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ARTICLE 29

ACOUSTIC EMISSION STANDARDS

SE-650 Standard Guide for Mounting Piezoelectric Acoustic Emission Sensors . . . . . . . . . . . . . 657
[ASTM E 650-85
(1992)]

SE-976 Standard Guide for Determining the Reproducibility of Acoustic Emission Sensor
[ASTM E 976-84 Response . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 661
(R1988)]

SE-1211 Standard Practice for Leak Detection and Location Using Surface-Mounted Acoustic
[ASTM E 1211-87 Emission Sensors. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 669
(1992)]

SE-1419 Standard Test Method for Examination of Seamless, Gas-Filled Pressure Vessels
(ASTM E 1419-96) Using Acoustic Emission. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 674.1

655 A99

ASME B&PVC sec5$$u460 04-29-99 05:30:34 pd: sec5a Rev 14.04


SE-650 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-650

STANDARD GUIDE FOR MOUNTING


PIEZOELECTRIC ACOUSTIC EMISSION SENSORS
SE-650

[Identical with ASTM Specification E 650-85 (1992)]

1. Scope 3.1.5 waveguide, acoustic — a device that couples


acoustic energy from a structure to a remotely mounted
1.1 This document provides guidelines for mounting
sensor. For example, a solid wire or rod, coupled to
piezoelectric acoustic emission (AE) sensors.
a sensor at one end and to the structure at the other.
1.2 This standard does not purport to address all
of the safety problems associated with its use. It is 3.2 Definitions
the responsibility of the user of this standard to establish 3.2.1 For definitions of additional terms relating
appropriate safety and health practices and determine to acoustic emission, refer to Terminology E 610.
the applicability of regulatory limitations prior to use.

2. Applicable Documents 4. Significance and Use

2.1 ASTM Standards: 4.1 The methods and procedures used in mounting
E 610 Terminology Relating to Acoustic Emission AE sensors can have significant effects upon the per-
E 976 Guide for Determining the Reproductability of formance of those sensors. Optimum and reproducible
Acoustic Emission Response detection of AE requires both appropriate sensor-mount-
ing fixtures and consistent sensor-mounting procedures.

3. Terminology
3.1 Description of Terms Specific to This Standard: 5. Mounting Methods
5.1 The purpose of the mounting method is to hold
3.1.1 bonding agent — a couplant that physically the sensor in a fixed position on a structure and to
attaches the sensor to the structure ensure that the acoustic coupling between the sensor and
3.1.2 couplant — a material used at the structure- the structure is both adequate and constant. Mounting
to-sensor interface to improve the transfer of acoustic methods will generally fall into one of the following
energy across the interface categories:

3.1.3 mounting fixture — a device that holds the 5.1.1 Compression Mounts — The compression
sensor in place on the structure to be monitored mount holds the sensor in intimate contact with the
surface of the structure through the use of force. This
3.1.4 sensor — a detection device that transforms force is generally supplied by springs, torque-screw
the particle motion produced by an elastic wave into threads, magnets, tape, or elastic bands. The use of a
an electrical signal couplant is strongly advised with a compression mount

657
SE-650 1998 SECTION V SE-650

to maximize the transmission of acoustic energy through the plane of their face, very high viscosity couplant
the sensor-structure interface. or a rigid bond is recommended.
5.1.2 Bonding — The sensor may be attached 6.3.3 The thickness of the couplant may alter
directly to the structure with a suitable adhesive. In the effective sensitivity of the sensor. The thinnest
this method, the adhesive acts as the couplant. The practical layer of continuous couplant is usually the
adhesive must be compatible with the structure, the best. Care should be taken that there are no entrapped
sensor, the environment, and the test procedure. voids in the couplant. Uneveness, such as a taper from
one side of the sensor to the other, can also reduce
sensitivity or produce an unwanted directionality in the
6. Mounting Requirements sensor response.

6.1 Sensor Selection — The correct sensors should 6.3.4 A useful method for applying a couplant
be chosen to optimally accomplish the acoustic-emission is to place a small amount of the material in the center
test objective. Sensor parameters to be considered are of the sensor face, then carefully press the sensor on
as follows: size, sensitivity, frequency response, surface- to the structure surface, spreading the couplant uniformly
motion response, and environmental and material com- from the center to the outside of the sensor face.
patibility. When a multichannel acoustic-emission test is
being conducted, a subset of sensors with characteristics 6.3.5 In some applications, it may be impractical
similar to each other should be selected. See Guide E to use a couplant because of the nature of the environ-
976 for methods of comparing sensor characteristics. ment (for example, very high temperatures or extreme
cleanliness requirements). In these situations, a dry
6.2 Structure Preparation — The contacting surfaces contact may be used, provided sufficient mechanical
should be cleaned and mechanically prepared. This will force is applied to hold the sensor against the structure.
enhance the detection of the desired acoustic waves The necessary contact pressure must be determined
by assuring reliable coupling of the acoustic energy experimentally. As a rough guide, this pressure should
from the structure to the sensor. Preparation of these exceed 0.7 MPa (100 psi).
surfaces must be compatible with the construction mate-
rials used in both the sensor and the structure. Possible 6.3.6 Great care must be taken when bonding a
losses in acoustic energy transmission caused by coat- sensor to a structure. Surface deformation, which can
ings such as paint, encapsulants, loose-mill scale, weld be produced by either mechanical loading or thermal
splatter, and oxides as well as losses due to surface expansion, may cause a bond to crack, peel off, or,
curvature at the contact area must be considered. occasionally, destroy the sensor. Bond cracking is a
source of acoustic emission. A compliant adhesive may
6.3 Couplant or Bonding Agent Selection: work in some cases. If differential expansion between
6.3.1 The type of couplant or bonding agent the sensor, the bond, and the surface is a possibility,
should be selected with appropriate consideration for a suitable bonding agent should be confirmed by exper-
the effects of the environment (for example, temperature, iment.
pressure, composition of gas, or liquid environment)
6.3.7 When bonds are used, the possibility of
on the couplant and the constraints of the application.
damaging either the sensor or the surface of the structure
It should be chemically compatible with the structure
during sensor removal must be considered.
and not be a possible cause of corrosion. In some
cases, it may be a requirement that the couplant be 6.3.8 The use of double-sided adhesive tape as
completely removable from the surface after testing. a bonding agent is not recommended.
In general, the selection of the couplant is as important
from an environmental standpoint as it is from the 6.4 Mounting Fixture Selection:
acoustical standpoint.
6.4.1 Mounting fixtures must be constructed so
6.3.2 For sensors that are primarily sensitive to that they do not create extraneous acoustic emission
particle motion perpendicular to their face, the viscosity or mask valid acoustic emission generated in the struc-
of the couplant is not an important factor. Most liquids ture being monitored.
or greases will work as a couplant if they wet the
surfaces of both the structure and the sensor. For those 6.4.1.1 The mount must not contain any loose
few sensors which are sensitive primarily to motion in parts or particles.

658
SE-650 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-650

6.4.1.2 Permanent mounting may require special 6.5.1 An acoustic waveguide should be mounted
techniques to prevent sensor movement caused by envi- so as to ensure that its surface will not contact any
ronmental changes. materials that will cause signal damping in the
waveguide.
6.4.1.3 Detection of surface waves may be sup-
pressed if the sensor is enclosed by a welded on fixture 6.5.2 If acoustic waveguides are used, when
or located at the bottom of a threaded hole. The acoustic-emission source location is being performed,
mounting fixture should always be designed so that it the extra time delay in the waveguides must be ac-
does not block out a significant amount of acoustic counted for in the source location program.
energy from any direction of interest.

