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Dense Medium Separation
Dense Medium Separation
INTRODUCTION
Dense Medium Separation(DMS) is the primarymethod used within the diamondindustryfor the
concentrationof diamondbearingore and dense mediumcyclonesnow representthe major primary
concentratingequipment. To reducedownstreamoperatingand equipmentcosts,it is essentialthat
this concentrationstage should reject the maximum amount of low-densityore, in addition to
maintainingoptimumdlamondrecovery.Two main classesof separatorshave been used i.e' bath
forcetypes.The mainfocus of this documentwill be on the centrifugalforcetype DMS
and centrifugal
separator.Bathtype separators(staticcone separators)will be brieflydiscussed.
OF OPERATIONAND MANAGEMENT
2. PRINCIPLES
The materialflow circuit is where the ore from the preparationsection is mixed with the
followedby separationwithinthe dense mediumcycloneand medium
medium(ferrosilicon),
7-1
removalafter separation.The materialreports to a sink (concentrate)or a float (tailings;
section.The medium flow circuitcan be divided into a correct medium circuitand a dilute
medium circuit. The dilute medium circuit consists primarilyof ferrosiliconrecovery anc
contaminantsremoval.Effluentfrom the float and sink washingscreensreportsto the dilute
mediumcircuitwherethe ferrosiliconis recoveredvia magneticdrum separatorsand recyclec
back to the correctmedium circuit.The correctmedium circuitconsistsof the densification
circuitand the mixingof correctmediumwith ore. The reologyof the correctmediumdepends
on the mediumproperties,and is diagnosticof the densityseparation.
2.2. Managementlssues
MediumProoerties
Ore Properties
Materialfeedrate
Ore feed size
Qualityof ore preparationbeforeDMS treatment
Ore characteristics
OperationalParameters
PhysicalDM CycloneProperties
7- 2
Magnetic drum separator performance(influencedby pickup gap, discharge gap,
magnetposition, and magneticloading)
volumetric
contentof magneticseparatoreffluent
Ferrosilicon
Productscreenadhesionlosses(determinedby screenvelocity,screentime, bed depth'
wash water,ore porosityand shaPe)
Housekeeping
Corrosion.
TYPICALEFFICIENCIES
3 . 1 . SeparationEfficiency
3.1.1. Methods
7- 3
size and densitythat reportsto one or other product(sink or float). This separation
curveis also knownas a Tromp curve.The Tromp curveis illustrated'in Figure l.
SEPARATIONCURVE
100
90 I
80
70 A,
'6 /
60
1 s o /
:<
I
; 4 0
30
:_L
20
10 -/'1
0
sG25 SG50 sc75
From this curve the SGso and the Ep values are determined.The SG5e value
(commonlyreferredto as the cut-point)is the pointwhere all particleswith this
specific
density,have an equal chance(50% probability)of reportingeitherto sinks or to floats
The Ep (Ecart ProbableMoyen)value (commonlyre'ferredto as the efficiencyor the
sharpnessof separation)can be calculatedby meansof the followingequation:
SG"-L9t'
Eo:
z
3.1.2. Application
ldeally,one must conducta tracertest with tracerssimilarin size to that of the average
diamondrecovered.Usuallythe averagesize diamondrecoveredis less than 1 mh
(square mesh). Conducting a tracer test with 2 mm or smaller tracers can
be
problematic,as the tracersare difficultto recoverand "hangup" withinthe circuit.
practicalpoint of view, it is suggestedto utilise 2 mm tracers only as an
from a
indicationthat diamondlossesdo not occur in the fine size ranges.Togetherwith this.
4 mm tracerscan be utilisedto establisha relativecut point anO fp vJlue. lf changes
7-4
are madeto the cycloneor wear partsare replaced,a full tracertest can be conducted
with the 4 mm tracers.Since a relativecut point and Ep value has been established
with the 4 mm tracers,it will be possibleto determinewhetherthe cycloneperformance
has been enhancedor not. The effectof each operationalparametercan be linkedto
the separationcurve.
