469.

31
Komp c1 c2 c3 c4 step1 step2 rho at 469.13
C5H9CH3 0.84798 0.27042 532.79 0.28276 1.964764 0.076576 11.07376
C5H10 1.124 0.28859 511.76 0.2506 1.978534 0.085536 13.14069

rho cair(g/cm3) rho (kg/m3) xi*Bmi/liq den rhoL

0.931968 931.9678 0.088183 931.7271
0.919848 919.848 0.001787
jmlh= 0.08997
xi BM xi.BM
0.976519 84.16 82.18383
0.023481 70 1.643677
BM camp 83.82751

yi BM yi.BM
0.976519 84.16 82.18383
0.023481 70 1.643677
83.82751

rho camp 32.69777

 SEPARATOR - 01

Tugas : Memisahkan campuran uap dan cair umpan yang keluar dari vaporizer - 01
sebanyak 20400 kg/jam

Data-data konstanta Antoine :

Senyawa C1 C2 C3 Tmin Tmax

C5H10 15.8574 2588.48 -41.79 -43 72
C5H9CH3 15.8023 2731 -47.11 -23 102

1 atm = 760 mmHg

Mencari Kondisi Separator

Pt = 15.02 atm TDP
T= 469.31 K 196.16 C

Senyawa flow rate kg/jam flow rate kmol/jam Yi Po Ki = Po/Pt Xi = Yi/Ki

C5H10 400 5.7142857143 0.023481 23.79418 1.58416618 0.014822
C5H9CH3 20000 237.6425855513 0.976519 14.88692 0.99114006 0.985248
Jumlah 20400 243.3568712656 1 1.000071

L/F = N = 0.2

F=L+V
V = (1 - N) * F = 194.6854970125 kmol/jam
L=F-V= 48.6713742531 kmol/jam

Gas keluar
Senyawa flow rate kmol/jam flow rate kg/jam yi Bmi yi * Bmi
C5H10 4.5714285714 320 0.023481 70 1.64367662
C5H9CH3 190.1140684411 16000 0.976519 84.16 82.1838311
Jumlah 194.6854970125 16320 1 83.8275077

Cair keluar
Senyawa flow rate kmol/jam flow rate kg/jam xi Bmi xi * Bmi liq den
C5H10 1.1428571429 80 0.023481 70 1.64367662 582
C5H9CH3 47.5285171103 4000 0.976519 84.16 82.1838311 612
Jumlah 48.6713742531 4080 1 83.8275077

Densitas gas
rhog = P*Bmcampuran/R/T = 32.697766888 kg/m^3 = 2.039422 lb/cuft

Densitas cair
rhol = Bmav/(xi*Bmi/liq den) = 611.3820678514 kg/m^3 = 38.13307 lb/cuft 931.7271

(1) Hitung vapour-liquid separation factor

vapor-liquid separation factor = 0.046833
(2) Dari Fig 5-1 Evans, diperoleh design vapour velocity factor :
Kv = 0.46 Kh= 0.575
Maximum design vapour velocity : 2.412047 fps 3.0150584

(3) Vapour flow rate : 4.8961 cuft/s 4.8961

Minimum vessel cross sectional area :

A min 2.0299

(4) Hitung diameter vessel

1.6081 ft = 19.2966 in =

Diambil ukuran standar dengan pembulatan kelipatan 6 in, D =

(5) Estimasi vapour liquid inlet nozzle :

rhomix = 10.8866 lb/cuft
Diambil :
= 329.9485 fps
=
= 197.969 fps
A = Qv/uvmin nozzle = 0.0148 ft2

Diameter Nozzle = 0.14 ft = 1.6499 in

OD = 2.00 in
Hv = 36 + 0.5*Feed Nozzle OD = 37 in, Hvmin= 37.5
Maka diambil Hvmin = 37.5 in 95.25 cm

(6) Estimasi ukuran vessel awal seperti Fig 5-2

Hv = 36 in + 0.5*(Feed Nozzle OD)

(7) Pilih Full Surge Volume dari Tab 5-1 atau 5-2
t= 4 menit = 240 s
Hitung volume vessel yang dibutuhkan :
QL = WL/rhoL = 0.0655 cuft/s
V = QL*t = 19.6391 cuft
Tinggi cairan :
6.2488 ft = 74.9856 in
190.463453 cm
(8) Cek geometri :
(HV+HL)/D= 4.6869 ...satisfactory, 3< (HV+HL)/D <5 ….
D= 24 in = 2 ft
H= 112.49 in = 9.37 ft

PERHITUNGAN TEBAL DINDING

Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c

Jari-jari dalam, R
Di = 2 ft = 24 in
R= 1 ft = 12 in
Tekanan, P
P = Pdesign - Pudara luar
Pudara luar = 1 atm
Pdesign = 7.81 atm
P = 6.81 atm = 100.107 psig
Maximal allowable stress
Material = Carbon Steel SA 283 Grade C
S= 12650 psig
Joint Effisiensi, E= 0.85
Corrosion All., c = 0.125

