BE Chemical Syllabus PDF

The Maharaja Sayajirao University of Baroda
Faculty: Technology and Engineering

Department: Chemical Engineering
Kalabhavan, Vadodara.
Contact Details :
Email ID: head-chemengg@msubaroda.ac.in
Name of the Program: B. E. - I Chemical
Type of the Program: S.S. of B.E.- I Chemical
Year I CORE / ELECTIVE / FOUNDATION 1: CORE CREDIT
PAPER CODE: CHL1201
Semester II PAPER NAME: PROCESS CALCULATIONS HOURS 45
Introduction:
Chemical Engineering and Chemical Industry. 04
UNIT – I
Steady state and unsteady state processes. hrs.
Unit Operations, Unit Processes and Process Flow Diagrams.
Basic Calculations:
State properties: Molecular weight, compositions, density, vapor pressure etc. for
gas, liquid and solid systems. 12
UNIT – II Thermal properties: Heat capacity, sensible heat, latent heat, heat of reaction, heat hrs.
of solution, enthalpy calculations etc. for gas, liquid and solid systems.
Techniques of problem Solution: Analytical, Graphical and Numerical.
Material Balances:
Material balance equations based on conservation principle. 10
UNIT – III
Material balances for non-reactive processes (Unit Operations). hrs.
Material balances for reactive processes.
Energy Balances:
Energy balances for closed and open systems based on energy conservation
principle. 11
UNIT – IV
Energy balances for non-reactive processes (Unit Operations), hrs.
Energy balances for reactive processes.
Coupled material and energy balances for single unit process.
Multiple Unit Processes:
Introduction to processes with multiple Units. 08
UNIT – V
Material balances on processes with recycle, purge, and bypass. hrs
Introduction to DOF analysis and solution strategy for multi-unit process.
REFERENCES
th
1 Bhatt and Vora: Stoichiometry, 4 Ed, Tata McGraw-Hill
D.M. Himmelblau and J. B. Riggs: Basic Principles and Calculations in Chemical Engineering, 8th
2
Ed, Prentice Hall.
R.M. Felder and R.W. Rousseau ‘Elementary Principles of Chemical Processes’ 3rd Ed, John Wiley
3
and Sons, 2000.
Faculty : Technology and Engineering
Department : Chemical Engineering
Contact Details :
E. mail ID :head-chemengg@msubaroda.ac.in
Name of the Program: B.E.- II CHEMICAL

Type of the Program: F.S of B.E.-II CHEMICAL
CORE / ELECTIVE / FOUNDATION 1 :CORE
Year II CREDIT
PAPER CODE : CHL1301
PAPER NAME: CHEMICAL ENGINEERING
Semester I HOURS 45
COMPUTATIONS
Introduction
05
UNIT – I Review of Chemical Engineering Calculations including units and
hrs.
conversions, Analytical versus Computational approach.
Types of Problems :
Chemical Engineering: 08
Property Estimation, Equilibrium, Transport Phenomena, Kinetics, Material hrs.
and Energy Balances, Process Simulation including Flow sheeting, Design
UNIT – II and Optimization, Molecular Simulation etc.
Mathematical Equations: Algebraic equations: linear / nonlinear
07
Differential Equations: Ordinary / Partial; Initial value, Boundary value
hrs.
Regression: linear / nonlinear
Computational Software
Introduction, Capabilities and Guidelines for
General mathematical software:
08
UNIT – III EXCEL, POLYMATH, SCILAB, GAMS, CFD etc.
hrs.
Specialized Software:
Property Estimation: GPEC, PE2000,VMG, EXCEL, PE/SAFT etc.,
Process Simulation: ChemSep, COCO, CHEMCAD etc.
Problem Solving
Mathematical formulation, DOF analysis and solution approach (algorithm), 12
UNIT – IV
Selection of software and implementation of algorithm (coding) for problem hrs.
solution, Analysis and validation of problem solution.
Flow sheet Simulation
05
UNIT – V Sequential and Simultaneous simulation,
hrs.
Introduction to partitioning and Tearing.
REFERENCES
1 B.A. Finlayson : Introduction to Chemical Engineering computing, 2nd Ed, Springer
Cutlip and Shacham: Problem Solving in Chemical Engineering with Numerical Methods, 2nd Ed,
2
Prentice Hall, 2000
3 Hanna and Sandall: Computational Methods in Chemical Engineering, Prentice Hall, 1997
4 G.V. Reklaitis, Introduction to Material and Energy Balances, John Wiley and Sons, 1983.
Contact Details :
E. mail ID : head-chemengg@msubaroda.ac.in
Name of the Program: B.E.CHEMICAL
Type of the Program: S.S. of B.E. -II CHEMICAL
Year II CORE / ELECTIVE / FOUNDATION 1 : CORE CREDIT
Semester II PAPER NAME : MECHANICAL OPERATIONS HOURS 45
Properties of particulate solid

Introduction to particle technology, Characterization of solid particles (size, 05
UNIT – I
shape, size distribution), particle size measurement techniques, Mixed hrs.
particles, specific surface of mixture, Particle population.
Screen analysis:
05
UNIT – II Screening equipment, Method of reporting screen analysis, Capacity and
hrs.
effectiveness of screens
Size reduction and enlargement:
Principles of comminution, Energy and power required for comminution, 05
UNIT – III
Laws of crushing, size reduction equipments, Industrial processes for particle hrs.
size enlargement, size enlargement equipments
Properties of masses of solids:
Storage of solids: Angle of repose, bulk storage, storage in bins and silos, 04
UNIT – IV
Conveying of solids: Codes for characterization of solids, screw conveyers, hrs.
belt conveyers, bucket elevators, pneumatic conveying of solids.
Mixing of powders and pastes: 03
UNIT – V
Mixers for cohesive and non-cohesive solids, Mixing Index hrs.
Agitation and mixing of liquids:
04
UNIT – VI Basic stirred tank design, Types of impellers, flow patterns, power
hrs.
consumption and scale up
Filtration:
Principles of filtration, constant pressure, constant rate filtration,
05
UNIT – VII compressible and incompressible cakes, cake resistance, filter media
hrs.
resistance, filter media, filter aids, filtration equipments (batch, continuous),
Selection criteria, Washing of filter cakes.
Gravity setting and sedimentation: Gravity clarifiers, sorting clarifiers, Batch 05
UNIT – VIII
sedimentation, rate of sedimentation, Design of thickeners and clarifiers hrs.
Centrifugal sedimentation: Principles of centrifugal sedimentation, Solid gas 04
UNIT – IX
separation, liquid solid separation. hrs.
Fluidization: Types of fluidization, Geldart classification of particles.
05
UNIT – X Minimum fluidization velocity, Pressure drop. Particulate and bubbling
hrs.
fluidization. Applications of fluidization.
REFERENCES
W.L. Mc Cabe, J.C. Smith, P. Harriot ‘Unit Operations of Chemical Engineering’ 7th Ed. McGraw
1
Hill, 2006.
2 J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol.- II, 6th Ed. Elsevier, 2003
3 G.G. Brown Ed. ‘Unit Operations’ John Wiley & Sons, 1950
C.G. Geankopolis ‘Transport Processes and Separation Process Principles’ 4th Ed, Prentice Hall
4
India, 2003.
Contact Details :
Name of the Program: B.E.CHEMICAL
Type of the Program: S. S of B.E.-II Chemical
PAPER CODE : CLE1403
Semester II PAPER NAME : THERMODYNAMICS AND ENERGY HOURS 45
SYSTEMS
06
UNIT – I Laws of thermodynamics, thermodynamic functions & their inter relations.
hrs.
PVT relationship and thermodynamic and Property estimation/calculations 07
UNIT – II
(U, H, S, G etc.) property charts. hrs.
05
UNIT – III Thermodynamics of flow processes
hrs.
02
UNIT – IV Refrigeration and Liquefaction
hrs.
03
UNIT – V Energy / lost work analysis.
hrs.
02
UNIT – VI Energy forms, Sources and Resources, flow of energy in ecosystem.
hrs.
Key alternative energy Sources such as Solar Energy, Wind Energy and 09
UNIT – VII
Tidal power etc. hrs.
Nuclear energy: Fission reaction, nuclear reactors including safety aspects, 04
UNIT – VIII
Fusion reactions and their prospects. hrs.
03
UNIT – IX Fuel cells
hrs.
04
UNIT – X Hydrogen Power & aspects of energy storage and other developments.
hrs.
REFERENCES
1 A.W. Culp ‘Principles of Energy conversion’ 2nd Ed, McGraw Hill, 1991,
2 M.M. El-Wakil ‘Power Plant Technology’2nd Ed, McGraw Hill, 1985
3 J.M. Smith, H.C. Van Ness & M.M. Abbot ‘Introduction to Chemical Engineering Thermodynamics’,
7th Ed, McGraw Hill, 2004.
4 S.R. Turns ‘Thermodynamics concepts and applications’, Cambridge University Press, 2006.
Kalabhavan, Vadodara
Contact Details :
E. mail ID :
Name of the Programme: B.E.CHEMICAL
Type of the Programme: S.S. of B.E.-II CHEMICAL
Semester II PAPER NAME : FLUID FLOW OPERATIONS HOURS 45
Nature of Fluids, Fluid statics and its applications, Manometers, Pressure 06

