Introduction To Jute Fibre Reinforced Composites

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Studies on mechanical properties of sisal and jute fiber hybrid sandwich


composite
C. Sivakandhan a, G. Murali b,⇑, N. Tamiloli b, L. Ravikumar c
a
Department of Mechanical Engineering, Sri Indu Institute of Engineering and Technology, Hyderabad, Telangana 501510, India
b
Department of Mechanical Engineering, Koneru Lakshmaiah Education Foundation, Guntur, Andhra Pradesh 522502, India
c
Department of Mechanical Engineering, Sri Sairam Engineering College, West Tambaram, Tamilnadu 600044, India

a r t i c l e i n f o a b s t r a c t

Article history: The present study deals with the Fabrication of hybrid composites and mechanical properties are tensile,
Received 22 April 2019 flexural, compression strength and impact of sisal fiber and jute fiber combination. Epoxy resin (LY556
Received in revised form 9 June 2019 grade) and hardener (HY951) is taken as the matrix and binder for the sisal and jute fiber combination.
Accepted 10 June 2019
The five different kinds of samples of jute/epoxy and sisal fiber/epoxy composite were made with the
Available online xxxx
fiber-matrix weight ratio of 35%. After fabrication, the test specimens were prepared as per in the
ASTM standards. The result shows the co-axial tensile strength of jute/epoxy and sisal fiber/epoxy com-
Keywords:
posite the result was increased 32% than sisal epoxy. The tensile, flexural, compression strength and
Hybrid composite
Jute fiber
impact of jute fiber/epoxy composites are higher than those of sisal fiber/epoxy composites at the same
Sisal fiber fiber loading. Additionally, the SEM images are studied in the different combinations.
Epoxy Ó 2019 Elsevier Ltd. All rights reserved.
Hardness Peer-review under responsibility of the scientific committee of the International Conference on Recent
Trends in Nanomaterials for Energy, Environmental and Engineering Applications.

1. Introduction tages include high strength to weight ratio, high strength at ele-
vated temperatures, high creep resistance sand high toughness
The composite material can be defined as the material which is [3]. These advantage scan also be in the form of high durability
composed of two or more distinct material on a macro scale with and design flexibility. Boopalan et al. investigated the mechanical
different properties to form a new material with a property that properties of raw jute and sisal fiber reinforced epoxy composites
is entirely different from the individual constituents. The cost of treated with sodium hydroxide and the results found better for
natural fiber Composites is low and light in weight but strength treated composites [4].
wise lower than synthetic fibers [1]. The primary phase of a com- Hybrid composites are more advanced composites as compared
posite materials called a matrix having a continuous character. In to conventional FRP composites. Hybrids can have more than one
other words, the matrix is a material which acts as a binder and reinforcing phase and a single matrix phase or single reinforcing
holds the fibers in the desired position there by transferring the phase with multiple matrix phases or multiple reinforcing and
external load to reinforcement. These matrixes are considered to multiple matrix phases. They have better flexibility as compared
be less hard and more ductile. The composite material consists of to other fiber reinforced composites. It usually contains a high
a matrix along with a fiber with some filler material. The reinforced modulus fiber with low modulus fiber. The high-modulus fiber
material can be either synthetic connatural fibers. In the demand of provides the stiffness and load bearing qualities, whereas the
increasing environmental security, several natural fibers reinforced low-modulus fiber makes the composite more damage tolerant
polymer composites (NFPCs) are brought into the competitive mar- and keeps the material cost low. Gupta et al. studied about the
ket. NFPCs provide a wide range of advantages over synthetic fiber dynamic mechanical properties and water absorption characteris-
based composites. Due to the superior properties of Natural fiber tics of hybrid sisal and jute fiber reinforced epoxy composites, from
composites. It become so popular and attractive [2]. These advan- their work they concluded that natural fibers are a better replace-
ment of synthetic fibers due to its acceptable mechanical proper-
⇑ Corresponding author. ties [5]. Srivastava et al. carried out an experimental work to
E-mail address: muralinitt@gmail.com (G. Murali). study the wear and frictional properties of the hybrid composite

https://doi.org/10.1016/j.matpr.2019.06.374
2214-7853/Ó 2019 Elsevier Ltd. All rights reserved.
Peer-review under responsibility of the scientific committee of the International Conference on Recent Trends in Nanomaterials for Energy, Environmental and Engineering
Applications.

