 –20 400
0 –20
Rise 2000.1 2040 2060 –20 400
1000 –30 –20
Rise 3000.0 3040 3060 –20 400
2000 –50 –10
Rise 3999.9 4040 4040 0 0
3000 –50 –20
Fall 3000.0 3020 3020 0 0
4000 –40
Fall 2000.1 2000 2020 –20 400
Fall 1000.2 1020 1020 0 0
Fall 0.0 20 20 0 0 The expanded uncertainty in each gauge correction
tabulated above is 20 kPa. This expanded uncertainty
Sum Diff2 1600 was estimated by combining the uncertainties associ-
N 8 ated with the reference standards and the calibration
process. The expanded uncertainty was calculated using
urep / kPa 7.1 a coverage factor k = 2.2 and defines an interval esti-
mated to have a 95 % level of confidence (see ISO
Guide to the Expression of Uncertainty of Measurement,
ings are in the Cycle 1 and 2 columns and the difference 1995).
Diff12,i and difference squared values are shown in the This gauge cannot be said to comply with the accu-
last two columns. racy requirements for a class 1 gauge as the corrections
The component urep is calculated by summing up all and uncertainty are too large.
the values of Diff1,22, dividing by 2N which is two times
the number of rising and falling pressure points, taking Example 2. A Digital Pressure Gauge
the square root of the result and multiply by 1 2 . The
In this example we are calibrating a 0 to 10000 kPa
value obtained for this gauge is urep = 7.1 kPa. Often
digital gauge, resolution 0.1 kPa, using a dead weight
there is no difference between the readings of cycle 1 tester with an expanded calibration uncertainty of
and 2 for this class of gauge. In that case urep = 0.
0.005 %, k = 2.0. We have chosen to calibrate this
gauge at ten pressures, including zero.
Standard and Expanded Uncertainty uc, Uc
The standard uncertainty for the gauge corrections is
pref Cycle 1 Cycle 2 Diff1,2 / Diff1,22
calculated by combining the uncertainty terms together Type
/ kPa / kPa / kPa kPa / kPa
as follows
Rise 999.73 997.5 997.6 -0.10 0.010
ucorr = u 2
ref +u2
res +u 2
rep
Rise 1999.48 1994.7 1994.5 0.15 0.023
Rise 2999.23 2991.3 2991.4 -0.05 0.002
Rise 3999.00 3987.8 3987.6 0.20 0.040
= (0.2 kPa)2 + (5.8 kPa)2 + (7.1 kPa)2
Rise 4998.76 4984.4 4984.1 0.25 0.063
Measurement Standards Laboratory of New Zealand • fax: +64 (0)4 931 3003 • e-mail: msl@irl.cri.nz • website: http://msl.irl.cri.nz 4
Following the previous example we have pcorr
pNom Uc
U 0.00005 / kPa Rise Fall / kPa
uref ( p) = ref × p = p = 0.000025 p / kPa / kPa
k 2
0 –0.1 0.2
and
1000 2.2 1.7 0.2
0.1 2000 4.9 4.0 0.2
ures = = 0.029 kPa .
2 3 3000 7.9 6.7 0.3
4000 11.3 9.8 0.3
Again the repeatability component is calculated from
the difference between the two calibration cycles and is 5000 14.5 13.1 0.3
urep = 0.08 kPa (see the table above). 6000 18.8 17.5 0.4
7000 23.3 22.4 0.4
Standard and Expanded Uncertainty uc, Uc
8000 28.2 27.3 0.5
Here the value of uref and urep are similar, so we can-
not use a single value for uref as we did for the class 1 9000 33.4 33.0 0.5
gauge. The gauge correction uncertainties will be pres- 10000 39.1 0.6
sure dependent. The table below shows the results of
the uncertainty calculations.
9000 0.22 0.08 0.03 0.24 0.53 [4] Accuracy (trueness and precision) of measurement
methods and results -- Part 3: Intermediate meas-
10000 0.25 0.08 0.03 0.26 0.58
ures of the precision of a standard measurement
method, Section 8, ISO 5725-3:1994.
MSL is New Zealand’s national metrology institute, operating within Industrial Research Limited under the authority of the
New Zealand Measurement Standards Act 1992.
Measurement Standards Laboratory of New Zealand • fax: +64 (0)4 931 3003 • e-mail: msl@irl.cri.nz • website: http://msl.irl.cri.nz 5