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Improvement of Clayey Soil With Lime and Industrial Sludge
Improvement of Clayey Soil With Lime and Industrial Sludge
Improvement of Clayey Soil With Lime and Industrial Sludge
https://doi.org/10.1007/s10706-018-0515-x
ORIGINAL PAPER
Abstract Industrial waste generation has reached up Keywords Clayey soil Improvement Lime
to millions of tons yearly. One way to solve the Copper sludge Steel sludge
problems of the large accumulating amount of waste
could be to incorporate it into the soil; thus, finding a
way for the use of industrial waste could be a quest for
soil improvement studies. Industrial sludge in certain 1 Introduction
pozzolanic form reacts with soil and possesses
cementitious properties. This paper illustrates the The growth of industry and industrial productions has
utilization of lime, steel and copper sludge in led to the production and accumulation of industrial
improvement of high plasticity clayey soil. The wastes (Brooks et al. 2011). In recent years, many
influence of stabilizer type, different curing times attempts have been reported by researchers in different
and various ratios of lime to sludge are evaluated by fields to solve biological and environmental problems
Atterberg limits, standard proctor compaction, uncon- originating from accumulation of industrial wastes
fined compressive strength and unconsolidated (Kamon and Nontananandh 1990; Wild and Kinuthia
undrained strength in triaxial test. The test results 1995; Al-Sharif and Attom 2000; Kamon and Gu
show that adding lime and sludge results in an increase 2001; Yin et al. 2007; Degirmanci et al. 2007; Lin and
in maximum strength. Moreover, the strength of soil Zhu 2009: Okoro and Vogtman 2011; Khandaker and
increases with the increase of curing time. Utilizing Anwar Hossain 2011; Brooks et al. 2011). Metallic
stabilizers also influences plasticity index and com- sludge that is usually produced in large amount is
paction parameters. Finally, the results demonstrate considered as industrial waste. Sludge is usually piled
that steel sludge has better performance than that of adjacent to factories and in open air in bulk form
copper sludge in term of strength development. (Kamon and Nontananandh 1990). This can cause
serious biological and environmental problems
(Brooks et al. 2011). Additionally, potentially valu-
able components of the sludge composition are lost in
the process. From a geotechnical engineering view-
R. Noorzad (&) S. Motevalian
point, sludge can be used for stabilization or improv-
Faculty of Civil Engineering, Babol Noshirvani
University of Technology, Babol, Iran ing soil engineering properties (Kamon and Gu 2001).
e-mail: rn0864@gmail.com One of the broadest approaches for stabilization of soil
S. Motevalian is cement or chemical stabilization, in which the soil is
e-mail: sara_cl67@yahoo.com mixed with cementitious materials such as cement,
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lime, fly ash, sludge, etc. (Kamon and Nontananandh concluded that the unconfined compressive strength of
1990; Wild and Kinuthia 1995; Al-Sharif and Attom soil increased with increasing curing temperature.
2000; Kamon and Gu 2001; Al-Rawas et al. 2005; Moreover, the swelling potential increased with
Guney et al. 2007; Yong and Ouhadi 2007; Yilmaz and increasing curing time and decreased with increasing
Civelekoglu 2009; Okoro and Vogtman 2011; Al- curing temperature.
Mukhtar and Lasledj 2014; Ajdari and Bahmyari The aforementioned studies have shown that there
2015). In the presence of water and through chemical are technological, economical and environmental
reactions, soil engineering properties is improved advantages in using the industrial by-products in soil
(Kamon and Gu 2001). Many studies for probing and stabilization but a few studies have accomplished to
analyzing the chemical stabilization of soil have been present effects of industrial sludge in soil improve-
accomplished in recent years (Kamon and Non- ment. Using of industrial sludge and waste guide to
tananandh 1990; Wild and Kinuthia 1995; Al-Sharif low-cost soil improvement. Hence, the present study
and Attom 2000; Kamon and Gu 2001; Okoro and was undertaken to investigate the effects of industrial
Vogtman 2011). Kamon and Nontananandh (1990) sludge such as steel and copper sludge on the
used cement and stainless-steel sludge to improve the geotechnical properties of high plasticity clayey soil.