Maka tebal dinding :

t = 0.2373489561 in
Dipilih tebal plat standar = 0.25 in = 1/ 4 in

PERHITUNGAN TEBAL HEAD

Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt = 2 ft = 24 in
t = 0.322931 in
Dipilih tebal plat standar = 0.375 in = 3/ 8 ( Ukuran min utk dia. 24 in)
Dari Tabel 5-8 B&Y, diambil sf = 2
ID = OD - 2t = 23.5 in
a = ID/2 = 11.75 in
Dari Tabel 5-7 B&Y
untuk t = 0.25 in, OD = 24 maka diperoleh icr = 4.375
r = 72
AB = a-icr = 7.375 in
BC = r-icr = 67.625 in
AC = ((BC^2)-(AB^2))^0.5 = 67.22165 in
b = r - AC = 4.7783517013 in
OA = t + b + sf = 7.101283 in
TBP
468.97952579 K 195.8295 C

Po K K.X
23.682987717 1.576763 0.037024
14.811680388 0.986131 0.962975
0.999999

xi*Bmi/liq den
0.0028241866
0.1342873057
0.1371114923

58.113597701
ft2 1.623899 ft2

3.2161007511 x 6 in 2.029873 (Atot min)

24 in Dmin = 1.607643 ft

329.949 fps

in

240 s

0.042956 cuft/s
10.30945 cuft
L= 5.078861 ft
L/D = 3.159196
( Ukuran min utk dia. 24 in)

in = 4 3/ 8
 SEPARATOR - 01

Tugas : Memisahkan campuran uap dan cair ammonia yang keluar dari vaporizer - 01
sebanyak 4327,74 kg/jam

Data-data konstanta Antoine :

Senyawa C1 C2 C3 Tmin Po at Tmin Tmax

NH3 16.9401 2132.5 -32.98 195.36 45.029824 239.65
H2O 18.3036 3816.44 -46.13 273.16 4.4518094 373.15

1 atm = 760 mmHg

Mencari Kondisi Separator

Pt = 7.1 atm
T= 288.5383535219 K

Senyawa flow rate kg/jam flow rate kmol/jam Yi Po Ki = Po/Pt Yi = Xi*Ki

NH3 4320.888 254.1698823529 0.99778331 7.11572917 1.0022154 0.999994
H2O 10.164 0.5646666667 0.00221669 0.01701661 0.0023967 5.31E-06
Jumlah 4331.052 254.7345490196 1 0.999999

L/F = N = 0.2

F=L+V
V = (1 - N) * F = 203.7876392157 kmol/jam
L=F-V= 50.9469098039 kmol/jam

Gas keluar
Senyawa flow rate kmol/jam flow rate kg/jam yi Bmi yi * Bmi
NH3 203.3359058824 3456.7104 0.99778331 17 16.962316
H2O 0.4517333333 8.1312 0.00221669 18 0.0399004
Jumlah 203.7876392157 3464.8416 1 17.002217

Cair keluar
Senyawa flow rate kmol/jam flow rate kg/jam xi Bmi xi * Bmi liq den
NH3 50.8339764706 864.1776 0.99778331 17 16.962316 639
H2O 0.1129333333 2.0328 0.00221669 18 0.0399004 998
Jumlah 50.9469098039 866.2104 1 17.002217

Densitas gas
rhog = P*Bmcampuran/R/T = 5.0989618293 kg/m^3 = 0.31803198 lb/cuft

Densitas cair
rhol = Bmav/(xi*Bmi/liq den) = 639.5398869145 kg/m^3 = 39.8893235 lb/cuft

(1) Hitung vapour-liquid separation factor

vapor-liquid separation factor = 0.02232272

(2) Dari Fig 5-1 Evans, diperoleh design vapour velocity factor :
Kv = 0.4
Maximum design vapour velocity : 4.46184733 fps
(3) Vapour flow rate : 6.6658 cuft/s

Minimum vessel cross sectional area :

A min 1.4940

(4) Hitung diameter vessel

1.3795 ft = 16.5545 in =

Diambil ukuran standar dengan pembulatan kelipatan 6 in, D =

(5) Estimasi vapour liquid nozzle :

rhomix = 3.5618 lb/cuft
Diambil :
= 188.7261 fps
=
= 113.236 fps
A = Qv/uvmin nozzle = 0.0442 ft2

Diameter Nozzle = 0.2372 ft = 2.8459 in

OD = 3.00 in
Hv = 36 + 0.5*Feed Nozzle OD = 37.5 in, Hvmin= 37.5
Maka diambil Hvmin = 37.5 in 95.25 cm

(6) Estimasi ukuran vessel awal seperti Fig 5-2

Hv = 36 in + 0.5*(Feed Nozzle OD)

(7) Pilih Full Surge Volume dari Tab 5-1 atau 5-2
t= 5 menit = 300 s
Hitung volume vessel yang dibutuhkan :
QL = WL/rhoL = 0.0133 cuft/s
V = QL*t = 4.9824 cuft
Tinggi cairan :
2.8183 ft = 33.8200 in
85.902822 cm
(8) Cek geometri :
(HV+HL)/D= 3.9622 ...satisfactory, 3< (HV+HL)/D <5 ….
D= 18 in = 1.5 ft
H= 71.32 in = 5.94 ft