Please cite this article as: C. Sivakandhan, G. Murali, N. Tamiloli et al., Studies on mechanical properties of sisal and jute fiber hybrid sandwich composite,
Materials Today: Proceedings, https://doi.org/10.1016/j.matpr.2019.06.374
2 C. Sivakandhan et al. / Materials Today: Proceedings xxx (xxxx) xxx

with different operating parameters; their study reveals that the Table 1
alkali treatment of fibers is used to increase the percentage reduc- Composite sample details.

tion of wear rate and friction coefficient [6]. Hariom Maurya et al. Sample Wt % of jute Wt % of Sisal Wt % of Epoxy and
[7] studied about the jute fiber reinforced with both polyester and number fiber fiber Hardener
epoxy resins; the results show that the jute reinforced epoxy com- Sample 1 0 35 65
posite exhibits better mechanical properties than jute polyester Sample 2 10 25 65
composites. Alves et al. [8] investigated the properties of sisal rein- Sample 3 20 15 65
Sample 4 25 10 65
forced epoxy composites using varying the fiber lengths (5, 10, 15, Sample 5 35 0 65
20 mm) with constant 30% of sisal fiber. The results of their work
reveal that 15 mm and 20 mm sisal fiber reinforced composite
shows significant improvement in the flexural and impacted prop-
3.1. Flexural test
erty. Loan et al. [9] studied through a case study design about the
possibilities for the replacement of glass fibers by natural jute
Flexural strength is carried out to find the ability of the material
fibers to produce a structural bonnet of an off-road vehicle (Buggy
to resist the deformation under the load. This is a three point bend
enclosures). Chandramohan et al. [10] discussed the optimum mix-
test is used to promote failure by inter-laminar shear. This test is
ing of fiber and resin of sisal banana & roselle hybrid composites in
conducted as per ASTM D790 standard by UTM. The specimen
dry and wet conditions. The mechanical properties of a hybrid
dimension is 13x127x3 mm. The flexural strength is expressed as
composite can be varied by changing volume ratio and stacking
modulus of rupture (MR) in psi (MPa). The flexural strength is cal-
sequence of different plies.
culated using the Eq. (1).

1.1. Problem identification


rf ¼ ð3Pmax LÞ=2bh2 ð1Þ
where,
Based on the literature presented in this chapter; it is found that pmax = maximum load at failure,
some researchers are carried out on Jute/sisal fiber reinforced com- b = specimen width, h = specimen thickness,
posites; they have found the Co-axial tensile properties and other L = specimen length between the two support points.
mechanical properties of these composite. There are many scopes
to characterize of Tran- axial properties of Jute/ sisal fibre rein- 3.2. Impact test
forced composites. So it is decided to carry out research the topic
of Co axial and Tran axial Tensile Properties of composite material The impact is a single point test that measures the resistance of
and analyses the mechanical properties of flexural behaviour, a material to impact from a swinging pendulum. The impactis
impact behaviour, compression behavior. defined as the kinetic energy needed to initiate fracture and con-
tinue the fracture until the specimen is broken. The ASTM D256
(13  66  13 mm) size is taken for the test.
2. Materials and methods
3.3. Scanning Electron Microscope (SEM)
Since the present study deals with the manufacturing of hybrid
composites, the material for reinforcement is chosen as sisal fiber,
SEM is a type of electron microscope that produces images of a
and jute fiber due to its suitable mechanical properties and epoxy
sample by scanning it with a focused beam of electrons. The mor-
resin (LY556 grade) and hardener (HY951) is taken as the matrix
phological characterisation of the composite surface is observed in
and binder for the composite. This process carried out with the
scanning electron microscope of Model TESCAN VEGA 3. The com-
help of compressive moulding. Work piece prepared in the dimen-
posite samples are adequately cleaned; air dried and are coated
sion 300x300x3 mm was used for casting the composite sheet. The
with 100Ao thick platinum in JEOL sputter ion coater and observed
sample specimen is shown in Fig. 1.There are five different kinds of
SEM at 20 KV. The fracture surface morphology of the composite
samples were made with the fibre–matrix weight ratio of 35%.The
specimens is observed with SEM.
sample is tabulated below the Table 1.

