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Keithley Model 261 Picoampere Source Instruction Manual PDF
Keithley Model 261 Picoampere Source Instruction Manual PDF
Picoampe:reSource
Instruction Manual
Keithley Instruments, Inc. warrants the following items for 90 days from the date of shipment: probes, cables. rechargeable batteries,
diskettes. and documentation.
During the warranty period, we will, at our option, either repair or replace any product that proves to bc defective.
To exercise this warranty, write or call your local Keithley representative, or contact Keithley headquarters in Cleveland, Ohio. You will
be given prompt assistance and return instructions. Send the product, transportation prepaid, to the indicated service facility. Repairs
will be made and the product returned, transportation prepaid. Repaired or replaced products are warranted for the balance of the origi-
nal warranty period, or at least 90 days.
LIMITATION OF WARRANTY
This warranty does not apply to delccts resulting from product modification without Keithley’s express written consent, or misuse of
any product or part. This warranty also does not apply to fuses, software, non-rechargeable batteries, damage from battery leakage, or
problems arising from normal wear or failure to follow instructions.
THIS WARRANTY IS IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING ANY IMPLIED
WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE. THE? REMEDIES PROVIDED HEREIN ARE
BUYER’S SOLE AND EXCLUSIVE REMEDIES.
NEITHER KEITHLEY INSTRUMENTS, INC. NOR ANY OF ITS EMPLOYEES SHALL BE LIABLE FOR ANY DIRECT, INDI-
RECT, SPECIAL, INCIDENTAL OR CONSEQUENTIAL DAMAGES ARISING OUT OF THE USE OF ITS INSTRUMENTS AND
SOFTWARE EVEN IF KEITHLEY INSTRUMENTS, INC., HAS BEEN ADVISED IN ADVANCE OF THE POSSIBILITY OF
SUCH DAMAGES. SUCH EXCLUDED DAMAGES SHALL INCLUDE, BUT ARE NOT LIMITED TO: COSTS OF REMOVAL
AND INSTALLATION, LOSSES SUSTAINED AS THE RESULT OF INJURY TO ANY PERSON, OR DAMAGE TO PROPERTY.
Keithley Instruments, Inc. * 28775 Aurora Road * Cleveland, OH 44139 * 216-248-0400 -Fax: 216-248-6168 * http:llwww.kcithley.com
Model 261 Picoampere Source
Instruction Manual
OUTPUT: lPl4A (10-1lA full range) to 1.1 x 10-4A, positive or negative, in eight decade
ranges.
AC&RACY: Exclusive of input drop consideration:
ACCURACY WITH WORST-CASE
10.00 SET-I-ING WITH SETTING
RANGE UOV SOURCE OTHER THAN
SETTING SPAN, AMPERE VOLTAGE) 10.00*
10-7 to KY5 10-7 to 1.1 x lrv4 iO.25% f0.25%
lti 10-s to1cF7 ?a.5 % M.5 %
1w9 10-9 to10-8 MO.6 % ffl.8 %
w-10 lo-l0 to 10-9 fo.6 % il.1 %
lo-11 l&11 to lo-10 ti.6 % a.3 %
lo-12 lo-12 to lo-11 M.7 % il.6 %
lo-12 lo-14 to 10-12 - 32.0 %
‘All accuracies are f the percentage given, a.01 x range switch setting.
LONG-TERM STABILITY: Will operate within stated specifications for three months after
calibration. After three months add 0.15% per month to 10-g through 10-12A range setting
accuracy specifications.
TEMPERATURE COEFFICIENT: ffl.l%/“C from 15°C to 30°C on 10-7 to 10-5A range settings.
Approximately O.l5%/“C on lo-12 to 10-gA range settings. Exact values for these ranges
supplied with instrument.
WARM-UP TIME: 1 hour.
LINE REGULATION: 0.01% for 10% change in line voltage.
SOURCE VOLTAGE: 0 to 11V in O.OlV’steps.
RESOLUTION: 3 significant figures from lO-12A to 1.1 x 10-4A.
RANGE RESISTORS: 105 to 10120 in decade steps; *5%.
RANGE RESISTOR ACCURACY: Value with power on, given on certificate.
~5 %:108 to 101252
lt0.1 %:107 to 106 n
~0.02%:105~.
OUTPUT ISOLATION: Low to ground: >109n shunted by O.OOl@
CERTIFICATION: A Calibration Certificate is furnished including range resistor values,
thermal coefficients, temperature and date of calibration. Certification traceable to the
National Institute of Standards and Technology is also available.
POWER: 10%125V or 210-250V (switch selected), 50-6QHz,6W.
DIMENSIONS, WEIGHT: 155mm high x 225mm wide x 300mm deep (6.25 in. x 9 in. x 12 in.).
Net weight 4.lkg (9 lbs.).
ACCESSORY SUPPLIED: Model 2611 Test Cable.
TABLE OF CONTENTS
Paragraph Title Page
LIST OF FIGURES
Figure Title Page
LIST OF TABLES
ii
SECTION 1
GENERAL INFORMATION
The Model 261 Picoampere Source is a secondary standard Changes pertaining to the instrument that occur after the
for use in calibrating picoammeters and electrometers. The printing of this manual will be found in an addendum included
output of the Model 261 can be adjusted between 10-‘4A and with this manual. Be sure to note any changes before attemp-
1.1 x 10.4A in eight decade ranges. The source has 3 digit ting to operate or service the instrument.
resolution for current outputs b#etween 10~12and 10~4A.
1.5 SAFETY TERMS
The current output of the Mlodel 261 is derived from a
variable voltage source and a selectable range resistance. The The WARNING heading used in this manual explains
voltage supply is highly ragulatled for stability and uses high- dangers that could result in personal injury or death.
quality components throughoul for reliability. The low side of The CAUTION heading used in this manual explains hazards
the output can be floated to avoid possible ground loop pro- that could damage the instrument.
blems.