PERHITUNGAN TEBAL DINDING

Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c

Jari-jari dalam, R
Di = 1.5 ft = 18 in
R= 0.75 ft = 9 in
Tekanan, P
 P = Pdesign - Pudara luar
Pudara luar = 1 atm
Pdesign = 7.81 atm
P = 6.81 atm = 100.107 psig
Maximal allowable stress
Material = Carbon Steel SA 283 Grade C
S= 12650 psig
Joint Effisiensi, E= 0.85
Corrosion All., c = 0.125

Maka tebal dinding :

t = 0.2092617171 in
Dipilih tebal plat standar = 0.25 in = 1/ 4 in

PERHITUNGAN TEBAL HEAD

Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt = 1.5 ft = 18 in
t = 0.27344832 in
Dipilih tebal plat standar = 0.3125 in = 5/16 ( Ukuran min utk dia. 18 in)
Dari Tabel 5-8 B&Y, diambil sf = 2
ID = OD - 2t = 17.5 in
a = ID/2 = 8.75 in
Dari Tabel 5-7 B&Y
untuk t = 0.25 in, OD = 18 maka diperoleh icr = 4.375
r = 72
AB = a-icr = 4.375 in
BC = r-icr = 67.625 in
AC = ((BC^2)-(AB^2))^0.5 = 67.4833313 in
b = r - AC = 4.5166687248 in
OA = t + b + sf = 6.79011705 in
Po at Tmax
751.234639
759.9430125

xi*Bmi/liq den
0.026545096
3.99803E-05
0.026585076

Table 4-11 Ludwig

ft2

2.75908406 x 6 in

18 in

150.981 fps

in
( Ukuran min utk dia. 18 in)

in = 4 3/ 8
TABLE 2.6 Vapor Pressure of Inorganic and Organic Liquids
P(mmHg) = Exp ( A - B/(T+C) ) atm = 760 mmHg
T dalam K
Cmpd. no. Name Formula BM A B C Tmin, K Ps at T min Tmax, K Ps at T max Tmax, C
22 Ammonia NH3 17 16.9401 2132.5 -32.98 195.36 45.029824 239.65 7.51E+02 -33.5
20 Water H2O 18 18.3036 3816.44 -46.13 273.16 4.4518094 373.15 7.60E+02 100
86 Acetonitril C2H3N 41 16.2874 2945.47 -49.15 229.26 0.9358236 354.75 7.72E+02 81.6
118 Propionitril C3H5N 55 15.9571 2940.86 -55.15 180.26 0.0005266 370.45 7.57E+02 97.3
120 Propylene C3H6 42 15.7027 1807.53 -26.15 87.86 1.255E-06 231.05 9.74E+02 -42.1

dari Menara Destilasi

.=(V/L+1).Zi/(V/L+1/K)
kgmol Senyawa fraksi (zi) Pio (Pa) K xi Yi
197.2741 NH3 ke Reaktor
98.3066 CH3CN 0.96869 5195.65624023 0.923641 0.970543 0.896433 Senyawa V(Kgmol)
0.0229 CH3CH2CN 0.000226 6036.26938417 1.073078 0.000226 0.000242 NH3 197.2741
3.1545 H2O 0.031084 3898.5485558 0.693052 0.031324 0.0217092 L/V= 39 CH3CN 2.2743
82.2669 C3H6 top product CH3CH2CN 0.0006
381.0250 Total 1 1.0021 0.9183842 H2O 0.0551
101.4840 condensable 2.2743 0.025 .=V/F C3H6 82.2669
279.5410 Non - Cond. 0.0006 0.975 = L / F 281.8711
Vapor 0.0551 SEPARATOR
2.537101 6 atm (ptot)
4560 mmHg
7.4015696 atm (pHC+H2O)
5625.1929 mmHg ke Tangki Penyimpan
164.48918 C Senyawa L(Kgmol)
437.63918 K bottom NH3 0.0000
CH3CN 96.0323
CH3CH2CN 0.0223
NB : Jika Kond. Ops (T,P) tertentu, trial V/l!!! H2O 3.0994
Sehingga didapat Sigma Yi = 1 C3H6 0.0000
99.1540
* Semua gas keluar sbg hasil atas.
Menghitung Dew Point

Senyawa V(Kgmol) Kg Yi Pio K Xi = Yi/Ki

NH3 197.2741 3353.66 0.6998736374 22.0703 3.67838308 0.1902667
CH3CN 2.2743 93.24797 0.0080687276 0.159054 0.026509 0.304377
CH3CH2CN 0.0006 0.033772 2.1784585E-06 0.41294 0.0688234 3.165E-05
H2O 0.0551 0.991412 0.0001954029 0.239526 0.03992102 0.0048947
C3H6 82.2669 3455.21 0.2918600536 22.06476 3.67746018 0.49957
281.8711 6903.143 1 0.99914
P= 6 atm
T= 55.49524 C
328.6452 K

Menghitung Bubble Point

Senyawa L(Kgmol) Kg Xi Pio K Yi=Ki*Xi

NH3 0.0000 0.000 0 138.1699 25.121804 0
CH3CN 96.0323 3937.323 0.9685162625 5.555612 1.01011135 0.9783093
CH3CH2CN 0.0223 1.227428 0.0002250728 6.750318 1.2273305 0.0002762
H2O 3.0994 55.78959 0.0312586647 4.338252 0.78877312 0.024656
99.1540 3994.34 1 1.0032415

