LGC Proficiency Testing Catalogue 2019

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Driving

Quality
Together

2019
Food & Feed
Water & Environment
Beverage
Clinical
Consumer Safety 0001
Forensics
Petroleum

lgcstandards.com/pt ISO/IEC 17043


Proficiency Testing
Proficiency Testing
LGC

LGC provides proficiency testing schemes with For further information please contact one of our local
localised support across a truly global network. sales offices.

LGC
Brazil
1 Hungary
6
11 Netherlands
Tel: +55 12 3302 5880 Tel: +49 (0)281 9887 0 Tel: +49 (0)281 9887 0
Email: bz@lgcgroup.com Email: de@lgcgroup.com Email: de@lgcgroup.com

1,700+ 12,000+
Bulgaria
2 India
7 12 Nordic countries
Tel: +359 (0)2 971 4955 Tel: +91 (0)90 8297 4025 Tel: +49 (0)281 9887 0
Email: bg@lgcgroup.com Email: india@lgcgroup.com Email: de@lgcgroup.com
China
3
Ireland
8 Poland
13
Tel: +86 400 9216156 Tel: 44 (0)161 762 2500 Tel: +48 22 751 31 40
Annual proficiency tests Laboratories served worldwide Email: pt.china@lgcgroup.com Email: ptcustomerservices@ Email: pl@lgcgroup.com
France
4 lgcgroup.com
Romania
14
Tel: +33 (0)3 88 04 82 82 Italy
9 Tel: +40 364 116890
Email: pt.fr@lgcgroup.com Tel: +39 02 22476412 Email: ro@lgcgroup.com
Germany
5 Email: it@lgcgroup.com
Russia
15
Tel: +49 (0)281 9887 0 10 Middle East Tel: +7 812 777 04 88
Email: de@lgcgroup.com Tel: +49 (0)281 9887 0 Email: ru@lgcgroup.com
Email: global.sales@lgcgroup.com

South Africa
16

Tel: +27 (0)11 466 4321


Email: sales.za@lgcgroup.com
Spain
17

Tel: +34 (0)93 308 4181


Email: es@lgcgroup.com
18 United Kingdom
Tel: +44 (0)161 762 2500
12
Email: ptcustomerservices@
lgcgroup.com
15
8
19 USA + Canada
18 11 13
5 Tel: +1 231 668 9700
4 6
14 Email: apigroup@lgcgroup.com
19 9
17
2

3 We serve laboratories
10 worldwide.
If you don’t see a local office
7
above please contact us:

160+
Tel: +44 (0)161 762 2500
Email: ptcustomerservices@
lgcgroup.com

Serving laboratories in over 1 16


160 countries worldwide

2 lgcstandards.com/pt lgcstandards.com/pt 3
Proficiency Testing
Proficiency Testing
LGC

Great results are born out of confidence and by


working with LGC Proficiency Testing you can have

LGC
the assurance that your decision making is informed,
reliable and effective.

If you are a laboratory seeking accreditation


to ISO/IEC 17025 or ISO 15189, or an organisation
looking for consistency in delivering a quality
product, then LGC will have a proficiency testing
scheme designed for you.

Driving Quality
Together
Fulfill accreditation Demonstrate competency Compare results with Proficiency Testing (PT) is a If you are managing multiple Using an accredited PT provider
requirements. to customers and regulatory laboratories around requirement for accreditation laboratories and are looking provides you with the assurance
bodies. the world. to ISO/IEC 17025 and ISO 15189. for consistency in results, of the quality and reliability of the
LGC operates PT schemes across LGC offers fully managed service. LGC is accredited to
the food, beverage, environmental, solutions for large groups. ISO/IEC 17043 by the United
clinical, pharmaceutical, consumer Multi-laboratory, multi-method Kingdom Accreditation Service
safety, forensic and petroleum and multi-analyst reporting (UKAS). In addition we are certified
sectors – your laboratory will get is all covered by our exclusive to ISO 9001.
the support it needs in demonstrating web based PORTAL platform.
the effectiveness of your quality
system.
Manage risk through Verify methods Educate and train staff.
early warning of and instrumentation.
potential problems.

4 lgcstandards.com/pt lgcstandards.com/pt 5
Proficiency Testing
LGC

Our world class experts provide a comprehensive PORTAL is the secure web based data reporting
service ensuring a reporting process focused on speed, and analysis tool exclusively available to LGC Proficiency
Testing scheme participants. It is a laboratory’s gateway
ease and efficiency and which delivers excellent value.
to improving performance, an online hub for results
submission, report downloads, data export and trend
analysis ­— anytime, anywhere.

Procurement, preparation, 6 — 12
dispensing and quality Weeks prior
control testing of test
materials.

Despatch of test Week 1


materials and instructions
to participants.

Participants analyse test Week 2 — 4 New features for 2019 include a fast, simple
Round materials and report results and responsive user interface, a brand new
reviewed. through PORTAL interactive PT report, enhanced trend analysis
Changes (portal.lgcstandards.com) charts, a PT event calendar and more.
made if as instructed and within the
required. specified deadline.

Results analysed and the Week 5


performance of laboratories
compared using appropriate
techniques, such as
performance scores.

Reports issued and Week 5


participants notified
once reports are available
on PORTAL.
Full control of all of your LGC Proficiency
Testing data 24 hours a day.

portal.lgcstandards.com
6 lgcstandards.com/pt 7
Proficiency Testing
Proficiency Testing
LGC

LGC Proficiency Testing schemes are operated in a


wide range of sectors from Food to Forensics, Clinical

LGC
to Consumer Safety. Whatever your quality needs, LGC
will have a scheme that delivers the confidence
in results that you are looking for.

Water &
Food & Feed Environment Beverage Clinical Consumer Safety Forensics Petroleum FAQS

12 QMS 22 AQUACHECK 30 BAPS 38 IPT 48 PHARMASSURE 54 QUARTZ 60 OIL 63 About


Food Water, Agricultural Brewing Analytes Immunosupressant Pharmaceutical Forensic Blood Oils & Fuels proficiency
Microbiology Soils & Sludges Toxicology testing

13 QDCS 24 QWAS 31 DAPS 39 TDM 49 COSMETICS 55 FAE 64 About LGC


Dairy Water Alcoholic Drinks Therapeutic Cosmetics & Forensic Analysis Proficiency
Chemistry Microbiology Drugs Toiletries for Explosives Testing

14 QMAS 25 AIR PT 33 MAPS 40 TOX 50 TOYTEST 56 FIRMS 65 About the LGC


Meat & Fish Air & Stack Malt Analytes Toxicology Toy Safety Forensic Proficiency
Emissions Isotope Testing process
Ratio Mass
Spectrometry
15 QFCS 26 CONTEST 33 QBS 41 DAU 51 NiMS 66 About LGC
Food Contaminated Soft Drinks Drugs of Abuse Nickel Migration Proficiency
Chemistry Land & Fruit Juice in Urine Testing schemes

16 QCS 27 HYGIENE 34 SUPS 42 DOF 67 About reporting


Chocolate Environmental Sugar Drugs in Oral & evaluating
Hygiene Fluid results
Monitoring

17 AFPS 43 DAH 70 About privacy


Animal Feed Drugs of Abuse & confidentiality
in Hair

18 QGS 71 About driving


Gelatine 44 CLS quality together
Clinical
Microbiology
19 STEC Laboratory
Shiga Toxin
E.coli

8 lgcstandards.com/pt lgcstandards.com/pt 9
Food & Feed 12

13
QMS
Food Microbiology

QDCS
Dairy Chemistry
Food & Feed
Scheme Selector

14 QMAS Scheme Distribution Test Test Material Matrix* Analyte Group*


Meat & Fish per year

Food & Feed


15 QFCS QMS 12 Microbiological Oatmeal and skimmed Comprehensive range of
Food Chemistry Food milk powder, tea, herb microorganisms of relevance
Microbiology and spice. to food products, including
16 QCS pathogens, indicator
Chocolate organisms, spoilage
organisms and probiotics.
17 AFPS
Animal Feeds QDCS 4 Chemical Butter, cheese, cream, Chemical parameters covering
Dairy Chemistry milk, milk powder, whey routine nutritional analysis and
18 QGS powder, yoghurt and more complex testing such as
Gelatine standard solutions. mycotoxins and antibiotics.

19 STEC QMAS 6 Chemical and Meat, fish Chemical and microbiological


Shiga Toxin E.coli Meat & Fish Microbiological and shellfish. parameters relevant to meat,
fish and seafood industry.
Trace elements, authenticity
and veterinary drug residues.
Salmonella and other pathogens,
indicator organisms.

QFCS 6 Chemical Bread, cake, cereals, Chemical parameters


Food Chemistry cured meat, flour, fruit/ covering nutritional analysis,
vegetable, hard cheese, toxic elements, pesticides
nuts, oils, ’ready to eat’ and other contaminants.
products, rice, tea and
standard solutions.

