p-azidobenzoic acid

0,52 mmol

Methylene
Chloride

To dissolve

*
Cu Catalyst

To stirr
1-nitro-4-[(prop-2-yn-1-yl)oxy]benzene
0,50 mmol
Ethanol
20 min
100 W Reaction
100°C

*
CuI or Cu0NPS
 –
O OH O + O
N –
O
+ O
N
Cu Catalyst
+ O
O
OH
N
+ N O
– N N N
N

CH
p-azidobenzoic acid
0,52 mmol

Methylene
Chloride

To dissolve

*
Cu Catalyst

To stirr
1-nitro-4-[(prop-2-yn-1-yl)oxy]benzene
0,50 mmol
Ethanol

24 h in mild
Reaction
conditions

*
CuI or Cu0NPS