Analisa Highscore Plus

Dahiyun Page 1 3/14/2019
This is the simple example template containing only headers for each report item and the
bookmarks. The invisible bookmarks are indicated by text between brackets.
Modify it according to your own needs and standards.
Measurement Conditions: (Bookmark 1)
Dataset Name Besi_Bagian A

File name J:\Pak Naila Mibarok\Besi_Bagian A.xrdml
Comment Configuration=Stage for flat samples/holders, Owner=User-1,
Creation date=5/23/2013 12:24:13 PM
Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001;
Minimum step size Omega:0.0001
Sample stage=Stage for flat samples/holders
Diffractometer system=EMPYREAN
Measurement program=C:\PANalytical\Data
Collector\Programs\standard general.xrdmp, Identifier={A972D4E3-603B-40B3-9A18-
68BB597B081D}
Measurement Date / Time 2/8/2015 7:31:16 PM
Operator User
Raw Data Origin XRD measurement (*.XRDML)
Scan Axis Gonio
Start Position [°2Th.] 10.0131
End Position [°2Th.] 119.9671
Step Size [°2Th.] 0.0260
Scan Step Time [s] 7.1400
Scan Type Continuous
PSD Mode Scanning
PSD Length [°2Th.] 3.35
Offset [°2Th.] 0.0000
Divergence Slit Type Fixed
Divergence Slit Size [°] 0.5000
Specimen Length [mm] 10.00
Measurement Temperature [°C] 25.00
Anode Material Cu
K-Alpha1 [Å] 1.54060
K-Alpha2 [Å] 1.54443
K-Beta [Å] 1.39225
K-A2 / K-A1 Ratio 0.50000
Generator Settings 40 mA, 40 kV
Diffractometer Type 0000000011141702
Diffractometer Number 0
Goniometer Radius [mm] 240.00
Dist. Focus-Diverg. Slit [mm] 100.00
Incident Beam Monochromator No
Spinning No
Main Graphics, Analyze View: (Bookmark 2)
Counts
Besi_Bagian A
3000 Carbon 87.8 %
Iron - Alpha 0.2 %
Chromium 0.2 %
Manganese 2.1 %
Nickel 3.6 %
Silicon - Vi 6.1 %
2000
1000
0
20 30 40 50 60 70 80 90 100 110
Position [°2Theta] (Copper (Cu))
Peak List: (Bookmark 3)
Pos. [°2Th.] Height [cts] FWHM Left [°2Th.] d-spacing [Å] Rel. Int. [%]
14.1611 0.32(3) 0.1802 6.24914 0.03
14.1967 0.16(2) 0.1805 6.24905 0.02
20.1137 0.55(7) 0.2359 4.41115 0.05
20.1644 0.27(3) 0.2364 4.41110 0.03
21.9708 0.9(2) 0.6510 4.04232 0.09
22.0263 0.43(9) 0.6513 4.04228 0.04
24.7181 2.8(4) 0.2821 3.59890 0.28
24.7807 1.4(2) 0.2827 3.59887 0.14
28.4177 0.22(5) 0.6988 3.13822 0.02
28.4901 0.11(2) 0.6994 3.13819 0.01
28.6313 3.3(5) 0.3229 3.11529 0.33
28.7042 1.6(2) 0.3237 3.11527 0.16
32.1073 0.48(7) 0.3603 2.78551 0.05
32.1895 0.24(4) 0.3612 2.78549 0.02
35.2762 2.6(4) 0.3952 2.54221 0.26
35.3670 1.3(2) 0.3962 2.54219 0.13
37.0810 6(1) 0.7786 2.42252 0.56
37.1767 3(1) 0.7796 2.42250 0.28
37.5908 5(1) 0.7839 2.39082 0.54