UNIT – I
measurements. hrs.
Introduction to fluid dynamics, classification of fluids, concept of viscosity,
viscometers, concept of potential flow, steam lines, average velocity, mass 06
UNIT – II
velocity etc. Laminar and Turbulent flow, dimensional analysis, Reynolds hrs.
number and its significance, Concept of boundary layer.
Basic equations of fluid flow, Equation of continuity, Bernoulli’s Theorem. 06
UNIT – III
hrs.
Incompressible flow in pipes and channels, Frictional losses in closed
UNIT – IV channels and pipe fittings, contraction and expansion losses, power 08
hrs.
requirement for flow.
Transportation of fluids, Pipes, pipe standards, fittings, pipe joints, valves and
their constructional features, Fluid moving machinery: Positive displacement 06
UNIT – V
and centrifugal pumps, centrifugal pump theory, concept of NPSH, pump hrs
performance and characteristics.
Flow measurement, Classification and selection of flow meters, Variable head
05
UNIT – VI and variable area meters including notched weirs, positive displacement
hrs
meters, coirolis meters, ultrasonic meters and various other quantity meters.
Introduction to compressible flow, flow through pipes and nozzles, Fans, 06
UNIT – VII
Blowers ejectors and compressors. hrs
Special cases: Single and two phase flow through packed beds, two-phase gas 02
UNIT – VIII
liquid flow in pipes, Essentials of gas solid flows. hrs
REFERENCES
1 W.L. Mc Cabe, J.C. Smith, P. Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw
Hill, 2006.
2 P.K. Kundu & I.M. Cohen ‘Fluid Mechanics’ 5th Ed, Academic Press, 2002
3 G.S. Sawhney ‘Fundamentals of fluid mechanics’, 2nd Ed, I.K. International
4 J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. I, 6th Ed, Elsevier, 2004.
Contact Details :
E.mail ID : head-chemengg@msubaroda.ac.in
Name of the Program: B.E. CHEMICAL
Type of the Program: F.S. of B.E.-III CHEMICAL
Year III CORE / ELECTIVE / FOUNDATION 1 : CORE CREDIT
Semester I PAPER NAME : MASS TRANSFER OPERATIONS – I HOURS 45
Molecular diffusion in fluids: 08

UNIT – I Stefan- Maxwell's diffusion equations Prediction of diffusion coefficients for gases and
hrs.
liquids.
04
UNIT – II Fundamentals of mass transfer, mass transfer coefficients, interphase mass transfer,
mass transfer theories hrs.
Gas absorption: Gas- liquid equilibria, solvent selection criteria, analysis of absorption
columns, graphical design of plate columns, Kremsers Soudres & Brown’s method. 08
UNIT – III Mass transfer analysis for design of packed absorption columns for gas absorption
hrs.
(HETP, HTU, NTU concept) Gas-liquid contacting equipments their classification and
selection.
06
UNIT – IV Humidification and dehumidification: Basic concepts, cooling towers and their
classification and selection, cooling tower design by enthalpy potential method. hrs.
Distillation: Introduction to distillation. Vapor liquid equilibria. Distillation techniques
08
UNIT – V viz. differential, flash, steam, fractionation, azeotropic and extractive distillation etc.
vapor liquid contacting equipment their constructional and operational features and hrs
design aspects.
Analysis of binary distillation: Material and energy balance around a distillation
column, concept of reflux, Lewis Sorel method of calculation, McCabe & Thiele 11
UNIT – VI method for determining number of ideal plates, feed stage location, optimum reflux
hrs.
ratio, condenser and reboiler heat duty, Ponchon & Savarit method for design of plate
column. Concept of plate efficiencies. Distillation in packed columns.
REFERENCES
1. R.E. Treybal ‘Mass – Transfer Operation’ 3rd Ed, Mc Graw Hill, 1981
2. J.D. Seader and E.J. Henley “Separation Process Principles”, 3rd Ed, J. Wiley & Sons, 1998
3. C.G. Geankopolis ‘Transport Processes and Separation Process Principles 4th Ed, Prentice Hall
India, 2003.
4. A.S. Foust et.al. ‘Principles of Unit Operations, 2nd Ed, John Wiley, 1972
5. W.L. Mc Cabe, J.C. Smith, P. Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw
Hill, 2006.
6. J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol I, 6th Ed, Elsevier, 2004
7. J.M. Coulson & J.F. Richardson’ Chemical Engineering’ Vol II, 5th Ed, Elsevier,2003
8. B.K. Dutta ‘Mass Transfer’ TMH, 2006.
Contact Details :
Name of the Program: B.E. Chemical
Type of the Program: S.S of B.E.-III CHEMICAL
PAPER NAME : PROCESS EQUIPMENT DESIGN II
Semester II HOURS 45
USE OF PERRY’S CHEMICAL ENGINEERS HANDBOOK
IS PERMITTED DURING EXAMINATION.
Design of piping systems for single phase and two-phase flows, piping colours
12
UNIT – I and codes. Selection and specifications of pipes, fittings, valves, pumps and
hrs.
compressors.
07
UNIT – II Design of gas – liquid, gas – solid, liquid – liquid and solid – liquid separators.
hrs.
Design of the heat exchanges (Kern’s method and Bell’s method), condensers 08
UNIT – III
and reboilers. hrs.
Design of vapor – liquid contacting equipments: Plate columns and packed 08
UNIT – IV
columns. hrs.
Specification of design variables. Design of multi-component distillation 07
UNIT – V
systems: FUG method and elements of rigorous methods. hrs
03
UNIT – VI Design of absorbers, driers and crystallizers.
hrs.
REFERENCES
1. Don Green and Robert H.Perry, ‘Perry’s Chemical Engineers Handbook’, 8th Ed, Mc- Graw Hill, 2008
2. S.M. Walas ‘Chemical Process Equipment’ Butterworth- Heinemann, 1999.
3. E.E. Ludwig ‘Applied Process Design of Chemical and Petrochemical Plants’ 4th Ed, Vol. I, II, III,
Gulf professional Publications, 1999.
4. N.P. Chopey ‘Handbook of Chemical Engineering Calculations’ 4nd Ed, McGraw Hill, 1994.
Department : Chemical Engineering Academic Year
Kalabhavan, Vadodara. 2014 -15
Contact Details :
Name of the Program : B.E. CHEMICAL