1.6 UNPACKING AND INSPECTION
1.2 MODEL 261 FEATURES
The Model 261 was carefully inspected before shipment.
Important Model 261 features iixlude: Upon receiving the unit, carefully unpack all items from the
shipping canon and check for any damage that might have
1. 11V Internal Source. The internal voltage source can be set occurred during transit. Report any damage to the shipping
to a value between 0 and 1’lV in O.OlV increments. This agent at once. Save the original packing material in case
permits accurate calibration of picoammeters and elec- reshipment becomes necessary. Contact the nearest Keithley
trometers with input voltagt! drops up to 1OmV without representative or the factory if the unit fails to function pro-
calibration correction. perly.
2. Stable High-Meg Resistance Standards. The high-
megohm resistance standards are selected for maximum The following items are included in every Model 261 ship-
stability. Individual temperature coefficients and resistance ment:
values are supplied with each instrument. 1. Model 261 Picoampere Source
3. Line Operation. The Model 261 is line operated from either 2. Model 261 Instruction Manual
105.125V or 210.250V power sources. Voltage selection is 3. Model 2611 Test Lead Cable
easily accomplished with the rear panel line voltage selec- 4. Additional accessories as ordered.
tion switch.
4. Eight Current Ranges. Eight current ranges are user select- 1.7 USING THE MODEL 261 INSTRUCTION MANUAL
able with a single front panel control.
5. Shielded Output Connector. The UHF output connector This manual is intended to familiarize the operator with the
on the front panel is Teflon@ insulated to minimize possi- operating controls and features of the Model 261 Picoampere
ble leakage problems. Source. Also included is information on calibration,
6. Floating Low Connection. The low side of the output con- maintenance and spare parts. The manual is divided into the
nection can be floated to miinimize the effects of ground following sections:
IOOPS. 1. Sections 2 and 3 contains pertinent operating information,
including applications and possible pitfalls to avoid when
1.3 WARRANTY INFORMATION using the source.
2. Section 4 covers performance verification and calibration
Warranty information may be found inside the front cover of procedures.
this manual. If warranty service is required, contact the 3. A complete description of operating theory is contained in
Keithley representative in your area or the factory to deter- Section 5.
mine the correct course of action. Keithley Instruments, Inc., 4. Troubleshooting and maintenance procedures are covered
maintains service facilities in the United States, West Ger- in Section 6.
many, Great Britain, the Netherlands, Switzerland and 5. Parts ordering information can be found in Section 7.
Austria. Information concerning the application, operation,
or setvice of your instrument may be directed to the applica- 1.8 SPECIFICATIONS
tions engineer at any of these locations. Addresses can be
found inside the front cover of this manual. A complete list of Model 261 specifications can be found im-
mediately preceding this section.
1-l
1.9 OPTIONAL ACCESSORIES by 19 inches deep. Two different covers are provided for use
with either 10 inch deep or 13 inch deep instruments. Contact
The Model 4003A Rack Mounting Kit allows the Model 261 your nearest Keithley representative or the factory for infor-
to be conveniently mounted in a standard 19 inch rack. The mation on ordering the Model 4003A.
overall dimensions of the Model 4003A kit is 5% inches high
1-2
SECTION 2
OPERATION
2.1 INTRODUCTION Voltage Switch. The voltage switch sets the source for
105.125V or 210.250V operation. A screwdriver can be used
This section contains information necessary to set up the to set the switch to the desired position.
Model 261 and operate the unit. Also included are compen-
sating equations necessary when using the source with FUSE. By unscrewing the fuse holder cap, the fuse is ac-
measuring instruments with higlh input voltage drops. cessable. See Section 6 for fuse replacement procedures.
2.2 FRONT PANEL CONTROLS AND TERMINALS Power Cord. The 3wire cord is permanently attached to the
rear panel. The opposite end of the power cord has a stan-
Figure 2-l shows the front panel of the Model 261, The func- dard 3-prong plug attached. This plug should be used only
tions of the various controls and terminals are described with grounded outlets.
below.
COM end GND terminals. The COM terminal is connected
POLARITY Switch. The POLARITY switch has four posi- to the low side of the source output. The GND terminal is
tions which are used to control power, turn the instrument connected to chassis ground, which is connected to the
output off and on, and set the polarity of the source output. power line ground wire in the 3.wire power cord. Normally,
In the AC OFF position, the IModel 261 power is discon- the GND and COM terminals are connected together with a
nected. In the OFF position, power is applied to the instru- shorting link, which is provided. The link can be removed to
ment, but the source is disconnected from the output jack. float the low side from ground.
When the POLARITY switch iri in this position, the output
resistance of the source is equal to the reciprocal of the 2.4 PREPARATION FOR USE
AMPERES switch setting, regwlless of the multiplier settings
in use. The + and - positions s,elect positive or negative cur- Before operating the Model 261, perform the following steps:
rent output values. 1. Set the line voltage selection switch to the appropriate set-
ting depending on the local power line voltage. Check to
Range (AMPERES) Switch. The range switch selects one see that the appropriate fuse is installed.
of eight decade current ranges between 10~5and 10.‘*A. The
actual output is affected by the positions of the three multi- CAUTION
plier switches. When the multiplier switches are in the 1 .OO Operating the source on en incorrect line
positions, the range switch indicates the actual output cur- voltage may damage the unit. possibly
rent. voiding the warranty.