6.4.2 The mounting fixture should provide support 7. Verification of Response


for the signal cable to prevent the cable from stressing
7.1 After the sensor(s) are mounted on a structure,
the sensor or the electrical connectors. In the absence
adequate response should be verified by injecting acous-
of a mounting fixture, some form of cable support
tic signals into the structure and examining the detected
should be provided. Care should be taken to ensure
signal either on an oscilloscope or with the AE system
that the cable can neither vibrate nor be moved easily.
to be used in the test. If there is any doubt as to the
False signals may be generated by the cable striking
sensor response, the sensor should be remounted.
the structure and by triboelectric effects produced by
cable movement. 7.1.1 The test signal may be injected by an
external source such as the Hsu-pencil source, or a
6.4.3 Where necessary, protection from the envi- gas jet (helium or other suitable gas), or by applying
ronment should be provided for the sensor or sensor an electrical pulse to another sensor mounted on the
and mounting fixture. structure. For a description of these methods see Guide
6.4.4 The mounting fixture should not affect the E 976.
integrity of the structure being monitored. 7.2 Periodic Verification — On an extended acoustic
6.4.4.1 Permanently installed mounting fixtures emission test, it may be desirable to verify the response
must be constructed of a material compatible with the of the sensors during the test. Verification should be
structure. Possible electrolyte effects or other forms performed whenever circumstances indicate the possibil-
of corrosion must be considered when designing the ity of a change in the coupling efficiency.
mounting fixture. 7.3 Post Verification — At the end of an acoustic
emission test, it is good practice to verify that all
6.4.4.2 Alterations of the local environment by
sensors are still working and that there have been no
the mount, such as removal of the insulation, must be
dramatic changes in coupling efficiencies.
carefully evaluated and corrected if necessary.

6.4.5 The mounting fixture should be designed


to have a minimal effect on the response characteristics 8. Report
of the sensor. 8.1 Any report of the mounting practice should
include details of the sensor mounting fixture(s), surface
6.5 Waveguides — When adverse environments
preparation method, and the couplant that was used.
make direct contact between the sensor and the structure
undesirable, an acoustic waveguide may be used to
convey the acoustic signal from the structure to the
9. Keywords
sensor. The use of a waveguide inserts another interface
with its associated losses between the structure and the 9.1 acoustic emission; acoustic emission sensors;
sensor and will distort, to some degree, the characteris- acoustic emission transducers; AE; bonding agent;
tics of the acoustic wave. couplant; mounting fixture; waveguide

659
SE-976 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-976

STANDARD GUIDE FOR


DETERMINING THE REPRODUCIBILITY OF
ACOUSTIC EMISSION SENSOR RESPONSE
SE-976

[Identical with ASTM Specification E 976-84 (R1988)]

1. Scope and components contributing to the sensitivity, the


acoustic emission sensor is the one most subject to
1.1 This guide defines simple economical procedures
variation. This variation can be a result of damage or
for testing or comparing the performance of acoustic
aging, or there can be variations between nominally
emission sensors. These procedures allow the user to
identical sensors. To detect such variations, it is desir-
check for degradation of a sensor or to select sets
able to have a method for measuring the response of
of sensors with nearly identical performances. The
a sensor to an acoustic wave. Specific purposes for
procedures are not capable of providing an absolute
checking sensors include: (1) checking the stability of
calibration of the sensor nor do they assure transferabil-
its response with time; (2) checking the sensor for
ity of data sets between organizations.
possible damage after accident or abuse; (3) comparing
1.2 This standard may involve hazardous materials, a number of sensors for use in a multichannel system
operations, and equipment. This standard does not to ensure that their responses are adequately matched;
purport to address all of the safety problems associated and (4) checking the response after thermal cycling or
with its use. It is the responsibility of the user of this exposure to a hostile environment. It is very important
standard to establish appropriate safety and health that the sensor characteristics be always measured with
practices and determine the applicability of regulatory the same sensor cable length and impedance as well
limitations prior to use. as the same preamplifier or equivalent. This guide
presents several procedures for measuring sensor re-
sponse. Some of these procedures require a minimum
of special equipment.
2. Applicable Documents
2.1 ASTM Standards:
E 610 Terminology Relating to Acoustic Emission
E 650 Practice for Mounting Piezoelectric Acoustic Emis- 4. Principles of Application
sion Sensors
E 750 Practice for Measuring the Operating Characteris- 4.1 The procedures given in this guide are designed
tics of Acoustic Emission Instrumentation. to measure the response of an acoustic emission sensor
to an arbitrary but repeatable acoustic wave. These
procedures in no way constitute a calibration of the
sensor. The absolute calibration of a sensor requires a
3. Significance and Use
complete knowledge of the characteristics of the acoustic
3.1 Acoustic emission data is affected by several wave exciting the sensor or a previously calibrated
characteristics of the instrumentation. The most obvious reference sensor. In either case, such a calibration is
of these is the system sensitivity. Of all the parameters beyond the scope of this guide.

661
SE-976 1998 SECTION V SE-976

4.2 The fundamental requirement for comparing sen- by roughly machining all surfaces except where the
sor responses is a source of repeatable acoustic waves. sensor and exciter are mounted and coating them with
The characteristics of the wave do not need to be a layer of metal-filled epoxy.
known as long as the wave can be reproduced at will.
5.2.2 Gas-Jet Test Block — Two gas-jet test blocks
The sources and geometrics given in this guide will
are shown in Fig. 3. The block shown in Fig. 3(a) is
produce primarily compressional waves. While the sen-
used for opposite surface comparisons, which produce
sors will respond differently to different types of waves,
primarily compressional waves. That shown in Fig.
changes in the response to one type of wave will imply
3(b) is for same surface comparisons which produce
changes in the responses to other types of waves.
primarily surface waves. The “nonresonant” block de-
4.3 These procedures all use a metal test block. Such scribed in 5.2.1 can also be used with a gas jet in
a block provides a convenient mounting surface for order to avoid exciting many resonant modes. The
the sensor and when appropriately marked, can ensure blocks in Fig. 3 have been used successfully but their
that the source and the sensor are always positioned design is not critical. However, it is suggested that the
identically with respect to each other. A block also relative positions of the sensor and the jet be retained.
provides mechanical loading of the sensor similar to
that experienced in actual use. Care must be taken 5.3 Signal Sources — Three signal sources are
when using these blocks to minimize resonances in the recommended: an electrically driven ultrasonic trans-
block so that the characteristics of the sensor are not ducer, a gas jet, and an impulsive source produced by
masked by these resonances. breaking a pencil lead.

4.4 These procedures allow comparison of responses 5.3.1 Ultrasonic Transducer — Repeatable acoustic
only on the same test setup. No attempt should be waves can be produced by an ultrasonic transducer
made to compare responses on different test setups, permanently bonded to a test block. The transducer
whether in the same or separate laboratories. should be heavily damped to provide a broad frequency
response and have a center frequency in the 2.25 to
5.0 MHz range. The diameter of the active element
5. Apparatus should be at least 1.25 cm (0.5 in.) to provide measurable
signal strength at the position of the sensor under
5.1 The essential elements of the apparatus for these test. The ultrasonic transducer should be checked for
procedures are: (1) the acoustic emission sensor under adequate response in the 50 to 200 kHz region before
test; (2) a metal block; (3) a signal source; and (4) permanent bonding to the test block.
measuring and recording equipment.
5.3.1.1 White-Noise Generator — An ultrasonic
5.1.1 Block diagrams of some of the possible transducer driven by a white-noise generator produces
experimental setups are shown in Fig. 1. an acoustic wave that lacks coherent wave trains of
5.2 Metal Blocks — The design of the metal block many wave lengths at one frequency. This lack of
is not critical. However, the use of a “nonresonant” coherent wave trains greatly reduces the number and
block is recommended for use with an ultrasonic trans- strength of the mechanical resources excited in a struc-
ducer and is required when the transducer drive uses ture. Therefore, an ultrasonic transducer driven by a
any form of coherent electrical signal. The preferred white-noise generator can be used with a resonant
materials are aluminum and low-alloy steel. block having parallel sides. However, the use of a
“nonresonant” block such as that described in 5.2.1 is
5.2.1 Conical “Nonresonant” Block — The Beattie strongly recommended. The generator should have a
block, shown in Fig. 2, can be machined from a 10 white noise spectrum covering at least the frequency
cm (4 in.) diameter metal billet. After the bottom is range from 10 kHz to 2 MHz and be capable of an
faced and the taper cut, the block is clamped at a 10 output level of 1 V rms.
deg. angle and the top face is milled. The dimensions
given will provide an approximate circle just over 2.5 5.3.1.2 Sweep Generator — The ultrasonic trans-
cm (1 in.) in diameter for mounting the sensor. The ducer can be driven by a sweep generator in conjunction
acoustic excitation should be applied at the center of with a “nonresonant” block. Even with this block, some
the bottom face. The conic geometry and lack of any resonances will be produced that may partially mask
parallel surfaces reduce the number of mechanical the response of the sensor under test. The sweep
resonances that the block can support. A further reduc- generator should have a maximum frequency of at least
tion in possible resonances of the block can be achieved 2 MHz and the sweep speed should be compatible