Type of the Program: S.S. of B.E.- III CHEMICAL
Semester II PAPER NAME : MASS TRANSFER OPERATIONS II HOURS 45
Liquid–Liquid extraction: Extraction equilibria and its graphical

12
UNIT – I representation, tie line correlations, prediction of 1-1 equilibria. Stage wise &
continuous contacting equipments their classification and selection, design of hrs.
multistage counter current extraction with and without reflux.
05
UNIT – II Leaching: Principles and leaching equilibria, unsteady state & steady state
operations, design of leaching systems, leaching equipment and systems. hrs.
Membrane Separation Processes: Reverse osmosis, ultra filtration, micro
08
UNIT – III filtration, dialysis, per vaporation etc. concepts and analysis, flux equations,
fouling and concentration polarization. Membrane modules their fabrication hrs.
and design.
07
UNIT – IV Drying: Concepts, calculations of rate of drying, classification and selection of
drying equipment. Design of batch and continuous driers. hrs.
Crystallization: Crystal geometry, solubility curves, supersaturation, theories
05
UNIT – V of nucleation & crystal growth, calculation of yield, classification and
selection of equipment for solution crystallization, MSMPR crystallization hrs
model, melt crystallization.
Adsorption & Ion exchange: Equilibrium considerations, stage wise
adsorption and continuous contact adsorption. Fixed bed adsorption, scale up 08
UNIT – VI for constant pattern front, Thermal swing and pressure swing adsorption.
hrs.
Counter current adsorption, simulated moving bed. Chromatographic
separations.
REFERENCES
1. R.E. Treybal ‘Mass-Transfer Operation’ 3rd Ed. Mc Graw Hill, 1981
2. J.D. Seader and E.J. Henley “Separation Process Principles”, 3rd Ed, J. Wiley & Sons,
3. C.G. Geankopolis’ Transport Process and Separation Process Principles’ 4th Ed, Prentice Hall India
2003.
4. A.S. Foust et.al. ‘Principles of Unit Operations, 2nd Ed, John Wiley, 1972
5. W.L. Mc Cabe, J.C. Smith, P. Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw
Hill, 2006.
6. J.K. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. 1, 6th Ed, Elsevier 2004.
7. J.K. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. 2, 5th Ed, Elsevier 2003.
8. B. K. Dutta ‘Mass transfer’ TMH, 2006
Department : Chemical Engineering Academic Year
Kalabhavan, Vadodara. 2014 -15
Contact Details :
E.mail ID :
Semester I HOURS 45
PAPER NAME : PROCESS EQUIPMENT DESIGN I
Selection of Materials of Construction for Process equipments and

07
UNIT – I ancillary equipments. Fabrication techniques used for process
equipments with emphasis on bending of plates, welding and various hrs.
finishing techniques. Non destructive testing of vessels.
Design of unfired process vessels subjects to internal pressure, design
14
UNIT – II of end closures and head, nozzles, flanges, manholes etc. Design of
unfired pressure vessels subjected to external pressure. Design codes hrs.
for pressure vessels. Testing of pressure vessels.
06
UNIT – III Design of non-pressure storage vessels with fixed and floating roofs.
Design of Horton spheres. Design codes for storage tanks and bullets. hrs.
04
UNIT – IV Design of tall vertical vessels with considerations of wind loads,
seismic activity and various eccentric loads. hrs.
UNIT – V Design and construction of autoclaves and high - pressure vessels. 05 hrs
04
UNIT – VI Design of foundation and supports, with special emphasis on skirt
supports and saddle supports. hrs.
UNIT – VII Design of ancillary equipments: Agitator design, tube sheet design, 04hrs.
ejector design etc.
01
UNIT – VIII Layout of process equipment in the chemical process industries.
hrs.
REFERENCES
1. L.E. Brownell and E.H. Young, ‘Process Equipment Design’, Wiley, 1959
B.C. Bhattacharya, ‘Introduction to chemical equipment design – Mechanical aspects’. CBS
2.
publishing Co., 2008
B.C. Bhattacharya and C.M. Narayanan, ’Computer aided design of chemical process
3.
equipment’, New Central Book Agency, 1992.
4. M.V. Joshi and V.V. Mahajani, ‘Process equipment design’, 3rd Ed.
Contact Details :
Type of the Program: F.S of B.E.-III CHEMICAL
CORE / ELECTIVE / FOUNDATION 1 : CORE
Year III CREDIT
PAPER NAME : CHEMICAL ENGINEERING
Semester I HOURS 45
THERMODYNAMICS
Thermodynamic functions and relations for mixtures:

09
UNIT – I Partial molar property, chemical potential, residual properties, fugacity
& fugacity coefficients, excess functions and activity coefficients, hrs.
correlations for excess Gibbs free energy.
06
UNIT – II PVT behavior including EOS for mixtures; Fugacity estimation/
calculations based on PVT behavior hrs.
03
UNIT – III Phase equilibrium criteria and VLE calculations for different pressure
ranges including flash calculations. hrs.
06
Activity coefficient calculation from experimental VLE data and data
UNIT – IV reduction, applications of Gibbs-Duhem relation for calculations of hrs.
and consistency check for VLE data
04
UNIT – V Phase diagrams for miscible, partially miscible and immiscible liquid
mixtures, introduction to LLE and VLLE calculations. hrs
Criteria of chemical equilibrium, effect of P and T on equilibrium
06
UNIT – VI conversion (Xe) and equilibrium constant (K), methods of evaluation
of K & Xe, Xe charts for Exothermic, Endothermic, Reversible and hrs.
irreversible reactions etc.
Equilibrium of complex reactions, introduction to equilibrium
conversion calculation under adiabatic and non-isothermal conditions, 08
UNIT – VII introduction to liquid phase, heterogeneous and electrochemical
hrs.
reaction equilibria, thermodynamic analysis of some chemical
reactions of industrial importance.
03
UNIT – VIII Prediction of thermodynamic properties by group contribution and
other methods. hrs.
REFERENCES
1. B.G. Kyle ‘Chemical Process Thermodynamics 3rd Ed, Prentice Hall India, 1994
2. J.M. Smith, H.C. Van Ness & M.M. Abbot ,“Introduction to Chemical Engineering
Thermodynamics”, 7th Ed, McGraw Hill, 2004.
3. Y.V.C. Rao, Chemical Engineering Thermodynamics, Universities Press (1997)
Contact Details :
Type of the Program: S.S. of B.E.-III CHEMICAL
Semester II PAPER NAME : CHEMICAL PROCESS HOURS 45
INDUSTRIES
Chemical Industries in India: An overview, Unit Process concept, 02