Multiplier Switches. The mull:iplier switches control the in- 2. Sat the Model 261 front panel controls as follows:
ternal voltage source of the instrument. These switches pro- POLARITY Switch: AC OFF
vide multiplying values that determine the actual output of Range Switch: Desired current range
the source. To determine the current output, multiply the Multiplier Switches: 10.00
current range by the multiplier s,etting. The multiplier switch- 3. Plug in the source to AC power and rotate the POLARITY
es control the output through the use of a 3-decade Kelvin- switch to the OFF position. The decimal point pilot light
Varley divider. The Xl and X.01 switches each have 11 posi- should come on, indicating the unit is receiving power. If
tions between 0 and 10; the X:1 switch has 10 positions be- not, disconnect the instrument from the power line and
tween 0 and 9. The illuminated decimal point between Xl and check to see that the fuse is good.
X.1 switches also serves as a pilot lamp.
2.5 BASIC OPERATING PROCEDURE
OUTPUT Receptacle. The OUTPUT receptacle is a
Teflon@ insulated UHF type connector. The low (threaded) Operation of the Model 261 is fairly straight forward. Once
side floats from ground unless the COM and GND terminals the unit is connected to the measuring instrument, the
on the rear panel are connected together. A chassis ground operator need only select the appropriate range and multiplier
terminal (GI is located next to the OUTPUT connector. switch settings and select the output current polarity. The
basic operating procedure is as follows:
2.3 REAR PANEL CONTROLS AND TERMINALS 1. Plug in the instrument to the appropriate power source and
rotate the POLARITY switch to the OFF position. The pilot
Figure 2-2 shows the rear panel of the source. The purpose of light should indicate that power is applied to the source.
the various controls and terminals is described below. Allow a one hour warm-up period for rated accuracy.
2-1
Figure 2-l. Front Panel Controls and Terminals
0 0
-- III
-- III-
-- ---
-II III
0 6
0 0
GROUND
AND
COMMON TERMINALS
VOLTAGE SWTCH FVSE LINE CORD
2-2
2. Connect the source to the measuring instrument as shown 2.6 ACCURACY CONSIDERATIONS
in Figure 2-3. Use the suppli’sd Model 2611 cable to make
the necessary connections. The range switch setting times the multiplier switch sening
3. Select the desired range and multiplier settings according gives the Model 261 current output. The accuracy of the out-
to the required output current. Some examples are shown put, however, depends upon several factors.
in Table 2-l. Note that accuracy figures are given with the
multiplier settings at 10.00. Output connections from the source to the picoammeter are
4. Place the POLARITY switc:h in the + or - position, very important, especially for the lower ranges. The accuracy
depending on the desired output polarity. of the current at the Model 261 OUTPUT receptacle will
mean little if poor or improper hookups are made from the
This procedure covers the basic steps for using the Model source to the picoammeter.
261; however, some precautiorls may be necessary to ensure
rated accuracy, as described irl the following paragraphs. 2.6.1 Input Voltage Drop (Voltage Burden)
Table 2-l. Current Output Examples For specified output accuracy, the voltage drop of the
measuring instrument must be less than l/1000 of the inter-
Desired Current Rang8 a I lklultiplier nal source voltage of the Model 261. The internal source
voltage in volts is read directly from the multiplier switch set-
60uA 10-E 6.00
tings, regardless of the range switch setting. The voltage
21 .ipA 10-l’ 2.17
drop of the picoammeter is a characteristic of that instru-
89.5nA 104 8.95
ment; it can be found in its instruction manual or it must be
lOO/J.A 10~5 10.0
calculated.
1.35pA 10~12 1.35
250nA 10-7 2.50
For picoammeter with a 1mV or less voltage drop, set the
7.5”A 1o-9 7.50
Model 261 multiplier switches to 1 .OO. For a voltage drop be-
455pA 10~10 4.55
tween 10 and lmV, set the multiplier switches to 10.00 and
3.66!.LA 10~6I 3.66
set the range switch one decade lower. This sening does not
affect the Model 261 accuracy for outputs greater than l@*A.
Note that even for a voltage drop l/100 of the source
voltage, an error of only 1% is added to the specified accur-
acy.
2.6.2 Proper Multiplier Settings
MooEL Z61~l CABLE When the Model 261 is used on the 10~s to 10~12ranges at
other than the calibrated temperature (stated on the calibra-
tion certificate furnished with the source1 a discrepancy in the
output current will occur. On other ranges the effect is not
significant.
I-Q
meters having fast response speeds. Tie down cables to
INPUT avoid vibrations. Cable movements cause meter jiner on the
10.sA and lower ranges due to capacitance changes.
I For currants 10.sA and less, carefully shield the output con-
MEASURING INSTRUMENT nections and the input connections of the picoammeter.
Unless the shielding is thorough, any changes in the elec-
trostatic field near the input circuitry will cause definite distur-
Figure 2-3. Connecting thle Model 261 Source bances on the measuring instrument.
2-3
Use high resistance, low-loss materials (such as Teflon@ The general magnitude of the voltage drop is dependent
(recommended), polyethylene or polystyrene) for insulation. upon the type of circuit the picoammeter uses. Feedback
The insulation leakage resistance of test fixtures and leads types have a low input voltage drop of approximately 1mV or
should be several orders of magnitude higher than the inter- less. Shunt types generally have a relatively large input
nal resistance of the source. If it is not, leakage losses will voltage drop (about 1OmV or more). However, some low-
cause lower readings. Coaxial cables used should be a low- current shunt-type ammeters can be calibrated as if they
noise type which employ a graphite or other conductive were the feedback type. To help determine the type of
coating between the dielectric and the surrounding shield picoammeter under calibration, a brief description of the cir-
braid. cuits follows.
I RF
I
The output current accuracy is specified under the assump- Figure 2-5. Simplified Circuit of Feed-Back Type
tion that the picoammeter input voltage drop is less than Picoammeter
l/1000 of the Model 261 source voltage. Most feedback elec-
trometers will easily meet this condition. Any error caused by 2.8.2 Shunt-Type Picoammeter
the picoammeter voltage drop may be eliminated by calcula-
tion if the voltage drop is known. However, only a 1% error is This type consists of a voltmeter, V, calibrated in amperes.
added if the voltage drop is 1 I100 of the source voltage. which responds to the IR drop across a shunt resistor, R,.