37.6879 3(1) 0.7849 2.39081 0.27
38.2151 2.0(3) 0.4284 2.35319 0.20
38.3140 1.0(2) 0.4295 2.35318 0.10
40.9743 12(2) 0.4602 2.20087 1.22
41.0809 6(1) 0.4614 2.20086 0.61
41.7763 20(4) 0.8290 2.16046 2.01
41.8852 10(2) 0.8302 2.16045 1.00
42.8226 41(8) 0.8408 2.11006 4.09
42.9345 20(4) 0.8421 2.11005 2.03
43.5526 70(9) 0.8492 2.07637 7.05
43.5726 509(32) 0.2761 2.07546 51.04
43.5885 72(6) 0.4910 2.07474 7.17
43.5885 163(13) 0.4910 2.07474 16.31
43.6153 998(69) 0.3754 2.07353 100.00
43.6608 34(4) 0.8505 2.07147 3.42
43.6666 35(4) 0.8506 2.07636 3.50
43.6867 252(16) 0.2776 2.07545 25.23
43.7026 35(3) 0.4923 2.07473 3.55
43.7026 81(7) 0.4923 2.07473 8.08
43.7295 494(36) 0.3764 2.07352 49.54
43.7751 17(2) 0.8518 2.07146 1.70
43.9997 68(10) 0.8544 2.05630 6.79
44.1150 34(5) 0.8558 2.05629 3.37
44.5388 125(8) 0.1000 2.03266 12.50
44.6556 62(4) 0.1000 2.03265 6.21
44.8989 42(8) 0.8651 2.01719 4.20
45.0168 21(4) 0.8665 2.01718 2.09
45.7633 16(3) 0.6444 1.98108 1.55
45.8837 8(2) 0.6462 1.98107 0.77
46.0833 1.0(2) 0.5209 1.96806 0.10
46.2047 0.48(8) 0.5224 1.96805 0.05
Pattern List: (Bookmark 4)
Visible Ref. Code Score Compound Displacemen Scale Factor Chemical

Name t [°2Th.] Formula
* 98-065-5131 37 Carbon 0.000 0.213 C1
* 98-018-0969 37 Iron - Alpha 0.000 0.065 Fe1
* 98-004-1505 42 Chromium 0.000 0.690 Cr1
* 98-065-5106 17 Manganese 0.000 0.098 Mn1
* 98-064-6091 31 Nickel 0.000 0.187 Ni1
* 98-008-9415 14 Silicon - Vi 0.000 0.126 Si1
Document History: (Bookmark 5)
Insert Measurement:
- File name = "Besi_Bagian A.xrdml"
- Modification time = "2/21/2015 7:19:58 PM"

- Modification editor = "Dahyu"
Default properties:
- Measurement step axis = "None"
- Internal wavelengths used from anode material: Copper (Cu)
- Original K-Alpha1 wavelength = "1.54060"
- Used K-Alpha1 wavelength = "1.54060"
- Original K-Alpha2 wavelength = "1.54443"
- Used K-Alpha2 wavelength = "1.54443"
- Original K-Beta wavelength = "1.39225"
- Used K-Beta wavelength = "1.39225"
- Irradiated length = "10.00000"
- Spinner used = "No"
- Receiving slit size = "0.10000"
- Step axis value = "0.00000"
- Offset = "0.00000"
- Sample length = "10.00000"
Interpolate Step Size:

- Derived = "Yes"
- Step Size = "0.01"
- Modification editor = "PANalytical"
Search & Match:

- Data Source = Profile
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "Yes"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "50"
- Min. new lines / total lines = "60"
- Search depth = "10"
- Minimum new lines = "5"
- Minimum scale factor = "0.1"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"

Rietveld Refinement:
- Step No. 1
- Title = "Scale factor"
- Min. Shift/ESD = "0.1"
- Switch off after usage = "False"
- Step No. 2
- Title = "Flat background"
- Step No. 3
- Title = "Zero shift"
- Refine spec. displ. = "False"
- Step No. 4
- Title = "Lattice parameters"
- Minimum weight % = "5"
- Step No. 5
- Title = "More background"
- No. additional parameters = "2"
- Step No. 6
- Title = "W (Halfwidth)"
Rietveld Refinement Finished:

- Finishing type = "Minimum shift"
- Step No. 1
- Step No. 2
- Step No. 3

- Step No. 4
- Step No. 5
- Minimum weight % = "-1"
- Step No. 6
- Step No. 7
- Title = "Prefered orientation"
- Switch off after usage = "True"
- Toggle directions = "False"

Edit Carbon Size Strain Analysis:

- Old Value = "None"
- Step No. 1
- Step No. 2
- Step No. 3

- Step No. 4
- Step No. 5
- Step No. 6
- Minimum weight % = "1.5"
- Step No. 7
- Title = "U, V (Halfwidth)"
- Refine U = "True"
- Refine V = "True"
- Step No. 8
- Title = "Peak shape parameters"
- Refine Asymmetry = "False"
- No. of parameters = "2"
- Refine anisotropic broadening = "False"