QCS 3 Chemical and Chocolate and Chemical and microbiological


Chocolate Microbiological cocoa powder. parameters relevant to the
chocolate and food testing
industries including nutritional
and elements analysis.

AFPS 4 Chemical and Animal feed: (e.g. broiler, Comprehensive range of


Animal Feeds Microbiological cattle, chicken, pig, chemical and microbiological
sheep), calf replacer analysis of animal feeds
and premix. covering proximates and
contaminants, Salmonella and
other pathogens, indicator
organisms.

QGS 2 Chemical and Gelatine, gelatine Physicochemical testing and


Gelatine Microbiological hydrolysate. microbiological parameters of
relevance to gelatine.

STEC 4 Microbiological Skimmed milk powder, Detection of pathogens,


Shiga Toxin ground beef powder, STEC E.coli (serovars O26;
E.coli with lyophilised vials. O45; O103; O111; O121; O145;
O157:H7).

* The full range and availability of test materials and analytes is determined on an annual basis and may be added
or removed. For accredited and non-accredited status please see current application form/scheme description.

10 lgcstandards.com/pt 11
QMS The LGC Quality in Microbiology
Scheme (QMS) is intended for use
by microbiologists working in the
In rare cases it may also lead
to civil and criminal charges. QDCS The LGC Quality in Dairy
Chemistry Scheme (QDCS) is a
comprehensive proficiency testing
For laboratories that perform the
analysis of dairy products using
traditional ‘wet’ chemistry
Food Microbiology food industry, including dairy, ready Laboratories carrying out
Dairy Chemistry scheme available to laboratories techniques, as well as determinations
meals, dried foods, herbs and spices microbiological testing need performing compositional and safety by infrared analysers and other
and many other sectors. to be able to demonstrate that analysis in the dairy sector. methods, participation in a relevant
Food & Feed

they are producing accurate and LGC Proficiency Testing scheme can
Food testing is an essential element meaningful results to help identify Laboratories may test dairy products provide confidence that results are
of the ‘Hazard Analysis Critical problems before they affect the to ensure a commercial product meaningful and accurate which, in

Food & Feed


Control Point’ (HACCP) process quality and safety of products. performs within preset quality turn, helps to ensure the safety of
in food production as it verifies the This can be achieved if a standards, or to look for adulterations dairy foodstuffs.
controls are working at the critical comprehensive quality assurance or contaminants that could adversely
points in manufacturing. Failures programme is conducted, which affect a product.
leading to food poisoning outbreaks includes regular participation
can have a devastating effect on in a suitable proficiency testing
reputation, brand value, a decline scheme.
in consumer confidence in the
product and ultimately profits.

Test material* Analyte* Test material* Analyte*

Oatmeal Enumeration of aerobic psychrotrophs. Butter Moisture, pH, Salt.


Detection of Shigella species, Vibrio parahaemolyticus, Vibrio species.
Hard & soft cheese Ash, Calcium, Fat, Lactose, Moisture, pH, Protein, Salt, Sodium.
Skimmed milk Enumeration of Salmonella species, Cronobacter species, Yersinia enterocolitica.
powder Double & Fat.
single cream
Oatmeal or Enumeration of Bacillus cereus, Bacillus species, Coagulase positive-
skimmed milk staphylococci, Coliforms, Clostridium perfringens, Enterobacteriaceae, Whipping cream Fat, Titratable acidity.
powder Enterococci, Escherichia coli, Lactic acid bacteria, Listeria monocytogenes,Listeria
species, Pseudomonas species, Staphylococcus species, Thermotolerant Freeze dried Aflatoxin M1, Antibiotics (penicillin and/or sulfur-based,
coliforms. Anaerobic sulphite-reducing bacteria, Mesophilic aerobic spores, milk beta lactam based), Phosphatase.
Mesophilic anaerobic spores, Thermophilic aerobic spores, Total aerobic
mesophilic count, Total anaerobic mesophilic count, Osmophilic yeast, Osmophilic Milk Calcium, Freezing point depression, Lactose, Protein, pH, Titratable acidity, Total
mould, Yeast, Mould, Yeast and mould. solids.

Detection of Clostridium species, Coliforms, Enterobacteriaceae, Escherichia coli, Skimmed, Fat.


Escherichia coli O157 (non toxigenic strain), Listeria monocytogenes, Listeria semi-skimmed
species, Salmonella species. & whole milk

Lyophilised Enumeration of Bifidobacterium species (Probiotic), Lactobacillus species (Probiotic), Skimmed milk Ash, Fat, Insolubility index, Moisture, Protein, Scorched particles, Titratable acidity,
material Campylobacter species. powder WPNI
Detection of Campylobacter species.
Identification of an unknown microorganism. Whole milk Fat, Insolubility index, Minerals (calcium, potassium, copper, sodium, chloride,
Identidication of Salmonella species (serology). powder iron, magnesium, manganese), phosphorus, zinc), Moisture, Protein, Titratable
acidity, WPNI.
Tea Enumeration of Coagulase positive-staphylococci, Coliforms, Total aerobic
mesophilic count, Yeast and mould. Milk powder Vitamins A, C, D.

Herbs, spice, tea Detection of Salmonella species. Whey powder Ash, Fat, Lactose, Moisture, Protein, Scorched particles.

Paper exercise Colony count and calculation of number of microorganisms. Whey protein Ash, Bulk density, Fat, Insolubility index, Lactose, Moisture, pH, Protein
(image) concentrate

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed. Yoghurt Fat, Protein, Total solids.
For accredited and non-accredited status please see current application form/scheme description.
Buffer solution pH.

Potassium COD.
hydrogen phthalate

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

12 lgcstandards.com/pt lgcstandards.com/pt 13
QMAS The LGC Quality in Meat and Fish
Analysis Scheme (QMAS) is intended
for chemists and microbiologists
human disease. Customers demand
products that are authentic and
genuine, preventing contamination
QFCS The LGC Quality in Food Chemistry
Scheme (QFCS) is specifically
designed to promote the quality and
factors that need to be considered
when producing food.
Meat & Fish working in, or providing analytical from both deliberate fraud and
Food Chemistry comparability in the measurement of The food we eat can contain
services to the meat, fish and accidental cross-contamination a range of analytes in food products. potentially harmful chemicals,
shellfish processing industries. during processing. some naturally occurring, some as
Food & Feed

An incredible variety of foodstuffs contaminants absorbed from soil


International consumption of meat Consumers want to be assured their are available worldwide and all year and water. Testing these end-use
and fish in human diets has food has been thoroughly tested by round. Technology now allows products is fundamental for food

Food & Feed


increased rapidly. Therefore the competent laboratories. EU Regulation suppliers to harvest, preserve and safety and stability. Consistent good
manufacturing processes need to be 882/2004 requires official control distribute within a short period of performance in a LGC Proficiency
highly regulated, to help prevent food laboratories to be accredited to time. Consequently food quality, Testing scheme will allow
safety issues occurring. ISO/IEC 17025 and use external consumer satisfaction and laboratories to show, with
means of monitoring performance government regulations are all confidence, the quality of results
Measures must be taken to prevent such as proficiency testing. to third parties.
contamination with hazardous
chemicals above specified limits, Test material* Analyte*
and to reduce the number of
microorganisms capable of causing Bread or cake Acidity, Ash, Calcium, Chloride, Dietary fibre (total), Fat, Iron, Moisture, Protein,
Sodium, (Total sugars– bread only), (Vitamins B1, B2, B3 – cake only).

Cereal based food Ash, Carbohydrate (total and available), Dietary fibre (total), Energy, Fat, Iron,
Moisture, Phosphate, Protein, Salt, Sodium, Sugars (total), Vitamins A, B1, B2, B3,
Chemistry* Analyte* B5, B6, B9, B12, C, D.

Dried and cured Ash, Carbohydrate, Dietary fibre, Energy, Fat, Moisture, pH, Phosphate, Protein, Cereal grain, Dried Arsenic, (Inorganic arsenic – rice only), Arsenic (total), Cadmium, Lead, Mercury,
meat Salt, Sodium, Sugars (total). fruit, Edible oil, (Selenium - green tea only).
Green tea, Rice
Lyophilised meat Nitrate, Nitrite.
Edible oil Anisidine value, Colour, Fatty acid compositions, Free fatty acids, Iodine value, Peroxide
Meat Fat (total), Hydroxyproline, Mono-unsaturated fats, Poly-unsaturated fats, or fat value, Saponification value (acid number), Unsaponifiable matter, Water.
Saturates, Total trans fatty acids. Arsenic (total), Cadmium, Lead, Mercury,
Phosphorus, Zinc. Species authenticity to be screened for presence of other meat Extra virgin 3,5 Stigmastadienes, Delta-7-stigmastenol, Ethyl esters, Fatty acid composition,
species. olive oil Free fatty acids (acidity), Insoluble impurities, K232, K270, Moisture and volatile
matter at 103°C, Peroxide value, Polyphenols (total), Sterols (total), Wax content.
Precooked, Ash, Calcium, Carbohydrate, Dietary fibre, Energy, Fat, Moisture, pH, Phosphate,
processed and raw Potassium, Protein, Salt, Sodium, Sugars (total). Olive oil 3,5 Stigmastadienes, Beta-sitosterol (apparent), Campesterol, Delta ECN 42, Delta
meat K, Erythrodiol and uvaol, Fatty acid composition, Free fatty acids (acidity), K270,
Rancimat stability at 120°C, Wax content.
Fish Fish speciation, Ash, Fat, Moisture, pH, Protein, Salt, Histamine, Trimethylamine (TMA),
Total volatile nitrogen (TVN), Arsenic (total), Cadmium, Lead, Mercury, Phosphorus, Mixed fat spread Omega 3, Omega 6, pH, Salt, Mono-unsaturates, Poly-unsaturates, Saturates,
Zinc. Total trans fatty acids,Vitamins A and D, Water.