unconfined compressive strength of soil. According to These effects checked out by Atterberg limits, com-
the research, adding stainlesssteel sludge to the paction, unconfined compressive strength and uncon-
mixture of soil and cement and also the increase of solidated undrained triaxial tests.
curing time increased the unconfined compressive
strength of the soil. Al-Sharif and Attom (2000)
employed burned sludge to stabilize clayey soil, and 2 Experimental Program
concluded that by adding the burned sludge to the
optimum value, the unconfined compressive strength 2.1 Materials
and the maximum dry unit weight increased and the
soil plasticity index decreased. Lin and Zhu (2009) The soil used herein was clayey soil obtained from
demonstrated that cement and calcium bentonite can Amol, a city in the north of Iran. The soil that used for
increase considerably the unconfined compressive preparing samples was collected in depth of 0.5
strength of soil. Also, they concluded that with (m) from ground surface. The surface layer of ground
increasing the curing time, unconfined compressive equal to 0.5 (m) removed and then the required soil
strength of the soil increased. Du et al. (2011) was provided. Physical properties and grain size
compared the effect of calcium carbide residuals and distribution curve of the soil are presented respectively
lime on the unconfined compressive strength of clayey in Table 1 and Fig. 1. Both wet sieving and hydrom-
soil, and found that calcium carbide was more eter method were conducted for grain size distribution
effective than samples containing lime. The results curve (ASTM D 422-63). All geotechnical tests were
also demonstrated that the soils containing calcium performed in according to American Standard Test
carbide showed better performance in increase of Method.
unconfined compressive strength compared to stabi- The copper sludge (CS), steel sludge (SS) (is a by-
lized soils with lime. Khandaker and Anwar Hossain producted from copper and steel industry) and lime
(2011) used rice husk ash and cement kiln dust to used in this investigation were supplied by local
improve clayey soil and concluded that stabilized soil companies. The specific gravity of CS, SS and lime
have shown satisfactory strength and durability char- were 3.22, 3.17 and 2.3, respectively.
acteristics. Brooks et al. (2011) employed fly ash and
limestone dust to stabilize some problematic soils. The 2.2 Testing Procedures and Combination
results of the study showed that unconfined compres- Schemes
sive strength and California Bearing Ratio of the
stabilized soil increased and plasticity index of the soil In this study in order to investigate the effects of
decreased. Aldaood et al. (2014) used lime and mixture of lime and sludge as stabilizer, first the
gypsum to improve the behavior of soil. They studied optimum content of lime for the clayey soil was
mechanical strength and swelling potential of soil and obtained based on unconfined compressive strength
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90
80
of lime to sludge for various goal for example
70 increasing strength, increasing maximum dry unit
60 weight and decreasing plasticity index.
50
40
30 2.3 Sample Preparation
20
10
0 The materials (soil, lime and sludge) passed through
0.001 0.01 0.1 1
Particle diameter (mm)
the N0. 40 sieve for all test specimens. Initially, oven-
dried soil and lime were mixed together for at least
Fig. 1 Grain size distribution for clay 10 min. Then, the oven-dried sludge (CS and SS) was
mixed with the mixture of soil and lime for at least
method. For this intent, samples containing 4, 6, 8, 10 5 min and the mixture was subsequently put into
and 12% (by dry weight) of lime were prepared. All plastic bags, where the mixing was continued by
tested specimens were prepared with the static com- shaking and over turning the bag for at least 5 min.
paction method at optimum moisture content and 95% Finally, the optimum moisture content was added to
of maximum dry unit weight. The maximum uncon- the mixture and was mixed for at least 20 min.