P= 5.5 atm
T= 156.331 C
429.481 K
Reaktor
Kg Yi wi
3353.66 0.699874 0.485674
93.24797 0.008069 0.013504
0.0251758 2.18E-06 3.65E-06
3.0293138 0.000195 0.000439
3455.2098 0.29186 0.50038
6905.1723 1 1

ki Penyimpan
Kg Xi wi
0.000 0 0
3937.323 0.968516 0.985726
1.227 0.000225 0.000307
55.790 0.031259 0.013967
0.000 0 0
3994.340 1 1
 SEPARATOR DRUM - 03

Tugas : Memisahkan campuran uap dan cair yang keluar dari vaporizer - 03 sebanyak 4608,636024 kg/jam

Alat : Silinder Vertikal, torispherical dished head

Input :
Umpan = campuran uap dan cairan
= 4608.64 kg/jam = 2.8198 lb/s
Wv = vapour flow rate
= 3840.53002 kg/jam = 2.3498 lb/s
Wl = liquid flow rate
= 768.106 kg/jam = 0.4700 lb/s

Kondisi operasi :
T = 35.7561 C P= 6.5 atm T = 308.9061
Fase Gas:
Senyawa Bmi yi yi*Bmi
H2 2 0 0
CH4 16 0 0
C3H8 44 0.003799929 0.16719688
C3H6 42 0.288626525 12.1223141
NH3 17 0.703264563 11.9554976
CH3CN 41 0.001215939 0.0498535
CH3CH2CN 55 2.31E-06 0.00012694
H2O 18 3.09E-03 0.05566889
1.00000198 24.3506578
Densitas Gas
rhog = P*Bmcampuran/R/T = 24.8731 kg/m^3 = 1.552775 lb/cuft

Fase Cair
Senyawa xi Liq. Den xi*Bmi xi*Bmi/Lden
C3H8 0.00235437 582 0.1036 0.000178
C3H6 0.14888824 612 6.2533 0.010218
NH3 0.39173428 639 6.6595 0.010422
CH3CN 0.04911064 782 2.0135 0.002575
CH3CH2CN 1.67E-04 782 0.0092 0.023392
H2O 0.40230637 998 7.2415 0.046607
1 22.2806 0.093392

Densitas cair rhol =Bmav/(ZIG xi*Bmi/rholi) = 238.571882 kg/m3 = 14.89352 lb/cuft

(1) Hitung vapour-liquid separation factor Table 4-11 Ludwig

vapor-liquid separation factor = 0.064578141

(2) Dari Fig 5-1 Evans, diperoleh design vapour velocity factor :
Kv = 0.45
Maximum design vapour velocity : 1.319010757 fps

(3) Vapour flow rate : 1.5133 cuft/s

 Minimum vessel cross sectional area :
A min 1.1473 ft2

(4) Hitung diameter vessel

1.2089 ft = 14.5072 in = 2.417871

Diambil ukuran standar dengan pembulatan kelipatan 6 in, D = 18

(5) Estimasi vapour liquid nozzle :

rhomix = 4.8090 lb/cuft
Diambil :
= 219.2939 fps
= 175.435
= 131.576 fps
A = Qv/uvmin nozzle = 0.0086 ft2

Diameter Noz 0.1048 ft = 1.2579 in

OD = 2.00 in
Hv = 36 + 0.5*Feed Nozzle OD = 37 in, Hvmin= 37 in
Maka diambil Hvmin = 37 in 93.98 cm

(6) Estimasi ukuran vessel awal seperti Fig 5-2

Hv = 36 in + 0.5*(Feed Nozzle OD)

(7) Pilih Full Surge Volume dari Tab 5-1 atau 5-2
t= 3 menit = 180 s
Hitung volume vessel yang dibutuhkan :
QL = WL/rhoL = 0.0316 cuft/s
V = QL*t = 7.0998 cuft
Tinggi cairan :
4.0161 ft = 48.1928 in
122.4097 cm
(8) Cek geometri :
(HV+HL)/D= 4.7329 ...satisfactory, 3< (HV+HL)/D <5 ….
D= 18 in = 1.5 ft
H= 85.19 in = 7.10 ft

PERHITUNGAN TEBAL DINDING

Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c

Jari-jari dalam, R
Di = 1.5 ft = 18 in
 R= 0.75 ft = 9 in
Tekanan, P
P = Pdesign - Pudara luar
Pudara luar = 1 atm
Pdesign = 7.81 atm
P = 6.81 atm = 100.107 psig
Maximal allowable stress
Material = Carbon Steel SA 283 Grade C
S= 12650 psig
Joint Effisiensi, E= 0.85
Corrosion All., c = 0.125

