Chemical Reactions

International University, Vietnam National University - HCMC 1
GENERAL CHEMISTRY LABORATORY
REPORT1
EXPERIMENT 1: CHEMICAL REACTIONS
Deadline: Right before Experiment 2 starts
Group: _________4_____ Section: ______________
Group members: ______________Phạm Thế Đức_________________
______________Phạm Quốc Khánh_________________
______________Võ Phạm Minh ĐĂng_________________
______________Trịnh Hoàng Huy_________________
Date: _________
Score: _________
1
This report must be typed and handed in together with the signed data sheet by the deadline
Revision: 2014.10.11 Semester I, 2014-2015
1. Reactions of Cu2+
Reaction Observation Chemical Equation

0.5M CuSO4 2NaOH + CuSO4 → Na2SO4 + Cu(OH)2
+ 2M NaOH
Precipitation: Cu(OH)2
Color: Sky blue

0.5M CuSO4 4NH4OH + CuSO4 → 4H2O+
+ 2M NH4OH [Cu(NH3)4]SO4
Precipitation Cu(OH)2,add
more NH4OH the
precipitation changes from
sky blue to dark blue

0.5M CuSO4 CuSO4+ K4[Fe(CN)6] → 2K2SO4
+0.5M K4[Fe(CN)6] +Cu2[Fe(CN)6]
The solution turn from sky

blue toslightly red, a little
precipitation at bottom is
red and brown

Comments:
2. Reactions of silver halides

KCl + AgNO3→ AgCl + KNO3
0.5M KCl
+ 0.1M AgNO3
Precipitation AgCL, color:
white
0.5M KCl KCl + AgNO3 + NH4OH→ AgCL + KOH +
+ 0.1M AgNO3 NH4NO3
+ 2M NH4OH
Precipitation AgCL, add
more nh4OH solution turn

to noncolor
0.5M KCl
+ 0.1M AgNO3
+ 2M KCN
0.5M KBr KBr + AgNO3 → KNO3 + AgBr
+ 0.1M AgNO3
Precipitation AgBr, color:
slightly yellow
0.5M KBr KBr + AgNO3 + NH4OH → AgBr + KOH +
+ 0.1M AgNO3 NH4NO3
+ 2M NH4OH
Precipitation AgBr add
more NH4OH,
precipitation remake
solution changes from
noncolor to white
0.5M KBr
+ 0.1M AgNO3

+ 2M KCN
0.5M KI KI + AgNO3→ KNO3 + AgI
+ 0.1M AgNO3
Precipitation orange
yellow
0.5M KI KI + AgNO3+ NH4OH → AgI +
+ 0.1M AgNO3 KNO3+NH4OH
+ 2M NH4OH
Precipitation brown yellow
AgI
0.5M KI
+ 0.1M AgNO3
+ 2M KCN
Comments:

3. Reactions of H2O2

0.1M KMnO4 2KMnO4 + 3H2SO4 + 5H2O2→ 8H2O + 2MnSo4 +
+ 2M H2SO4 5O2 + K2SO4
+ H2O2
The solution KMnO4
Color purple turn to
noncolor,vaporization
0.1M KI KI + H2SO4 + H2O2 → H2O+ K2SO4 +I2
+ 2M H2SO4
+ H2O2
The solution from
noncolor to yellow
brown
H2O2 O2↑ H2O2 + MnO2 → MnO+H2O+O2
+ MnO2
Comments:

4. Reactions of Nitrate

1M NaNO3 2NaNO3+ 6FeSO4+ 4H2SO4 → 3Fe2(SO4)3+ 4H2O
+ FeSO4 +Na2SO4+2NO
+ concentrated
H2SO4
NO↑:smell heavily.
Color of solution
:from noncolor to
brown
1M NaNO2 2NaNO2+ 2FeSO4+ 2H2SO4 → Fe2(SO4)3+ 2H2O
+ FeSO4 +Na2SO4+2NO
+ concentrated
H2SO4
↑NO:Brown red
color,mix tube gently
the color turn from

black to non color

1M NaNO3 NaNO3+ 2FeSO4+ 6CH3COOH → 2(CH3COO)3Fe
+ FeSO4 +2SO3 + 3H2O
+ concentrated
CH3COOH
Color of solution
:Brown red color,mix
tube gently the color
changes from dark
green to black
Comments:
5. Reactions of KMnO4

0.5M Na2SO3 5Na2SO3 + 3H2SO4 + 2KMnO4 → 3H2O +
+ 2M H2SO4 2MnSO4 +
+ 0.1M KMnO4 5Na2SO4 + K2SO4
The color of KmnO4

Turn from purple to
noncolor
0.5M Na2SO3 2KMnO4 + Na2SO3 + 2NaOH → H2O + Na2SO4 +
+ 6N NaOH K2MnO4 + Na2MnO4
+ 0.1M KMnO4
The color of KmnO4
Turn from purple to
slightly green.mix
tube gently milk
coffee color
0.5M Na2SO3 2KMnO4+H2O+3Na2SO3 → 2KOH+3Na2SO4 +
+ H2O 2MnO2
+ 0.1M KMnO4
Precipitation The
color of KmnO4 Turn
from purple to
noncolor
Comments:
6. Reaction of Potassium Dichromate (K2Cr2O7)

