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Hot Filtration Melting Point Determination: NOT Closed
Hot Filtration Melting Point Determination: NOT Closed
Hot Filtration Melting Point Determination: NOT Closed
Simple distillation
-receiving flask in ICE bath
-water in NEAR receiving flask
-thermometer just below the side-arm of the
distillation head, outlet adaptor covers 3-way
distilling adaptor
-roundbottom flask w/ sample 1/2 - 2/3 full
a. same level of surr. water
b. boiling chips
c. heated
-glass joints are well-fitted!
-vacuum adapter open to air
-rate of dripping: 2 drops distillate/sec
-DO NOT distill to dryness
E8: Relative Rates of Bromination
Steam Distillation
-2 round-bottom flasks
– Both with HEAT ON
– Flask 1: 1/2 full water (w/ pressure
regulator)
– Flask 2: sample (closer to condenser,
w/ thermometer → mind the level)
– Connected thru steam glass tube
-UNSUBMERGED: thermometer, steam glass
tube
-SUBMERGED: pressure regulator
-Condenser and receiving flask
Reflux
• Receiving flask w/ condenser on top
– Water in nearest the flask
– Flask half full
– Surrounded by water/oil bath (same
level as flask)
• Hot plate: ON