UNIT – I
Flow sheet symbols. hrs.
Industrial acids and gases: 06
UNIT – II
Sulfuric acid, Phosphoric acid, hydrogen etc. hrs.
Nitrogenous and Phosphatic Fertilizers: 06
UNIT – III
Ammonia, Urea, Diammonium phosphate, triple super phosphate etc. hrs.
06
UNIT – IV Chlor-alkali Industries: Soda ash, Caustic soda
hrs.
Pulp and paper: Pulping techniques, paper making, paper machines, 02
UNIT – V
black liquor, recovery etc. hrs
Cement and Lime: 02
UNIT – VI
Types of cement, manufacture by wet process and dry process, etc. hrs.
Petroleum and petrochemicals: 09
UNIT – VII
General outlook, various products and derivatives hrs.
Polymerization processes: 04
UNIT – VIII
Polyolefins, polystyrene, nylons etc. hrs.
Pharmaceuticals and pesticides: 02
UNIT – IX
Bulk drugs and antibiotics, DDT,BHC, malathion etc. hrs.
Detergents, oils and fats: 02
UNIT – X
LAB derivatives, fat splitting, transesterification, biodiesel etc. hrs.
Dyes, intermediates and pigments: Classification, chromophores, 02
UNIT – XI
synthesis techniques, H acid, titanium dioxide etc. hrs.
Coal and coal chemicals: 02
UNIT – XII
Classification, coking, liquefaction, destructive distillation. hrs.
REFERENCES
1. R.N. Shreve, ‘Chemical Process Industries’, 5th Ed, McGraw-Hill, 1997
2. C. Dryden, ‘Outline of Chemical Technology’,3rd Ed, TMH, 1974
3. J.A. Kent ‘Riegel’s Handbook of Industrial Chemistry’10th Ed., Springer Science & Business
Media, 2003
4. Kirk and Othmer, ‘Encyclopedia of Chemical Technology’, 5th Ed, 24 volumes, 2006.
Contact Details :
Semester I HOURS 45
PAPER NAME : HEAT TRANSFER OPERATIONS
Modes of heat Transfer: Transfer by conduction. General differential

equation for heat conduction, steady state analytical and numerical 07
UNIT – I
methods for flat, cylindrical and spherical geometry. Extended surface hrs.
heat transfer, Insulation.
Heat transfer by convection: Free & forced convection, film & overall
heat transfer coefficients, concept of convective resistances in series. 07
UNIT – II Dimensional analysis of convection, physical significance of the
hrs.
dimensionless numbers. Laminar & turbulent flow heat transfer inside
tubes & outside of tubes.
Heat exchangers: Classification and selection, double pipe heat
exchanger analysis, parallel and counter flow heat transfer, LMTD, 09
UNIT – III
design considerations, NTU method of heat exchanger analysis and hrs.
design, Shell & tube heat exchanger calculations.
Heat transfer with phase change: Regimes of boiling heat transfer,
various correlations. Heat transfer during condensation, drop and film 07
UNIT – IV
condensation, Nusselt’s equation and its applications, condensation hrs.
over tube banks.
Heat transfer by radiation: Laws of radiant heat transfer, concept of
black body and grey body. Radiation between surfaces, view factors, 09
UNIT – V radiation between reflecting surfaces, absorption and emission by
hrs
gases, luminous & non luminous gases, combined modes of heat
transfer.
Evaporation: Types of evaporators their classification and selection.
Single effect and multiple effect evaporators, capacity and economy, 06
UNIT – VI
feed arrangement to multiple effect evaporators. Evaporator hrs.
calculations for single effect and multiple effects.
REFERENCES
th
1. D.Q. Kern, Process Heat Transfer, 5 Ed, McGraw-Hill, 1965
2. Y.V.C. Rao, Heat transfer, 2nd, Ed.
3. J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. I, 6th Ed, Elsevier, 2004
4. F.P. Incropera & D.P. Dewitt ‘Fundamental of Heat and Mass transfer’, John Wiley & Sons,
1996
5. J.D. Seader and E.J. Hanley “Separation Process Principles”, J. Wiley & Sons, 1998.
Contact Details :
Name of the Program : B.E. Chemical
Type of the Program: S.S. of B.E.-III Chemical
Semester II PAPER NAME : CHEMICAL REACTION HOURS 45
ENGINEERING II
Fundamentals of heterogeneous reacting systems, the influence of mass 08

UNIT – I transfer on reaction rates, introduction and analysis of fluid-fluid
hrs.
systems, kinetic regimes and rate analysis.
Classification and selection of fluid-fluid reactors based on reaction 05
UNIT – II
regimes. Design of fluid-fluid reactors. hrs.
Kinetics of fluid-solid non catalytic reactions, determination of rate 11
UNIT – III determining steps, various models of gas solid reactions. Classification
hrs.
and design of non catalytic fluid particle reactors.
Heterogeneous catalysis, nature of catalysis, components of commercial 03
UNIT – IV catalysts, catalyst preparation characterization of catalysts, catalyst
hrs.
poisoning and regeneration.
Fluid solid catalytic reaction kinetics (surface catalysis intrinsic
kinetics), kinetics in porous catalyst particles, effective diffusivity, 09
UNIT – V
particle effectiveness factors, temperature dependency, Laboratory hrs
reactors and analysis of rate data.
Design outline of fixed-bed, fluid-bed, trickle-bed and slurry reactors, 09
UNIT – VI
isothermal and adiabatic operations. Selected case studies in design. hrs.
REFERENCES
1. O.Levenspiel “Chemical Reaction Engineering”, 3rd Ed, John Wiley & Sons, 1999
2. H. Scott Fogler ‘Elements of Chemical Reaction Engineering’, 4th Ed, Prentice Hall India,
2005.
3. L Schmidt, ‘The Engineering of Chemical Reactions’, 2nd Ed, Oxford, 2008.
4. J.M. Smith, ‘Chemical Engineering Kinetics’, 3rd Ed, McGraw-Hill, 1981
5. C.N. Satterfield ‘Heterogeneous Catalysis in Industrial Practice 2nd Ed, McGraw-Hill 1993.
Contact Details :
Name of the Programme : B.E. CHEMICAL
Type of the Programme: F.S. of B.E.-III CHEMICAL
Semester I PAPER NAME : CHEMICAL REACTION HOURS 45
ENGINEERING I
Introduction to chemical kinetics, types of reactions, kinetics of 04