2M K2Cr2O7 C2H5OH + H2SO4 + K2Cr2O7→CH3COOH +
+ 6M H2SO4 H2O + K2SO4 + Cr2(SO4)3
+ C2H5OH
Solution divide into 3
part, 3 color black,
brown orange,
slightly blue. The
tube is hotter
Comments/Conclusions:
7. A. Reactions of Fe3+


0.5M FeCl3
+ 0.5M KCN
0.5M FeCl3 FeCl3 + 3KSCN → 3KCL+ Fe(SCN)3
+ 0.1M KSCN
Solution tuwrn from

brown to blood color
0.5M FeCl3 FeCl3 + 3KOH → Fe(OH)3 + 3KCL
+ 2M KOH
Precipitation red
brown
0.5M FeCl3 4FeCl3 + 3K4[Fe(CN)6 → Fe4(Fe(CN)6)3 + 12 KCl
+ 0.5M K4[Fe(CN)6]
Precipitation : Dark
blue

0.5M FeCl3 FeCl3 + 3NH4OH → 3NH4Cl + Fe(OH)3
+ 2M NH4OH
Precipitation dark
brown
Comments:
7. B. Reactions of Fe2+

0.5M FeSO4
+ 0.5M KCN
0.5M FeSO4 2FeSO4 + KSCN → K2SO4 + Fe(SCN)2

+ 0.1M KSCN
Solution changes
from yellow to dark
brown

0.5M FeSO4 FeSO4 + 2KOH → Fe(OH)2 +K2SO4

+ 2M KOH
Precipitation:
Fe(OH)2 Color slightly
green
0.5M FeSO4 2FeSO4 + K4[Fe(CN)6] → Fe2[Fe(CN)6] +
+ 0.5M K4[Fe(CN)6] 2K2SO4
Precipitation, color
slightly green, mix
tube gently more
blue
0.5M FeSO4 FeSO4 + 2NH4OH → Fe(OH)2 + ( NH4) 2SO4
+ 2M NH4OH
Precipitation Fe(OH)2
color slightly green
Comments:

8. Reactions of Al3+

0.5M Al2(SO4)3 Al2(SO4)3 + 6NaOH → 2Al(OH)3 +3Na2(SO4)
+ 2M NaOH
Precipitation white
0.5M Al2(SO4)3 Al2(SO4)3 + 3NaOH + 3HCl→3NaCl + Al2O3 +
+ 2N NaOH 3H2SO4
+ 2M HCl
Precipitation white
color, add more hcl
precipitation
dissappeared
0.5M Al2(SO4)3 Al2(SO4)3 + 6NaOH → 2Al(OH)3 +3Na2(SO4)
+ 2M NaOH Al(OH)3 + NaOH → NaAlO2 + 2H2O
+ 2M NaOH
Precipitation white

then precipitation
disappeared
Comments:
9. Flame test
Solution Dominant flame Wavelength Frequency Photon energy

color (m) (s1) (J)
LiCl violetflame 423 709220 4.6*10^-28
NaCl Orange flame 609 492611 3.2*10^-28
KCl Blue-violet 455 659341 4.3*10^-28
flame
CaCl2 Red orange 622 482315 3.1*10^-28
flame
BaCl2 Yellow-green 577 519931 3.4*10^-28
flame
Comments:






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International University, Vietnam National University - HCMC 1

GENERAL CHEMISTRY LABORATORY

Group: _________4_____ Section: ______________

Group members: ______________Phạm Thế Đức_________________

______________Phạm Quốc Khánh_________________

______________Võ Phạm Minh ĐĂng_________________

______________Trịnh Hoàng Huy_________________

Reaction Observation Chemical Equation

Color: Sky blue

more NH4OH the

precipitation changes from

sky blue to dark blue

+0.5M K4[Fe(CN)6] +Cu2[Fe(CN)6]

The solution turn from sky

Revision: 2014.10.11 Semester I, 2014-2015

blue toslightly red, a little

red and brown

2. Reactions of silver halides

Reaction Observation Chemical Equation

Precipitation AgCL, color:

+ 0.1M AgNO3 NH4NO3

Precipitation AgCL, add

more nh4OH solution turn

Revision: 2014.10.11 Semester I, 2014-2015

Precipitation AgBr, color:

+ 0.1M AgNO3 NH4NO3

Precipitation AgBr add

solution changes from

Revision: 2014.10.11 Semester I, 2014-2015

+ 0.1M AgNO3 KNO3+NH4OH

Precipitation brown yellow

Revision: 2014.10.11 Semester I, 2014-2015

Reaction Observation Chemical Equation

+ 2M H2SO4 5O2 + K2SO4

The solution KMnO4

Color purple turn to

The solution from

Revision: 2014.10.11 Semester I, 2014-2015

Reaction Observation Chemical Equation

color,mix tube gently

the color turn from

Revision: 2014.10.11 Semester I, 2014-2015

black to non color

+ FeSO4 +2SO3 + 3H2O

:Brown red color,mix

tube gently the color

changes from dark

Reaction Observation Chemical Equation

+ 0.1M KMnO4 5Na2SO4 + K2SO4

The color of KmnO4

Revision: 2014.10.11 Semester I, 2014-2015

Turn from purple to

+ 6N NaOH K2MnO4 + Na2MnO4

The color of KmnO4

Turn from purple to

tube gently milk

color of KmnO4 Turn

Group: _______4_ Section: ____________

Group members: Phạm Thế Đức___

Phạm Quốc Khánh___

Võ Phạm Minh ĐĂng___

Trịnh Hoàng Huy___