fined compressive strength of samples for 28 days Specimens were prepared with the static compaction
curing was compared and the optimum content of lime method at the optimum moisture content and 95% of
was determined as 10%. The optimum lime content the maximum dry unit weight. The soil mixture was
was then replaced with various contents of steel and placed in the mold as five layers. At the end of
copper sludge (lime/sludge: 40/60, 60/40, 80/20, compaction of each layer, for a better bonding of
90/10 and 10% lime) and the physical and engineering layers, the surface of layer was scratched and next
properties of the mixture were determined by means of layer was compacted. The process of compaction of
the Atterberg limits (ASTM D 431810), standard the soil mixture in the mold was 15 min for all test
proctor compaction (ASTM D 698-07el), unconfined samples. Because of brittle behavior of the soil
compressive strength (ASTM D 2166) and unconsol- mixture, samples were prepared in triplex mold. The
idated undrained triaxial (ASTM D 2850-03a) test. optimum moisture content and maximum dry unit
Both the unconfined compressive strength and uncon- weight of the soil mixed with different percentage of
solidated undrained strength test were determined on lime and sludge were determined by standard com-
a hydrolic mashin under the strain-control condition at paction test (Tables 3 and 4). Specimens were
the loading speed of 0.6 mm/min and 3 confining demolded 3 min after compaction and stored in a
pressures of 600, 800 and 1000 (kPa) for unconsoli- curing room (maintained at 25 ± 2 °C and 95 ± 2%
dated undrained triaxial tests. When water entered in RH) and wrapped in two plastic bags until testing at 15
the cell, samples remain under the confining pressure and 28 days for unconsolidated undrained triaxial tests
for at least 45 min. The loading speed of 1.2 mm/min and 3, 7, 15 and 28 days for unconfined compressive
was considered for unconfined compressive strength strength. Compaction and Atterberg limits test were
tests. Loading was continued until the load valued carried out immediately after mixing the soil and
decreased with increase of strain for unconfined stabilizers. Distilled water is used for preparing all the
compressive strength test and until 15% strain was specimens.
reached for unconsolidated undrained strength test.
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Cylindrical specimens (with 38-mm-diameter and thickness decreases more with increase of lime content
76-mm-height) were used for unconsolidated and consequently the liquid limit and plastic limit
undrained triaxial test and unconfined compressive decrease as well (Degirmanci et al. 2007; Brooks et al.
strength test. Three specimens were made for each 2011).
type of test. Two specimens were used for tests, The second mechanism that reduces the plasticity
providing difference in tests result, third specimen was index of the soil is pozzolanic reaction between soil
used. and stabilizer, which forms cementitious compounds
that bind soil particles together and fill the void
between soil particles and thus reduce the plasticity
3 Results and Discussion index of the soil (Brooks et al. 2011). Adding 10%
lime to the soil decreased plasticity index from 29 to 3.
3.1 Effects of Stabilizer on Atterberg Limits More reduction in plasticity in the mixture of soil and
lime compared to the state that sludge was used as
The effects of lime and the mixture of lime and steel stabilizer too, can be attributed to more short time
sludge on the Atterberg limits of the soil are presented reaction and more reduction in double layer thickness.