662
SE-976 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-976

FIG. 1 BLOCK DIAGRAMS OF POSSIBLE EXPERIMENTAL SETUPS

with the XY recorder used. It is recommended that a enough energy is generated above 200 kHz for effective
sweep generator be used with an a-c voltmeter with a use with a spectrum analyzer.
logarithmic output.
5.3.2 Gas Jet — Suitable gases for this apparatus
5.3.1.3 Pulse Generator — The ultrasonic trans- are extra dry air, helium, etc. A pressure between 150
ducer may be excited by a pulse generator. The pulse and 200 kPa (20 to 30 psi) is recommended for helium
width should be either slightly less than one-half the or extra dry air. Once a pressure and a gas have been
period of the center frequency of the transducer (≤0.22 chosen, all further tests with the apparatus should use
ms for a 2.25 MHz transducer) or longer than the that gas and pressure. The gas jet should be permanently
damping time of the sensor, block, and transducer attached to the test block [see Figs. 3(a) and 3(b)].
(typically >10 ms). The pulse repetition rate should be
low (<100 pulses/s) so that each acoustic wave train 5.3.3 Pencil Lead Break — A repeatable acoustic
is damped out before the next one is excited. wave can be generated by carefully breaking a pencil
lead against the test block. When the lead breaks, there
5.3.1.4 The pulse generator should be used with is a sudden release of the stress on the surface of the
an oscilloscope and camera or, in single-pulse mode, block where the lead is touching. This stress release
with the counter in an acoustic emission system. Not generates an acoustic wave. The Hsu pencil source

663
SE-976 1998 SECTION V SE-976

FIG. 2 THE BEATTIE BLOCK

uses a mechanical pencil with a 0.3 mm diameter lead should be stored in a form that allows an easy compari-
(0.5 mm lead is also acceptable but produces a larger son, either with another sensor or with the same sensor
signal). The Nielsen shoe, shown in Fig. 4, can aid at a different time.
in breaking the lead consistently. Care should be taken
5.4.1 Preamplifier — The preamplifier, together
to always break the same length of the same type of
with the sensor to preamp coaxial cable, provides an
lead (lengths between 2 and 3 mm are preferred).1 The
electrical load for the sensor, amplifies the output, and
lead should always be broken at the same spot on the
filters out unwanted frequencies. The electrical load on
block with the same angle and orientation of the pencil.
the sensor can distort the low-frequency response of
The most desirable permanent record of a pencil lead
a sensor with low inherent capacitance. To prevent this
break is the wave form captured by a transient recorder
from occurring, it is recommended that short sensor
or oscilloscope.
cables (< 2 m) be used and the resistive component
5.4 Measuring and Recording Equipment — The of the preamplifier input impedance be 20 kV or greater.
output of the sensor under test must be amplified before The preamplifier gain should be fixed. Either 40 to 60
it can be measured. After the measurement, the results dB gains are suitable for most sensors. The bandpass
of the preamplifier should be at least 20 to 1200 kHz.
1 Pentel 2H lead has been found satisfactory for this purpose. It is recommended that one preamplifier be set aside

664
SE-976 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-976

FIG. 3 GAS-JET TEST BLOCKS

to be used exclusively in the test setup. However, it analyzer. A suitable spectrum analyzer should be capable
may be appropriate at times to test a sensor with the of displaying a spectrum covering the frequency range
preamplifier assigned to it in an experiment. from 20 kHz to 1.2 MHz. The amplitude should be
displayed on a logarithmic scale covering a range from
5.4.2 Spectrum Analyzers — A very useful instru-
at least 50 dB in order to display the entire dynamic
ment for testing sensor response is the spectrum ana-
range of the sensor. The spectrum can be recorded
lyzer. Spectrum analyzers can be used with acoustic
photographically from an oscilloscope. However, the
signals generated by ultrasonic transducers that are
most useful output is an XY plot of the spectrum as
driven by either white-noise generators or tracking-
shown in Fig. 5.
sweep generators, by gas-jet sources or by acoustic
signals, produced by any source, that are captured on 5.4.3 Voltmeters — An a-c voltmeter can be used
a transient recorder and replayed into the spectrum to measure sensor outputs produced by signals generated

665
SE-976 1998 SECTION V SE-976

by an ultrasonic transducer driven by a sweep generator.


The response of the voltmeter should be flat over the
frequency range from 10 kHz to 2 MHz. It is desirable
that the voltmeter either have a logarithmic output or
be capable of driving a logarithmic converter. The
output of the voltmeter or converter is recorded on an
XY recorder as a function of frequency.

5.4.3.1 The limited dynamic range of an rms


voltmeter makes it less desirable than an a-c averaging
voltmeter when used with a sweep generator. However,
a rough estimate of a sensor performance can be
obtained by using an rms or a-c sensor voltmeter to
measure the output of a sensor driven by a wide band
source such as a white-noise generator or a gas jet.

5.4.4 Acoustic Emission System — A sensor can


be characterized by using an acoustic emission system
and an impulsive source such as a pencil lead break
or an ultrasonic transducer driven by a pulse generator.
The acoustic emission count from a single pulse should
be measured at three different gain settings, spanning
at least 20 dB and with the lowest gain such that the
signal is only marginally detectable. An average of the FIG. 4 GUIDE RING FOR IMPULSIVE SOURCE
count from at least 10 pulses should be taken at each
gain level. Data recorded will be the average count,
gain setting and all other significant settings of the
acoustic emission system.
several measurements before the final data is recorded to
5.4.5 Transient Recorders and Storage Oscillo- ensure reproducibility. During the initial measurements,
scopes — The waveform generated by a sensor in display the preamplifier output on an oscilloscope to
response to a single pulse or a pencil lead break can see that the signals are not being clipped by overdriving
be measured and stored by a transient recorder, digital the preamplifier. Establish written procedures and follow
oscilloscope, or some other storage oscilloscope. This them to ensure reproducibility over long periods of time.
waveform can then be recorded either photographically
or, if the capability exists, on an XY recorder. Digitiza-
tion rates should be at least 10 samples per highest
frequency period in the waveform. Lower rates will
result in distortion of the wave shape. When comparing 7. Interpretation of Results
wave forms, emphasis should be placed on the initial
7.1 Short-term reproducibility of results, covering
few cycles and on the large amplitude features. Small
such actions as removing and remounting the sensor,
variations late in the waveform are often produced by
should be better than 3 dB if the test is conducted under
slight changes in the coupling or position of the sensor
normal working conditions. Long-term reproducibility of
under test.
the test system should be checked periodically by the
use of a reference sensor that is not exposed to the
risk of environmental damage. Variations of sensor
response greater than 4 dB indicates damage or degrada-
6. Procedure
tion, and the cause of the discrepancy should be further
6.1 Place the sensors under test on the test block investigated. While there are no set criteria for accept-
in as near to identical positions as possible. Use identical able limits of sensor degradation, a sensor whose sensi-
forces to hold the sensor and block together. A low- tivity had fallen by more than 6 dB would generally be
viscosity couplant is desirable to ensure reproducible considered unfit for further service in acoustic emission
and thin couplant thicknesses. For all setups, take measurements.