Shellfish Arsenic (total), Cadmium, Lead, Mercury, Phosphorus, Zinc. Flour Ash, Calcium, Fat, Gluten, Iron, Moisture, Protein.

Meat, cheese, cake Water activity.


Microbiology* Analyte*
Pre-prepared food Ash, Carbohydrate (total and available), Cholesterol, Dietary fibre (total), Energy,
Lyophilised meat Coagulase-positive staphylococci, Coliforms, Clostridium perfringens, (ready meals) Fat, Moisture, Phosphate, Protein, Salt, Mono-unsaturates, Poly-unsaturates,
Enterobacteriaceae, Escherichia coli, Lactic acid bacteria, Mould, Pseudomonas, Saturates, Sodium, Sugars (total), Trans fatty acids (total).
Sulphite-reducing clostridia, Total aerobic mesophilic count, Yeast.
Pesticides in fruit/ Fungicides, Herbicides, Organochlorine, Organophosphorus, Synthetic
Detection of Listeria species, Listeria monocytogenes, Salmonella species. vegetable pyrethroids, Triazines.

Lyophilised fish or Coagulase-positive staphylococci, Enterobacteriaceae, Escherichia coli, Total Pesticides in Fungicides, Herbicides, Organochlorine, Organophosphorus, Synthetic
shellfish + Vial aerobic mesophilic count. green tea pyrethroids.

Detection of Salmonella species, Vibrio parahaemolyticus, Vibrio species. Nuts Aflatoxins B1, B2, G1, G2, Total Aflatoxins.

Lyophilised meat + Detection of Campylobacter species, Escherichia coli O157 (non-toxigenic strain). Snacks Acrylamide.
Vial
Standards solutions Benzoic acid, Sorbic acid, Sulfur dioxide. Acesulfame K, Aspartame, Saccharin,
* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed. Sucralose. Allura red, Brilliant blue, Carmoisine, (Indigo carmine, Ponceau 4R,
For accredited and non-accredited status please see current application form/scheme description. Quinoline yellow, Sunset yellow, Tartrazine.

Tomato paste/puree Ash, Brix, pH, Salt, Total solids.

Vegetables Nitrate, Perchlorates.

14 lgcstandards.com/pt lgcstandards.com/pt 15
QCS AFPS The LGC Animal Feeds Proficiency
Scheme (AFPS) is specifically
designed to meet the needs of
Major food safety crises have
occurred as a result of the
contamination of animal feed
Chocolate Animal Feeds laboratories performing chemical causing risks to animal and human
or microbiological analysis health. The resulting recalls have
of animal feeds. caused significant financial damage
Food & Feed

as large quantities of product have


Animal feed quality is highly to be destroyed; and considerable
regulated since many animals, damage to the reputation of

Food & Feed


or their products, will ultimately businesses involved. Participation
be converted into food for human in the LGC AFPS Proficiency
consumption. Testing scheme can form part of a
comprehensive quality system that
seeks to promote high standards
and avoid potential risks.

The LGC Quality in Chocolate Consumption of contaminated


Scheme (QCS) is intended for chocolate is rare yet there have
chemists and microbiologists working been sporadic global outbreaks
in the chocolate and cocoa powder which have led to product recalls.
manufacturing industries. The consequences could include
damaged reputations, possible legal
Chocolate products are one actions resulting in huge financial
of the specific food commodities damage and more. A comprehensive
whose composition is controlled quality assurance programme which
at European level. Directive includes regular participation in a
2000/36/EC ‘relating to cocoa and suitable proficiency testing scheme,
chocolate products intended for may help to safeguard against such
human consumption’, sets common negative outcomes.
rules and definitions with regard Chemistry* Analyte*
to the composition, manufacture,
packaging and labelling of chocolate Animal feed ADF, Ash insoluble in hydrochloric acid, Crude (ash, fat, fibre, protein), Moisture,
and cocoa products. NDF, PPD, Starch, Sugars. Aflatoxins B1, B2, G1, G2, Total Aflatoxins,
Ochratoxin-A.

Animal feed, Arsenic, Cadmium, Calcium, Chloride, Chromium, Cobalt, Copper,


pre-mix Iron, Lead, Magnesium, Manganese, Mercury, Phosphorus, Potassium, Selenium,
Chemistry* Analyte* Sodium, Zinc.

Chocolate Butyric acid, Fat, Moisture, Nitrogen (total), Sugars (total), Theobromine. Wet pet food Ash insoluble in hydrochloric acid, Crude (ash, fat, fibre, protein),
Moisture, Starch, Sugars.
Cocoa powder Ash, Fat, Moisture, Theobromine, Arsenic (total), Cadmium, Lead.

Microbiology* Analyte*
Microbiology* Analyte*
Simulated Enumeration of Clostridium perfringens, Clostridium species Coliforms,
Chocolate and Enumeration of Coliforms, Enterobacteriaceae, Enterococci, animal feed Enterobacteriaceae, Escherichia coli, Total viable count, Yeast and Mould. Detetction
cocoa powder Total aerobic mesophilic count, Yeast and Mould. of Escherichia. coli O157 Listeria monocytogenes, Listeria species, Salmonella
Detection of Salmonella species. species.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed. * The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description. For accredited and non-accredited status please see current application form/scheme description.

16 lgcstandards.com/pt lgcstandards.com/pt 17
QGS STEC Most Escherichia coli (E.coli)
strains are harmless and can
live in the gut of humans without
As the organisms are pathogens,
the test is qualitative rather than
quantitative, seeking to identify the
Gelatine Shiga Toxin E.coli causing any issues. However Shiga presence of these organisms rather
toxin-producing E.coli (STEC) strains than enumerating the levels.
can cause serious illness and there
Food & Feed

is therefore a requirement to test for The primary aim of the LGC Shiga
these organisms in foods which may toxin E.coli (STEC) Scheme is to
be of risk of contamination by STEC. enable laboratories performing the

Food & Feed


A comprehensive quality assurance microbiological analysis of food and
programme featuring the LGC STEC dairy products to monitor their
Proficiency Testing scheme is an performance and compare with
excellent way of helping to keep that of their peers. STEC also aims
consumers safe and ensuring to provide information to participants
reputations for quality are maintained. on technical issues and
methodologies relating to testing
There are many different strains of of food and dairy products.
STEC, and these can be distinguished
by their serology. The main ones found
to cause illness in humans are
serovars O26, O45, O103, O111, O121,
O145 AND O157:H7, known as ‘the big
six’ in the USA.
The LGC Quality in Gelatine The most common use of gelatine
Scheme (QGS) has been developed is in the food and pharmaceutical
in collaboration with the trade body, industries as well as in the
Gelatine Manufacturers of Europe cosmetics, photographic and
(GME). printing industries.

GME members account for nearly If a laboratory is involved in the


half of the worldwide gelatine quality control analysis of gelatine,
production and the key role of the QGS provides test materials in
GME is to ensure that gelatine is gelatine and gelatine hydrolysate
manufactured to a consistently high matrices to represent a realistic
quality for the benefit of gelatine challenge, with relevant chemical,
customers and consumers. physical, and microbial tests.

Chemistry* Analyte* Test Material* Analyte*

Gelatine Ash, Gel strength (Bloom), Isoelectric point, Moisture, pH, Viscosity. Skimmed milk Detection of pathogens, STEC E.coli
powder with (serovars O26; O45; O103; O111; O121; O145; O157:H7).
lyophilised vials

Microbiology* Analyte*
Ground beef Detection of pathogens, STEC E.coli
Gelatine Enumeration of mesophilic anaerobic spores, Sulphite-reducing bacteria, Total powder with (serovars O26; O45; O103; O111; O121; O145; O157:H7).
hydrolysate aerobic mesophilic count, Clostridium perfringens, Coliforms, Enterobacteriaceae lyophilised vials
Escherichia coli, Staphylococcus aureus, Salmonella species.
* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed. For accredited and non-accredited status please see current application form/scheme description.
For accredited and non-accredited status please see current application form/scheme description.