Refer to Figure 2-6. The voltmeter can be one of two kinds:
2-4
A high impedance voltmeter, such es an electrometer, which where E”, is the percent of error due to the picoammeter in-
has an extremely high input impedance, Zi; or a low im- put voltage drop;
pedance voltmeter. Vi is the picoammeter input voltage drop in volts;
V, is the Model 261 source voltage, read directly in volts
High Impedance Voltmeter-The input voltage drop, liR,, of e from the multiplier switch settings.
picoammeter using a high-impedance voltmeter is usually
1mV or more, due to voltmeter sensitivity limitations. Rise When the input resistance is known:
time is usually slow, possibly several minutes for very low cur-
rent levels. Typical values are:
Equation 4
Input current to picoammetelr, Ii = 10.‘ZA
Picoammeter shunt resistor, R,= 10’92
Voltmeter input impedance, ;Z,= 10’4fl where Ri is the picoammeter input resistance in ohms:
Input voltage drop, Vi= 10mV Rs is the Model 261 source resistance, which is the
reciprocal of the range switch sening.
Low Impedance Voltmeter-The circuit of a shunt-type pico-
ammeter using a low-impedance voltmeter is essentially the 2.9.2 Compensating Equation
same as Figure 2-6, except a more sensitive but lower input
impedance voltmeter is used. A lower input voltage drop If the voltage drop is known, the actual Model 261 output
results, but response speed and maximum current sensitivity current can be calculated. Equation 5 gives the output current
are usually less. The voltage drop is liR,. Typical values are: value if the input voltage drop is the only significant source of
Input current to picoammeter, Ii = 10.‘DA error.
Picoammeter shunt resistance, R,= 106fl
Voltmeter input impedance, ;Z, =9x 1070 la = I&V, Vi) Equation 5
Input voltage drop, Vi = lOO@V
where Ia is the actual output current from the Model 261;
Is is the range switch setting (reciprocal of range resistor
valuel;
Vs is the Model 261 source voltage, read directly in volts
from the multiplier switch settings;
Vi is the picoammeter input voltage drop in volts.
2-6
X10.2 Compensating Equations Using equation 8 completely compensates for the error due
to the input voltage drop.
Since the picoammeter voltage drop can be found, the Model
261 output current can be corrected. Equation 6 gives the 2.11 COMPENSATION FOR INPUT VOLTAGE DROP OF
output current value if the input voltage drop is the only SHUNT-TYPE LOW-IMPEDANCE PICOAM-
significant source of error and if the voltage drop is less than METERS
l/l0 the source voltage.
For the most part, the voltage drop for this type picoammeter
la = I,(V, - vi1 Equation 6 is about the equivalent of that of the feedback-type
picoammeter-about 1mV or less. Following the directions in
where I8 is the actual output current from the Model 261; paragraph 2.6 will ensure that Model 261 output currents are
Is is the range switch setting (reciprocal of range resistor within the specified accuracy.
value);
V, is the Model 261 source voltage, read directly in volts To compensate for output current difference caused by input
from the multiplier switch setting; voltage drops, use equation 8. This calculation will be
Vi is the picoammeter input voltage drop in volts. precise, since the voltage drop is read directly from the
picoammeter.
Using this correction, accuracy is nominally f0.5% (Model
261 accuracy). This error results from the factory calibration 2.12 RANGE RESISTOR VOLTAGE COEFFICIENT
method used for the Model 261 that adjusts the source volt-
age from that indicated to match the range resistor used. Ordinarily, the voltage coefficient of high-megohm resistors
can lead to significant errors. However, the range resistors
For greater accuracy, or if the input drop is more than 0.1 used in the Model 261 have an extremely low voltage coeffi-
times the source voltage, use equation 8 to compensate for cient of only 5ppmlV. This low value results in a worst-case
the error. The following equation is based on the calibration current change due to voltage coefficient of only 0.0055%
procedures. with the multiplier switches set for 1lV. Thus. the output
discrepancy because of voltage coefficient is one or two
v,, = v,IR,I)= V,R,,l, Equation 7 orders of magnitude smaller than other sources of error, and
l/Is car? be ignored for all practical purposes.
where V,, is the actual source voltage; 2.13 COMPENSATION FOR TEMPERATURE COEFFI-
V, is the Model 261 source voltage, read directly in volts CIENT
from the multiplier switch setting;
I?,, is the actual source resistance from the calibration cer- When the Model 261 is used for range switch settings above
tificate supplied with the Model 261; 10~sor when the unit is operated at the temperature indicated
Is is the Model 261 range switch setting (reciprocal of range on the calibration certificate, no significant errors will occur in
resistor value). the output. However, for range switch settings between
l@sA and lUJ2A. the change in range resistance because of
Using equation 7 in equation 6 and substituting V,, for V,, temperature coefficient can affect the output considerably.
Ia= I,lI,V,R,, -vi1 Equation 8 The Model 261 is calibrated at a specified temperature
f0.5”C. which is stated on the calibration certificate, for the
where Ia is the actual output current from the Model 261; various ranges. The certificate also lists the temperature coef-
Vi is the picoammeter input voltage drop in volts read from ficients by range.
the meter.
Table 2-2. Causes of Discrepancy in Model 261 Output Current and Correction Index
Equation to Compensate
cause of Discrepancy in Output Current for Discrepancy
Picoammeter input voltage drop more than 5
6 or 8
all I 2.11 8
Low-Impedance
Model 261 ambient temperature differs from all 10~8to 10-14 2.13 9
that stated in Calibration Certificate
2-6
Compensating Equation-The effect of temperature dif- where la is the actual or compensated Model 261 current out-
ferences on the Model 261 current can be calculated using put;
equation 9. This gives the output current value if the Is is the indicated current output (range switch setting
temperature effect is the only silgnificant source of error. tlmes the multiplier switch settings);
T2 is the room temperature in OC;
I (l+(T,-T,)x.Olxtg Equation9 T, is the calibration temperature in “C;
la=l~*~s[ tc is the temperature coefficient of the range resistor in
%/OC given on the calibration certificate.
