PERCOBAAN 1

Kons EDTA 0.097560976 N Adsorben 142 gram

Flowrate 32.4 ml/menit Ca 2+ awal 2500 mg

0.0324 liter/menit

Waktu V sampel V1 V2 V EDTA 1 V EDTA 2 V av

No Ca2+ (ppm)
(menit) (ml) (ml) (ml) (ml) (ml) (ml)

1 0 100 10 10 6.3 6.9 9.75 9.520756098

2 5 125 10 10 3.1 6 4.55 3.55441561

3 10 95 10 10 5.1 5 5.05 5.190803594

4 15 95 10 10 2.9 2.8 2.85 2.929463415

5 20 81 25 25 3 2.8 2.9 3.49606745

6 25 52 25 25 6.2 6.5 6.35 11.92441839

7 30 73 25 25 6 6.4 6.2 8.293458069

8 35 70 25 25 6.8 6 6.4 8.927888502

9 40 70 25 25 5.6 6.1 5.85 8.160648084

10 45 66 25 25 7 7 7 10.35668884

11 50 61 25 25 5.2 6.2 5.7 9.124558177

12 55 75 25 25 6 6.1 6.05 7.877001626

13 60 62 25 25 5.6 6.5 6.05 9.528630999

14 65 52 25 25 5.8 5.8 5.8 10.89159475

15 70 59 25 25 5.8 6 5.9 9.764878049

16 75 67 25 25 5.6 6.3 5.95 8.671794685

17 80 61 25 25 5.4 5.4 5.4 8.644318273

18 85 68 25 25 5.3 5.9 5.6 8.041664275

19 90 70 25 25 5.5 5.3 5.4 7.532905923

20 95 62 25 25 5.3 5.3 5.3 8.347395751

21 100 67 25 25 5.6 4.3 4.95 7.2143502

 Konsentrasi Ca 2+ vs Waktu
14
12
Ca 2+ (ppm)

10
8
6
4
2
0
0 20 40 60 80 100 120
time (menit)

Log Ca2+ vs Log Xm/m

1.245

1.24
y = -0.0252x + 1.2536
Log Xm/m

1.235 R² = 0.9646

1.23 Series1
Linear (Series1)
1.225

1.22
0 0.5 1 1.5
Log Ca2+

Xm/m vs Konsentrasi Ca2+

14
Konsentrasi Ca2+ (ppm)

12
y = -14.2x + 250
10
R² = 1
8
6 Series1
4 Linear (Series1)
2
0
16.6 16.8 17 17.2 17.4 17.6
Xm/m

PERCOBAAN 2

V standarisasi 27 ml Limbah 10 L
Kons EDTA 0.074074074 N Adsorben 142 gram

Flowrate 66 ml/menit Ca 2+ awal 3500 mg

0.066 liter/menit

Konsentrasi Ca 2+ vs Waktu
8
7
6
Ca 2+ (ppm)

5
4
3
2
1
0
0 10 20 30 40 50 60 70 80
time (menit)

Waktu V sampel V1 V2 V EDTA 1 V EDTA 2 V av

No Ca2+ (ppm)
(menit) (ml) (ml) (ml) (ml) (ml) (ml)

1 0 100 25 25 6.2 6.8 9.6 7.117511111

2 5 196 25 25 6.9 7.8 7 2.647883598

3 10 178 25 25 6.3 8.2 7.25 3.019777362

3 15 141 25 25 6.8 6.1 6.45 3.391544523

4 20 160 25 25 6.6 7.5 7.05 3.266826389

5 25 155 25 25 6.9 7.6 7.25 3.467873357

6 30 149 25 25 6.5 7 6.75 3.358724832

7 35 151 25 25 6.9 7.7 7.3 3.584287466

8 40 144 25 25 8.3 9.3 8.8 4.530823045

9 45 147 25 25 6.4 7.4 6.9 3.480075586

10 50 146 25 25 8.3 6.8 7.55 3.83399036

11 55 145 25 25 6.8 7.7 7.25 3.707037037

12 60 143 25 25 7.3 7.7 7.5 3.888500389

13 65 148 25 25 8.4 9.9 9.15 4.583701201

14 70 155 25 25 9.5 8.6 9.05 4.328862605

15 75 149 25 25 0 0

Xm/m Vs Konsentrasi Ca2+ (ppm)

5
Konsentrasi Ca2+ (ppm)

4.5
4
3.5
3 y = -14.2x + 350
2.5 R² = 1
2
1.5
1
0.5
24.3 24.32 24.34 24.36 24.38 24.4 24.42 24.44 24.46 24.48
Xm/m

Log Ca2+ vsLog Xm/m

1.39
1.389
1.388 y = -0.013x + 1.3944
R² = 0.9709
Log Xm/m

1.387
1.386
Series1
1.385
1.384 Linear (Series1)
1.383
1.382
0 0.2 0.4 0.6 0.8 1
Log Ca2+