in Table 2. The effect of copper sludge on Atterberg
limits was similar to steel sludge and here, only the 3.2 Effects of Stabilizers on Compaction
results of steel sludge on Atterberg limits are pre- Parameters
sented. It is clear from Table 2 that adding stabilizers
to the soil decreased the liquid limit and plasticity The variation of dry density with increase of moisture
index and increased the plastic limit; however, with content for different ratios of lime to copper sludge is
increase of the ratio of lime to sludge from 40
60 to 100 to
shown in Fig. 2. The changes in maximum dry density
0 (10% lime) decreased the plasticity index, liquid and optimum moisture content at the various ratios of
limit and plastic limit. Moreover, decreasing the lime lime to copper and steel sludge are presented respec-
content and increasing the sludge content resulted in tively in Tables 3 and 4. As distinguished in Fig. 2, in
increasing the Atterberg limits. Maximum and mini- mixture of soil and 10% lime the maximum dry
mum reduction in the plasticity index (PI) of the soil density of the soil decreased from 1.63 to 1.5 and
occurred at the mixture of soil with 10% lime and at optimum moisture content increased from 21.33 to
the ratio of lime to sludge (40 25.92. With increase of ratio of lime to sludge from 40
60) respectively. These 60
observations can be attributed to two underlying to 100 to 0 (10% lime), maximum dry density
mechanisms, namely cation exchange and soil addi- decreased. The decrease of the maximum dry density
tive pozzolanic reaction. Adding lime to the soil can be justified by two reasons. First, because of
causes cation exchange that leads to flocculation, and lighter specific gravity (Gs) of the lime compared to
results in a decrease in double layer thickness, so the solid particles of soil, replacing a part of the soil
liquid limit and plastic limit reduce. Double layer with lime in the compaction mold, results in a decrease
1.65
Table 2 Effect of ratio of lime to s-sludge on Atterberg limits 90/10-CS
80/20-CS
LL PL PI 1.6
Ratio s lime 60/40-CS
Dry density (qr/cm )
sludge 40/60-CS
1.55 100/0
100 40 37 3 clay
0 = 10%lime 1.5
90 44 40 4
10 = 90ss
1.45
80 45 40 5
20 = 80ss
60 47 41 6 1.4
40 = 60ss
40 49 43 6 1.35
60 = 40ss 15 17 19 21 23 25 27 29 31 33
0 54 25 29
0 = clay Moisture content (%)
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Table 3 Compaction
Ratio lime Maximum dry density (g/cm3) Optimum moisture content (%)
parameters for admixture of c sludge
soil, lime and copper sludge
100 1.5 25.92
0 = 10%lime
90 1.49 25
10 = 90cs
80 1.54 24.5
20 = 80cs
60 1.58 24
40 = 60cs
40 1.61 24
60 = 40cs
0 1.63 21.33
0 = clay
Table 4 Compaction
Ratio lime Maximum dry density (g/cm3) Optimum moisture content (%)
parameters for admixture of s sludge
soil, lime and steel sludge
100 1.5 25.92
0 = 10%lime
90 1.48 25
10 = 90ss
80 1.52 24.5
20 = 80ss
60 1.54 24
40 = 60ss
40 1.6 24
60 = 40ss
0 1.63 21.33
0 = clay
in the maximum dry unit weight (Khandaker and test on the mixture of soil and stabilizers was done
Anwar Hossain 2011). In addition, as reported by right after adding water to it, so pozzolanic materials
Brooks et al. (2011), due to cationic exchange reaction do not have sufficient time for chemical reaction
and the integration of soil structure, the void between (Kolawole 1988).
soil particles increases; consequently, the maximum According to the results, replacing a portion of lime
dry unit weight decreases. The increase of optimum with sludge resulted in increasing the maximum dry
moisture content is due to lime hydration and density compared to the mixture of soil and 10% lime
additional water is needed (Khandaker and Anwar and with increase of sludge content, maximum dry
Hossain 2011; Du et al. 2011). Also, as shown in density increased. But at the ratio of lime to sludge
Fig. 2, maximum dry density increases from 1.5 to equal to 90 to 10, a slight decrease of the maximum dry
1.61 with decrease of ratio of lime to sludge from 100 density is observed. This behavior is due to the fact
to 0 (10% lime) to 40 60 compared to the mixture of soil
that the compaction parameters of soil depend on the
and 10% lime (except at a ratio of lime to sludge equal grain size distribution and also on the specific gravity
to 90 to 10). Meanwhile, optimum moisture content (Gs) of soil and stabilizers; consequently, with
decreases slightly from 25.92 to 24. As the amount of replacing the optimum lime content with sludge that
lime that is replaced with sludge increases, the has a higher Gs compared to soil and lime, the
increase of maximum dry unit weight and the decrease maximum dry density increases. However, stabilizers
of optimum moisture content are amplified. The initially cover the soil particles by coating the surface,
sludge has higher Gs compared to lime, therefore resulting in larger grains. As a result, these grains fill
replacing a part of lime with sludge in a compaction more spaces and the void spaces between grains
mold, results in an increase in the maximum dry increases, thereby decreasing the maximum dry unit
density. The slight reduction in optimum moisture weight to a point where these void spaces are
content with decreasing ratio of lime to sludge is due compensated and the maximum dry unit weight
to the fact that the sludge is a pozzolanic material; thus increases thereafter. Only stabilizers with high Gs
in the presence of water at short time, chemical are able to create these effects (Khandaker and Anwar
reaction is insignificant, but the lime immediately Hossain 2011).