666
SE-976 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-976

FIG. 5 EXAMPLE OF AN X-Y RECORDER PLOT FROM A SPECTRUM ANALYZER


(150 kHz RESONANT SENSOR)

667
SE-1211 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-1211

STANDARD PRACTICE FOR


LEAK DETECTION AND LOCATION USING
SURFACE-MOUNTED ACOUSTIC EMISSION SENSORS
SE-1211

[Identical with ASTM Specification E 1211-87 (1992)]

1. Scope E 750 Practice for Characterizing Acoustic Emission In-


strumentation
1.1 This practice describes a passive method for
E 976 Guide for Determining the Reproductability of
detecting and locating the steady state source of gas
Acoustic Emission Response
and liquid leaking out of a pressurized system. The
E 1002 Method for Testing for Leaks Using Ultrasonics
method employs surface-mounted acoustic emission sen-
E 1316 Terminology for Nondestructive Examinations
sors (for noncontact sensors see Method E 1002), or
sensors attached to the system via acoustic waveguides
(for additional information, see Terminology E 1316),
and may be used for continuous in-service monitoring
and hydrotest monitoring of piping and pressure vessel
systems. High sensitivities may be achieved, although
the values obtainable depend on sensor spacing, back- 3. Summary of Practice
ground noise level, system pressure, and type of leak.
This practice is not intended to provide a quantitative 3.1 This practice requires the use of contact sensors,
measure of leak rates. amplifier electronics, and equipment to measure their
output signal levels. The sensors may be mounted
1.2 The values stated in inch-pound units are to be before or during the test period and are normally left
regarded as the standard. SI units are provided for in place once mounted rather than being moved from
information only. point to point.

1.3 This standard does not purport to address all 3.2 Detection of a steady-state leak is based on
of the safety problems, if any, associated with its use. detection of the continuous, broadband signal generated
It is the responsibility of the user of this standard to by the leak flow. Signal detection is accomplished
establish appropriate safety and health practices and through measurement of some input signal level, such
determine the applicability of regulatory limitations as its root-mean-square (RMS) amplitude.
prior to use.

3.3 The simplest leak test procedure involves only


detection of leaks, treating each sensor channel individu-
ally. A more complex test requires processing the signal
2. Applicable Documents
levels from two or more sensors together to allow
2.1 ASTM Standards: computation of the approximate leak location, based
E 650 Guide for Mounting Piezoelectric Acoustic Emis- on the principle that the leak signal amplitude decreases
sion Sensors as a function of distance from the source.

669
SE-1211 1998 SECTION V SE-1211

4. Significance and Use 6.1.1 Known existing leaks and their distance from
the areas to be monitored should be noted so that their
4.1 Leakage of gas or liquid from a pressurized
influence on the capabilities of the method can be
system, whether through a crack, orifice, seal break,
evaluated.
or other opening, may involve turbulent or cavitational
flow, which generates acoustic energy in both the 6.1.2 Type of vessel, pipeline, or installation to
external atmosphere and the system pressure boundary. be examined, together with assembly, or layout draw-
Acoustic energy transmitted through the pressure bound- ings, or both, giving sufficient detail to establish dimen-
ary can be detected at a distance by using a suitable sions, changes of shape likely to affect flow characteris-
acoustic emission sensor. tics, positions of welds, and the location of components
4.2 With proper selection of frequency passband, such as valves or flanges, and attachments to the vessel
sensitivity to leak signals can be maximized by eliminat- or pipe such as pipe hangers where leaks are most
ing background noise. At low frequencies, generally likely to arise. Regions with restricted accessibility due
below 100 kHz, it is possible for a leak to excite to walls, the existence or location of cladding, insulation,
mechanical resonances within the structure that may or below surface components must be specified.
enhance the acoustic signals used to detect leakage. 6.1.3 When location of the peak is of primary
interest, quantitative information regarding the leakage
rates of interest and whenever possible the type of leak
5. Interferences is necessary.
5.1 External or internal noise sources can affect the 6.1.4 Extent of monitoring, for example, entire
sensitivity of an acoustic emission leak detection system. volume of pressure boundary, weld areas only, etc.
Examples of interfering noise sources are:
6.1.5 Material specifications and type of surface
5.1.1 Turbulent flow or cavitation of the inter- covering (for example, paint or other coating) to allow
nal fluid; the acoustic propagation characteristics of the structure
5.1.2 Noise from grinding or machining on the to be evaluated.
system;
6.1.6 Proposed program of pressure application or
5.1.3 Airborne acoustic noise, in the frequency process-pressure schedule, specifying the pressurization
range of the measuring system; schedule together with a layout or sketch of the pressure-
application system and specifying the type of fluid used
5.1.4 Metal impacts against, or loose parts fre-
during the test, for example, gas, water, or oil.
quently striking the pressure boundary; and
5.1.5 Electrical noise pick-up by the sensor 6.1.7 Time of monitoring, that is, the point(s) in
channels. the manufacturing process, or service life at which the
system will be monitored, or both.
5.2 Stability or constancy of background noise can
also affect the maximum allowable sensitivity, since 6.1.8 Frequency range to be used in the monitoring
fluctuation in background noise determines the smallest equipment.
change in level that can be detected. 6.1.9 Environmental conditions during examination
5.3 The acoustic emission sensors must have stable that may affect instrumentation and interpretation of
characteristics over time and as a function of both the results; for example, temperature, moisture, radioactiv-
monitoring structure and the instrumentation system ity, vibration, pressure, and electromagnetic interference.
test parameters, such as temperature. 6.1.10 Limitations or restrictions on the sensor
5.4 Improper sensor mounting, electronic signal con- mounting procedure, if applicable, including restrictions
ditioner noise, or improper amplifier gain levels can on couplant materials.
decrease sensitivity.
6.1.11 The location of sensors or waveguides and
preparation for their installation to provide adequate
coverage of the areas specified in 6.1.3. Where particular
6. Basic Information
sections are to be examined with particular sensors,
6.1 The following items must be considered in prepa- the coverage of the vessel or system by sensor subgroups
ration and planning for monitoring. shall be specified. The sensor locations must be given

670
SE-1211 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-1211

as soon as possible, to allow positioning difficulties to 8. Verification of Equipment Performance


be identified.
8.1 Characterization consists of two stages. The first
6.1.12 The communications procedure between the stage concerns periodic calibration and verification of
acoustic emission staff and the control staff, the time the equipment under laboratory conditions. This proce-
intervals at which pressure readings are to be taken, dure is beyond the scope of this practice (see Practice
and the procedure for giving warning of unexpected E 750) but the results must be made available to the
variations in the pressure system. system owners if requested. The second stage concerns
in-situ verification to check the sensitivities of all
6.1.13 Requirements for permanent records, if ap- channels and the satisfactory operation of the detection
plicable. equipment. For every calibration operation, a written
procedure shall be prepared.
6.1.14 Content and format of test report, if required.
8.2 In-situ sensitivity check of all sensors should be
6.1.15 Acoustic Emission Examiner qualifications performed by placing a leak signal simulator (see Guide
and certification, if required. E 976) at a specified distance from each sensor and
recording the resulting output level from the amplifier,
as referred to the amplifier input terminal. Amplifier
gains may also be adjusted as appropriate to correct
7. Apparatus for sensitivity variations.
7.1 Sensors — The acoustic emission sensors are 8.3 Periodic sensitivity checks shall be made during
generally piezoelectric devices and should be mounted long tests (days) or if any environmental changes occur.
in accordance with Practice E 650 to ensure proper The relative sensitivity check is accomplished by driving
signal coupling. The frequency range of the sensors various sensors or activating various leak simulation
may be as high as 1 MHz, and either wideband or devices such as water or gas jets and measuring the
resonant sensors may be employed. The higher frequen- outputs of the receiving sensors. The ratio of the outputs
cies can be used to achieve greater discrimination of two receiving sensors for a given injection point
against airborne or mechanical background noise. should remain constant over time. Any change in the
ratio indicates a deviation in performance. In this way,
7.2 Amplifiers — Amplifiers should have sufficient all sensors on a system may be compared to one or
gain to allow the signal processing equipment to detect several reference signals and proper adjustments made
the level of acoustic background noise on the pressurized (see Guide E 976).
system. The sensor/amplifier bandwidth should be se-
lected to minimize background noise. 8.4 When leak location calculations are to be per-
formed, the acoustic attenuation between sensors should
7.3 Signal Processor — The signal processor mea- be characterized over the frequency band of interest,
sures the RMS level, the acoustic emission signal power, especially if the presence of discontinuities, such as
the average signal level, or any other similar parameters pipe joints, may be suspected to affect the uniformity
of the continuous signal. A leak location processor to of attenuation. The measurements should then be fac-
compute the source location from signal levels and tored into the source location algorithm.
attenuation data may be included. Alarm set-points may
also be included as a processor function.