Maka tebal dinding :

t = 0.20926172 in
Dipilih tebal plat standar = 0.3125 in = 5/16 in

PERHITUNGAN TEBAL HEAD

Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt = 1.5 ft = 18 in
t = 0.273448322 in
Dipilih tebal plat standar = 0.3125 in = 5/16 ( Ukuran min utk dia. 18 in)
Dari Tabel 5-8 B&Y, diambil sf = 2
ID = OD - 2t = 17.375 in
a = ID/2 = 8.6875 in
Dari Tabel 5-7 B&Y
untuk t = 0.3125 in, OD = 18 maka diperoleh icr = 4.375 in =
r = 72
AB = a-icr = 4.3125 in
BC = r-icr = 67.625 in
AC = ((BC^2)-(AB^2))^0.5 = 67.4873541 in
b = r - AC = 4.51264586 in
OA = t + b + sf = 6.786094182 in
08,636024 kg/jam

Table 4-11 Ludwig

 x 6 in

in

fps
min utk dia. 18 in)

4 3/ 8
 SEPARATOR DRUM - 04

Tugas : Memisahkan uap sebanyak 6983,936 kg/jam dan cairan sebanyak 29601,45 kg/jam
yang berasal dari Separator-04
Alat : Silinder Vertikal, torispherical dished head

Input :
Umpan = campuran uap dan cairan
= 22978.80 kg/jam = 14.0595 lb/s
Wv = vapour flow rate
= 5691.434 kg/jam = 3.4823 lb/s
Wl = liquid flow rate
= 17287.370 kg/jam = 10.5772 lb/s

Kondisi operasi :
T = 27.4259 C P= 6.5 atm T = 300.5759
Fase Gas:
Senyawa Bmi yi yi*Bmi
H2 2 0.275945 0.55189
CH4 16 0.273664 4.378624
C3H8 44 0.001942 0.085448
C3H6 42 0.130673 5.488266
NH3 17 0.315874 5.369858
CH3CN 41 0.000536 0.021976
CH3CH2CN 55 1.22E-06 6.71E-05
H2O 18 0.001365 0.02457
1 15.9207
Densitas Gas
rhog = P*Bmcampuran/R/T = 16.7130 kg/m^3 = 1.0433554 lb/cuft

Fase Cair
Senyawa xi Liq. Den xi*Bmi xi*Bmi/Lden
C3H8 0.002341 582 0.1030 0.000177
C3H6 0.130432 612 5.4781 0.008951
NH3 0.361623 639 6.1476 0.009621
CH3CN 0.050293 782 2.0620 0.002637
CH3CH2CN 2.08E-04 782 0.0114 0.021386
H2O 0.455103 998 8.1919 0.042594
1 21.9940 0.085366

Densitas cair rhol =Bmav/(ZIG xi*Bmi/rholi) = 257.6448 kg/m3 = 16.084203 lb/cuft

(1) Hitung vapour-liquid separation factor Table 4-11 Ludwig

vapor-liquid separation factor = 0.773613

(2) Dari Fig 5-1 Evans, diperoleh design vapour velocity factor :
Kv = 0.18
Maximum design vapour velocity : 0.683428 fps

(3) Vapour flow rate : 3.3376 cuft/s

 Minimum vessel cross sectional area : Untuk Vapor space = 20
A min 24.4179 ft2

(4) Hitung diameter vessel

5.5772 ft = 66.9269 in = 11.15448

Diambil ukuran standar dengan pembulatan kelipatan 6 in, D = 72

(5) Estimasi vapour liquid nozzle :

rhomix = 4.0965 lb/cuft
Diambil :
= 202.3988 fps
= 161.919
= 121.439 fps
A = Qv/uvmin nozzle = 0.0206 ft2

Diameter Nozzle = 0.1620 ft = 1.9445 in

OD = 2.00 in
Hv = 36 + 0.5*Feed Nozzle OD = 37 in, Hvmin= 37 in
Maka diambil Hvmin = 37 in 93.98 cm

(6) Estimasi ukuran vessel awal seperti Fig 5-2

Hv = 36 in + 0.5*(Feed Nozzle OD)

(7) Pilih Full Surge Volume dari Tab 5-1 atau 5-2
t= 10 menit = 600 s
Hitung volume vessel yang dibutuhkan :
QL = WL/rhoL = 0.6576 cuft/s
V = QL*t = 493.2105 cuft
Tinggi cairan :
17.4367 ft = 209.2408 in
531.4716 cm
(8) Cek geometri :
(HV+HL)/D= 3.4200 ...satisfactory, 3< (HV+HL)/D <5 ….
D= 72 in = 6 ft
H= 246.24 in = 20.52 ft

PERHITUNGAN TEBAL DINDING

Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c

Jari-jari dalam, R
Di = 6 ft = 72 in
 R= 3 ft = 36 in
Tekanan, P
P = Pdesign - Pudara luar
Pudara luar = 1 atm
Pdesign = 6.5 atm
P = 5.5 atm = 80.85 psig
Maximal allowable stress
Material = Carbon Steel SA 283 Grade C
S= 12650 psig
Joint Effisiensi, E= 0.85
Corrosion All., c = 0.125

Maka tebal dinding :

t = 0.3969172944 in
Dipilih tebal plat standar = 0.3125 in = 5/16 in

PERHITUNGAN TEBAL HEAD

Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt = 6 ft = 72 in
t =
0.604483 in
Dipilih tebal plat standar = 0.625 in = 5/ 8 ( Ukuran min utk dia. 72 in)
Dari Tabel 5-8 B&Y, diambil sf = 2
ID = OD - 2t = 71.375 in
a = ID/2 = 35.6875 in
Dari Tabel 5-7 B&Y
untuk t = 0.3125 in, OD = 72 maka diperoleh icr = 4.375 in =
r = 72
AB = a-icr = 31.3125 in
BC = r-icr = 67.625 in
AC = ((BC^2)-(AB^2))^0.5 = 59.93887 in
b = r - AC = 12.0611314025 in
OA = t + b + sf = 14.66561 in
 K