100
2-712-a
SECTION 3
APPLICATIONS
3.1 INTRODUCTION to determine any circuit limitations. Always set the picoam-
meter for the best possible sensitivity
The Model 261 was designed to serve as a secondary source 61OC
in calibrating picoammeters an’d electrometers. While this is NULL DETECTOR
the primary purpose of the unit, it can also be used for
various other applications, irxzluding current suppression,
galvanometric measurements, and ohmmeter calibration.
This section briefly covers the methods for each of these ap-
plications; these examples by no means exhausts the possibi-
lities of using the Model 261. I
UNKNOWN MODEL 261
3.2 CURRENT SUPPRESSION CURRENT CURRENT SOURCE
Figure 3-1. Current Suppression Circuit Connections
The Model 261 can be used to suppress steady background
currents so that a picoammeter or electrometer can measure 3.3 GALVANOMETRIC MEASUREMENTS
small variations in signal. For example, the Model 261 can be
used to cancel phototube dark currents while the picoam- In practice, using the Model 261 for galvanometric measure-
meter measures small variations in the normal output of the ments is very similar to the current suppression procedures
phototube. discussed in the previous paragraph. In this application, the
Model 261 bucks out an unknown current, while a measuring
The basic circuit for current suppression is shown in Figure instrument, such as the Keithley Model 614, serves as a null
3.1, Because of its popularity, the Keithley Model 610C is detector.
used as the current measuring device. Other instruments with
similar characteristics will serve equally well in this applica- The basic circuit for galvanometeric measurements is shown
tion. Using the Models 261 and 6lOC, suppression up to 1000 in Figure 3-2. Iu is the unknown current; V, is the Model 261
times full scale is possible. Suppression up to at least 100 source voltage and Rs is the source resistance. Is is the
times full scale is possible with most picoammeters. source current, while IM is any residual current seen by the in-
strument. R, is the picoammeter feedback resistor; k, the
The basic procedure for current suppression is as follows: amplifier gain; R, the multiplier resistance.
I. Connect the Models 261 and 610C to the unknown currant
as shown in Figure 3-l; use the Model 2611 test cable or Follow the same basic procedure for this measurement as
other similar coaxial cable. described in the last paragraph. Once maximum nulling is
2. Set the Model 261 to the desired current as described in achieved, the unknown currant value can be determined by
Section 2. Set the output polarity of the source opposite to adding the Model 261 source output value to any residual
that of the unknown currem. Also set the source output value shown on the measuring instrument.
value as close as possible to the unknown current.
3. Set the Model 610C FEEDBACK switch to FAST. In this
mode, the Model 610C acts as a feedback tvpe picoam-
mater.
t Iu
4. Set the Model 61OC to the least sensitive current range.
Varv the Model 261 source outout until a null is reached.
5. Grabually increase the Model SiOC sensitivity, nulling the
current with the Model 261 c1zmtroIs in each case. Keep the
Model 610C multiplier switch on 1.
6. Set both the Models 261 and 610C range switches to the
1
same setting. If the electrometer is set to a lower range,
the Model 261 source resistance will divide the Model 610C
feedback current, impairing its zero stability.
7. Switch the electrometer multiplier setting gradually from 1
to 0.001. In the lowest sening, the Model 610C current
I J
sensitivity is 1000 times the ‘unknown current.
hi 1. RF -L
The basic procedure for using this method with other instru- -
ments is the same. Check the picoammeter’s specifications Figure 3-2. Galvanometric Measurements
3-1
3.4 OHMMETER CALIBRATION WARNING
Disconnect the instrument from the power
The Modal 261 contains calibrated resistance standards, line before removing the top cover. Failure
which make it useful for checking high resistance measuring to observe this precaution may result in
instruments. The front panel AMPERES switch setting indi- personal injury or death due to electric
cates the reciprocal of the internal source resistance. For ex- shock.
ample, the source resistance will be 1MR if the AMPERES
switch is in the 10-s position. The exact resistance for any Remove the link between the GND and COM terminals on
position of the AMPERES switch can be found listed on the the rear panel of the sourca. The outer shell of the OUT-
supplied calibration certificate. PUT jack is the guard terminal, while the G binding post
next to it is connected to the low side of the ohmmeter.
The basic procedure for ohmmeter calibration is as follows: 6. Observe the ohmmeter reading and compare it to the ap-
1. Set the POLARITY switch to the OFF (not AC OFF1 posi- propriate value listed on the calibration certificate. Range
tion. resistor values will be within the stated tolerance for up to
2. Set the AMPERES switch to the reciprocal of the desired three months after factory calibration.
resistance. MODEL 261
3. Connect the ohmmeter to the Model 261 OUTPUT con-
nector using an appropriate coaxial cable. See Section 2
for precautions to be taken when making connections.
4. Carefully shield connections when making measurements
greater than 1OW. Use guarded connections for
measurements of 1OW and more, as shown in Figure 3.3. zx&.?&:.-..
Guarded connections are necessary in such cases to
minimize the shunting effects of cable and connector
leakage resistance. For example, using the 1O’Q range, a
10W leakage resistance will add an error of 1%. To make Figure 3-3. Guarded Circuit For Ohmmeter Calibration
the proper connections within the unit, place the CAL-
OPERATE switch in the CAL position (see Section 4).
3-2
SECTION 4
PERFORMANCE VERIFICATION AND CALIBRATION
4.1 INTRODUCTION one hour to stabilize an instrument that is 10°C 116’-‘F) out-
side the allotted range.