UNIT – I homogeneous reactions, temperature dependency of reactions.
hrs.
Formulation and analysis of simple and complex rate equations. 06
UNIT – II Interpretation of rate data in constant and variable volume systems.
hrs.
Introduction to reactor design, concept of ideal reactors, development of
11
UNIT – III design expression for batch, tubular and stirred tank and semi-batch
reactors, multiple reactor systems, reactors in series and parallel, recycle hrs.
reactor, advantages and limitations in applications.
Multiple reactions, concept of selectivity, maximizing the desired 09
UNIT – IV product in series and parallel reaction system. Introduction to process
hrs.
design for some industrial reactors.
RTD and non-ideal reactor analysis, one parameter models for non-ideal
10
UNIT – V reactor RTD and their equivalence, conversion calculations using RTD
measurements. The use of RTD models for evaluation of reactor hrs
performance.
Equilibrium conversions, heats of reaction and temperature, Optimum
temperatures for isothermal and non-isothermal operations, product 05
UNIT – VI distribution and effect of temperature in multiple (complex) reactions.
hrs.
Evaluation of adiabatic and non-adiabatic reactor performance, thermal
stability or reactors.
REFERENCES
1. O. Levenspiel “Chemical Reaction Engineering”, 3rd Ed, John Wiley & Sons, 1999
2. H. Scott Fogler ‘Elements of Chemical Reaction Engineering’, 4th Ed, Prentice Hall India,
2005.
3. L Schmidt, ‘The Engineering of Chemical Reactions’, 2nd Ed, Oxford, 2008.
Contact Details :
Type of the Program: F.S. of B.E.- CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : CORE CREDIT
PAPER CODE : CHL 1703
Semester I PAPER NAME : INSTRUMENTATION AND PROCESS HOURS 45
CONTROL
Introduction to measurement: instruments for measurement of process

12
UNIT – I variables such as, temperature, flow, liquid level, Pressure.
hrs.
Instrumentation symbols and labels, Essentials of error analysis.
Introduction to process control, block diagram representation of control loop,
control strategies, mathematical modeling of physical systems, linear system
08
UNIT – II analysis, dynamics of first order, second order and higher order systems
hrs.
using transfer functions, transient response, linearization of non linear
models.
Open loop and closed loop transfer functions. Design of single loop feedback
06
UNIT – III control system. Stability of closed loop, effect of loop parameters on ultimate
hrs.
gain, effect of dead time, Routh’s test.
Basic components of control system, sensors and transmitters, control valves,
feedback controllers, actions, types, reset-windup. Tuning of feedback 07
UNIT – IV
controllers, tuning controllers for integrating processes, synthesis of hrs.
feedback controllers, tuning rules.
Stability of control systems, Frequency response analysis, Bode and Nyquist 06
UNIT – V
stability criteria. hrs
Advanced control strategies, feed forward, cascade, advanced supervisory,
06
UNIT – VI model predictive control, multivariable control, introduction to digital
hrs.
control principles, microprocessor based control.
REFERENCES
Luyben, ‘Process Modeling, Simulation and Control for Chemical Engineers’, 2nd Ed, McGraw-
1.
Hill – 1990.
2. Bequette, ‘Process Dynamics’, Prentice Hall, 1998.
3. Coughanor ‘Process systems analysis and control’ 2nd Ed, McGraw-Hill, 1991.
Contact Details :
Type of the Program: F.S. of B.E. - IV CHEMICAL
Year IV PAPER CODE : CHL1704 CREDIT
PAPER NAME : POLYMER SCIENCE AND
Semester I TECHNOLOGY HOURS 45
Introduction & Basic Concepts, Polymer based industries and feedstocks. 02

UNIT – I
Classification of Polymers. hrs.
State of polymer, structure property relations and transition temperatures.
11
UNIT – II Polymer solutions and characterization of polymers (MW & its experimental
hrs.
determination), polymer fractionation.
Chain polymerization: Mechanism and kinetics; copolymerization.
08
UNIT – III Condensation polymerization, coordination polymerization, Techniques of
hrs.
polymerization.
Plastics–Materials & some typical manufacturing process, (poly olefins, 09
UNIT – IV
PVC, PS, PMMA, Epoxy resins etc.) Testing of Polymers. hrs.
Rubbers and fibers, materials & some typical manufacturing process, Testing
08
UNIT – V of rubbers and elastomers. Mechanical properties: Elasticity, viscoelasticity,
hrs
factors affecting mechanical behavior etc.
07
UNIT – VI Processing of plastics and rubbers.
hrs.
REFERENCES
1. F.W. Billmeyer, Text book of Polymer Science, 3rd Ed, Wiley, 1984
2. C.E. Carraher, Introduction to polymer chemistry, Traylor and Francis, 2007
3. F. Rodriguez, ‘Principles of polymer systems’ 4th Ed, Traylor and Francis, 1996.
Contact Details :
Type of the Program: F.S. of B.E.-IV Chemical
Year IV CREDIT
PAPER CODE: CHL1705
PAPER NAME: SAFETY HEALTH AND
Semester I HOURS 45
ENVIRONMENT
Types of hazards in the chemical industry, accident and loss statistics, 04

UNIT – I nature of the accident process.
hrs.
Toxicology and industrial hygiene, models for toxic release.
General aspects of fires and explosions, design to prevent fires and 06
UNIT – II explosions, Fire and explosion indices, Phenomena of vapour cloud
hrs.
explosion, flash fires and BLEVE
Safety considerations in design, installation, operation and maintenance of 05
UNIT – III selected process equipment, relief system and flares etc. hrs.
Hazard and operability studies Hazard analysis ‘What if’ analysis. 04
UNIT – IV Failure modes and effect analysis, fault tree analysis, event tree analysis. hrs.
Acceptable risk and safety properties, protective equipment for personal
and plant for various hazards, safety procedure, emergency response. 04
UNIT – V
Disaster management, insurance, workers safety and public liability, other hrs
liabilities.
Ecology, classification of ecological factors, fundamental ecological
variables, Ecological principles governing use of natural resources,
Atmosphere, hydrosphere and climates, cycles of principal biogenetic 08
UNIT – VI
elements and water cycle, perturbation of cycles due to human hrs.
interference, its consequences and mitigation.
Green house effect, global warming, air pollution acts & legislations.
Assessment of air quality, sampling and measurement. Control of dusts,
mists and aerosols in industrial processes using different equipments. 06
UNIT – VII
Control of toxic releases, SOX &NOX, using absorption, and adsorption hrs.
other chemical treatment techniques.
Water quality assessment and water quality management, Physical,
chemical and biochemical techniques of water pollution control. Water 08
UNIT VIII
pollution prevention and control acts. hrs.
Solid waste management. Landfills, nuclear waste management schemes.
REFERENCES
Crowl and Louver ‘Chemical Process safety: Fundamentals with Applications:’ 3nd Ed., Prentice
1.
Hall, 2011
2. Valsaraj, ‘Elements of environmental engineering’ CRC press, 1998
3. Sanders, ‘Chemical process safety’ 3rd Ed, Elsevier, 2005.
Contact Details :
E.mail ID :head-chemengg@msubaroda.ac.in
Type of the Program :F.S. of B.E.-IV CHEMICAL
Year IV CORE/ELECTIVE/FOUNDATION 1 : CORE CREDIT
Semester I PAPER NAME : TRANSPORT PHENOMENA HOURS 45
The role of transport phenomena in the understanding of chemical