begins to react in the presence of water. Compaction
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compressive strength(kPa)
Compressive Strength
Maximum unconfined
2000
1500
The influence of various ratios of lime to steel and
copper sludge and curing time on the unconfined 1000
90/10-CS
compressive strength of the soil, is presented in Figs. 3 80/20-CS
500 60/40-CS
and 4. In these figures, it can be seen that the 40/60-CS
0
unconfined compressive strength (UCS) of the soil 3 8 13 18 23 28 33
increased considerably with adding lime and the Curing me (day)
mixture of lime and sludge to the soil. Also, with the
Fig. 4 Influence of lime, c-sludge and curing time on
increase of curing time, the unconfined compressive unconfined strength
strength of the samples is increased. Corresponding to
Fig. 3, the increase of unconfined compressive As shown in the Figs. 3 and 4, the unconfined
strength at the ratios of lime to steel sludge equal to compressive strength of soil increased with increasing
90 to 10 and 40 to 60 were maximum and minimum, ratio of lime to sludge and curing time. The improve-
respectively. Since at the ratio of lime to sludge equal ment in strength was greater at certain ratios. This
to 40 to 60, the unconfined compressive strength of behavior is attributed to the chemical reactions
soil was less compared to the mixture of soil and 10% between soil and stabilizers that occur in the presence
lime. It can be inferred that at this ratio, replacing a of water and produce cementitious materials that bind
portion of optimum lime content with sludge does not the grains of soil, fill the void between soil particles
have beneficial effects on increase of the soil strength. and cause the improvement of strength (Kamon and
The effects of copper sludge content and curing time Nontananandh 1990; Yin et al. 2007; Brooks et al.
on the maximum unconfined strength is shown in 2011). Three fundamental reactions in soil stabiliza-
Fig. 4. tion are cation exchange, flocculating and pozzolanic
The behavior of samples containing copper sludge reaction. Cation exchange and flocculating are short
was similar to samples containing steel sludge. The time reaction and pozzolanic reaction is long time.
difference is that the maximum strength occurred at With increase of curing time more pozzolanic reaction
the ratio of lime to sludge equal to 80 to 20 for copper takes place and lead to increase of the strength.
sludge. With respect to the results of Figs. 3 and 4, it Perusing microstructure of stabilized soil showed that
can be concluded that the steel sludge was more the void between soil particles which was obvious
effective on increase of the strength of soil compared without curing time was filled with cementitous gel the
to copper sludge. void was not remarkable (Kamon and Gu 2001). e.g.
In Table 5, the results of unconfined compressive The UCS of the sample at the ratio of lime/sludge =
strength test for various ratios of lime to sludge and 80/20 increased from 1052.85 (kPa) to 2193.77 (kPa)
various curing time are presented. for copper sludge and from 986.85 to 2097.77 (kPa)
for steel sludge with increase of curing time. Accord-
ing to Table 5, when the combination of lime and
Maximum unconfined compressive
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between the stabilizer and soil that all amount of lime 5000
90/10-28-800 80/20-28-800
and sludge take place in the reaction and the magni- 60/40-28-800 40/60-28-800
4000
tude of residual lime and sludge is the lowest, thereby 100/0-28-800 0/0-800
produce larger quantities of cementitious gel, leading Deviatoric stress (kPa) 3000
to greater increase in the strength (lime/c-sludge = 80/
20 and lime/s-sludge = 90/10) (Kamon and Non- 2000
tananandh 1990; Brooks et al. 2011).