This section contains information necessary to verify that 2. Turn on the power to the Model 261 and allow it to warm
Model 261 performance is within specified accuracy and to up for at least one hour before beginning verification or cal-
calibrate the instrument. Moclel 261 specifications may be ibration procedures.
found at the front of this manual. Ideally, performance varifi-
cation should be performed when the unit is first received to 4.5 VERIFICATION PROCEDURE
make sure that no damage or change in calibration has
occurred during shipment. The verification procedure may Model 261 operation is based on connecting an accurate,
also be performed if accuracy !is suspect or following calibra- known resistor in series with a stable, accurate voltage
tion. If instrument performamx is substandard, calibration source. The resulting current is easily predicted with Ohm’s
may be performed as described et the end of this section. law. This same principle can be used to verify Model 261 par-
formance; if both the resistance and voltage are within speci-
NOlTE fications, it can be assumed that the output current is accu-
If the instrument does not meet specifications, rate as well.
and less than three months have passed since
the date of shipment, contact your Keith& 4.5.1 Top Cover Removal
representative or the factov to determine the
action to be taken. The procedure in this section require that the top cover be
removed to allow access to test points and the CAL-
4.2 ENVIRONMENTAL COhlDlTlONS OPERATE switch. To remove the top cover. proceed as
follows:
All measurements should be made at an ambient temperature
between lB°C and 26°C 165O 11082°F) with a relative humidi- WARNING
ty less than 80%. Disconnect the Model 261 from the power
line and other instrumentation before
4.3 RECOMMENDED TEST EQUIPMENT removing the top cover.
Recommended test equipmenlt for Model 261 performance 1. Remove the four screws securing the top cover to the
verification and calibration is listed in Table 4-l. Different chassis.
equipment may be used as long as the accuracy specifica- 2. Grasp the top cover by the handle, and gently pull the
tions are at least four times better than Model 261 specifica- cover up and back until it clears the chassis.
tions. If less accurate equipment is used, additional 3. To replace the cover, reverse the above procedure.
allowances must be made for test equipment inaccuracy.
4.5.2 Range Resistor Verification
4.4 INITIAL CONDITIONS
The following procedure outlines a method which can be
Before performing the following procedures, make sure the used in the field to measure the actual value of the high
Model 261 meets the followin!> conditions: megohm range rasistors. The inherent drift of these resistors
1. If the unit has been subjected to temperatures below lB°C sets the 3-month accuracy limit of the Model 261. Note that
(65°F) or above 26°C (62°F). allow sufficient time for it to resistor verification is also necessary to complete calibration.
reach a temperature within this range. Generally, it takes
Measuring System
Measurement of l&s through 10-12 range resistors.
Measurement of Power Supply. Kelvin-Varley Voltage Divider
4-1
Table 4-2. Range Resistor Verification
NOTE
This last step must be performed to return the
unit to the stated specifications.
4.6 CALIBRATION
Multipli
Switch
Settin,g
Range
Switch
Setting Adjustment
I 10 x R Volts
Wl= Range Resistor)
I
Tolerance
lO.OC 106 R113 R = 10-C Range Resistor * 5mV
10.00 107 R114 R = 1W Range Resistor * 5mV
10.00 108 R115 R = 1W Range Resistor * 5mV
lO.OCl 109 R116 R = l&9 Range Resistor * 5mV
10.00 10’0 R117 R = l&lo Range Resistor * 5mV
10.00 10” R118 R = l@” Range Resistor * 5mV
10.00 10’2 RllS R = 10-12 Range Resistor * 5mV
4-3144
SECTION 5
THEORY OF OPERATION
5-l
The range switch, OUTPUT jack, and the range resistors are resistors, which are mounted on the multiplier switches 5103,
encased in a floating shield which is normally connected to S104, and S105. These resistors (R120 through R1521 are
the low side of the output. The shield is connected as a guard used to divide the 1lVDC supplied by the voltage supply
when the calibration switch SlOl, is in the CAL position. down to the selected voltage between 0 and 11V in 0.01 in-
crements. The voltage is selected with the three multiplier
5.3.3 Kelvin-Varley Voltage Divider switches, S103 through S105.
5-2
SECTION 6
MAINTENANCE
6.1 INTRODUCTION The range resistors are specially selected and aged 10 ensure
rate accuracy for three months after calibration. Normally,
This section contains maintenance and troubleshooting pro- these resistors do not need replacement. If replacements are
cedures for the Model 261 Picoammeter Source. It is recom- necessary. order them from Keithley Instruments, Inc. In an
mended that these procedures be followed as closely as emergency, these parts can be ordered from another source,
possible to maintain the accuracy of the instrument. but their accuracy or stability cannot be guaranteed. This
could seriously affect the accuracy of the source on one or
6.2 SERVICING SCHEDULE more ranges. In any case, recalibration will be necessary if
one of the range resistors is replaced.
The Model 261 requires no periodic maintenance beyond the
normal care required of high-#quality elecfronic equipment. CAUTION
Normally. no part should need replacement except the fuse. Do not touch the body of the range rasis-
tars at any time. Contamination of the
Ideally, the high-megohm range resistors should be checked special insulating material may cause
every three months to ensure instrument accuracy. Refer to leakage, affecting the accuracy of the
Section 4 for procedures to be used. The source may also be source output. The 10’2 resistor assembly
calibrated if accuracy is suspect Use the procedures outlined on S102 is not field installable; the instru-
in Section 4 when calibrating the unit. Alternately. the Model ment must be returned to the factory for
261 may be returned to Keithley Instruments. Inc. for calibra- repair and calibration if this assembly must
tion. be replaced. Do not use any spray-on clean-
ing material on the S102 assembly.