Table 4-11 Ludwig

%

x 6 in

in

fps
n utk dia. 72 in)

4 3/ 8
 SEPARATOR DRUM - 05

Tugas : Memisahkan uap sebanyak 6983,936 kg/jam dan cairan sebanyak 29601,45 kg/jam
yang berasal dari Separator-04
Alat : Silinder Vertikal, torispherical dished head

Input :
Umpan = campuran uap dan cairan
= 5687.82 kg/jam = 3.4801 lb/s
Wv = vapour flow rate
= 1847.285 kg/jam = 1.1303 lb/s
Wl = liquid flow rate
= 3840.537 kg/jam = 2.3498 lb/s

Kondisi operasi :
T = -7.3214 C P= 8 atm T = 265.8286
Fase Gas:
Senyawa Bmi yi yi*Bmi
H2 2 0.494009 0.988018
CH4 16 0.489923 7.838768
C3H8 44 6.34E-05 0.00279
C3H6 42 0.00597 0.25074
NH3 17 0.010034 0.170578
CH3CN 41 1.06E-07 4.35E-06
1 9.250898

Fase Cair
Senyawa xi Liq. Den xi*Bmi xi*Bmi/Lden
C3H8 0.0038 582 0.1672 0.000287
C3H6 0.288627 612 12.1223 0.019808
NH3 0.703263 639 11.9555 0.01871
CH3CN 0.001214 782 0.0498 6.36E-05
CH3CH2CN 2.76E-06 782 0.0002 0.038868
H2O 0.003093 998 0.0557 0.077449
1 24.3506 0.155186

Densitas cairan rhol =Bmav/(ZIG xi*Bmi/rholi) = 156.9124 kg/m3 = 9.7957 lb/cuft

Densitas Gas
rhog = P*Bmcampuran/R/T = 3.392663 kg/m^3 0.211797 lb/cuft

(1) Hitung vapour-liquid separation factor Table 4-11 Ludwig

vapor-liquid separation factor = 0.305703

(2) Dari Fig 5-1 Evans, diperoleh design vapour velocity factor :
Kv = 0.32
Maximum design vapour velocity : 2.152592 fps

(3) Vapour flow rate : 5.3365 cuft/s

 Minimum vessel cross sectional area : Untuk Vapor space = 20
A min 12.39553 ft2

(4) Hitung diameter vessel

3.9737 ft = 47.6847 in = 7.947448

Diambil ukuran standar dengan pembulatan kelipatan 6 in, D = 48

(5) Estimasi vapour liquid nozzle :

rhomix = 1.4404 lb/cuft
Diambil :
= 120.0158 fps
= 96.013
= 72.009 fps
A = Qv/uvmin nozzle = 0.0556 ft2

Diameter Nozzle 0.2661 ft = 3.1931 in

OD = 4.00 in
Hv = 36 + 0.5*Feed Nozzle OD = 38 in, Hvmin= 38 in
Maka diambil Hvmin = 38 in 96.52 cm

(6) Estimasi ukuran vessel awal seperti Fig 5-2

Hv = 36 in + 0.5*(Feed Nozzle OD)

(7) Pilih Full Surge Volume dari Tab 5-1 atau 5-2
t= 10 menit = 600 s
Hitung volume vessel yang dibutuhkan :
QL = WL/rhoL = 0.2399 cuft/s
V = QL*t = 143.9294 cuft
Tinggi cairan :
11.4489 ft = 137.3872 in
348.9634 cm
(8) Cek geometri :
(HV+HL)/D= 3.6539 ...satisfactory, 3< (HV+HL)/D <5 ….
D= 48 in = 4 ft
H= 175.39 in = 14.62 ft

PERHITUNGAN TEBAL DINDING

Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c

Jari-jari dalam, R
Di = 4 ft = 48 in
 R= 2 ft = 24 in
Tekanan, P
P = Pdesign - Pudara luar
Pudara luar = 1 atm
Pdesign = 8 atm
P = 7 atm = 102.9 psig
Maximal allowable stress
Material = Carbon Steel SA 283 Grade C
S= 12650 psig
Joint Effisiensi, E= 0.85
Corrosion All., c = 0.125

Maka tebal dinding :

t = 0.3560032215 in
Dipilih tebal plat standar = 0.375 in = 3/ 8 in

PERHITUNGAN TEBAL HEAD

Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt = 4 ft = 48 in
t = 0.531917 in
Dipilih tebal plat standar = 0.5625 in = 9/16 ( Ukuran min utk dia. 48 in)
Dari Tabel 5-8 B&Y, diambil sf = 1.5
ID = OD - 2t = 47.25 in
a = ID/2 = 23.625 in
Dari Tabel 5-7 B&Y
untuk t = 0.375 in, OD = 48 maka diperoleh icr = 3 in =
r = 48
AB = a-icr = 20.625 in
BC = r-icr = 45 in
AC = ((BC^2)-(AB^2))^0.5 = 39.99512 in
b = r - AC = 8.0048831106 in
OA = t + b + sf = 10.0368 in
 K