7.4 Leak Signal Simulator: 9. Procedure


7.4.1 A device for simulating leaks should be 9.1 Pre-Examination Requirements:
included to evaluate the effectiveness of the monitor 9.1.1 Before beginning the acoustic emission moni-
system. The following could be considered: a sensor toring, ensure that the following requirements are met:
on the pressure boundary driven from a random noise
generator, a small water jet, or a gas jet. 9.1.1.1 Evaluate attenuation effects, that is, the
change in signal amplitude with sound-propagation dis-
7.4.2 When leak location processing is to be tance, so as to define the effective area covered by
performed, leak simulation should be carried out initially each individual sensor; and in the case of sensor
over a sufficiently large number of diverse points to subgroups, the maximum distance between sensing
verify proper operation of the location algorithm. points.

671
SE-1211 1998 SECTION V SE-1211

9.1.1.2 Ensure that sensors are placed at the 10. Report


predetermined positions. If it is necessary to modify
10.1 Report the following information:
these positions during installation, record the new sensor
locations. Record the method of attachment of the 10.1.1 date of examination;
sensors and the couplant used.
10.1.2 identity of examining personnel;
9.1.1.3 Review the operating schedule to identify 10.1.3 sensor characteristics and locations;
all potential sources of extraneous acoustic noise such as
nozzle-plug movement, pump vibration, valve stroking, 10.1.4 method of coupling sensors to the structure;
personnel movement, fluid flow, and turbulence. Such 10.1.5 acoustic emission system and its character-
sources may require acoustic isolation or control so istics;
that they will not mask relevant leak emission within
the vessel or structure being examined. Uncontrolled 10.1.6 operating conditions;
generation of acoustic interference by conditions such
10.1.7 initial calibration results (laboratory);
as rain, sleet, hail, sand, wind (for unprotected vessels),
chipping, or grinding, shall be evaluated and its effect 10.1.8 in-situ calibration results and equipment
minimized by acoustic isolation insofar as is practical. verification;
A record shall be made of such sources.
10.1.9 results of measurements;
9.2 Acoustic Emission Monitoring: 10.1.10 analysis and verification of results;
9.2.1 The noise level of each channel or each
group shall be continuously or periodically recorded, 10.1.11 results of visual (or other) examination(s);
as required. Pressure or other significant parameters, 10.1.12 presentation of the numbers and locations
or both, will normally be recorded to allow correlation of leaks detected;
with the acoustic emission data response.
10.1.13 analysis of background noise measure-
9.2.2 When an increase in noise level attributable ments;
to a leak has been detected, the examiner shall inform
the system owner who will then look for the origin 10.1.14 estimate of quality and measurement and
of the leak and its nature. If the leak is found to be causes of any reduced sensitivity; and
outside the area of interest on the structure being 10.1.15 conclusions and recommendations.
monitored (extraneous leak) it must be stopped or
reduced to a level necessary to ensure satisfactory
monitoring. If extraneous leaks cannot be stopped, then
11. Keywords
the effect of such signals on the acoustic emission
system sensitivity shall be noted. A report shall be 11.1 acoustic emission; continuous monitoring; hy-
prepared following the visual (or other) examination drotest; leak detection; nondestructive testing; piping
for leaks. system; pressure vessels.

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SE-1211 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-1211

APPENDIX

(Nonmandatory Information)

X1. APPLICATIONS EXAMPLES


X1.1 The following examples were selected to illus-
trate applications of acoustic emission leak detection,
and are not intended to provide detailed descriptions
of the application.
X1.1.1 Acoustic Emission Leak Detection of a
Safety/Relief Valve — A safety/relief valve having a
leaking pilot-disk seat was tested under laboratory
conditions in order to determine the correlation of the
leak noise with leak rate or second-stage pressure. The
leak rate, downstream temperature, and the RMS voltage
of the acoustic signal were plotted against the second-
stage pressure in Fig. X1.1. The acoustic emission
sensor was clamped onto the external housing of the
pilot works. The signal was bandpass filtered in the
range from 5 to 10 kHz. The downstream temperature
was measured by a thermocouple in the vicinity of the
“pilot valve discharge line.” As the second stage pressure
increased from 40 to 200 psi (280 to 1400 kPa), the
leak rate increased 59%, the temperature increased 9%, FIG. X1.1 EXAMPLE OF ACOUSTIC EMISSION LEAK
and the acoustic emission RMS voltage increased 370%. DETECTION IN A SAFETY/RELIEF VALVE OF A
Therefore, the sensitivity of the acoustic detection was NUCLEAR POWER PLANT
excellent (see Fig. X1.1).
X1.1.2 Acoustic Emission Leak Detection from
Seawater Ball Valves — The U.S. Navy Acoustic
Valve Leak Detector (AVLD) monitors leak-associated
acoustic emission energy in the frequency range of 10
to 100 kHz. This frequency range was chosen because
there is significant energy emitted by leaky valves, and
energy in this range is rapidly attenuated with increasing
distance from the source. Therefore, background noise
can be electronically separated from the signal. Figure
X1.2 shows the estimated leak rate versus acoustic
emission level for a 4 in. ball valve.
X1.1.3 Acoustic Emission Leak Detection of a
Submerged Crude Oil Transfer Line — A section of
12 in. diameter steel pipe terminating on an offshore
drilling platform was inspected for confirmation of a
suspected leak. During acceptance hydro testing of the
line it was noted that pressure delayed at about 60
psi/h (410 kPa/h) starting at about 3200 psig (22 MPa). FIG. X1.2 ESTIMATING LEAK RATE FROM
These signal readings were compared with readings ACOUSTIC EMISSION LEVEL IN 4 in.
taken on two adjacent pipes, and on the nearest support SEAWATER BALL VALVES

673
SE-1211 1998 SECTION V SE-1211

TABLE X1.1
SIGNAL READINGS

Location RMS Reading Comment


6-in. pipe riser 0.200 at 60 dB gain reference
10-in. pipe riser 0.210 at 60 dB gain reference
12-in. pipe riser 0.300 at 60 dB gain leaking pipe
Corner support leg 0.210 at 60 dB gain reference

Location RMS Reading Comment


6-in. pipe riser 0.200 at 60 dB gain reference
10-in. pipe riser 0.200 at 60 dB gain reference
12-in. pipe riser 0.200 at 60 dB gain leak noise is stopped
Corner support leg 0.210 at 60 dB gain reference

leg for the structure (see Table X1.1). The additional


readings were used to determine the amount of signal
that was caused by sea motion and other structural
interfering noise. The initial readings were taken with
the platform in a shut-down condition and all construc-
tion workers onshore. The readings indicated about a
50% increase in signal level on the leaking pipe as
compared to the other two risers and the support leg.
This indicated leakage in close proximity to the detection
point, in effect, verifying that leakage was in the
connecting spool piece flanges. Following tightening
by a diver of the identified leakage flange, the acoustic
emission examiner determined that the leak had been
stopped. No further indications of leakage were detected;
either by mechanical means (pressure drop) or by
acoustic emission.

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SE-1419 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-1419

STANDARD TEST METHOD FOR EXAMINATION OF A99

SEAMLESS, GAS-FILLED PRESSURE VESSELS USING


ACOUSTIC EMISSION1
SE-1419

(Identical with ASTM Specification E 1419-96)