Edit Iron - Alpha Size Strain Analysis:

- Step No. 1
- Step No. 2

- Step No. 3
- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7
- Refine U = "True"
- Refine V = "True"
- Step No. 8

Edit Chromium Size Strain Analysis:

- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7
- Refine U = "True"
- Refine V = "True"
- Step No. 8

Edit Manganese Size Strain Analysis:


- Old Value = "Size only"
- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7
- Refine U = "True"
- Refine V = "True"
- Step No. 8


Edit Nickel Size Strain Analysis:


- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7

- Refine U = "True"
- Refine V = "True"
- Step No. 8

Edit Silicon - Vi Size Strain Analysis:

Edit Silicon - Vi Size Strain Analysis:

- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7
- Refine U = "True"
- Refine V = "True"
- Step No. 8


- Old Value = "Size and Strain"
- Step No. 1
- Step No. 2
- Step No. 3

- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7


- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4

- Step No. 5
- Step No. 6
- Step No. 7


- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7
- Refine U = "True"
- Refine V = "True"
- Step No. 8


- Step No. 1
- Step No. 2
- Step No. 3

- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7


- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4

- Step No. 5
- Step No. 6

- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7

- Refine U = "True"
- Refine V = "True"
- Step No. 8



- Step No. 1
- Step No. 2
- Step No. 3
- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7
- Refine U = "True"
- Refine V = "True"
- Step No. 8


- Step No. 1
- Step No. 2
- Step No. 3

- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7



- Step No. 1
- Step No. 2
- Step No. 3

- Step No. 4
- Step No. 5
- Step No. 6
- Step No. 7

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Dahiyun Page 1 3/14/2019

Measurement Conditions: (Bookmark 1)

Dataset Name Besi_Bagian A

Main Graphics, Analyze View: (Bookmark 2)

Peak List: (Bookmark 3)

37.5908 5(1) 0.7839 2.39082 0.54

Pattern List: (Bookmark 4)

Visible Ref. Code Score Compound Displacemen Scale Factor Chemical

Document History: (Bookmark 5)

- Modification time = "2/21/2015 7:19:58 PM"

Interpolate Step Size:

Search & Match:

- Threshold factor = "3"

Rietveld Refinement Finished:

- Title = "Zero shift"

Rietveld Refinement Finished:

Edit Carbon Size Strain Analysis:

- No. additional parameters = "3"

Rietveld Refinement Finished:

Edit Iron - Alpha Size Strain Analysis:

- Min. Shift/ESD = "0.1"

Rietveld Refinement Finished:

Edit Chromium Size Strain Analysis:

Rietveld Refinement Finished:

Edit Manganese Size Strain Analysis:

Edit Manganese Size Strain Analysis:

- No. of parameters = "2"

Rietveld Refinement Finished:

Edit Nickel Size Strain Analysis:

Edit Nickel Size Strain Analysis:

- Title = "U, V (Halfwidth)"

Rietveld Refinement Finished:

Edit Silicon - Vi Size Strain Analysis:

Edit Silicon - Vi Size Strain Analysis:

Rietveld Refinement Finished:

Edit Nickel Size Strain Analysis:

- Refine spec. displ. = "False"

Rietveld Refinement Finished:

Edit Chromium Size Strain Analysis:

- Min. Shift/ESD = "0.1"

Rietveld Refinement Finished:

Edit Chromium Size Strain Analysis:

Rietveld Refinement Finished:

Edit Iron - Alpha Size Strain Analysis:

- Refine spec. displ. = "False"

Rietveld Refinement Finished:

Edit Iron - Alpha Size Strain Analysis:

- Min. Shift/ESD = "0.8"

Rietveld Refinement Finished:

- Title = "U, V (Halfwidth)"

Rietveld Refinement Finished:

Edit Carbon Size Strain Analysis:

Edit Carbon Size Strain Analysis:

Rietveld Refinement Finished:

Edit Manganese Size Strain Analysis:

- Refine spec. displ. = "False"

Rietveld Refinement Finished:

Edit Manganese Size Strain Analysis:

Edit Chromium Size Strain Analysis:

- Min. Shift/ESD = "0.1"

Rietveld Refinement Finished:

More items… (Bookmark 6)

More items… (Bookmark 7)