3.2. MediumConsumptionEfficiency
3.2.1. Methods
7-5
Of these the adhesion and effluent losses are generally the most significant
lossesare frequentlythe largestsinglecomponentof the operatingcostsof
Ferrosilicon
densemediumplants,amountingto 10-4oo/o of dense mediumplantoperatingcosts.
3.2.2. Application
4. OPERATINGCONDITIONS
4.1.1.1. CycloneDiameter
The major role of cyclone diameter is the effect that it has on centrifugal
acceleration. Higher accelerationsare required for finer particles in an
7-6
attempt to overcome the drop in separationefficiencyas a function of
decreasingparticlesize. The cyclonediameterselectedwill in-turnstipulate
the minimumoperatinghead, maximumparticlefeed size and the resultant
volumetriccapacity.
7-7
4.1.1.2. BarrelLength
4.1"1.3. VoftexFinder
4.1.1.4. lnlet
The inlet diametercan vary between 0.2D to 0.27D. The larger inlet wili
resultin an increasedcyclonecapacityand a reducedwear rate in the barrel
sectionof the cyclone. Cyclonesare suppliedwith rectangular,square or
circulartangentialfeed openings. Involute inlets (rectangularor sQUarar
result in reduced inlet turbulence(+ 40%), higher density differentialsanc
increasedcapacities. Generallystated, "involute"designsgive moderately
higher differentials in comparison to the "tangential" designs, bui
deteriorationin efficiencyalso startsat a higherdifferential.
The top of the inlet should be flush with the roof of the cycloneto eliminate
any "deadspace"which assistsin shortcircuitingand particlehang-up.
Increasing
the openingsize:
. Increasesthe cyclonethroughput
. Increasesthe densitydifferential
o Increasesthe cycloneseparationefficiencyto an optimumfollowedby a
reductionin separationefficiency.
4.1.1.5. SpigotDiameter
7- B
reduce particlehang-upwithin the cone section of a cyclone and the
resultant wear rate. However, the increase in spigot diameter is
associatedwith a reductionin separationefficiencyand hencecufpoint.
the densitvdifferential
4.1 1 6 ;",::;s
4.1.1.7. CycloneComponents
4.1.2.1. On-LineNon-ContactNuclearGauges
Although these devices involve slightly higher capital costs, they have
nonethelessprovenextremelycost efficient.The mainreasonsare:
. Long lifeexpectancy
. Simpleand quickmaintenance
o Solid-statesensingand actuationof the process
7- 9
There are three main types of radiationdevices in use today;the phola
multiplieriscintillatorcounter, the Geiger Muller tube and the ionisatioe
chamber.
r Beta- electronemissiononly
. Gamma - this radioactiveemissionis similarto that of radio and ligh
waves in that it is basically electromagneticin form, although oi
a
differentmagnitudeof frequency. This llectromagnetic radiationalsc
exhibits particle acceleration characteristics,the particles beins
termedphotons.
,commonly
see rable 2 for the energyleveland half-lifeof severalradioactivesources.
4.1.2.2. Safety
7-10
Aeration(air bubbles)is a commonfault which has detrimentaleffectson
densitygaugesand is not easilynoticed.Air is suckedintothe pump due
to poor sealsor cavitation.Sump level controlplus correctlydesignedin-
flowswillcurethis problem.
The source decay will cause a slow change in the calibrationof the
density gauge. This change commensuratewith other slow changes
taking place in the electronicsystem as well as pipe wear or scaling,
resultsin the needfor "standardisation".