18 lgcstandards.com/pt lgcstandards.com/pt 19
Water & Environment 22

24
AQUACHECK
Water, Agricultural Soils
& Sludges

QWAS
Water & Environment
Scheme Selector

Water Microbiology
Scheme Distribution Test Test Material Matrix* Analyte Group*
25 AIR PT per year
Air & Stack Emissions

26 CONTEST AQUACHECK 20 Chemical, Clean waters and waste Inorganic, organic and
Contaminated Land Water, Ecotoxicological, waters, agricultural soils elemental analytes for
Agricultural Soils Physical and and sewage sludge. qualitative and quantitative
27 HYGIENE & Sludges Radiochemical analyses. Determination of
Environmental Hygiene radiochemical

Water & Environment


Monitoring and ecotoxicological
parameters.

QWAS 10 Microbiological Waters (e.g. bathing, Routine microbiological


Water environmental, testing, indicator organisms
Microbiology mineral, potable, and complex pathogens.
process, recreational,
sea, surface, waste)
and simulated
effluent sludge.

AIR PT 6 Chemical and Filters, tubes and Gravimetric, organic and


Air & Stack Physical impinger solutions. elemental analytes at a
Emissions range of concentrations.

CONTEST 5 Chemical and Soil extracts, soil Inorganic, organic and


Contaminated Physical materials, solid waste, elemental analytes
Land standard solutions and measured in soil, leachates
trammel fines. and standard solutions.

HYGIENE 3 Microbiological Swabs, contact Routine microbiological


Environmental plates, dip slides testing, indicator organisms
Hygiene and ATP systems. and complex pathogens.
Monitoring

* The full range and availability of test materials and analytes is determined on an annual basis and may be added
or removed. For accredited and non-accredited status please see current application form/scheme description.

20 lgcstandards.com/pt lgcstandards.com/pt 21
AQUACHECK Test material* Analyte*

Water, Agricultural Soils Clean water


(Organics)
Acid herbicides, Acrylamide, BTEX, Chlorinated solvents, Chlorophyll a,
Fungicides, Geosmin and MIB, Haloform solvents, OC and OP pesticides, PAHs,
& Sludges PCBs, PFOA, PFOS, Formaldehyde, Phenols, Taste and odour, Triazines and Urea
herbicides, UV absorbing organics constituents.

Clean water Aqueous tritium, Gross alpha, Gross beta.


(Radiochemistry)

Ground water Metals, Toxic metals.


(Metals)

Qualitative water Organics by purge, trap and/or headspace GCMS, Qualitative determination
Water & Environment

Water & Environment


(Organics) of unknown contaminant.

Clean water BOD, Chromium (VI), COD, DOC, MBAS, Metals, Non-ionic surfactants,
(Inorganics) Suspended solids, Toxic metals, Turbidity.

Poorly buffered pH.


water

Soil Arsenic, Cadmium, Chromium, Copper, Lead, Mercury, Molybdenum, Nickel,


The industry leading LGC Process waters must be kept clean Vanadium, Zinc, Selenium, Total boron, Water extractable boron, Fluoride, Total
AQUACHECK scheme has been in to ensure product quality. As water nitrogen, Total phosphorus, Total potassium, Cobalt, Iron, Manganese, Total
continuous operation since 1985. sources can change regular testing solids, Loss on ignition, pH, Extractable phosphorus, Extraction of potassium,
Test materials are provided for the is advised. Extraction of magnesium, Extraction of sodium, Organic carbon content,
analysis of major inorganic/organics; Conductivity, Carbonate content.
metals; phenols; organochlorine Participation in the LGC
pesticides and many others. AQUACHECK scheme allows Clean water Chlorine (free, total), Inorganic disinfection by-products.
laboratories to identify problems
Water is vital in sustaining all natural before they affect the quality and Hard and soft Colour, Conductivity, Major inorganic components, Nutrients and others, pH, TDS.
systems. Each source requires safety of waters. Participants will water (Inorganics)
regular analyses to determine safety be able to demonstrate
and suitability of use. Potable water independently that they are Ecotoxicology Ecotoxicology tests.
must be good in quality and quantity producing accurate and meaningful
and free from harmful chemicals and results to laboratory management High salinity Conductivity, Major ions, pH, TOC, TDS.
microorganisms. Discharged water and customers. potable water
from local wastewater treatment
plants and industry must comply Wastewater Acid herbicides, AOX, BTEX, Chlorinated solvents, Haloforms, OC and OP
with environmental guidelines. pesticides, Phenols, PCBs, PAHs, Triazines and Urea herbicides. Mineral oil,
Oil and grease.

Effluents & BOD, Chromium (VI), COD, DOC, Metals, MBAS, Non-ionic surfactants, Non
wastewater specific analytes, Nutrients and other analytes, Settleable solids, Suspended
solids, Toxic metals, Turbidity.

Effluents & Ammonia, Cyanide, Major wastewater analytes, Metals, Nitrogen, Phenol (total),
wastewater Phosphate, Sulfate, Sulfide (total).
(Industrial)

Sludge Arsenic, Cadmium, Chromium, Cobalt, Copper, Fluoride, Iron, Lead, Manganese,
Mercury, Molybdenum, Nickel, Selenium, Total boron, Total nitrogen, Total
phosphorus, Total potassium, Vanadium, Zinc.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

22 lgcstandards.com/pt lgcstandards.com/pt 23
QWAS The LGC Quality in Water Analysis
Scheme (QWAS) has been
specifically developed for the
Regulations specify how often
water sources are sampled, how
sampling is done, how analysis will
AIR PT The LGC AIR PT scheme is
a partnership between LGC and
the UK Health and Safety Laboratory
activity and so requires regular
monitoring to assess exposures and
the effectiveness of containment or
Water Microbiology microbiological analysis of waters be performed, what microorganisms
Air & Stack (HSL). ventilation. Many everyday activities
and effluent sludge. are to be tested, and the acceptable Emissions create air pollutants with known or
limits for the target microorganisms. The scheme is operated by LGC suspected harmful effects on human
Microorganisms occur in water and is supported by the technical health and the environment. Such
naturally and the majority are For laboratories responsible for expertise at HSL. The scheme pollution can cause both short and
relatively harmless. However the analysis of waters, particiption in combines our scientific and long term effects on human, plant
contamination of water from faecal a relevant LGC Proficiency Testing production expertise in different and animal life.
sources can lead to large outbreaks scheme can provide confidence that areas, providing an integrated
of disease. results of these analyses and the scheme for all laboratories Participation in the AIR PT scheme
equipment used to produce those undertaking analysis of samples supports a laboratory’s quality
In many countries, water microbiology results are meaningful and accurate from various fields of air monitoring. system in the monitoring and
Water & Environment

is the subject of legislation. which, in turn, helps to ensure the measurement of air quality in a wide

Water & Environment


safety of water. We take air for granted: it is range of contexts.
ubiquitous, essential, and life-giving.
However, it is easily polluted by our

Test Material* Analyte* Test material* Analyte*

Bathing, Coagulase-positive staphylococci, Staphylococcus species, Workplace air Aldehydes, Chromium (VI), Lactose, Metals, Respirable grade quartz by FTIR
recreational Sulphite-reducing Clostridia. (filters) and XRD.
& surface water
Workplace air VOCs (charcoal sorbent and thermal desorption).
Bathing, surface Enterococci (faecal streptococci), Escherichia coli, Faecal coliforms, Total (diffusion tubes)
& wastewater coliforms, Salmonella species.
Workplace air Metals.
Effluent sludge Escherichia coli, Salmonella species. (dust)

Environmental Legionella pneumophila by culture, Legionella pneumophila by PCR. Legionella Ambient air (filters) Anions, Metals.
water species by culture, Legionella species by PCR.
Ambient air Nitrogen dioxide (as nitrite), VOCs (thermal desorption).
Potable water Clostridium perfringens, Coliforms, Enterococci (faecal streptococci), Escherichia (diffusion tubes)
coli, Pseudomonas aeruginosa, Sulphite-reducing Clostridia, Sulphite-reducing
Clostridia spores ONLY, Total aerobic count at 22°C and 37°C, Legionella species Indoor/chamber air Qualitative and quantitative VOCs (charcoal sorbent and thermal desorption).
(low levels). (diffusion tubes)

Identification of (non-pathogenic) organism to correct family, genus or Stack emissions Ammonia, Hydrogen chloride, Hydrogen fluoride, Mercury, Nitrogen oxides
species level. (impinger solutions) as (NO2), Sulphur dioxide, Metals, Volume of solution.