Table 4-11 Ludwig

%

x 6 in

in

fps
min utk dia. 48 in)

3
 SEPARATOR DRUM - 06

Tugas : Memisahkan uap sebanyak 6983,936 kg/jam dan cairan sebanyak 29601,45 kg/jam
yang berasal dari Separator-04
Alat : Silinder Vertikal, torispherical dished head

Input :
Umpan = campuran uap dan cairan
= 33885.38 kg/jam = 20.7326 lb/s
Wv = vapour flow rate
= 6983.936 kg/jam = 4.2731 lb/s
Wl = liquid flow rate
= 29601.450 kg/jam = 18.1115 lb/s

Kondisi operasi :
T = 80.4205 C P= 6.5 atm T=
Fase Gas:
Senyawa Bmi yi yi*Bmi
H2 2 0.000468 0.000936
CH4 16 0.000288 0.004608
C3H8 44 0.001283 0.056452
C3H6 42 0.070863 2.976246
NH3 17 0.190864 3.244688
CH3CN 41 0.06238 2.55758
CH3CH2CN 55 0.000349 0.019195
H2O 18 0.673505 12.12309
1 20.9828
Fase Cair
Senyawa xi Liq. Den xi*Bmi xi*Bmi/Lden
NH3 0.143222 639 2.4348 0.003810288
CH3CN 0.072117 782 2.9568 0.00378107
CH3CH2CN 0.000405 782 0.0223 2.84847E-05
H2O 0.784256 998 14.1166 0.014144898
1 19.5305 0.021764741

Densitas cairan
rhol =Bmav/(ZIG xi*Bmi/rholi) = 897.3437469 kg/m3 = 56.0192

Densitas Gas
rhog = P*Bmcampuran/R/T = 4.70077169 kg/m^3 0.293458919 lb/cuft

(1) Hitung vapour-liquid separation factor

vapor-liquid separation factor = 0.30677354

(2) Dari Fig 5-1 Evans, diperoleh design vapour velocity factor :
Kv = 0.4
Maximum design vapour velocity : 5.51206471 fps

(3) Vapour flow rate : 14.5611 cuft/s

Minimum vessel cross sectional area : Untuk Vapor space =

A min 2.6417 ft 2
A min 13.2084
(4) Hitung diameter vessel

4.1019 ft = 49.2234 in =

Diambil ukuran standar dengan pembulatan kelipatan 6 in, D =

(5) Estimasi vapour liquid nozzle :

rhomix = 4.0545 lb/cuft
Diambil :
= 201.3590 fps
=
= 120.815 fps
A = Qv/uvmin nozzle = 0.0904 ft2

Diameter Nozzle = 0.3393 ft = 4.0721 in

OD = 5.00 in
Hv = 36 + 0.5*Feed Nozzle OD = 38.5 in, Hvmin= 39
Maka diambil Hvmin = 39 in 99.06 cm

(6) Estimasi ukuran vessel awal seperti Fig 5-2

Hv = 36 in + 0.5*(Feed Nozzle OD)

(7) Pilih Full Surge Volume dari Tab 5-1 atau 5-2
t= 10 menit = 600 s
Hitung volume vessel yang dibutuhkan :
QL = WL/rhoL = 0.3233 cuft/s
V = QL*t = 242.4817 cuft
Tinggi cairan :
15.2401 ft = 182.8818 in
464.5197517 cm
(8) Cek geometri :
(HV+HL)/D= 4.1089 ...satisfactory, 3< (HV+HL)/D <5 ….
D= 54 in = 4.5 ft
H= 221.88 in = 18.49 ft

PERHITUNGAN TEBAL DINDING

Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c

Jari-jari dalam, R
Di = 4.5 ft = 54 in
R= 2.25 ft = 27 in
Tekanan, P
P = Pdesign - Pudara luar
Pudara luar = 1 atm
Pdesign = 6.5 atm
P = 5.5 atm = 80.85 psig
Maximal allowable stress
Material = Carbon Steel SA 283 Grade C
 S= 12650 psig
Joint Effisiensi, E= 0.85
Corrosion All., c = 0.125

Maka tebal dinding :

t = 0.3289379708 in
Dipilih tebal plat standar = 0.375 in = 3/ 8 in

PERHITUNGAN TEBAL HEAD

Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt = 4.5 ft = 54 in
t = 0.48461209 in
Dipilih tebal plat standar = 0.5 in = 1/ 2 ( Ukuran min utk dia. 54 in)
Dari Tabel 5-8 B&Y, diambil sf = 2
ID = OD - 2t = 53.25 in
a = ID/2 = 26.625 in
Dari Tabel 5-7 B&Y
untuk t = 0.375 in, OD = 54 maka diperoleh icr = 3.25
r = 54
AB = a-icr = 23.375 in
BC = r-icr = 50.75 in
AC = ((BC^2)-(AB^2))^0.5 = 45.04633032 in
b = r - AC = 8.9536696833 in
OA = t + b + sf = 11.4382818 in
 353.5705 K

lb/cuft

Table 4-11 Ludwig

Table 4-11 Ludwig

20 %
ft 2
 8.203899 x 6 in

54 in 137.16 cm

161.087 fps

in
( Ukuran min utk dia. 54 in)

in = 3 1/ 4
 SEPARATOR DRUM - 07

Tugas : Memisahkan uap sebanyak 3475,90 kg/jam dan cairan sebanyak 3988,947 kg/jam
yang berasal dari Menara Destilasi 2
Alat : Silinder Vertikal, torispherical dished head