'7
1,1
, - l l
. Densitysensorassembly
. UNIPROtransmitter
. Standardisation
. Theoreticalcalibration
. Two pointcalibration
. Absorberset-uo
. Calibrationchecks
A high viscosityresultsfrom:
r Highmediumdensity
r Fine particlesize distribution(fineferrosilicon)
7-12
. lrregularshapedparticles(milledferrosilicongrade)
. The presenceof low densitycontaminating
solids
. Magnetisation
of the medium
A low viscosityresultsfrom:
o Low mediumdensity
. Coarseparticlesize distribution(coarseferrosilicon)
. Smoothroundedparticles(atomisedferrosilicongrade)
. A clean,de-magnetised, medium
uncontaminated
The stabilityof the medium is the tendency of the medium solids to settle out. All
conventionaldense mediumis inherentlyunstable.The reciprocalof the rate at which
the medium settles out under gravity is a measure of the stability.In general it is
desirableto have a stablemediumbecauseif the mediumsettlesout too readily,then
separators,pipelinesand pumps will sand up. With an unstablemedium,strong
densitygradientscan result in the separator,which will detractfrom the separator's
performance.The differencebetweenthe underflowdensityand the overflowdensityis
calledthe differential.Densitydifferentialsin cyclonicseparatorsshould not exceed
400-500kg/m'. Operatingconditions,includingmedium grade should be tuned to
therebymaximisingthe separationefficiency.
optimisethe differential
4.1.5. Inversion
7-13
It has been suggestedthat to maintaininversionessentiallyrequiresa residencetime
that is sufficientto allow the slowly settlingsolids to migraieto the overflowwhich, rn
turn, impliesa slow rate of revolution,a high inletvelocityloss factorand a low cyclone
velocityconstant. These are all associatedwith a medium operatingwitfr i nigl
viscosity. Pointsmay thereforeexist withinthe cycloneat which solid bJdy rotationis
approached' A situation,which is reinforcedby the presenceof high yieid stresses
Minimal variationin the tangentialvelocitywill thereforebe experiencedacross the
radiusof the cyclone.
' The coarsergrades are preferredto finer grades becauseunder most conditions
mediumlossesoccur preferentiallyin the finer sizes.The coarsergradesare ofter-
also cheaper.
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r Atomised ferrosiliconwill also be preferred when operating under corrosive
conditionsor wherehighlyporousgroundis to be treated.
Tables 3,4,5 and 6 list the required particle size distributions,bulk chemical
compositionsand relevant physical data that have to be adhered to by the
manufacturersof ferrosilicon.The followingqualityassuranceprovisionshave been
implementedto ensure that the final ferrosiliconproduct conforms to the required
specifications:
7 -15
Table 4: Particle Size Distributions - Atomised Ferrosilicon
Silicon: + 0.2%
Carbonwith 1.0%maximumcontent: + 0.05%
Carbonwith 0.5% maximumcontent: + 0.02%
lron: + 0j%
Referto lable 6 for the applicablephysicaldata.
7-16
Table 6: Ferrosilicon Physical Data
a) Reducedpumpmaintenance
(glandpacking,voluteand impellerreplacement).
. Pressurestability
e Actualpressure
As mentionedearlier,fluctuationsin cyclone inlet pressurecan have a detrimental
effect on separationefficiency.ldeally,the cyclone inlet pressureshould remain as
7-17
stableas possibleunder feed conditions.This is achievedby monitoringthe follow,^,3
factors:
7-18
lf a DMS plant does not have an adequatepressurecontrol system with pressure
transducerson all operationalcyclones,the managementof the DMS plantwill become
problematic.A pressure reading is the closest one can get to what is actually
happeninginsidethe cyclone.