Process water Pseudomonas species, Total aerobic count, Yeast, Mould, Yeast and mould (total). Stack emissions Dust (total solids).
(rinsing solution)
Sea water Enterococci (faecal streptococci), Escherichia coli, Faecal coliforms, Total
coliforms. Gravimetric filters Dust by gravimetry (mass of solids), Fly ash, Metals.
(workplace air,
Lyophilised Unknown microorganism. ambient air, stack
material emissions)

Paper exercise Colony count and calculation of number of microorganisms. * The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
(image) For accredited and non-accredited status please see current application form/scheme description.

LGC is the accredited provider of the PT scheme.


* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

24 lgcstandards.com/pt lgcstandards.com/pt 25
CONTEST The LGC CONTEST scheme offers
a comprehensive range of analytes
in soils, soil extracts and standards
which corrode over time releasing
toxic substances into previously
clean soils.
HYGIENE
Contaminated Land solutions for the analysis of metals,
Environmental Hygiene
inorganic contaminants, organics, Participation in a proficiency testing Monitoring
soil leachates and solid waste. scheme for soil, such as CONTEST,
is a requirement of the UK
Land contamination can pose both Environment Agency’s Monitoring
environmental and human health Certification Scheme (MCERTS)
risks. The main causes of ‘Performance Standard for
contamination are the direct Laboratories Undertaking Chemical
discharge of industrial wastes, Testing of Soil’.
domestic pollution, over-usage of
pesticides, oil and fuel dumping,
Water & Environment

leaching of wastes from landfills and

Water & Environment


leaking underground storage tanks

Test material* Analyte* Regular hygiene monitoring In healthcare, regular environmental


of environmental surfaces and monitoring can demonstrate
Soil, acid extract Chromium (VI), Metals, Toxic metals. equipment in manufacturing cleaning and disinfection has been
of soil, standard and healthcare is a key part carried out correctly, helping
solution of any quality system. to reduce the potential spread
of infection.
Soil and/or Ammonia, Cyanide (complex, free, total), Dry matter, Easily liberated sulfide, Ensuring control of microbial
standard solution Fluoride (total), Loss on ignition, pH, Sulfate (total), Sulfur (total), Thiocyanate, contamination can directly affect Participation in the LGC HYGIENE
Water soluble (boron, chloride, fluoride, sulfate), BTEX, Distillable phenolic the quality of both product scheme can help to demonstrate
substances, Elemental sulfur, Phenols, PAHs, PCBs, TOC, TPHs, VOCs. and patient care. that environmental monitoring
is effective and under control.
Soil, standard BTEX, TPH, VOCs, OC pesticides. In food and beverage industries,
solution it can help avoid food spoilage and Regular monitoring allows
food poisoning, both of which can information to be collected to
Soil leachate COD, Conductivity, Cyanide (complex, free), Major ions, Metals, pH, damage brand value and profits. review and assess hygiene quality
PI,Thiocyanide, TOC/DOC, Toxic metals. to ensure legislative standards are
In pharmaceutical manufacturing, being met. It also helps to determine
Soil waste and DOC, Dry matter content ratio, Major ions, Metals, PI, TDS, Toxic metals. parenteral medicines, and the the effectiveness of control systems
leachate (Waste environment they are produced designed to prevent microbial
acceptance in, need to be free from harmful contamination.
criteria) microbial strains.

Standard solution Qualitative test of SVOCs.

Trommel fines Loss on ignition (FINES). Test material* Analyte*

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed. Surface testing Enumeration of Enterobacteriaceae, Total aerobic mesophilic count, Yeasts
For accredited and non-accredited status please see current application form/scheme description. by swabbing and/or Moulds.

Detection of Listeria species, Salmonella species.

Surface testing by Total aerobic mesophilic count.


Contact plates

Surface testing by Enumeration of Coliforms, Total viable count.


dip-slides

Surface testing by ATP levels.


ATP monitoring

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

26 lgcstandards.com/pt lgcstandards.com/pt 27
Beverage 30

31
BAPS
Brewing Analytes

DAPS
Alcoholic Drinks
Beverage
Scheme Selector

32 MAPS Scheme Distribution Test Test Material Matrix* Analyte Group*


Malt Analytes per year

33 QBS
Soft Drinks & Fruit Juice BAPS up to 12 Chemical, Ales, craft beers, lagers, Routine and complex
Brewing (Chemistry) Microbiological and alcohol free/low chemical tests relevant to
34 SUPS Analytes and Sensory alcohol beers. the brewing industry for
Sugar 6 quality control and product
(Microbiology) characterisation. Brewery
spoilage microorganisms.
12 Sensory assessments
(Sensory) in aroma and taste evaluation.

DAPS 4 Chemical Distilled spirits, whisky, Chemical tests including


Alcoholic wort, ciders, wines esters relevant for alcoholic
Drinks and fortified wines, beverages and intermediate
liqueurs, cream liqueurs, process samples.
and other alcoholic
beverages.

Beverage
MAPS 12 Chemical and Brewing/distilling malted Chemical and physical tests
Malt Physical barley, barley, malt flour, for quality checks and
Analytes malted wheat and complex analysis, including
black/crystal malt. mycotoxins analysis.

QBS 4 Chemical and Carbonated drink, Chemical tests for quality


Soft Drinks Microbiological carbonated drink checks and complex
& Fruit Juice (degassed), dilutable/ parameters including
ready to drink fruit juice, vitamins and mycotoxins.
soft drink and apple Comprehensive range
juice. of microorganisms of
relevance to beverage
products, including
pathogens, indicator
organisms and spoilage
organisms.

SUPS 12 Chemical and Cane or beet sugar, Chemical tests of relevance


Sugar Microbiological raw sugar and to the sugar processing,
molasses. food and beverage industries.
Microorganisms of relevance
to sugar products, including
pathogens and indicator
organisms.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added
or removed. For accredited and non-accredited status please see current application form/scheme description.

28 lgcstandards.com/pt lgcstandards.com/pt 29
BAPS The LGC BAPS scheme is jointly
run by LGC Proficiency Testing and
Campden BRI, promoting quality in
aroma and taste characteristics
of real beers and can compare their
results with the Campden BRI
DAPS The LGC DAPS Alcoholic Drinks
scheme covers a wide range of
products including distilled spirits,
Consistent analytical performance
in the laboratory, supported by
participation in the LGC Proficiency
Brewing Analytes the measurement of chemical, sensory panel that provide an expert
Alcoholic Drinks wine, ciders and prepared lifestyle Testing scheme, can help ensure
microbiological and sensory analytes profile for the sample to enable drinks, such as ready-to-drink the consistency of the product,
in real beer. immediate training of panels if cocktails and fruit based beverages. keeping customers loyal to their
required. favourite drinks.
Routine and complex chemical tests Whilst alcohol content is an
for quality control and product For laboratories that perform the important analysis for duty
characterisation are available in our analysis of beer, participation in payment purposes, there are many
lager and ale test materials. BAPS can provide confidence that other analytes that influence the
results are meaningful and accurate flavour of the product.
Microbiological test materials contain which in turn, helps to ensure
organisms typically encountered in consistency in the quality of beer
the brewing industry. For sensory and integrity of the brand.
analysis, participants evaluate various
Beverage

Chemistry* Analyte* Test Material* Analyte*

Lager/ale Alcohol by volume, Bitterness, Carbon dioxide, Colour at 430nm, Gravity Fermented and Alcohol, Gravity (original, residual, final), pH (fermented only), Residual fermentable