03
UNIT – I engineering.
Fluids classification. Transport properties. Introduction to non- hrs.
Newtonian fluids. Two parameter models.
Lagrangian and Eulerian concept of motion, control volume 05
UNIT – II approach, overall and differential mass balances in Cartesian,
hrs.
cylindrical co-ordinate systems.
05
UNIT – III Shell momentum balance approach; Application to selected problem.
hrs.
04
UNIT – IV Equation of motion and its application.
hrs.
Boundary Layer theory von Karman’s analysis, exact solutions using 06
UNIT – V stream functions. Turbulence concepts mixing length hypothesis,
hrs
universal velocity profile and its application.
05
UNIT – VI Shell energy balance approach: Applications to selected problems.
hrs
05
UNIT – VII Convective Heat transport : Asymptotic solutions of typical flow
problems etc. hrs
04
UNIT – VIII Fick’s law of diffusion application of differential balances to mass
transfer, critical analysis correlations for mass transfer. hrs
04
UNIT – IX Mass transfer theories Convection – Diffusion problems in
homogenous and heterogeneous media. hrs
04
UNIT – X Analogy between Momentum heat and mass transfer.
hrs
REFERENCES
1. Bird Stewart and Lightfoot, ‘Transport Phenomena’ 2nd Ed, Wiley, 2002
2. Welty, Wicks, Wilson &Rorer ‘Fundamentals of Momentum heat & mass transfer,
Wiley, 2001.
Contact Details :
Type of the Program: F.S of B.E.-IV CHEMICAL
CORE / ELECTIVE / FOUNDATION 1 :
Year IV CREDIT
PAPER CODE : 1711L
PAPER NAME : COMPUTER AIDED DESIGN
Semester I LABORATORY HOURS
Students will be assigned computational / simulation exercises to be worked
UNIT – I out using flow sheet simulators with special emphasis on property estimation
and process optimization.
Contact Details :
Type of the Program: F.S of B.E.-IV CHEMICAL
Year IV CREDIT
PAPER CODE : 1702
PAPER NAME : INDUSTRIAL TRAINING
Semester I HOURS
Each student will undergo industrial training for minimum period of two
weeks during summer vacations after appearing in S.S. BE III examinations.
UNIT – I After the training students will prepare a report on the training incurred by
them in the industry, this report has to be duly certified by the trainers from
the industry where training was undertaken.
During the time of training the students will either identify a suitable product
to prepare a detailed project report or the product will be assigned to them by
UNIT - II
the department to work out a project report that has to be submitted by the
end of SS BE IV for evaluation.
Contact Details :
Type of the Program: F.S. of B.E.-IV CHEMICAL
CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE
Year IV CREDIT
PAPER CODE: CHL 1708
PAPER NAME ELECTIVE-I : A: COLLOID AND
Semester I HOURS 45
SURFACE SCIENCE
04
UNIT – I Nature of colloidal dispersions: Scope and variables.
hrs.
Particle size and shape, transport properties of suspensions, sedimentation 05
UNIT – II
and diffusion. hrs.
Liquid surfaces and interfaces, thermodynamics of surfaces, surface tension, 05
UNIT – III
contact angle, interfacial tensions, surface energies. hrs.
Colloidal structures in surfactant solutions, micellar phase diagrams,
05
UNIT – IV adsorption from solution and monolayer formation, soft interfaces, Langmuir
hrs.
Blodge films.
Dispersions, rheology of dispersions, electrical charges in dispersions, forces
06
UNIT – V of attraction and repulsion between particles Electro kinetics and zeta
hrs
potential.
Colloidal and dispersion stability, DLVO theory, electrostatic and polymer 07
UNIT – VI
induces colloidal stability. hrs.
07
UNIT – VII Emulsions, foams and micro emulsion.
hrs.
Industrial applications to surface coating industry, pharmaceutical industry, 06
UNIT VIII
oil recovery etc. hrs.
REFERENCES
1. R.J. Hunter, Foundations of colloid science, 2nd Ed Oxford, 2006
2. Lyklema, ‘Fundamentals of interfacial and colloid science’, Vol. I – V Academic press, 1982
3. Cosgrove, ‘Colloid Science’ Blackwell Publishing, 2005.
Contact Details :
Type of the Program F.S. of B.E.-IV CHEMICAL
Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE CREDIT
Semester I PAPER NAME ELECTIVE : B CATALYSIS: SCIENCE & HOURS 45
TECHNOLOGY
Basics of Catalysis: Emergence of catalysis science & technology, a brief 03

UNIT – I history importance of catalysis and catalyst technology, Fundacioncatalytic hrs
phenomena & principles. .
Homogeneous and Enzyme catalysis: Elementary steps in homogeneous
catalysis, metal complex catalysis in liquid phase, liquid exchange dissociation
&coordination, oxidative addition, reductive elimination, insertion and
10
migration. Structure/Activity relationships, steric effects. A symmetric
UNIT – II hrs
homogeneous catalysis, industrial examples, homogeneous catalysis without
.
metals, cleric acid/base catalysis, organocolysis,
Essentials of enzyme catalysis –Michaelis – Menten reaction, Scaling up
homogeneous catalysis, catalyst recovery & recycle, Hybrid catalysts.
Heterogeneous Catalysis: Concept of active site model catalyst systems, real
10
catalysts, promoters, modifiers, poisons, preparation of solid catalysts, selection
UNIT – III hrs
of support catalyst characterization. Surface characterization, temperature
.
programmed techniques, spectroscopy & microscopy, selected care studies.
Catalytic Reactor Design: The LHHW model, general behavior of catalyst
particles & pellets, heat and mass transfer aspects, Thiele modulus and 08
UNIT – IV effectiveness factor. Choice of reactors in lab and plants collection & analysis hrs
of data from lab. Reactors. Fundamentals of catalytic reactor design, selected .
care studies.
Catalyst Deactivation: Causes and mechanism of deactivation, prevention and
regenerative treatment of catalyst decay, selected care studies. 07
UNIT – V
Optimal distribution of catalyst in a single pellet. Optimal distribution of hrs
catalyst in a reactor.
Environmental Catalysis :
1. Mobile sources: Automotive gasoline catalytic converters, catalytic
abatement of emissions from diesel engines, Trends in emission control for 07
UNIT – VI mobile sources. hrs
2. Stationary sources: Catalytic reduction of NOX catalytic oxidation of VOC .
emissions, catalytic oxidation of CO emission, Kinetics & reactor design for
CO & VOC oxidation.
REFERENCES
1. Morbidelli, Cavnilidis & Varma Catalyst design Cambridge Univ. press 2001.
2. Twigg, ‘Catalyst Handbook’ Manson publications, 1996.
3. Bartholonew and Farrauto ‘Fundamentals of Industrial catalytic processes’ Wiley Interscience, 2006.
Contact Details :
Type of the Program:F.S. of B.E.IV CHEMICAL
PAPER CODE :CHL1701
Semester I PAPER NAMEELECTIVE : C ADVANCES IN HOURS 45
SEPARATION SCIENCE
The structure of separation processes, definitions of separation and separative

04
UNIT – I work, characterization of concentration distribution. The morphology of
hrs.
separations processes.
04
UNIT – II Adsorptive bubble separation techniques, principles, application and design.
hrs.
06
UNIT – III Membrane processes, classification, principles, applications and design.
hrs.
Melt crystallization, zone refining, short path distillation and super critical 08
UNIT – IV
extraction. hrs.
Electrical separations: Electrophoresis, electrodialysis, protein purification 07
UNIT – V
using isoelectric focusing in gels, field flow fractionation. hrs
Chromatographic separation principles. Applications and scale up, separations 07
UNIT – VI
based on simulated moving beds, affinity chromatography. hrs.
Extractive separations using liquid membranes, reverse micelles and micro 05
UNIT – VII
emulsions. hrs.
Features of separation of isotopes, isomers and other complex molecules using 04
UNIT – VIII
novel separation techniques. hrs.
REFERENCES
1. Wankat, ‘Rate based separation’, Elsevier, 2005.
2. King, ‘Separation processes’, 2nd Ed, McGraw Hill, 1980.
3. Li, ‘Recent developments in separation science’, Vol I –V, CRC press, 1980
Contact Details :
Name of the Programme: B.E. CHEMICAL
Type of the Programme: F.S. of B.E.-IV CHEMICAL
PAPER CODE :CHL1707
Semester I PAPER NAMEELECTIVE: D PETROLEUM HOURS 45
ENGINEERING
Prospecting for petroleum, exploration methods, reserve appraisals, 05