6.3 TOP COVER REMOVAL
6.5 TROUBLESHOOTING
Maintenance or troubleshooting of the unit will require that
the top cover be removed. The following procedures include instructions for repairing
troubles which may occur in the Model 261. Use the pro-
WARNING cedures outlined and only specified replacement parts. Com-
These instructions ara intended for qual- ponrnts can be identified with the help of the schematic and
ified servicing persalnnel only. Do not component layout drawings at the end of Section 7. In addi-
remove the top cover unless qualified to do tion, Section 7 contains several drawings pertaining to
so. Also, disconnect the Model 261 from resistor locations.
the power line and other instruments
before removing the top cover. Failure to If the trouble cannot be located, the instrument may be
observe these precautions may result in returned to Keithley Instruments, Inc. for repair services.
serious personal injury or death because of Contact your nearest Keithley representative or the factorv
the possibility of electric shock. for information.
To remove the top cover, use the following procedures: 6.5.1 Troubleshooting Equipment
1. Disconnect the Model 261 from the power line.
2. Remove the screws securing the top cover to the chassis. The following equipment is recommended for use when
3. Grasp the handle on the top cover and carefully separate troubleshooting the Model 261: Keithley Model 179A or
the cover from the chassis. similar DC voltmeter with 0.04% basic DC accuracy and a
minimum input impedance of IOMR.
The cover can be installed by reversing this procedure. Be
sure to line up the holes in the (cover with those in the chassis 6.5.2 Common Faults
before replacing the screws.
Table 6-l lists the most common troubles that might affect
6.4 PARTS REPLACEMENT the Model 261. If the steps listed in the tatle do nor rectify the
problem, a step-by-step circuit analysis may be required. Use
Section 7 lists the replaceable parts available for the Model the operating theory covered in Section 5 for this purpose.
261. When replacing parts, lbe sure to use only reliable
replacements which meat orilginal specifications. Replace
parts only as necessary.
6-1
Table 6-l. Troubleshooting Guide
6-2
SECTION 7
REPLACEABLE PARTS
7.1 INTRODUCTION 1. Instrument Model Number
2. Instrument Serial Number
This section contains replacement parts information and a 3. Part Description
schematic diagram and component drawings for the Model 4. Circuit Designation (where applicable)
261. 5. Keithley Part Number
Table 7-1 lists the replaceable Iparts for the Model 261. Parts If the instrument is to be returned to the factor, for service,
are listed alphabetically accorcling to circuit designation. complete the service form which follows this section and
return it with the instrument.
7.3 ORDERING PARTS
7.5 SCHEMATIC DIAGRAM AND COMPONENT
To place an order for Model 26’1 parts or obtain parts informa- LAYOUTS
tion, contact your Keithley representative or the factory. See
the inside front cover of this manual for addresses. When Parts list, schematic diagram and component location draw-
ordering parts, include the following information: ings are shown on the following pages.
0 0
A202
D204
D201 0202, -j t- - I1
YLVL
-* -R204 Q203 T
f---+ II205
a201 I7209
- D206
R203 f----w
0
R207
D207
-I t-
c201 D208
JZOZ (3
3
0 c202
8
0204
7-1
I l-----J
Table 7.1. Model 261 Parts List
Circuit Keithley
Desig. Description Location Part No.
Cl01 Capacitor, .l@F. 50V. Mylar Chassis c-41-0.1
c201 Capacitor, 5OOpF. 25V. Aluminum Electrolytic Voltage Supply c-94500
c202 Capacitor, 5OOgF. 25V. Aluminum Electrolytic Voltage Supply c-94-500
c203 Capacitor, .22gF, 5OOV. Ceramic Disc Voltage Supply c-22-.01
C204 Capacitor, 5OOpF. 25V. Aluminum Electrolvtic Voltage Supply c-94500
D201 Rectifier. Silicon, 1 N645 Voltage Supply RF-14
D202 Rectifier, Silicon, 1 N645 Voltage Supply RF-14
D203 Rectifier. Silicon, 1 N645 Vclkage Supply RF~l4
D204 Diode, Zener, lN706 Voltage Supply DZ- 1
D205 Rectifit!r. Silicon, 1 N645 Voltage Supply RF-14
0206 Rectifi#?r. Silicon, lN645 Voltage Supply RF~l4
D207 Diode, Zener. 1 N823 Voltage Supply DZ-36
D208 Rectifier, Silicon, 1 N645 Voltage Supply RF-14
OS201 LED, Fled Front Panel PL-67
F201 Fuse, ‘l/8A, 250V. (105125V Operation) Rear Panel FU-20
F201 Fuse, ‘1/16A. 25OV. (21025OV Operation) Rear Panel FU-21
JlOl Bindin! Post, G Front Panel BP-15
J102 Binding Post. GND Rear Panel BP-1lG
J103 Binding Post, COM Rear Panel BP-11B
J104 Receptacle. UHF Front Panel cs-84