The actualcyclone inlet pressureshould also not be too high or too low as this can
affectseparaiionefficiencynegatively.An idealoperatingpressurerangesfrom 10D to
12D.lf the oressureis reducedto less than 8.5D,the vortex insidethe cyclonewill "fall
flat",resultingin highyields.ldeallythe turbulenceof the feed to the cycloneand inside
the cycloneshouldbe reducedas much as possible.An increasein operatingpressure
will resultin an increasein cyclonewear rate and turbulencewithinthe cyclone. The
percentageof misplaced materialwill increase significantly.lt is thus possibleto
in"rea." the cut-pointof a dense mediumcyclonethat operateswith a low operating
pressure(12D) to well above 3.'15Um3 withoutthe danger of losingdiamonds.The
percentageof misplacedmaterial will be low. However,this cannot be done with a
cyc|one operating with a high operating pressure(+14D), as the danger of |osing
diamonds will increase Refer
significantly. to Figure2-
100
90
>fr-:.-
I __\_
80 t_Plqnno!ol.ossEs l-
70
o
; 6 0
I
o- 50
E<
E 4 0
=
()
30
I
20
, / l
10
./' I
o
sc5o
,o,"t-1Ti-n,
7-19
A ratio of less than 4:1 will affect the separationefficiencyadversely.Over-feedinga
cyclonewill result in spigot crowdingwhich in{urn can lead to diamond losses and
excessiveyields. Underfeedingcan lead to an increasein yield as a result of more
misolacedfloat materialin the concentrate.The use of excessivemedium is wasteful
of power and requiresextra screeningand cleaningcapacity. For a high degree of
concentrationmedium to ore ratios of 7:1 should be maintainedfor fine particle
separationand 5:1 for coarseparticleseparation.
Cyclonediameter(mm) M i n i m u mh e a d( m ) Maximumparticlesize(mm)
750 6.7 50
A'7
660
560 5 40
450 4 32
350 3.2 25
Feed preparationrefers to the removalof the finest fractionsfrom the crushed DMS
feed by wet screeningusing high-pressure water sprays. Factorsinfluencingeffective
feed preparationare volume of spray water, ore bed depth and residencetime o"
screen. Average recommendedspray water volume is 40m'ih per meter width o{
screen. This figure is an averageand will vary accordingto the size distributionof the
7 -20
ore. Ineffectivefeed preparationwill resultin the contamination of the correctmedium.
The screen must also ensure adequate drainageas to prevent excessivesurface
moistureon the ore particlesfrom significantly alteringthe circulatingmediumdensity.
The acceptableamount of fines in the feed preparationscreen oversize may not
exceed 7oh.
After separationhas taken place insidethe cyclone,the sink and float productreports
to the sink and float washingscreensrespectively. These screensare usuallydivided
into a drain and washing section. The ferrosilicon recoveredvia the drain section
usually reports to the correct medium circuit. Ferrosiliconrecoveredon the wash
sectionusually reports to the dilutemedium circuit.
Ferrosilicon is lost by way of adhesionon the rinsedscreenproduct.
Factorsinfluencingadhesionlosses are:
7-21
Table 8: Influence of Particle size on screen width and Rinsing watx
Requirements (relative requirement I mm = 1.0)
Flood boxes are preferredover sprays for washing with dirty water becau
they are less prone to wear and blockage. This is usually achieved
restrictingthe flow of materialover the screenbv meansof weirs or L-s
panels.
a Coarseore - 30t/mscreenwidth
a Fineore - 26tlmscreenwidth
4.2.1.2. Porosity
7-22
of feed - adheringlossesincreaseexponentially
Uniformdistribution with
bed depth and localisedthicker areas are very detrimentalto good
medium recovery. For good washing a bed depth no greater than 3
timesthe averageparticlediameteris required.
. feed preparation.
Inefficient
. Abrasionof ore particlesin the circuit.
r of agglomeratesnot brokendown on the feed preparationscreen.
Disintegration
4.2.2.1. lmprovedMagneticSeparatorDesign
. lmprovedmagnetdesignsproducinghigh intensityfieldstrengths.
7 -23
o Availabilityof largercapacitymachines.
Correctsizing of magneticseparators
7 -24
settingsand optimisationof the settingsis done whilstthe magnetic
separatoris in operation.The gap settingbetweenthe drum and the
discharge lip should be set at 5 mm smaller than the distance
between the drum and tank. On maintenanceday remove the
flangeson both sides of the tank and measurethe gap betweenthe
drumand the tank by usingan insidecaliper,this measurement must
be equal on both sides. Recordthe gap on both sides betweenthe
drum and the dischargelip. These dimensionsare to be recorded
for each magneticseparator.
lmportantto note is that if the bottom trough in the pick-up zone is not
concentricwith the drum, or is bowed parallelto the drum axis, performance
will be imoaired.lt is thus imoortantthat care needs to be taken to clean
ferrosiliconout of the separatorwheneverthe plantis shut down. lf this is not
done the ferrosiliconwill corrodeand form a hardscaleor accretion.This will
altergap settingsand distortthe magneticfield.