1. Scope prior to use. Specific precautionary statements are given


in Section 7.
1.1 This test method provides guidelines for acoustic
emission (AE) tests of seamless pressure vessels (tubes)
of the type used for distribution of industrial gases.
1.2 This test method requires pressurization to a 2. Referenced Documents
level greater than normal use. Pressurization medium
2.1 ASTM Standards:
may be gas or liquid.
A 388/A 388M Practice for Ultrasonic Examination of
1.3 This test method does not apply to vessels in Heavy Steel Forgings2
cryogenic service. E 543 Practice for Evaluating Agencies That Perform
Nondestructive Testing3
1.4 The AE measurements are used to detect and E 650 Guide for Mounting Piezoelectric Acoustic Emis-
locate emission sources. Other nondestructive test sion Sensors3
(NDT) methods must be used to evaluate the significance E 976 Guide for Determining the Reproducibility of
of AE sources. Procedures for other NDT techniques Acoustic Emission Sensor Response3
are beyond the scope of this test method. See Note 1. E 1316 Terminology for Nondestructive Examinations3
NOTE 1 — Shear wave, angle beam ultrasonic inspection is com-
monly used to establish circumferential position and dimensions of 2.2 ASNT Standards:4
flaws that produce AE. SNT-TC-1A Recommended Practice for Nondestructive
Testing Personnel Qualification and Certification
1.5 The values stated in inch-pound units are to be
ANSI/ASNT CP-189 Standard for Qualification and Cer-
regarded as the standard. The values given in parentheses
tification of Nondestructive Testing Personnel
are for information only.
1.6 This standard does not purport to address all of 2.3 Military Standard:
the safety concerns, if any, associated with its use. It MIL-STD-410 Nondestructive Testing Personnel Quali-
is the responsibility of the user of this standard to fication and Certification5
establish appropriate safety and health practices and
determine the applicability of regulatory limitations 2 Annual Book of ASTM Standards, Vol 01.05.
3 Annual Book of ASTM Standards, Vol 03.03.
4 Available from American Society for Nondestructive Testing, 1711
1 Thistest method is under the jurisdiction of ASTM Committee E-
7 on Nondestructive Testing and is the direct responsibility of Arlingate Plaza, P.O. Box 28518, Columbus, OH 43228-0518.
Subcommittee E07.04 on Acoustic Emission Method. 5 Availablefrom Standardization Documents Order Desk, Bldg. 4
Current edition approved May 10, 1996. Published July 1996. Section D, 700 Robbins Ave., Philadelphia, PA 19111-5094, Attn:
Originally published as E 1419-91. Last previous edition E 1419-91. NPODS.

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SE-1419 1998 SECTION V SE-1419

2.4 Code of Federal Regulations: 5. Significance and Use


Section 49, Code of Federal Regulations, Hazardous Ma-
5.1 Because of safety considerations, regulatory agen-
terials Regulations of the Department of Transporta-
cies (for example, U.S. Department of Transportation)
tion, Paragraphs 173.34, 173.301, 178.36, 178.37, and
require periodic tests of vessels used in transportation
178.456
of industrial gases (see Section 49, Code of Federal
2.5 Compressed Gas Association Standard: Regulations). The AE testing has become accepted as
Pamphlet C-5 Service Life, Seamless High Pressure Cyl- an alternative to the common hydrostatic proof test. In
inders7 the common hydrostatic test, volumetric expansion of
vessels is measured.

3. Terminology 5.2 An AE test should not be used for a period of


one year after a common hydrostatic test. See Note 2.
3.1 Definitions — See Terminology E 1316 for
general terminology applicable to this test method. NOTE 2 — The Kaiser effect relates to decreased emission that is
expected during a second pressurization. Common hydrostatic tests
3.2 Descriptions of Terms Specific to This Standard: use a relatively high test pressure (167% of normal service pressure).
(See Section 49, Code of Federal Regulations.) If an AE test is
3.2.1 fracture critical flaw — a flaw that is large performed too soon after such a pressurization, the AE results will
be insensitive to a lower test pressure (that is, the lower pressure
enough to exhibit unstable growth at service conditions. that is associated with an AE test).
3.2.2 marked service pressure — pressure for 5.3 Pressurization:
which a vessel is rated. Normally this value is stamped
on the vessel. 5.3.1 General practice in the gas industry is to
use low pressurization rates. This practice promotes
3.2.3 normal fill pressure — level to which a
safety and reduces equipment investment. The AE tests
vessel is pressurized. This may be greater, or may be
should be performed with pressurization rates that allow
less, than marked service pressure.
vessel deformation to be in equilibrium with the applied
load. Typical current practice is to use rates that approxi-
mate 500 psi/h (3.45 MPa/h).
4. Summary of Test Method
4.1 The AE sensors are mounted on a vessel, and 5.3.2 Gas compressors heat the pressurizing me-
emission is monitored while the vessel is pressurized dium. After pressurization, vessel pressure may decay
above normal fill pressure. as gas temperature equilibrates with ambient conditions.

4.2 Sensors are mounted at each end of the vessel 5.3.3 Emission from flaws is caused by flaw growth
and are connected to an acoustic emission signal proces- and secondary sources (for example, crack surface
sor. The signal processor uses measured times of arrival contact and contained mill scale). Secondary sources
of emission bursts to determine linear location of emis- can produce emission throughout vessel pressurization.
sion sources. If measured emission exceeds a prescribed 5.3.4 When pressure within a vessel is low, and
level (that is, specific locations produce enough events), gas is the pressurizing medium, flow velocities are
then such locations receive secondary (for example, relatively high. Flowing gas (turbulence) and impact
ultrasonic) inspection. by entrained particles can produce measurable emission.
4.3 Secondary inspection establishes presence of flaws Considering this, acquisition of AE data may commence
and measures flaw dimensions. at some pressure greater than starting pressure (for
example, 1⁄3 of maximum test pressure).
4.4 If flaw depth exceeds a prescribed limit (that is,
a conservative limit that is based on construction mate- 5.3.5 Maximum Test Pressure — Serious flaws
rial, wall thickness, fatigue crack growth estimates, and usually produce more acoustic emission (that is, more
fracture critical flaw depth calculations), then the vessel events, events with higher peak amplitude) from second-
must be removed from service. ary sources than from flaw growth. When vessels are
pressurized, flaws produce emission at pressures less
6 Available
than normal fill pressure. A maximum test pressure
from Superintendent of Documents, U.S. Government
Printing Office, Washington, DC 20402. that is 10% greater than normal fill pressure allows
7 Available from Compressed Gas Association, Inc., 1235 Jefferson measurement of emission from secondary sources in
Davis Highway, Arlington, VA 22202. flaws and from flaw growth.

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SE-1419 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-1419

5.3.6 Pressurization Schedule — Pressurization


should proceed at rates that do not produce noise
from the pressurizing medium and that allow vessel
deformation to be in equilibrium with applied load.
Pressure holds are not necessary; however, they may
be useful for reasons other than measurement of AE.
5.4 Excess background noise may distort AE data
or render them useless. Users must be aware of the
following common sources of background noise: high
gas-fill rate (measurable flow noise); mechanical contact
with the vessel by objects; electromagnetic interference
(EMI) and radio frequency interference (RFI) from
nearby broadcasting facilities and from other sources;
leaks at pipe or hose connections; and airborne sand
particles, insects, or rain drops. This test method should
not be used if background noise cannot be eliminated
or controlled. FIG. 1 ESSENTIAL FEATURES OF THE APPARATUS

6. Basis of Application
6.1 Personnel Qualification — The NDT personnel 7.2 Couplant must be used to acoustically connect
shall be qualified in accordance with a nationally recog- sensors to the vessel surface. Adhesives that have
nized NDT personnel qualification practice or standard acceptable acoustic properties, and adhesives used in
such as ANSI/ASNT CP-189, SNT-TC-1A, MIL-STD- combination with traditional couplants, are acceptable.
410, or a similar document. The practice or standard 7.3 Sensors may be held in place with magnets,
used and its applicable revision shall be specified in adhesive tape, or other mechanical means.
the contractual agreement between the using parties.
7.4 The AE sensors are used to detect strain-induced
6.2 Qualification of Nondestructive Testing Agen- stress waves produced by flaws. Sensors must be held
cies — If specified in the contractual agreement, NDT in contact with the vessel wall to ensure adequate
agencies shall be qualified and evaluated as described acoustic coupling.
in Practice E 543. The applicable edition of Practice
E 543 shall be specified in the contractual agreement. 7.5 A preamplifier may be enclosed in the sensor
housing or in a separate enclosure. If a separate pream-
6.3 Time of Examination — The time of examination plifier is used, cable length, between sensor and preamp,
shall be in accordance with 5.2 unless otherwise spec- must not exceed 6 ft (1.83 m).
ified.
7.6 Power/signal cable length (that is, cable between
6.4 Procedures and Techniques — The procedures preamp and signal processor) shall not exceed 500 ft
and techniques to be used shall be as described in (152.4 m). See A1.5.
this test method unless otherwise specified. Specific
techniques may be specified in the contractual 7.7 Signal processors are computerized instruments
agreement. with independent channels that filter, measure, and
convert analog information into digital form for display
6.5 Extent of Examination — The extent of examina- and permanent storage. A signal processor must have
tion shall be in accordance with 4.2 and 10.9 unless sufficient speed and capacity to independently process
otherwise specified. data from all sensors simultaneously. The signal proces-
sor should provide capability to filter data for replay.
A printer should be used to provide hard copies of
7. Apparatus test results.
7.1 Essential features of the apparatus required for this 7.7.1 A video monitor should display processed
test method are provided in Fig. 1. Full specifications are test data in various formats. Display format may be
in Annex A1. selected by the equipment operator.