Beverage
(apparent, original, present), Haze (0ºC, 20ºC), Original extract, pH, Refractive simulated wort sugars (total amount of glucose, maltose, maltotriose).
index, Sulfur dioxide, Total gas pressure.
Clear/dark distilled Acidity (total, volatile), Alcoholic strength (actual, apparent), Chill difference, Colour,
Lager 2-Methyl butanol, 3-Methyl butanol, 2+3 Methyl butanol. Acetaldehyde, Calcium, spirit & scotch Density, Ethyl carbamate, Fructose, Glucose, Sucrose, Sugars (total), NDMA, pH,
Carbohydrate (total), Chloride, Copper, Diacetyl as VDK, Dimethyl disulfide, whisky Refractive index, Specific gravity, Total solids, Turbidity (Haze). 2-Methyl butanol,
Dimethyl sulfide, Energy value (kcal), Energy value (kJ), Ethyl acetate, Ethyl 3-Methyl butanol, 2 + 3 Methyl butanols, Acetal, Acetaldehyde, Ethyl acetate,
hexanoate, Foam stability (HRV), Free alpha amylase, Free diacetyl, Free Furfural, Iso-amyl acetate, Iso-butanol, Methanol, n-Butanol, n-Propanol. Calcium,
2,3-pentanedione, Glucose, Hydrogen sulfide, Iron, Iso-alpha-acids, Iso-amyl Copper, Iron, Magnesium, Potassium, Sodium. 5-HMF, Coniferaldehyde, Ellagic
acetate, Iso-butanol, Magnesium, Maltose, Maltotetraose, Maltotriose, acid, Gallic acid, Scopoletin, Sinapaldehyde, Syringaldehyde, Syringic acid, Vanillic
Methanethiol, Methylthioacetate, Nitrate, n-Propanol, Phosphate, Polyphenols acid, Vanillin. 2-Phenethyl acetate, 2-Phenethyl ethanol, Ethyl decanoate, Ethyl
(total), Potassium, Sodium, Sulfate, Tetra-iso-alpha-acids, TSN, Zinc dodecanoate, Ethyl hexadecanoate, Ethyl hexanoate, Ethyl octanoate, Ethyl
tetradecanoate, Ethyl-9-Hexadecenoate.
Dark/craft ale Alcohol by volume, Bitterness, Colour at (430nm, 530nm), Diacetyl as VDK, Free
2,3-pentanedione, Free diacetyl, Iso-alpha-acids, Tetra-iso-alpha-acids. Simulated spirit Alcoholic strength (actual, apparent), Citric acid, Ethyl carbamate, Fructose,
Glucose, Sucrose, Sugars (total), Glycerol, Maltose, NDMA, pH, Propylene glycol.
Alcohol free/low Alcohol by volume (qualitative, quantitative), Bitterness, Colour at 430nm, Gravity
alcohol beer (apparent, present), pH. Non chill filtered 2-Phenethyl acetate, 2-Phenethyl ethanol, Ethyl decanoate, Ethyl dodecanoate,
whisky Ethyl hexadecanoate, Ethyl hexanoate, Ethyl linoleate, Ethyl linolenate, Ethyl
octadecanoate, Ethyl octanoate, Ethyl oleate, Ethyl tetradecanoate, Ethyl-9-
hexadecenoate.
Sensory* Analyte*
Ciders Acidity (total, volatile), Actual alcoholic strength, Carbon dioxide, Colour, Haze, pH,
Lager/ale Alcoholic/Solvent, Astringent, Bitter, Body, Burnt, Caramel, Cereal, DMS, Fruity/ Specific gravity, Sulfur dioxide (total).
Citrus, Fruity/Estery, Hop, Linger, Malty, Other sulfur, Oxidised/Aged, Sour, Sweet,
and others. White/rosé and Acidity (total, volatile), Alcoholic strength (actual), Ascorbic acid, Citric acid, Colour
red wine at (420nm, 520nm, 620nm), Copper, Fructose, Glucose, Iron, Lactic acid, Malic
acid, pH, Reducing sugars, Sorbic acid, Specific gravity, Sulfur dioxide (free, total).

Ready to drink Acidity (total, volatile), Alcoholic strength (actual), Ascorbic acid, Benzoic acid,
Microbiology* Analyte* Brix, Carbon dioxide, Citric acid, Colour absorbance, Density, Dissolved oxygen,
pH, Refractive index, Sorbic acid, Specific gravity, Sugars (total).
Lyophilised material Identity of organisms, Lactic acid bacteria count, Total aerobic bacterial count,
High level/ Total aerobic microbial count. Total anaerobic microbial count, Wild yeast, count: Liqueur 2-Methyl butanol, 3-Methyl butanol, 2 + 3 Methyl butanols, Acidity (total, volatile),
low level Identity of organisms. Acetal, Acetaldehyde, Alcoholic strength (actual), Brix (total), Ethyl acetate,
Furfural, Iso-amyl acetate, Iso-butanol, Methanol, n-Butanol, n-Propanol, pH,
Refractive index, Residue, Specific gravity, Total solids.
* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description. Cream liqueur Specific Gravity, Actual Alcoholic Strength, pH, Residue, Iso-Butanol, 2+3
Methylbutanols, Furfural, Total Brix, Refractive Index (20°C), Total solids.
LGC is the accredited provider of the PT scheme.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.
Campden BRI
food and drink innovation

30 lgcstandards.com/pt lgcstandards.com/pt 31
MAPS The LGC MAPS scheme covers
test materials from the full range
of barley and malted barley used
and Institute of Brewing and Distilling
(IBD) methods, as well as
a number of other physical and
QBS The LGC Quality in Beverages
Scheme (QBS) is specifically tailored
for chemists and microbiologists
contamination from microorganisms,
chemicals and foreign matter could
compromise product quality.
Malt Analytes for brewing and distilling. chemical methods.
Soft Drinks working in the soft drinks and fruit
& Fruit Juice juice industries (including carbonated It is vital to prevent these types
Malt is a complex product and Meeting the demanding specifications drinks). of errors as they can lead to the
forms a key ingredient in brewing laid down by brewers and distillers is manufacture of out-of-specification
and distilling. It is considered to be critical to the business of any maltster Soft drinks and fruit juices are widely product resulting in product wastage
at the heart of the process, providing and is greatly dependent on the consumed throughout the world and and disposal, lost production and
most of the sugars and complex quality of the malting barley. For this these global customers expect their the associated costs.
carbohydrates which produce reason the accuracy of the laboratory beverages to always look and taste
the alcohol and flavour of the analysis is essential as it will ultimately the same. The industry continuously The LGC QBS scheme will allow
final product. decide if the product is suitable for aims to meet these high expectations. laboratories to monitor analytical
use in the production plant. However, maintaining and confirming quality, helping to ensure that
These test materials are analysed the quality and reliability of a given products are being manufactured
for a wide range of analytes, using product is a considerable challenge to the highest standards.
European Brewing Convention (EBC) for production facilities and quality
control laboratories meaning that
Beverage

Test Material* Analyte* Chemistry* Analyte*

Brewers and Alpha amylase, Cold water extract, Diastatic power (DP IoB and DPWK), Dimethyl Apple juice Patulin.

Beverage
distillers malt sulfide (free, total), Dimethyl sulfide precursor, EBC fraction IV, EBC reject fraction,
Friability, Glassy (whole) corns, Glycosidic nitrile, Hartong VZ45, Homogeneity, Carbonated drinks Acidity (as citric acid monohydrate), Brix, Carbon dioxide, Fructose, Glucose, pH,
Malt mod homogeneity, Malt modification, Moisture, NDMA, Nitrogen (total), Partly Sucrose.
unmodified grains, Phenols (total), Residual sulfur dioxide, Sieving tests.
Carbonated drinks Acesulfame K, Aspartame, Benzoic acid, Caffeine, Cyclamic acid (as free acid),
Brewers and Beta glucan, Boiled wort colour, Colour, Extracts, Extract difference, FAN, (degassed) Saccharin (as free imide), Sorbic acid (as free acid), Sucralose, Sulfur dioxide (free,
distillers malt Fermentability (boiled), Kolbach index, pH, TSN, Viscosity. total).
(EBC wort)
Dilutable and Acesulfame K, Acidity (as citric acid monohydrate), Aspartame, Benzoic acid, Brix,
Brewers and Beta glucan, Colour, Extracts, Extract difference, FAN, Fermentability (boiled, ready to drink Caffeine, Cyclamic acid (as free acid), Fructose, Glucose, pH, Saccharin (as free
distillers malt unboiled), pH, Predicted spirit yield, Soluble extract difference, Soluble extract, imide), Sorbic acid (as free acid), Sucrose, Sulfur dioxide (free, total).
(IOB wort) SNR, TSN, Viscosity.
Fruit juice Acidity (as citric acid monohydrate), Brix, Calcium, Fructose, Glucose, pH,
Barley BRF (8ml test), EBC fraction IV, EBC reject fraction, Germinative capacity, Phosphorus, Potassium, Magnesium, Sodium, Antimony, Cadmium, Iron, Lead, Tin,
Germinative energy, Hectolitre weight, Moisture, Nitrogen (total), Sieving tests, Zinc.
Thousand corn weight.
Liquid material Vitamin C (Ascorbic acid).
Black malt Colour, Moisture.
Soft drink Antimony, Cadmium, Calcium, Iron, Lead, Magnesium, Phosphorus, Potassium,
Crystal malt Colour, Degrees of crystallisation, Moisture. Sodium, Tin, Zinc. Vitamin B3 (Nicotinamide), Vitamin B5 (Pantothenic acid),
Vitamin B6 (Pyridoxine), Vitamin B12 (Cyanocobalamin), Vitamin C (Ascorbic acid),
High diastatic Moisture, DPWK, Diastatic Power, Alpha Amylase, IoB Soluble Extract 0.7mm, Vitamin E (DL-alpha-Tocopherol), Total steviol glycosides, Rebaudioside A.
power malt TSN (Total Soluble Nitrogen) FAN (Free Alpha Amino Nitrogen), Glycosidic Nitrile.

Malt flour NDMA. Mycotoxin analysis (Ochratoxin A and Deoxynivalenol (DON)).