7 -25
4.2.3. Medium Densification
. Blockage
. Energyrequirements
4.2.4. Corrosion
Ferrosiliconis an alloy consistingof iron (Fe) and silicon (Si); there are therefore
discrete elements of silicon in a matrix of iron. lron which is exposed to the
environment,may corrode(oxidise)accordingto the followinggeneralreaction:
Fe e F e , * + x e . . . . . . . . . . . . . =. 9 y m V
. Clay slimes - the interactionof the green oxide corrosionproductand the slime
solids producesa viscousmedium,detrimentallyeffectingthe densityseparatior.
7 -26
The exact effectthat clays have on the rate of the corrosionprocessis not well
understoodbe it chemical(modifyingthe solubilityof the protectiveoxide layer)or
physical(abrasionor blindingof the alloysurfaceto oxygendiffusion).
. High concentrations
of chlorideions in solution,and
. A suitablereductionhalf reactionmust exist i.e. H' ions to form H2 (hydrogen
gas). This occursreadilyonly if the concentration of H* ions is high (i.e.low
pH) At high pH values, the concentrationof H* ions is relativelylow and
consequentlythe H-/Hz reduction half reaction and therefore corrosion is
suppress_ed.Carbondioxideshould be added to the water reticulationsystem
should a pH modifier be required. This will prevent the introductionof a
complexingagentintothe processstreamfor stabilising free Fe'* ions.
4.2.6. Housekeeping
7-27
4.2.7. General
The first hydraulicdense medium separatorequipmentused was the static cone separator
The functionof a DMS cone is to separatelight materialfrom heavymaterialusingferrosilicon
or magnetiteas a dense medium. Cones generallyoperateat a specificgravity of between
2.65 and 3.0 and the recommendedgrade ferrosiliconis 65D. Ore from the feed preparation
screen enters the DMS cone at a constantfeed rate. The cone agitatorensures that the
ferrosilicondoes not settleand that materialdoes not stick to the sides of the cone. The lighter
fractionof materialwill floatwith the heavierfractionsinkinE.
> Feedsize distribution- each classof separatorhas a fixed operatingrangein terms of feec
particlesize distribution.Bathstypicallyhave been used for particlesrangingfrom 6 mm to
1 5 0m m .
The top size that could be treatedusing a cone was traditionallydeterminedby the size of
the airlift. lt has been foundthat an airliftmore than 10 inchesin diameteris uneconomicin
air consumption.The ratio betweenairliftdiameterand maximumparticlesize is generally
takenas 2.5 or 3 to 1, givinga maximumparticlesizeof betweenz5 and 100 mm.
Feed mediumviscosity
Feedtonnage- overfeedingor over sizedmaterialcan resultin the cone chokino.
Componentsand relatedequipmentof the cone
. Powerdips
. Powerfailure
' Air failure- the cone has certainmajordisadvantages,
in that it requiresa largevolume
of air,thus increasingthe overallpowerconsumptionof the individualunit.
7 -28
a Reductionin air pressure
a A blockagein the air lift (if applicable)
a Worn air jets
a Defectiveor worn cone agitator.
LIFECYCLEMANAGEMENT
the
Life cycle managementimpliesthe maximisingof the life of equipmentparts withoutaffecting
overallprocessefficiencY.
5.1. EquipmentLife
The life cycle managementof all pumps, screen panels and accessoriesin the DMS is
life
discussedin othersectionsof this handbook.The primaryfocus of this sectionwill be on the
cycle managementof the DMS cyclone.Criticalreplacement parts on the DM cyclone are the
vortexfinder,spigot,overflowhood (if present),barrelsectionand inlet. Note that the vortex
plateat
finderlengthls ihe minimumverticaliengthfrom the lip of the vortexfindertube to the
the top of the inletsection.