4. Results and discussions


3. Mechanical testing
The mechanical properties of the Jute/Sisal fiberhybrid epoxy
The test specimens were prepared and undergone different composites prepared for this present investigation is presented in
mechanical tastings namely Tensile test, flexural test and impact this discussion. The results of various characterization tests are
test as per the ASTM standards. The specimen size and shape for reported here. These include evaluation of tensile strength, flexural
corresponding tests are as follows. strength, impact strength and compression values are tabulated in
Table 2 and the properties are discussed.

4.1. Tensile test

A composite specimen is subjected to Tensile testing to measure


the force required to break the test specimen and the extent to
which the specimen stretches or elongates to that breaking point.
The physical properties of materials at a temperature that stimu-
late intended end user environment. The most common specimen
for ASTM D3039 has a constant rectangular cross section, 25 mm
wide and 250 mm long is used to study. Random directional tensile
specimens were cut in the longitudinal and transverse direction for
Fig. 1. Compression molding process. tensile test. According to ASTM D 3039 type IV sample the tensile

Please cite this article as: C. Sivakandhan, G. Murali, N. Tamiloli et al., Studies on mechanical properties of sisal and jute fiber hybrid sandwich composite,
Materials Today: Proceedings, https://doi.org/10.1016/j.matpr.2019.06.374
C. Sivakandhan et al. / Materials Today: Proceedings xxx (xxxx) xxx 3

Table 2
Mechanical properties values.

S. No Co-axial tensile strength (N/mm2) Tran-axial tensile strength (N/mm2) Flexural strength (N/mm2) Impact strength (J)
J0/s35 15.38 17.99 32.17 0.85
J10/s25 14.51 14.84 40.95 0.4
J20/s15 15.91 9.72 29.65 0.55
J25/s10 15.78 5.37 34.49 0.55
J35/s0 22.53 12.91 56 0.4

test specimens were carried out, using a tensile testing machine specimen, when the specimen was freely supported by a beam.
with crosshead speed of 2 mm/min and a gauge length of The flexural modules are evaluated from the slope of the initial
150 mm. Three specimens were tested for each set of samples portion of the load-deflection curve. The Fig. 2 shows that incorpo-
and meant values were tabulated in Table 2. ration of Jute and Sisal fiber at a 35:0 wt% relative weight fraction
leads to hybrid composites having a superior flexural strength. The
4.1.1. Co-axial tensile test maximum flexural strength of the composite was 56.31 N/mm2.
The co-axial tensile strength of hybrid composite at 35.0 wt% Flexural strength is nothing but a strength combining the tensile
Jute and Sisal fiber were 22.53 N/mm2. As can be seen Fig. 2, and compressive strengths and deviates with the interfacial shear
increasing weight fraction of jutefiber resulted in the positive strength between the fiber and matrix. It was observed from
effect on tensile properties of hybrid composites. The maximum Fig. 2 that the flexural strength and modulus of Jute/Sisal fiber/
tensile stress value of the composites was 22.53 N/mm2. This is epoxy composite increased with increasing jute fiber. If adding
probably due to the lost of the integrity of the matrix and insuffi- sisal fiber will reduce flexural strength.
cient wetting between fibre and matrix as a result of high fiber
loading. 4.3. Impact test

