RESULT ANALYSIS

Volume of NaOH = 30 L

Volume of Et(Ac) = 30 L

Initial concentration of NaOH = 0.1 M

Initial concentration of Et(Ac) = 0.1 M

Flow rate = 200 mL/min

Table 1: Result of The Experiment

Time Temperature Flow rate Flow rate Total Residence Conductivity Concentration Conversion
(min) (°C) of NaOH, of Et(Ac) flow rate time, t(min) (mS/cm) of NaOH, X (%)
FNAOH FEt of 𝐶𝑁𝑎𝑂𝐻 (M)
(mL/min) (mL/min) FNAOH+FEt
(mL/min)
0 35.6 197 208 405 24.69 9.62 0.0401 0.00
5 35.5 202 207 409 24.45 8.14 0.0296 26.18
10 35.5 207 206 413 24.21 7.08 0.0220 45.14
15 35.5 204 205 409 24.45 6.27 0.0162 59.60
20 35.6 205 205 410 24.39 5.61 0.0115 71.32
25 35.6 202 205 407 24.57 5.05 0.0075 81.30
30 35.7 202 205 407 24.57 4.60 0.0043 89.28
35 35.7 205 203 408 24.51 4.24 0.0017 95.76
 Volume of NaOH = 30 L

Volume of Et(Ac) = 30 L

Initial concentration of NaOH = 0.1 M

Initial concentration of Et(Ac) = 0.1 M

Flow rate = 300 mL/min

Table 2: Result of The Experiment

Time Temperature Flow rate Flow rate Total Residence Conductivity Concentration Conversion
(min) (°C) of NaOH, of Et(Ac) flow rate time, t(min) (mS/cm) of NaOH, X (%)
FNAOH FEt of 𝐶𝑁𝑎𝑂𝐻 (M)
(mL/min) (mL/min) FNAOH+FEt
(mL/min)
0 35.7 303 307 610 16.39 10.71 0.0479 0.00
5 35.6 302 307 609 16.42 9.82 0.0416 13.15
10 35.6 304 305 609 16.42 8.54 0.0324 32.36
15 35.5 303 304 607 16.47 7.86 0.0276 42.38
20 35.5 302 304 606 16.50 6.91 0.0208 56.58
25 35.3 303 303 606 16.50 5.17 0.0084 85.46
30 35.4 303 304 607 16.47 4.52 0.0037 92.28
35 35.4 303 304 607 16.47 4.11 0.0008 98.32
 Concentration of NaOH (M) Vs
Conductivity( mS/cm)
12
Concentration of NaOH (M)

10
8 y = 140x + 4
6
4
2
0
0 0.01 0.02 0.03 0.04 0.05 0.06
Conductivity (mS/cm)

Figure 1: Graph Concentration of NaOH (M) vs Conductivity (mS/cm)

Conversion X (%) Vs Time (min)

120
y = 3.1329x
100 R² = 0.901
Conversion X (%)

80

60
Coversion X (%)
40 Linear (Coversion X (%))

20

0
0 10 20 30 40
Time (min)

Figure 2: Graph Conversion (%) against Time (min) For Flow rate 200 (mL/min)
 Conversion X (%) Vs Time (min)
120
y = 3.0008x
100 R² = 0.9805
Conversion X (%)

80

60
Coversion X (%)
40 Linear (Coversion X (%))

20

0
0 10 20 30 40
Time (min)

Figure 3: Graph Conversion (%) against Time (min) For Flow rate 300 (mL/min)
CALCULATION

Flowrate = 200 mL/min

Reaction rate constant, k 

C A0  C A 
 avg C 2A

0.1𝑀 − 0.0017𝑀
𝑘=
24.48 min× 0.0017^2

𝑘 = 1389.45 𝑀/𝑚𝑖𝑛

Rate of reaction, -rA  kCA2

-rA= 1389.45 𝑀/ min × 0.00172 M

-rA= 0.0040 𝑀^2/𝑚𝑖𝑛

Flowrate = 200 mL/min

Reaction rate constant, k 

C A0  C A 
 avg C 2A

0.1𝑀 − 0.0008𝑀
𝑘=
16.46 min× 0.0008^2

𝑘 = 9416.77 𝑀/𝑚𝑖𝑛
Rate of reaction, -rA  kCA2

-rA= 9416.77 𝑀/ min × 0.00082 M

-rA= 0.0060 𝑀^2/𝑚𝑖𝑛

APPENDIX

For both flow rate (200 mL/min & 300mL/min)

A. concentration of NaOH based on Figure 1 : Table 1

Equation of the graph: 𝑦 = 140𝑋 + 4

Slope of the graph: 140

𝑦 = 𝑚𝑋 + 𝐶
𝑚𝑆
𝑤ℎ𝑒𝑟𝑒 𝑌 = 𝑐𝑜𝑛𝑑𝑢𝑐𝑡𝑖𝑣𝑖𝑡𝑦 ( )
𝑐𝑚
𝑚 = 𝑠𝑙𝑜𝑝𝑒 𝑜𝑓 𝑡ℎ𝑒 𝑔𝑟𝑎𝑝ℎ

𝑋 = 𝑐𝑜𝑛𝑐𝑒𝑛𝑡𝑟𝑎𝑡𝑖𝑜𝑛 𝑜𝑓 𝑁𝑎𝑂𝐻 (𝑀)

𝑚𝑆
9.62 = 140𝑋 + 4
𝑐𝑚
= 0.0401 𝑀

B. conversion, X (%) at minute 5 Table 1 :

𝐶𝑁𝑎𝑂𝐻 (𝑡=0) − 𝐶𝑁𝑎𝑂𝐻

×= × 100%
𝐶𝑁𝑎𝑂𝐻 (𝑡=0)
0.0296𝑀 − 0.0401𝑀
𝑋= × 100%
0.0401𝑀
𝑋 = 26.18 %

C. Residence Time at minute 5 Table 1 :

VCSTR
Residence Time ,  
F0
10000 𝑚𝐿
=
405 𝑚𝐿 /𝑚𝑖𝑛

= 24.69 𝑚𝑖𝑛