Input :
Umpan = campuran uap dan cairan
= 7466.90 kg/jam = 4.5686 lb/s
Wv = vapour flow rate
= 3475.90 kg/jam = 2.1267 lb/s
Wl = liquid flow rate
= 3988.947 kg/jam = 2.4406 lb/s

Kondisi operasi :
T = 118.75728 C P= 5.5 atm T = 391.9073 K
Fase Gas:
Senyawa Bmi yi yi*Bmi
NH3 17.031 0.986062 16.79362192
CH3CN 41.053 0.013344 0.547811232
CH3CH2CN 55.08 4.64E-06 0.000255571
H2O 18.015 0.000589 0.010610835
1 17.35229956 (Bmcampuran)

densitas gas = P*Bmcampuran/R/T

densitas gas = 2.9675967201 kg/m^3 0.1853 lb/cuft

Fase Cair
Senyawa xi Liq. Den xi*Bmi xi*Bmi/Lden
NH3 0 639 0.0000 0
CH3CN 0.95508 782 39.2089 0.050139257
CH3CH2CN 0.000221 782 0.0122 1.55661E-05
H2O 0.044699 998 0.8053 0.000806866
1 40.0263 0.05096169

Densitas cairan
rhol =Bmav/(ZIG xi*Bmi/rholi) = 785.4198847 kg/m3 = 49.0320 lb/cuft

(1) Hitung vapour-liquid separation factor

0.2823

(2) Dari Fig 5-1 Evans, diperoleh design vapour velocity factor :
Kv = 0.4
Maximum design vapour velocity :

= 6.4951 fps

(3) Vapour flow rate :

11.4796 cuft/s

Minimum vessel cross sectional area : Untuk Vapor space = 20 %

A min 1.7674 ft 2
A min 8.837093 ft2
(4) Hitung diameter vessel

3.3552 ft = 40.2625 in = 6.710423 x 6 in

Diambil ukuran standar dengan pembulatan kelipatan 6 in, D = 42 in

(5) Estimasi vapour liquid nozzle :

rhomix = 3.0139 lb/cuft
Diambil :
= 173.6064 fps
= 138.885 fps
= 104.164 fps
A = Qv/uvmin nozzle = 0.0827 ft2

Diameter Nozzle 0.3245 ft = 3.8939 in

OD = 4.00 in
Hv = 36 + 0.5*Feed Nozzle OD = 38 in, Hvmin= 38 in
Maka diambil Hvmin = 38 in 96.52 cm

(6) Estimasi ukuran vessel awal seperti Fig 5-2

Hv = 36 in + 0.5*(Feed Nozzle OD)

(7) Pilih Full Surge Volume dari Tab 5-1 atau 5-2
t= 22 menit = 1320 s
Hitung volume vessel yang dibutuhkan :
QL = WL/rhoL = 0.0498 cuft/s
V = QL*t = 82.1304 cuft
Tinggi cairan :
8.5330 ft = 102.3963 in
260.0866342 cm
(8) Cek geometri :
(HV+HL)/D= 3.3428 ...satisfactory, 3< (HV+HL)/D <5 ….
D= 42 in = 3.5 ft
H= 140.40 in = 11.70 ft

PERHITUNGAN TEBAL DINDING

Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c

Jari-jari dalam, R
Di = 3.5 ft = 42 in
R= 1.75 ft = 21 in
Tekanan, P
P = Pdesign - Pudara luar
Pudara luar = 1 atm
Pdesign = 5.5 atm
P = 4.5 atm = 66.15 psig
Maximal allowable stress
Material = Carbon Steel SA 283 Grade C
 S= 12650 psig
Joint Effisiensi, E= 0.85
Corrosion All., c = 0.125

Maka tebal dinding :

t= 0.2546718601 in
Dipilih tebal plat standar = 0.3125 in = 5/16 in

PERHITUNGAN TEBAL HEAD

Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt = 3.5 ft = 42 in
t =
0.35381275 in
Dipilih tebal plat standar = 0.375 in = 3/ 8 ( Ukuran min utk dia. 42 in)
Dari Tabel 5-8 B&Y, diambil sf = 1.5
ID = OD - 2t = 41.375 in
a = ID/2 = 20.6875 in
Dari Tabel 5-7 B&Y
untuk t = 0.3125 in, OD = 42 maka diperoleh icr = 2.625 in = 2 5/ 8
r = 40
AB = a-icr = 18.0625 in
BC = r-icr = 37.375 in
AC = ((BC^2)-(AB^2))^0.5 = 32.72058555 in
b = r - AC = 7.2794144498 in
OA = t + b + sf = 9.1332272 in