The impact strength of Jute/Sisal fiber hybrid epoxy composites


4.1.2. Tran axial tensile strength
the impact energy increasing with increasing weight fraction of
The effect of Jute/Sisal fiber hybrid epoxy composite is pre-
sisal fiber upto 35 wt%. The relationship between fiber loading
sented in the tensile strength of hybrid composite at 0:35 wt% Jute
and impact strength is shown in Fig. 2. The load which applied
and Sisal fiber were 17.99 N/mm2. As can be seen Fig. 2, increasing
on fibers is transferred by shear to the fibers, may exceed the
weight fraction of jute fiber resulted in negative effect on tensile
fiber/matrix interfacial bond, and deboning May occur. The fric-
properties of hybrid composites. The maximum tensile stress value
tional force along the interface may transfer the stress to the
of the composites was 17.99 N/mm2. This is probably due to the
deboned fiber. If the fiber stress level exceeds the fiber strength,
lost of the integrity of the matrix and insufficient wetting between
fibers may break. The obtained results reveals that the fiber is cap-
fiber and matrix as a result of high fiber loading.
able of absorbing energy due to its strong interfacial bonding
The tensile strength of a composite material is mainly depen-
between the fibre and matrix up to 35 wt% sisal fiber loading. How-
dent on the strength and modulus of fibers, the strength and chem-
ever, at higher loadings, the inter fiber interaction decreases the
ical stability of the matrix and fibers in transferring stress across
effective stress transfer between the fiber and matrix. This con-
the interface. When fiber reinforced composites are subjected to
tributes to a decrease in impact properties at higher fiber loadings.
load, the fibers act as carries of load and stress is transferred from
The high impact strength sisal fiber was found 0.85 J.
the matrix along the fibers leading to effective and uniform stress
distribution, which results in a composite having excellent
4.4. Compression test
mechanical properties.

The main aim of a compression test is to determine the ability of


4.2. Flexural test the material to withstand the compressive force under the com-
pressive load during a period of time to measure the parameters
The flexural test was performed by the three-point bending such as strain, stress, and deformation. Compression testing of a
method according to ASTM D 790, and a crosshead speed of specimen prepared according to ASTM D 3410. The effect of
2 mm/min. 3-specimens was tested and the averages were Jute/sisal fiber hybrid epoxy composite is presented in Fig. 2. wt.
calculated. The maximum load was applied in the middle of the % Jute, and sisal fiber was53.09 N/mm2. The fibers act as carries
of load and stress is transferred from the matrix along the effective
and uniform stress distribution, When fiber reinforced composites
are subjected to load. Due to this result, it leads a good composite
having excellent mechanical properties. At a low level of fiber load-
ing, the matrix is not restrained by enough fibers causing the bond
between matrix and fiber to break, leaving the matrix diluted by
non-reinforcing deboned fiber.

4.5. SEM images

Fig. 3 shows the different samples and images. The variation of


mechanical properties of prepared composite specimens through
phase information shown by means of the topography properties.
A figure clearly shows the poor bonding capacity of the composite
so that mechanical properties are reduced. Sample 3shows the
Fig. 2. Mechanical properties of Jute/Sisal fiber hybrid epoxy composite. jute-sisal fibre bundles, which indicate that these fibres were not

Please cite this article as: C. Sivakandhan, G. Murali, N. Tamiloli et al., Studies on mechanical properties of sisal and jute fiber hybrid sandwich composite,
Materials Today: Proceedings, https://doi.org/10.1016/j.matpr.2019.06.374
4 C. Sivakandhan et al. / Materials Today: Proceedings xxx (xxxx) xxx

Fig. 3. Different samples images.

adequately wet by epoxy polymer resin and thus led to low stress.  The SEM analysis of the different hybrid composite with jute
SEM images indicate that presence of -jute fibres which indicate composites which gives excellent mechanical properties com-
that medium interfacial bonding between epoxy and jute and gives pared to jute and sisal hybrid epoxy composite.
excellent mechanical properties compared to composite.
References
5. Conclusions
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Please cite this article as: C. Sivakandhan, G. Murali, N. Tamiloli et al., Studies on mechanical properties of sisal and jute fiber hybrid sandwich composite,
Materials Today: Proceedings, https://doi.org/10.1016/j.matpr.2019.06.374

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