Apartfrom all the high wear parts,it is also necessaryfor regularinspeclionof the inletsection
grooving'
and the cone section.Certainareas insidethese partsare exposedto high wear and
Instabilitygrooves at flanged ends (between inlet piece and cone and between cone and
spigot)can act as "inward steps"and can cause misplacement of diamonds'
7 -29
Cyclone parts should be run as close to the wear limits as possibleto ensure maximu-
'changed
efficiencyin the sectionbut shouldbe out' beforereachingthe wear limitif there is a^
obviousdefector severewear in one area that could lead to failureof the part.An example,s
the notch or bite that can develop at the bottom of the vortex finder. Cyclonesare usual-r
inspectedon a monthlybasis but where high operatingpressuresare present,the inspectior
frequencycan be increased.Cyclonesshould be inspectedimmediatelyif their performance
becomesunsatisfactorily.
As a general rule, the spigot diametershould not increaseto more than 10o/oof its origind
diameter(spigotsmust be regularlyinspectedand changedafter 3 to 6 mm diameterwear.,
Measurethe diameterat 45" intervalsand take the averaqeas the effectivediameter.All
wear areas should be replaced at the discretionof the Metallurgist.This should be do
accordingto the rule mentionedabove:
It is recommendedto change out the entire cycloneat one time, thus minimisingdown tirre-
Cyclonescould then be disassembledand individualcomponentsmeasuredfor the degree
wear in order to assesstheir suitabilitvfor re-use.Componentssuitablefor re-usewould t
cyclones,with specialattentionbeing paid to the componentjoints
be used in "refurbished"
ensurethe internalgeometryof the cycloneis acceptable.The use of oversizespigotswou
allow this procedureto be followed,thus making full use of low-wearcyclone componen
withoutcompromisingeithercycloneefficiencyor overallperformance.
6. SUMMARY
7-30
INEFFICIENTSEPARATION
choked water
Medium densitY Water entering the correct . Wash hopper
overflowinto drain hoPPer
remains low or mediumsumP via drain area
fluctuating. of screen. . Spray water rePorting to drain
section (sPraY water oPened
excessivelY)- adjust spray water
valve
o High percentage water entering
cyilone feed with ore - inefficient
de-watering bY feed PreParation
screen
of
Water entering the correct o Adjust underflow sPigots
to allow more
medium sumP via magnetic magnetic seParator
separatordischarge. water to effluent
e AdjustdischargegaPsetting
. Lowerthe magnet
. Underflowspigotspossiblychoked
7 -31
SEPARATION
INEFFICIENT
7 _2."
INEFFICIENTSEPARATION
'
No Problem Possible Causes PossibleSolutions i
5 Low efficiency lnletpressuretoo high . Reducemediumfeed to mixingbox
(HighEp value) while maintaining a minimurr
ratioof 5:1
medium:ore
. Reduce ore feed-rate but not
the cyclone
underfeeding
Mediumviscosityhigh a lncorrectmediumselection
a Replaceor cleanmedium
1. Napier-Munn,
T. J., DRL CY 05, Researchinto the operationand performance
of a 600 mm hea.
mediumcyclone,16 June 1985.
2 . Engelbrecht,
J. A. and BosmanJ., MultotecCyclones,Designcriteriafor an improvedlargediame:
densemediumcyclone.
1 2 .Trainingmanual,Densemediumseparation,
De Beers- FinschMine.
16. DiamondProcessing
Handbook,Proformastructure:Volume
4.
7-36
22. Malvern Engineering,Permanent Magnetic wet Drum Separators- Installation,operation and
maintenanceInstructions.
Napier-Munn,
T.J.,Densityinversionin densemediumcyclones.
IndustrialProcessMeasuring& Control,ProcessAutomation(Pty)Ltd.
7 -37