Microbiology* Analyte*
Malted wheat Moisture, DPWK, Diastatic Power, Alpha Amylase, Protein, Extract: 0.2mm, Boiled
Wort Colour, Kolbach Index, EBC Fermentability (Boiled), IoB Extract 0.7mm, pH, Fruit juice Enumeration of Lactic acid bacteria, Mould, Total aerobic mesophilic count, Yeast.
Colour, TSN (Total Soluble Nitrogen), SNR (Soluble Nitrogen Ratio), FAN (Free
Alpha Amino Nitrogen), Viscosity, Beta Glucan. Detection of Escherichia coli, Escherichia coli O157 (non toxigenic strain), Listeria
monocytogenes, Salmonella species.
* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description. Liquid material Enumeration of Lactic acid bacteria, Mould, Thermophilic acidophilic bacteria,
(membrane Total aerobic mesophilic count, Yeast.
filtration)
Detection of Escherichia coli, Guaiacol producing thermophilic acidophilic
bacteria, Listeria monocytogenes.

Soft drink Enumeration of Lactic acid bacteria, Mould, Total aerobic mesophilic count, Yeast.
Detection of Escherichia coli.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

32 lgcstandards.com/pt lgcstandards.com/pt 33
SUPS The LGC SUPS scheme is suitable
for all laboratories who analyse sugar
and sugar products.
validated methods of analysis
to aid the trade in sugar and
sugar products.
Sugar
The quality of sugar has to be ICUMSA representatives are involved
continually maintained, because in the review of progress and
in addition to its sweet taste it brings performance of SUPS and provide
additional benefits to the foods and advice on the operation and future
beverages it is used in, such as developments of the scheme.
improving texture, enhancing flavour,
providing consistency, providing Participating in SUPS will provide
natural preservation and many more. data to help identify performance
issues with methods used and will
LGC collaborates with the underpin the quality of the analytical
International Commission for Uniform results used to inform the
Methods of Sugar Analysis (ICUMSA) commercial decisions about
who provide robust, internationally the product.
Beverage

Chemistry* Analyte*

Cane or beet sugar Ash, Colour, Moisture, Polarisation, Reducing sugars, Reflectance grade,

Beverage
Sulfur dioxide, Sediment (insoluble), Turbidity. Arsenic, Cadmium, Copper, Iron,
Lead, Mercury.

Molasses Dry substance, Fermentable sugars, pH, Reducing sugars, Sucrose, Sulfated ash.

Raw sugar Ash, Colour, Dextran, Moisture, Polarisation, Reducing sugars, Starch.

Microbiology* Analyte*

Lyophilised Enumeration of Thermophilic acidophilic bacteria (TAB), Total aerobic mesophilic


material count, Osmophilic yeast and mould, Yeast and mould.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

LGC is the accredited provider of the PT scheme.

34 lgcstandards.com/pt 35
Clinical 38

39
IPT
Immunosupressant

TDM
Therapeutic Drugs
Clinical
Scheme Selector

40 TOX Scheme Distribution Test Test Material Matrix* Analyte Group*


Toxicology (Apr-Mar) per year

41 DAU
Drugs of Abuse in Urine IPT 12 Clinical Blood and plasma. Routine quantification of
Immunosup- Immunosuppressant drugs
42 DOF pressant including Ciclosporin;
Drugs in Oral Fluid Tacrolimus; Sirolimus;
Everolimus; Mycophenolic Acid.
43 DAH
Drugs of Abuse in Hair TDM 12 Clinical Blood, serum and urine. Routine quantification of
Therapeutic therapeutic drugs including
44 CLS Drugs Anti-epileptics; Cardiac;
Clinical Microbiology Analgesics; Substance abuse
Laboratory treatments; Psychoactives;
Antibiotics; Smoking-related.

TOX 12 Clinical Blood, serum and urine. Drug and alcohol


Toxicology determination; case studies.

DAU 4 Clinical Urine from volunteers Mixtures of drugs and/or their


Drugs of Abuse and known drug users. metabolites from six major
in Urine classes.

DOF 4 Clinical Oral fluid from Mixtures of drugs and/or their


Drugs in volunteers and known metabolites from six major
Oral Fluid drug users. classes.

DAH** 4 Clinical Human hair. Mixtures of drugs and/or their


Clinical

Clinical
Drugs of metabolites from six major
Abuse in Hair classes.

CLS** 12 Clinical & Range of relevant Bacteriology,


Clinical Microbiology materials. Mycobacteriology, Mycology,
Microbiology Parasitology, Virology,
Laboratory Molecular Multiplex discipline.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added
or removed. For accredited and non-accredited status please see current application form/scheme description.

** Please note that the DAH and CLS schemes are currently not included in our scope of accreditation.

36 lgcstandards.com/pt 37
IPT TDM The LGC Therapeutic Drugs
Monitoring (TDM) proficiency testing
scheme provides independent
The operation of the LGC TDM
scheme is supported by an Advisory
Group consisting of members of
Immunosuppressant Therapeutic Drugs performance assessment for the the professional bodies, scheme
Monitoring routine quantification of a wide range participants, and others experienced
of anti-epileptic and other in the field. The scheme reports on
therapeutic drugs. the performance of U.K. participants
(who have clinical responsibilities) to
TDM is a measurement of specific the National Quality Assurance
drug concentration levels at timed Advisory Panels for Chemical
intervals in patients, usually through Pathology.
blood/serum samples, and is
necessary where control of drug
concentrations is required to achieve
optimum treatment for the patient, or
where there is a narrow range
between the therapeutic
and toxic levels.

Test Material* Analyte*

Therapeutic Amikacin, Carbamazepine, Carbamazepine+CBZ-epoxide, Caffeine, CBZ-epoxide,


The LGC Immunosuppressant To successfully make these drug mixture Clonazepam, Digoxin, Ethosuximide, Gentamicin, Lamotrigine, Lithium,
proficiency testing scheme provides informed decisions laboratories (lyphilised human Methotrexate, Phenobarbitone, Phenytoin, Primidone, Theophylline, Tobramycin,
independent performance need to demonstrate that drug serum) Vancomycin, Valproate.
assessment for laboratories measurements are reliable,
performing quantification of reproducible and accurate. Anti-epileptic Brivaracetam, Felbamate, Gabapentin, Lacosamide, Levetiracetam,
immunosuppressant drugs in blood drugs OH-oxcarbazepine, Pregabalin, Perampanel, Retigabine (Ezogabine), Rufinamide,
and plasma. The operation of the LGC IPT (lyophilised human Tiagabine, Topiramate, Vigabatrin, Zonisamide.
Clinical

scheme is supported by an serum)


Immunosuppressant drugs are Advisory Group consisting of
a class of drugs that suppress, members of the professional Cardiac drugs Amiodarone, Desethylamiodarone, Flecainide.
or reduce, the strength of the bodies, scheme participants, (lyophilised human
body’s immune system. and others experienced in the field. serum)

Clinical
In addition to being used to prevent The scheme reports on the Analgesic mixture Diclofenac, Ibuprofen, Tramadol.
organ rejection, they are often used performance of U.K. participants (lyophilised human
to treat autoimmune disorders (who have clinical responsibilities) serum)
such as lupus, psoriasis, and to the National Quality Assurance
rheumatoid arthritis. Advisory Panels for Chemical Substance abuse Buprenorphine, EDDP, Methadone, Norbuprenorphine.
Pathology. & treatment
Regular blood tests are essential for (lyophilised human
monitoring therapeutic levels and serum)
whether dosage changes
are needed. Psychoactive Amisulpride, Amitriptyline/Nortriptyline, Aripiprazole/Dehydroaripiprazole,
drugs Citalopram/Norcitalopram, Clomipramine/Norclomipramine, Clozapine/
(lyophilised human Norclozapine, Doxepin/Nordoxepin, Dothiepin/Northiaden, Duloxetine,
serum, new born Escitalopram, Fluphenazine, Fluvoxamine, Haloperidol, Imipramine/Desipramine,
calf serum) Fluoxetine/Norfluoxetine, Maprotiline/Normaprotiline, Mianserin, Mirtazapine/
Normirtazapine, Olanzapine, Paroxetine, Perphenazine, Quetiapine/Norquetiapine,
Risperidone/HO-risperidone, Sertraline/ Norsertraline, Sulpiride, Thioridazine,
Trazodone, Trimipramine/Nortrimipramine, Venlafaxine/ Norvenlafaxine,
Test Material* Analyte* Ziprasidone, Zuclopenthixol.

Human blood Ciclosporin/Tacrolimus, Everolimus, Sirolimus. Non-smoking Cotinine, Nicotine.


compliance
Plasma Mycophenolic acid. (lyophilised human
serum)
* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description. Antibiotics Amikacin, Gentamicin, Teicoplanin, Tobramycin, Vancomycin.
(liquid human Atomoxetine, Methylphenidate. Ritalinic Acid.
serum)

Clobazam and Clobazam, Norclobazam.