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SE-1419 1998 SECTION V SE-1419

7.7.2 A data storage device, such as a floppy disk, 10.2 Isolate vessel to prevent contact with other
may be used to provide data for replay or for archives. vessels, hardware, and so forth. When the vessel cannot
be completely isolated, indicate, in the test report,
7.7.3 Hard copy capability should be available external sources which could have produced emission.
from a graphics/line printer or equivalent device.
10.3 Connect fill hose and pressure transducer. Elimi-
nate any leaks at connections.
8. Safety Precautions
10.4 Mount an AE sensor at each end of each tube.
8.1 As in any pressure test of metal vessels, ambient Use procedures specified in Guide E 650. Sensors must
temperature should not be below the ductile-brittle be at the same angular position and should be located
transition temperature of the pressure vessel construction at each end of the vessel so that the AE system can
material. determine axial locations of sources in as much of the
vessel as possible.

10.5 Adjust signal processor settings. See Appendix


9. Calibration and Standardization
X1 for example.
9.1 Annual calibration and verification of pressure
transducer, AE sensors, preamplifiers (if applicable), 10.6 Perform a system performance check at each
signal processor (particularly the signal processor time sensor (see 9.3). Verify that peak amplitude is greater
reference), and AE electronic waveform generator than a specified value (see Table X1.2). Verify that
should be performed. Equipment should be adjusted so the AE system displays a correct location (see Note
that it conforms to equipment manufacturer’s specifica- 3) for the mechanical device that is used to produce
tions. Instruments used for calibrations must have cur- stress waves (see 9.4 and Table X1.2). Prior to pressur-
rent accuracy certification that is traceable to the Na- ization, verify that there is no background noise above
tional Institute for Standards and Technology (NIST). the signal processor threshold setting.

9.2 Routine electronic evaluations must be performed NOTE 3 — If desired location accuracy cannot be attained with
sensors at two axial locations, then more sensors should be added
any time there is concern about signal processor per- to reduce sensor spacing.
formance. An AE electronic waveform generator should
be used in making evaluations. Each signal processor 10.7 Begin pressurizing the vessel. The pressurization
channel must respond with peak amplitude reading rate shall be low enough that flow noise is not recorded.
within ⫾2 dBV of the electronic waveform generator
output. 10.8 Monitor the test by observing displays that
show plots of AE events versus axial location. If
9.3 A system performance check must be conducted unusual response (in the operator’s judgment) is ob-
immediately before, and immediately after, each test. served, interrupt pressurization and conduct an investi-
A performance check uses a mechanical device to gation.
induce stress waves into the vessel wall at a specified
distance from each sensor. Induced stress waves stimu- 10.9 Store all data on mass storage media. Stop the
late a sensor in the same way as emission from a flaw. test when the pressure reaches 110% of normal fill
Performance checks verify performance of the entire pressure or 110% of marked service pressure (whichever
system (including couplant). is greater). The pressure shall be monitored with an
accuracy of ⫾2% of the maximum test pressure.
9.3.1 The preferred technique for conducting a
performance check is a pencil lead break. Lead should 10.9.1 Examples:
be broken on the vessel surface no more than 1.5 in.
(3.8 cm) from the sensor. The 2H lead, 0.5-mm diameter, 10.9.1.1 A tube trailer is normally filled to a
3-mm long should be used (see Fig. 4 of Guide E 976). gage pressure of 2640 psi (18.20 MPa). Pressurization
shall stop at 2904 psi (20.02 MPa).

10.9.1.2 A gas cylinder is normally filled to a


10. Procedure
gage pressure of 613 psi (4.23 MPa). The marked
10.1 Visually examine accessible exterior surfaces service pressure is 2400 psi (16.55 MPa). Pressurization
of the vessel. Note observations in test report. shall stop at 2640 psi (18.20 MPa).

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SE-1419 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-1419

10.10 Perform a system performance check at each 11.1.6 Normal fill pressure and marked service
sensor (see 9.3). Verify that peak amplitude is greater pressure.
than a specified value (see Table X1.2).
11.1.7 Pressurization medium.
10.11 Reduce pressure in vessel to normal fill pressure
11.1.8 Pressure at which data acquisition com-
by bleeding excess gas to a receiver, or vent the vessel.
menced.
10.12 Raw AE data should be filtered to eliminate
11.1.9 Maximum test pressure.
emission from nonstructural sources, for example, elec-
tronic noise. 11.1.10 Locations of AE sources that exceed ac-
ceptance criteria. Location shall include distance from
10.13 Replay test data. Examine the location distribu-
end of vessel that bears the serial number (usually this
tion plots (AE events versus axial location) for all
is stamped in the vessel wall).
vessels in the test.
11.1.11 Signature of test operator.
10.14 Based on data replay, determine whether sec-
ondary examination (ultrasonic examination) is required. 11.1.12 Stacking chart that shows relative locations
(Ultrasonic examination should be performed in accord- of vessels (if a multiple vessel array is tested).
ance with Practice A 388/A 388M.) Appendix X1
11.1.13 Visual examination results.
provides examples of such determinations.
11.1.14 AE test results, including events versus
location plots for each vessel and cumulative events
11. Report versus pressure plot for each vessel.
11.1 Prepare a written report from each test. Report
the following information:
12. Precision and Bias
11.1.1 Name of the owner of the vessel and the
12.1 Location accuracy is influenced by factors that
vehicle number (if appropriate).
affect elastic wave propagation, by sensor coupling,
11.1.2 Test date and location. and by signal processor settings.
11.1.3 Previous test date and previous maximum 12.2 It is possible to measure AE and produce AE
test pressure. See Note 4. source locations that cannot be verified by other NDT
methods. If such emission are measured, and are pro-
NOTE 4 — If the operator is aware of situations where the vessel
was subject to pressures that exceeded normal fill pressure, these duced by flaws, such flaws are small and are not of
should be described in the report. structural significance.

11.1.4 Any U.S. Department of Transportation


(DOT) specification that applies to the vessel. 13. Keywords
11.1.5 Any DOT exemption numbers that apply 13.1 acoustic emission; cylinders; flaws; gas pressure;
to the vessel. seamless; steel

ANNEX

(Mandatory Information)

A1. INSTRUMENTATION SPECIFICATIONS A1.1.2 Sensitivity shall be greater than −77 dBV
(referred to 1 V/␮bar, determined by face-to-face ultra-
A1.1 Sensors
sonic test) within the frequency range of intended use.
A1.1.1 The AE sensors shall have high sensitivity A1.1.3 Sensitivity within the range of intended
within the frequency band of 20 to 1200 kHz. Sensors use shall not vary more than 3 dB over the intended
may be broad band or resonant. range of temperatures in which sensors are used.

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SE-1419 1998 SECTION V SE-1419

A1.1.4 Sensors shall be shielded against electro- A1.5 Power/Signal Cable


magnetic interference through proper design practice
A1.5.1 The power/signal cables provide power to
or differential (anticoincidence) element design, or both.
preamplifiers, and conduct amplified signals to the main
A1.1.5 Sensors shall be electrically isolated from processor. These shall be shielded against electromag-
conductive surfaces by means of a shoe (a wear plate). netic interference. Signal loss shall be less than 1 dB/
100 ft (30.48 m) of cable length. Standard coaxial
A1.2 Signal Cable
cable is generally adequate. Signal loss from a power/
A1.2.1 The sensor signal cable which connects signal cable shall be no greater than 3 dB.
sensor and preamplifier shall not sensor output more
A1.6 Power Supply
than 3 dB [6 ft (1.83 m) is a typical maximum length].
Integral preamplifier sensors meet this requirement. A1.6.1 A stable, grounded, power supply that
They have inherently short, internal, signal cables. meets the signal processor manufacturer’s specification
A1.2.2 Signal cable shall be shielded against elec- shall be used.
tromagnetic interference. Standard coaxial cable is gen- A1.7 Signal Processor
erally adequate.
A1.7.1 The electronic circuitry gain shall be stable
A1.3 Couplant within ⫾2 dB in the temperature range from 40 to
A1.3.1 A couplant shall provide adequate ultrasonic 100°F (4.4 to 37.8°C).
coupling efficiency throughout the test. A1.7.2 Threshold shall be accurate within ⫾2 dB.
A1.3.2 The couplant must be temperature stable A1.7.3 Measured AE parameters shall include:
over the temperature range intended for use. threshold crossing counts, peak amplitude, arrival time,
A1.3.3 Adhesives may be used if they satisfy rise time, and duration for each hit. Also, vessel internal
ultrasonic coupling efficiency and temperature stability pressure shall be measured.
requirements. A1.7.4 The counter circuit shall count threshold
A1.4 Preamplifier crossings within an accuracy of ⫾5% of true counts.