J201 Test Jsck Voltage Supply TJ-4
J202 Test Jsck Voltage Supply TJ-5
P201 Cord Set, 6 foot Rear Panel co-5
MO1 Transistor, PNP, Germanium, 2N1372 Voltage Supply TG-8
Dzo2 Transistor, PNP, Silicon, 40319 Voltage Supply TG~50
0203 Transistor. PNP. Germanium, 2N1372 Voltage Supply TG-8
a204 Transistor, PNP, Germanium, 2N1372 Voltage Supply TG-8
a205 Transistor. PNP, Germailium, 2N1372 Voltage Supply TG-8
RlOl Resistor, 100kR. .02%. 1/2W Wirewound 5102 R-47.100k
R102 Resistor. 1MlI 1%. %W, Carbon 5102 R-12.1M
R103 Resistor. 10MR. 1%. % W, Carboti s102 R-12.10M
R104 Resistor, 100Mn. 1% 5102 R-289.l00b
R105 Resistor, 1GO. 1% 5102 R-289.IG
R106 Resistor, IOGR, 2% s102 R~Z89-10G
R107 Resistor, 10OGQ 2% 5102 R-289-1 ooc
R108” Resistor, Assembly, 1TlI. 2% 5102 320428
R109 Resistor, 10Mn. 10%. %W. Composition 5102 R-I-IOM
RllO Resistor. 1.5MQ. 10%. % W. Composition s102 R-l-1.5M
Rlll Resistor, 150kR. 10%. ‘/W. Composition s102 R~1~150k
R113 Potentiometer, 200R. % W. 10% Calibration Board RP-104200
R114 Potentiometer, 2000. % W. 10% Calibration Board RP-104200
R115 Potentiometer. 2OOfl. KW. 10% Calibration Board RP-104200
R116 Potentiometer, 2OOfI. % W. 10% Calibration Board RP-104-200
R117 Potentiometer, ZOO? % W. 10% Calibration Board RP-104200
A118 Potentiometer, 200R. K W. 10% Calibration Board RP-104200
R119 Potentiometer, 2000. K W. 10% Calibration Board RP-104-200
R120 Resistor. 12.811. .l%. %W, Wirewound s103 R-67-12.8
R121 Resistw, 12.6Q ,196. %W. Wirewound s103 R-67-12.8
R122 Resistor. 12.60. .l%. %W, Wirewound s103 R-67-12.8
R123 Resistor, 12.60, .l%. % W, Wirewound 5103 R-67-12.8
R124 Resistor. 12.61). .l%. ‘/.W. Wirewound s103 R-67-12.8
R125 Resistor. 12.6R. .l %. % W, Wirewound s103 R-67-12.8
R126 Resistor. 12.8R. .l%, %W, Wirewound s103 R-67-12.8
R127 Resistor, 12.m. .l%, %W. Wirewound s103 R-67-12.8
R128 Resistor. 12.6R. .l%, %W. Wirewound 5103 R-67-12.8
R129 Resistor, 12.811. .l O%, ‘/W. Wirewound 5103 R-67-12.8
R130 Resistor, 12.m. .l%. ‘/W. Wirewound 5103 R-67-12.8
R131 Resistor, 12.6lI. .l%. ‘/W. Wirewound 5104 R-67-12.8
R132 Resistor, 12.8R. .l%. ‘/W. Wirewound 5104 R-67-12.8
R133 Resistor. 12.8R. .l%. ‘/W. Wirewound s104 R-67-12.8
R134 Resistor. 12.80, .l%. ‘/.W, Wirewound s104 R-67-12.8
R135 Resistor. 12.8R. .l %. )/I W, Wirewound s104 R-67-12.8
R136 Resistor, 12.8R. .l%. %W, Wirewound 5104 R-87-12.6
I108 is n eld installable.
7-3
Table 7-1. Model 261 Parts List (Cont.)
CiVXM Kelthley
Desig. Description Locatkm Part No.
RI37 Resistor, 12.8Q .I%. 1/4W, Wirewound s104 R-67-12.8
RI38 Resistor, 12.8Q .I%. 1/4W, Wirewound s104 R-67-12.8
I31 39 Resistor, 12.8Q, .l%, 1/4W, Wirewound s104 R-67-12.8
R140 Resistor, 12.8Q .l%. ll4W. Wirewound s104 R-67-12.8
Iv41 Resistor, 640, .I%, 1/4W, Wirewound s105 R-67-64
R142 Resistor, 64Q .l%, 1/4W. Wirewound s105 R-67-64
RI43 Resistor, 64Q .I%, 1/4W. Wirewound s105 R-67-64
R144 Resistor, 64Q .I%. 1/4W. Wirewound 5105 R-67-64
RI45 Resistor, 64R, .l%, 1/4W, Wirewound 5105 R-67-64
R146 Resistor, 64fL .I%. 1/4W, Wirewound s10.5 R-67-84
RI47 Resistor, 64G .l%. 1/4W, Wirewound s105 R-67-84
RI48 Resistor, 64R, .l%, 1/4W, Wirewound 5105 R-67-64
R149 Resistor, 64Q, .l%, 1/4W, Wirewound 5105 R-67-64
R150 Resistor, 64R. .l%, 1/4W, Wirewound 5105 R-67-64
RI51 Resistor, 84R, .I%, 1/4W, Wirewound s105 R-67-64
R152 Resistor, 64R, .l%, 1/4W, Wirewound 5105 R-67-64
R153 Resistor, 32R, .I%, 1/2W, Wirewound 5103 R-67-32
R154 Resistor, 1.8kR, 10%. 1/2W, Composition R-1.1.8k
T201 TR-78
7-4
To 101&I
Resistor
Assembly
LWOW
Keithley
Description - Part No.
t
Handle HH-18
Bottom Cover Assembly 17148C
Support Assembly Bail Left 192058
Support Bail Left 147038
Support Assembly Bail fqigh 192068
Support Bail Right 147058
Feet FE-5
Feet (Rubber Ball) FE-6
Bottom Panel 17149c
Front Panel/Chassis Asey. 185598
Cable Clamp cc-4
I
Shorting Link BP-6 Figure 74. 10’2R Resistor Assembly IR108)
Label MC-30
Range Switch Shield As,sy. 185368
Front Panel Assembly - 18464C
7-6
Figure 7-5. X.01 Multiplier Switch, S103
-
Figure 7-6. X.01 Multiplier Switch, 5104
1
il
==Y=
-
-
-
34 -
-
-
6 DECK
pl/
2
I0 - z , DECK,
7-6
1
Service Form
Model No. Serial No. Date
Name and Telephone No. _
Company
List all control settings, describe problem and check boxes that apply to problem.
Cl Intermittent cl Analog output follows display 0 Particular range or function bad; specify
Where is the measurement being performed7 (factory, controlled laboratory, out-of-doors, etc.)
Any additional information. (If special modifications have been made by the user, please describe.)