1000
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3500
3000 4 Conclusion
2500
2000 The effects of lime, copper and steel sludge on the
1500
cs-600 Atterberg limits, compaction parameters, unconfined
1000 cs-800 compressive strength and shear strength parameters of
500 cs-1000
clayey soil were studied. It is concluded from the test
0
0 20 40 60 80 100 120 results that the adding lime and the mixture of lime and
Ratio of lime to c-sludge(40=40ss) sludge cause considerable changes in the engineering
properties of the soil. Results showed that the engi-
Fig. 8 Effect of ratio of lime to c-sludge on maximum
deviatoric stress after 28 days curing neering properties of stabilized soil depend on various
factors such as lime and sludge content, curing time
3500 and type of sludge. It was shown from the test results
Maximum deviatoric stress (kPa)
3000
that adding stabilizer reduced the plasticity index,
increased the optimum moisture content and
2500
decreased the maximum dry density of the soil. It
2000
was observed that the strength of stabilized soil
1500 ss-28-800
increases with increasing the curing time. At the ratio
cs-28-800
1000 of lime to sludge equal to 90/10, 80/20 and 60/40, the
ss-15-800
500 cs-15-800 increase in the strength was greater compared to the
0 mixture of soil and 10% lime, but at the ratio of lime to
0 20 40 60 80 100 120
sludge equal to 40/60, the increase in the strength was
Ratio of lime to sludge (40=40ss , 40=40cs)
less than the ratio of lime to sludge equal to 100/0. The
Fig. 9 Effect of type of sludge and curing time and on maximum gain in unconfined compressive strength
maximum deviatoric stress at confining pressure 800 (kPa) was accomplished at the ratio of lime to sludge equal
to 90/10 for steel sludge and 80/20 for copper sludge.
28 days curing time are presented in Table 7. It is Similar results were obtained for the shear strength
clear that adding lime or combination of lime and parameters of the soil. The maximum cohesion and
sludge as stabilizer, increases cohesion and angle of angle of internal friction was accomplished at the ratio
internal friction of the soil. of lime to sludge equal to 90/10 for steel sludge and
Considering the figures and tables that were 80/20 for copper sludge after 28 days.
presented, the maximum strength for 28 days curing
time occurs at the ratio of lime to sludge equal to 90 to
10 and 80 to 20 for steel and copper sludge,
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Table 6 Maximum deviatoric stress at various ratios and confining pressure (r3) at different curing time
Soil mix 15 day 28 day
r3 = 600 (kPa) r3 = 800 (kPa) r3 = 1000 (kPa) r3 = 600 (kPa) r3 = 800 (kPa) r3 = 1000 (kPa)
Table 7 Cohesion and angle of internal friction tested at potential of expansive soil from Oman. Build Environ
curing time of 28 and 15 days 40:681–687
Al-Sharif M, Attom M (2000) The use of burned sludge as a new
Soil mix 15 day 28 day soil stabilization. In: ASCE environmental and pipline
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C (kPa) U (°) C (kPa) U (°)
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stabilized with fly ash and limestone dust in Philadelphia.
Clay* 231 2 –
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90ss 424.6 27.3 504.3 29.6 phosphygypsum in soil stabilization. Build Environ
80ss 404.9 26.7 458.8 28.36 24(9):3393–3398
Du YJ, Zhang YY, Liu SY (2011) Investigation of strength and
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90cs 393 26.1 443 28 Ghosh A, Subbaro C (2007) Strength characteristics of class F
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