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Lab 4 - Tubular Flow Reactor
Lab 4 - Tubular Flow Reactor
Lab 4 - Tubular Flow Reactor
0 THEORY
A tubular flow reactor (TFR) is a tube or pipe through which reactants flow and are converted
into product. Several of TFR arrange in parallel or series, both horizontal and vertical orientations
are common. The TFR reactor may have a varying diameter along the flow path and has continuous
gradient of concentration in the direction flow [1]. In these reactors, conditions of temperature,
pressure, and gas fluid residence time can be carefully controlled [2]. Chemical reactions take
place in a stream of gas that carries reactants from the inlet to the outlet. Presence of catalyst in
tubes uniform loading is ensured by using special equipment that charges same amount of catalyst
to each tube at a definite rate.
Tubular flow reactors resemble batch reactors in providing initially high driving forces,
which decrease as the reaction progress down the tubes. In TFR, the flow can be laminar as with
viscous fluids in small-diameter tubes and greatly deviate from ideal plug-flow behavior, or
turbulent, as with gases [1]. Laminar flow are more prefer in tubular flow as the mixing and heat
transfer are improved. For small scale reaction such as in small laboratory and in pilot plant reactor,
establishing turbulent flow can result in inconveniently long reactors or may require unacceptably
high feed rates . The tubular flow reactor is one of three reactor types which are interchangeable
on the reactor service unit. The reactions are monitored by conductivity probe as the conductivity
of the solution changes with conversion of reactant to product.
Apparatus:
Materials:
a) Both pumps P1 and P2 were switched off. Valves V2 and V6 were closed.
b) The heaters were switched off.
c) Cooling water was kept to circulate through the reactor while the stirrer motor was switched
on to allow the water jacket to cool down to room temperature.
d) The power for the control panel was switched off.
11.0 RECOMMENDATIONS
There are several factor that can be fix and take into consideration for the experiment run smoothly
and get accurate result. First recommendation is ensure all the equipment is properly calibrated,
functioning, clean and ready to use. Equipment that are malfunction can affected the result as it
influence measurement of mass and volume. Secondly, student must follow the procedure given
carefully. Open and close the valve correctly according to the procedure, perform general start up
and general shut down procedure to run the experiment smoothly. Start the experiment after 1
minutes to stable the conductivity for inlet and outlet. Next, make sure flow rate remain constant
throughout the experiment. Next, check the storage tank all the time during experiment to make
sure there are enough solution for experiment. Lastly, take each measurement multiple times and
take an average reading in order to get more accurate and precise results.
References:
[1] Nasir, H. (2015). Types of Chemical reactors. Production and Operation Engineer, pp 81.
[2] https://link.springer.com/chapter/10.1007/978-1-4471-5307-8_9
[3]https://www.researchgate.net/publication/308797261_RESIDENCE_TIME_DISTRIBUTION
_RTD_IN_OPERATING_PLANT_A_REVIEW
[4] http://www.umich.edu/~essen/html/byconcept/chapter13.pdf