UNIT – I
Exploration & production, petroleum management. hrs.
Well logging and Basin modeling, Natural gas coal bed methane, gas hydrate 09
UNIT – II
and deep water exploration hrs.
Reservoir characterization, Physico-Chemical environment of petroleum 10
UNIT – III
reservoirs in relation to oil and gas recovery systems. hrs.
Flow through porous media, mechanism of entrapment and mobilization of 05
UNIT – IV
oil in porous media. hrs.
Enhanced oil recovery techniques using surfactant & polymer flooding, 06
UNIT – V
reservoir management techniques. hrs
Drilling, Production, platform engineering and transportation. 06
UNIT – VI
Safety aspects in Petroleum production. hrs.
04
UNIT – VII Hydrocarbon resources and petroleum supply scenario.
hrs.
REFERENCES
1 James Speight, The Chemistry and Technology of Petroleum, CRC Press, Fifth Edition.
2 Boyun Guo, William C. Lyons, Ali Ghalambor, Petroleum Production Engineering: A computer
assisted approach. Gulf Publication.
Contact Details :
Name of the Program B.E. Chemical
Type of the Program: S.S. of B.E.-IV Chemical
Year IV PAPER CODE : CHL 1801 CREDIT
PAPER NAME : MODELING SIMULATION AND
Semester II OPTIMIATION HOURS 45
Role of Modeling, Simulation and Optimization (MSO) in process design – 02

UNIT – I
Synthesis Analysis, hrs.
Modeling: Introduction, Classification of process models, Model Building, 08
UNIT – II Characteristics of mathematical models. hrs.
Simulation: Analytical and Numerical methods for solving model equations,
06hr
UNIT – III Accuracy and error analysis, Approaches to Process Simulation, Commercial
s.
simulators.
Optimization Introduction: Optimization problem and its formulation,
07
UNIT – IV General approach for solution, Objective functions, Classification of
hrs.
Optimization problems and methods.
Optimization techniques:
-Continuity, convexity and conditions for maxima / minima
-Analytical methods: Direct search (without constraints) Lagrangian
Multiplier (with constraints), Calculus of Variation. 16
UNIT – V -Newton and quasi Newton methods for single and multivariable search hrs
-Linear (LP) and non linear (NLP) programming with constraints
-Mixed Integer Programming: MILP and MINLP
-Global Optimization Techniques
Applications of modeling simulation and optimization to chemical processes
and equipments. Fluid flow, heat Transfer, separations, reaction systems and 06
UNIT – VI
reactors etc. Use of spreadsheets and MATLAB for Simulation and hrs.
Optimization.
REFERENCES
1. Edgar, Himmelblau, and Lasdon ‘Optimization of Chemical Process’ McGraw-Hill, 1990
2. Babu, ‘Process Plant Simulation’. Oxford, 2005
3. Ramiez, ‘Computational methods for process simulation’, Butterworth, 1992.
Contact Details :
Type of the Program: SS BEIV CHEMICAL
Year IV CREDIT
PAPER CODE : 1806
Semester II PAPER NAME : SEMINAR HOURS
Students will be assigned a topic for which a detailed literature survey has to be
carried out. Students will refer to various books and journals for the same and
UNIT – I
prepare a report. The report has to be submitted at the end of SS BE IV for
evaluation.
Contact Details :
Year IV CREDIT
PAPER NAME : PROCESS SYNTHESIS AND
ECONOMICS
Introduction, role of process synthesis in process design, hierarchy of

synthesis steps. Synthesis Tree, approaches for synthesis, heuristics for 08
UNIT – I
process synthesis. Project engineering, plant location, plant layout and hrs.
utilities.
Attainable Regions and reactor networks: Concepts and implementation 06
UNIT – II
techniques, reactor – separator – recycle network. hrs.
Heat & Power integration: Heat Exchanger Networks –Stream matching,
heat loops and minimum heat exchangers. Heat integration in 08
UNIT – III
Distillation trains. Minimum energy requirement targets and pinch hrs.
analysis
Project scheduling. Scheduling of batch processes. Optimization of
08
UNIT – IV cycle time and number of units. CPM/PERT, identification of critical
hrs.
path & critical activities
Project cost estimation and cost of production estimation. Interest,
UNIT – V investment costs, depreciation, profitability, criteria cash flow diagram, 08 hrs
cost indices.
Economics of selecting alternatives and replacement cost, economy of
scale, marginal cost, break even analysis and optimization. Inventory 07
UNIT – VI
Control, taxes and insurance, legal aspects, liabilities, patent indemnity hrs.
etc.
REFERENCES
1. Robin Smith, ‘Chemical Process Design and Integration’, Wiley, 2005.
Biegler, Grossmann and Westerberg, ‘Systematic Methods of Chemical Process Design’, Prentice
2.
Hall, 1997.
3. Seider, Seader, Lewin, ‘Product and Process Design Principles’, 2nd Ed., Wiley 2004.
Peters and Timmerhaus, ‘Plant design and economics for chemical engineers’ 4th Ed,
4.
McGraw-Hill, 1991.
Contact Details :
Type of the Program: SS BE IV CHEMICAL
Year IV CREDIT
PAPER NAME : ELECTIVE II : A :
NANOTECHNOLOGY
Nanotechnology foundations: Definition, historical perspective, effects of 03

UNIT – I
nanoscience and nanotechnology in various fields hrs.
Properties of nanostructured materials: Shape and size dependent
07
UNIT – II properties, colour, melting point, density of states, band gap, magnetism
hrs.
etc.
Synthesis of nanoparticles: Top down and bottom up approaches, Nano
10
UNIT – III particles via colloids, micelles, vesicles, polymers, crystalline and zeolite
hrs.
hosts. Mechanical attrition, high energy ball milling.
Characterization techniques of nanostructured materials: Scanning electron
microscopy, Transmission electron microscopy, scanning tunneling 10
UNIT – IV
microscopy, atomic force microscopy, X-ray diffractometer, spectroscopy, hrs.
UV-Vis, Raman, EDX, AES etc.
Fabrication : Crystal growth, epitaxy, lithography, etching, masking, 07
UNIT – V
MEMs hrs
Applications relevant to the chemical industry: Catalysis, fuel cells,
08
UNIT – VI coatings, nanocomposite polymers, fluid inks, dyes, block copolymers and
hrs.
dendrimers.
REFERENCES
1. K. J. Klabunde , ‘Nanoscale materials in Chemistry’, Wiley Interscience, 2001.
2. J. Poole and S. Owens, ‘ Introduction to Nanotechnology’ Wiley, 1998
3. C.N.R Rao, Chemistry of Nanomaterials’ Wiley, 2007
Contact Details :
Type of the Program: S.S. of B.E.-IV CHEMICAL
PAPER NAME ELECTIVE II : B BIOTECHNOLOGY
Introduction to Biotechnology. Basic microbiology and recombinant DNA 04