A1.4.1 The preamplifier shall have noise level no A1.7.5 Peak amplitude shall be accurate within
greater than 7 ␮V rms (referred to a shorted input) ⫾2 dBV.
within the bandpass range. A1.7.6 Arrival time at each channel shall be accu-
A1.4.2 The preamplifier gain shall vary no more rate to within ⫾1.0 ␮s.
than ⫾1 dB within the frequency band and temperature A1.7.7 Duration shall be accurate to within ⫾10 ␮s.
range of use.
A1.7.8 Threshold shall be accurate to within
A1.4.3 The preamplifier shall be shielded from ⫾1 dB.
electromagnetic interference.
A1.7.9 Arrival time shall be accurate to 0.5 ␮s.
A1.4.4 The preamplifiers of differential design
shall have a minimum of 40-dB common mode rejection. A1.7.10 Rise time shall be accurate to ⫾10 ␮s.
A1.4.5 The preamplifier shall include a bandpass A1.7.11 Parametric voltage readings from pressure
filter with a minimum of 24-dB/octave signal attenuation transducers shall be accurate to within ⫾5% of the
above and below the 100 to 300-kHz frequency band. marked service pressure.

674.6

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SE-1419 ARTICLE 29 — ACOUSTIC EMISSION STANDARDS SE-1419

APPENDIX

(Nonmandatory Information)

X1. EXAMPLE INSTRUMENT SETTINGS AND on the cylindrical portion or end of the tube, then that
REJECTION CRITERIA part of the tube must be inspected with a secondary
NDT method (for example, ultrasonic inspection). Any
X1.1 A database and rejection criteria are established
flaw that is detected must be precisely located, and
for some DOT specified vessels. These have been
flaw dimensions must be determined.
described in the NDT Handbook.8 More recent criteria
are described in this section. Some vessel types, typical
dimensions, and service pressures are listed in Table
X1.1. X1.4 Rejection Criterion:

X1.2 Criteria for determining the need for secondary


inspection were established while working with AE X1.4.1 Vessels that contain flaws that are large
equipment with setup conditions listed in Table X1.2. enough to be “fracture critical flaws,” or that contain
flaws large enough to grow to fracture critical size
X1.3 Need for secondary inspection is based on
before another retest is performed, shall be removed
examination of location distribution plots (that is, plots
from service.
of AE events versus axial location) after AE data
acquisition is completed.

X1.3.1 Cylindrical Portion of Vessel — The DOT X1.4.2 “Fracture critical” flaw dimensions are
3AAX and 3T 3AA and 107A tubes are currently based upon fracture mechanics analysis of a vessel
retested with this AE test method. For 3AAX and 3T using strength properties that correspond to materials
and 3AA tubes, if five or more AE events occur within of construction.
an 8-in. (20.3-cm) axial distance, on the cylindrical
portion of a tube, then that part of the tube must be
inspected with a secondary NDT method (for example, X1.4.3 Analyses of DOT 3AAX and 3T tubes are
ultrasonic inspection). Any flaw that is detected must described by Blackburn and Rana.9 Fracture critical
be precisely located, and flaw dimensions must be flaw depths were calculated, and fatigue crack growth
determined. (under worst case conditions) was estimated. Flaw
depths that could grow to half the fracture critical size
X1.3.2 Ends of Vessel — For DOT 3AAX and
were judged too large. They should not remain in
3T and 3AA tubes, if five or more AE events are
service. Based upon this conservative approach, DOT
measured outboard of a sensor, each of these events
Specification 3AAX and 3T tubes with maximum flaw
is detected by both sensors, and the peak amplitude
depths of 0.10 in. (2.54 mm), or more, should be
at the “first hit” sensor is 43 dBV or more, then the
permanently removed from service.
end of the tube at the “first hit sensor” (that is, the
sensor with five or more first hits) must be inspected.
Any flaw that is detected must be precisely located,
and flaw dimensions must be determined using second- X1.4.3.1 The DOT 3AAX and 3T cylinders
ary NDT method (for example, ultrasonic inspection). have been evaluated by Blackburn and Rana.9 The
maximum allowable flaw depth was calculated to be
X1.3.3 The DOT 107A tubes are tested with 0.10 in. (2.54 mm).
sensors mounted on the end flanges. If five or more
AE events occur within 8-in. (20.3-cm) axial distance
9 Blackburn, P. R., and Rana, M. D., “Acoustic Emission Testing
and Structural Evaluation of Seamless, Steel, Tubes in Compressed
8 Miller,
R. K., and McIntire, P., Nondestructive Testing Handbook, Gas Service,” Transactions of the American Society of Mechanical
2nd ed., Vol 5, Acoustic Emission Testing, American Society for Engineers, Journal of Pressure Vessel Technology, Vol 108, May
Nondestructive Testing, Columbus, OH, 1987, pp. 161–165. 1986, pp. 234–240.

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SE-1419 1998 SECTION V SE-1419

TABLE X1.1
SPECIFIED CYLINDERS, TYPICAL DIMENSIONS, AND SERVICE PRESSURES

DOT DOT DOT DOT DOT


Specification 3AAX 3T 3A 3AA 107A
Outside diameter, in. (cm) 22 (55) 22 (56) 9.63 (25) 9.63 (25) 18 (46)
Nominal wall thickness, in. (cm) 0.54 (1.37) 0.42 (1.07) 0.31 (0.79) 0.25 (0.64) 0.75 or 0.86 (1.9 or 2.2)
Length, ft (m) 18 to 40 (0.5 to 12) 12 to 32 (4 to 10) 33 (10)
Typical service pressure, psi (MPa) 2400 (16.6) 2600 or 3300
(18 or 23)
Typical fill pressure, psi (MPa) 600 to 3000 (14.14 to 20.68) 2600 to 3300

Alternate retest method hydrostatic test, at 1.67 times marked service pressure every five years with volumetric expansion
measurement

TABLE X1.2 X1.4.3.2 The DOT 3AA and 3A cylinders were


ACOUSTIC EMISSION EQUIPMENT, evaluated by Blackburn.10 Maximum allowable depths
CHARACTERISTICS, AND SETUP CONDITIONS were calculated and 0.06 in. (1.524 mm) was specified
for both specifications.
Sensor sensitivity −77 dBV ref. 1V/␮bar, at ~150 kHz
Couplant silicone grease
Preamplifier gain 40 dB (×100)
Preamplifier filter 100 to 300-kHz bandpass X1.4.3.3 The DOT 107A cylinders have been
Power/signal cable length <500 ft (152.4 m) evaluated by Toughiry.11 The maximum flaw depth was
Signal processor threshold 32 dBV (for example, 1 uV p 0 dBV calculated to be 0.150 in. (3.81 mm).
at preamplifier input)
Signal processor filter 100 to 300-kHz bandpass 10 Docket No. 11099, Application for Exemption, Appendix II, “Maxi-
Dead time 10 ms
mum Allowable Flaw Depth, 3A and 3AA Tubes,” U.S. Department
Background noise <27 dBV (for example, 1 uV p 0 dBV of Transportation, Jan. 14, 1988.
at preamplifier input) 11 Toughiry, M. M., Docket No. 11059, Application for Exemption
Sensitivity check >80 dBV (for example, 1 uV p 0 dBV
from the Requirements of Hazardous Materials Regulations of the
at preamplifier input) DOT, U.S. Bureau of Mines, Helium Field Operation, June 1993.

674.8

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