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Lampiran 2. Perhitungan

A. Perhitungan Kadar

Diketahui :

Mr TTIP : 284,22 gr/mol

ρ : 0,967 gr/cm3

Target Sintesis : 2,73 gr

1.1. Menghitung % massa Ti 99,7 %

0,997 × Ar Ti Mr TTIP
massa TTIP = Mr Ti × × 2,73 gr
0,997 V0,003 O2 Ar Ti

0,997 × 47,9 284,22

= × × 2,73 gr
(0,997 × 47,9) + (0,003 × 50,94) + (2 × 16) 47,9

= 9,6809 gram
m 9,6809 gram
Volume TTIP = = 0,967 gram/cm3 = 10 mL
ρ

Massa atom Ti dalam TTIP

𝐴𝑟 (𝑇𝑖)
Ti (gr) = garam (gr) × 𝑀𝑟 (𝑔𝑎𝑟𝑎𝑚)

47,9 g/mol
Ti (gr) = 9,6809 gr × 284,22 g/mol

Ti (gr) = 1,6315 gr

1.2. Menghitung % massa V 0,3 %

0,003 × Ar V Mr V(acac)3
massa V(acac)3 = Mr Ti × × 2,73 gr
0,997 V0,003 O2 Ar V

0,003 × 50,94 348,2388

= × × 2,73 gr
(0,997 × 47,9) + (0,003 × 50,94) + (2 × 16) 50,94

= 0,0357 gram
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𝐴𝑟 (𝑉)
V (gr) = garam (gr) × 𝑀𝑟 (𝑔𝑎𝑟𝑎𝑚)

50,94 g/mol
V (gr) = 0,0357 gr × 348,2388 g/mol

V (gr) = 0,0052 gr