UNIT – I
technology hrs.
06
UNIT – II Kinetics of enzyme catalysis including immobilized enzyme technology
hrs.
Kinetics of substrate utilization product formation and biomass production in 07
UNIT – III
cell culture. hrs.
07
UNIT – IV Transport phenomena in Bioprocess systems.
hrs.
05
UNIT – V Aeration/Agitation/Media sterilization/Air fertilization.
hrs
06
UNIT – VI Design and analysis of bioreactors.
hrs.
03
UNIT – VII Downstream processing techniques.
hrs.
Industrial Biotech products – Ethyl alcohol based on various substrates
07
UNIT – VIII including lignocelluloses. Penicillin citric Acid, SCP, Bio-fertilizers, Baker’s
hrs.
yeast – other modern biotech products.
REFERENCES
1 Bailey & Ollis, ‘Biochemical Engineering’,2nd Ed, McGraw – Hill, 1986.
2 Moo-Young, ‘Comprehensive biotechnology’ Vol I to V, Elsevier, 1984.
3 Belter, Cussler and Hu, ‘Bioseparations’ Wiley, 1988.
Contact Details :
Type of the Program: SS. of B.EIVChemical
Year IV PAPER CODE: CHL1807 CREDIT
PAPER NAME ELECTIVE II: D PETROCHEMICAL
Semester II TECHNOLOGY HOURS 45
Scope of Petrochemical industry in India, Feedstock for petrochemicals 03

UNIT – I
hrs.
Naphtha cracking/Gas Cracking – separation and purification of cracker 06
UNIT – II
products (olefins and diolefins) hrs.
Production and purification of synthesis gas. C1 based petrochemicals 06
UNIT – III
(methanol, formaldehyde, acetic acid etc.) hrs.
Petrochemicals from various unit processes like oxidation, dehydrogenation,
12
UNIT – IV chlorination, oxychlorination, ammoxidation, hydration, dehydration,
hrs.
nitration, polymerization etc.
Aromatics production, isolation of aromatics, separation of C8 aromatics.
12
UNIT – V Benzene derivatives, ethylbenzene, styrene etc, xylene derivatives, phthalic
hrs
anhydride, terpthalic acid, dimethyl terpthalate etc.
Miscellaneous aspects of petrochemical production: Safety and Health
06
UNIT – VI aspects, environmental aspects, Clean Technologies, Future beyond
hrs.
Petroleum.
REFERENCES
P. Desikan and T.C. Sivakumar, ‘Unit processes in Organic Chemical Industries’, IIT Madras,
1.
1982.
2. E.C. Leonard, ‘Vinyl and Diene Monomers’, Wiley 1969.
3. H.G. Franck & J.W. Stadelhofer, ‘Industrial Aromatic Chemistry’, Springer Verlag, 1988.
Contact Details :
CORE / ELECTIVE / FOUNDATION 1 :ELECTIVE
Year IV CREDIT
PAPER CODE: CHL1810
PAPER NAME: ELECTIVE D:POLYMER
PROCESSING
Basic aspects of Polymers: Functionality, types, structure-property 04

UNIT – I relationship, processing fundamentals, processing aids and additives. hrs.
Morphology, rheology and flow of polymers. 06
UNIT – II
hrs.
Heat and mass transfer in polymer systems, mixing of polymers, mixing 07
UNIT – III equipments. hrs.
Extrusion of polymers, extrusion equipment, calendering. 10
UNIT – IV
hrs.
Moulding of polymers: Blow, compression, transfer, rotational and 10hrs
UNIT – V
injection moulding techniques, analysis and equipments.
Other processing techniques: Sheet forming, fiber spinning, pultrusion, 08
UNIT – VI techniques and equipments. hrs.
REFERENCES
1. B.R.Gupta, ‘Polymer Processing Technology’, Asian Books Pvt. Ltd, 2008
2. Z. Tadmor and C.G.Gogos, ’Principles of Polymer Processing’ John Wiley and Sons, 1979
Contact Details :
Year IV CREDIT
PAPER NAME : PETROLEUM REFINERY
ENGINEERING
Development of Petroleum Refining industry in India. Crude evaluation 04

UNIT – I
and Testing of refinery products. hrs.
Primary processing of crude, preparation, atmospheric and vacuum 05
UNIT – II
distillation, flow sheets process, conditions and Equipment. hrs.
Catalytic cracking and hydrocracking. Principles, feed-stocks, catalysts and 08
UNIT – III
hardware hrs.
Catalytic reforming: Principles, feed-stocks, catalysts and hardware. 06
UNIT – IV
Extraction of aromatics hrs.
06
UNIT – V Vis-breaking, coking, isomerization, alkylation and polymerization
hrs
04
UNIT – VI Treatment of petroleum products. Hydrodesulphurization.
hrs.
Refining of Lube distillates: Deasphalting, solvent extraction, dewaxing 08
UNIT – VII
etc. Production of bitumen, waxes and greases hrs.
04
UNIT – VIII Processing natural and associated gases.
hrs.
REFERENCES
1. James Speight, "The Chemistry and technology of petroleum", 2nd ed., Marcel Dekker, 1991
2. R.A. Meyers, ’Handbook of Petroleum refining processes’, 3rd Ed., McGraw-Hill, 2004.
3. Nelson, ‘Petroleum Refining Engineering’, McGraw-Hill, 1949
4. B. K. Bhaskar Rao, "Modern Petroleum Refining Processes", Oxford and IBH, 1984
Contact Details :
Year IV CREDIT
PAPER CODE : 1805
Semester VIII PAPER NAME : PROJECT HOURS
Identify a suitable product and prepare a detailed project report or the product will
UNIT – I be assigned to them by the department to work out the project report. The report
has to be submitted at the end of SS BE IV for evaluation.

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The Maharaja Sayajirao University of Baroda

Faculty: Technology and Engineering

Name of the Program: B.E.- II CHEMICAL

Properties of particulate solid

Nature of Fluids, Fluid statics and its applications, Manometers, Pressure 06

Molecular diffusion in fluids: 08

Name of the Program : B.E. CHEMICAL

Liquid–Liquid extraction: Extraction equilibria and its graphical

Selection of Materials of Construction for Process equipments and

Thermodynamic functions and relations for mixtures:

Chemical Industries in India: An overview, Unit Process concept, 02

Modes of heat Transfer: Transfer by conduction. General differential

Fundamentals of heterogeneous reacting systems, the influence of mass 08

Introduction to chemical kinetics, types of reactions, kinetics of 04

Introduction to measurement: instruments for measurement of process

Introduction & Basic Concepts, Polymer based industries and feedstocks. 02

Types of hazards in the chemical industry, accident and loss statistics, 04

The role of transport phenomena in the understanding of chemical

Basics of Catalysis: Emergence of catalysis science & technology, a brief 03

The structure of separation processes, definitions of separation and separative

Prospecting for petroleum, exploration methods, reserve appraisals, 05

Role of Modeling, Simulation and Optimization (MSO) in process design – 02

Introduction, role of process synthesis in process design, hierarchy of

Nanotechnology foundations: Definition, historical perspective, effects of 03

Introduction to Biotechnology. Basic microbiology and recombinant DNA 04

Scope of Petrochemical industry in India, Feedstock for petrochemicals 03

Basic aspects of Polymers: Functionality, types, structure-property 04

Development of Petroleum Refining industry in India. Crude evaluation 04

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