Norclobazam

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

38 lgcstandards.com/pt lgcstandards.com/pt 39
TOX The LGC Toxicology (TOX)
proficiency testing scheme is
designed to provide an independent
For laboratories performing these
analyses, participation in TOX can
provide confidence that results are
DAU The LGC Drugs of Abuse in Urine
(DAU) scheme is designed to provide
an independent performance
Laboratories and clinics are
encouraged to participate
in suitable PT/EQA schemes
Toxicology performance assessment of meaningful and accurate.
Drugs of Abuse assessment of laboratories and to ensure the highest standard
laboratories undertaking clinical in Urine clinics that provide routine services of drug testing is achieved
and/or forensic toxicological The operation of our TOX scheme is for detection of drugs of abuse through independent assessment
analytical services. supported by an Advisory Group in urine. of measurement quality.
consisting of members of the
Toxicological analyses may be professional bodies, scheme Human urine has been used for The operation of the LGC DAU
undertaken on biological specimens, participants, and others experienced many years to detect the presence scheme is supported by an
predominantly blood, serum and in the field. The scheme reports on of illicit drugs. Urine testing may be Advisory Group consisting of
urine. In general, analyses are the performance of U.K. participants requested for a variety of reasons, members of professional bodies,
undertaken for a range of substances (who have clinical responsibilities) including health care, occupational scheme participants, and others
including prescription and non- to the National Quality Assurance monitoring, insurance screening, experienced in the field. The scheme
prescription drugs, illicit drugs Advisory Panels for Chemical legal and forensic purposes. Errors reports on the performance of U.K.
and alcohol. Pathology. in tests could have severe participants (who have clinical
consequences, such as dismissal responsibilities) to the National
from work or miscarriage of justice. Quality Assurance Advisory
Panels for Chemical Pathology.

Test Material* Analyte* Test Material* Analyte*

Human serum Ethanol, Paracetamol (Acetaminophen), Salicylic acid. Urine test materials Amfetamines and stimulants, Cannabinoids, Cocaine and metabolites, Ethyl
obtained from glucuronide, Ethyl sulfate, Gamma-Hydroxybutyrate (GHB), Minor tranquillizers,
Human blood Carboxyhaemoglobin, Ethanol, Paracetamol (Acetaminophen), Salicylic acid. volunteers and Non-opiate narcotics, Opiates. Other current drugs and/or metabolites may also
known drug users be included.
Urine Ethanol. which regularly
Clinical

contain mixtures
Lyophilised urine Gammahydroxybutyrate. of drugs and their
metabolites
Whole blood Acetone, Ethanol, Ethylene glycol, Isopropyl alcohol, Methanol.

Table to be * The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.

Clinical
Human serum Toxicology case studies include various analytes with clinical or forensic scenario. For accredited and non-accredited status please see current application form/scheme description.
and urine

Whole blood
toxicology created
Test materials contain analytes which are pre-defined by our Advisory Group and
the requests of participants.

Lyophilised human Diazepam, Nitrazepam, Nordazepam, Oxazepam, Temazepam.


serum Zaleplon, Zolpidem, Zopiclone.
Alprazolam, Bromazepam, Clonezepam, Lorazepam, Midazolam.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

test materials and analytes is determined on an annual basis and may be added or removed, for
accredited and non-accredited status please see current application form/scheme description. The
full range and availability of test materials and analytes is determined on an annual basis and may
be added or removed, for accredited and non-accredited status please see current application
form/scheme description.

40 lgcstandards.com/pt lgcstandards.com/pt 41
DOF The LGC Drugs in Oral Fluid (DOF)
scheme provides performance
assessment for laboratories and
methods are utilised, the information
obtained may be very misleading
and inaccurate.
DAH** The LGC Drugs of Abuse in Hair
(DAH) scheme is suitable for
laboratories performing forensic
the assessment of the regularity of
drug use (or continued abstinance)
and sample stability.
Drugs in Oral Fluid clinics who provide analytical
Drugs of Abuse analysis of hair for drugs of
services for drugs in oral fluid. To minimise this risk, laboratories in Hair abuse and provides an independent Test materials provided consist
Samples are provided as real should perform routine quality assessment of measurement quality. of real cut (2–3mm pieces) human
human oral fluid. control tests and participate in hair that has been declared free from
suitable PT/EQA schemes. Drugs and their metabolites become common drugs of abuse.
Advances in technology have incorporated in hair when ingested.
enabled oral fluid testing for the The operation of our DOF scheme An analysis for these drug residues The analytes are then incorporated
presence of many drugs. Oral fluid is supported by an Advisory Group can provide a useful assessment by a method that includes soaking.
collection is often less invasive, consisting of members of the of an individual’s intake of drugs Drugs (and/or metabolites) from six
relatively easy to perform, and, in professional bodies, scheme over a prolonged period of time. major classes are included
forensic situations, can be achieved participants, and others experienced during the scheme year.
under close supervision to prevent in the field. The scheme reports on The detection time of drugs in hair
adulteration or substitution of the performance of U.K. participants is significantly greater than other The operation of our DAH scheme
the samples. (who have clinical responsibilities) samples commonly tested such is supported by an Advisory Group
to the National Quality Assurance as blood, urine and saliva. consisting of members of the
Drug testing is extremely accurate Advisory Panels for Chemical professional bodies, scheme
and reliable when all aspects Pathology. Advantages of analysing hair participants, and others experienced
of the testing process are carried samples for the presence of drugs in the field.
out correctly. However, if poor include a large window of detection,
procedures and inadequate testing
Clinical

Test Material* Analyte* Test Material* Analyte*

Oral fluid test Amfetamines and stimulants, Cannabinoids, Cocaine and metabolites, Human hair Identification and quantification of Amfetamines and stimulants, Benzodiazepines,
materials obtained Minor tranquillizers, Non-opiate narcotics, Opiates, Other current drugs Cannabinoids Cocaine and metabolites, Opiates.
from volunteers and/or metabolites may also be included.

Clinical
and known drug Other current drugs and/or metabolites may also be included.
users which
regularly contain * The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
mixtures of For accredited and non-accredited status please see current application form/scheme description.
drugs and their
** Please note that the DAH scheme is currently not included in our scope of accreditation.
metabolites from
six major classes

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

42 lgcstandards.com/pt lgcstandards.com/pt 43
CLS** Test Material* Analyte*

Clinical Microbiology Bacteriology Blood culture, CSF culture, Ear/Eye culture, Group B, Strep culture, N.
gonorrhoeae culture, Sputum, Stool culture, Throat culture, Urine colony count,
Laboratory Urine culture, Wound culture, Susceptibility Testing, Bordetella pertussis,
Bordetella Parapertussis, Bordetella parapertussis, C. difficile Toxin, C. difficile
Antigen, Chlamydia trachomatis, Neisseria gonorrhoeae, Gram Stain
Interpretation, Leukocytes, Stain Quality, Sputum Specimen Quality, Bacterial
vaginosis, Nugent Score, Group B Strep, Legionella pneumophila Antigen,
Methicillin-Resistant Staphylococcus aureus culture, Methicillin-Resistant
Staphylococcus aureus, Staphylococcus aureus, Mycoplasma pneumoniae,
Streptococcus pneumoniae Antigen, Group A Strep, Group C/G Strep,
Vancomycin-Resistant Enterococcus.

Mycobacteriology Acid Fast Bacilli Smear, Mycobacterium tuberculosis complex; Rifampin


resistance, Mycobacteriology culture ID.

Mycology Mycology culture ID.

Parasitology Blood parasite ID, Trichomonas vaginalis.

Virology HPV; HPV genotyping, RSV Antigen; Influenza A, Antigen; Influenza B Antigen;
Influenza A or B Antigen; Adenovirus Antigen, Rotavirus Antigen.
The LGC Clinical Microbiology Focusing on the detection,
Laboratory (CLS) scheme is characterisation and quantification Molecular Multiplex
for laboratories performing of bacteria, viruses, fungi and
microbiological analysis of parasites microbes, the CLS Blood Pathogen Acinetobacter sp, Acinetobacter Baumannii, Citrobacter sp., Enterobacteriaceae,
clinical samples and provides scheme ensures that laboratories Panel (multiplex) Enterobacter sp., Enterobacter cloacae complex, Enterococcus sp., Enterococcus
an independent assessment of are able to diagnose, treat and faecalis, Enterococcus faecium, Escherichia coli, Haemophilus influenza, Klebsiella
measurement quality. The CLS prevent infectious diseases. oxytoca, Klebsiella pneumoniae, Listeria sp., Listeria monocytogenes, Neisseria
Clinical

scheme also provides information meningitides, Proteus sp, Pseudomonas aeruginosa, Serratia marcescens,
to participants on technical issues The operation of our CLS scheme Staphylococcus sp., Staphylococcus aureus, Staphylococcus epidermidis,
and methodologies relating to is supported by an Advisory Staphylococcus lugdunensis, Streptococcus sp., Streptococcus agalactiae,
Clinical Microbiology. Group. Streptococcus anginosus group, Streptococcus Pneumoniae, Streptococcus
pyogenes, Candida albicans, Candida glabrata, Candida krusei, Candida

Clinical
Test materials mimic clinical parapsilosis, Candida tropicalis, Resistance Gene.
specimens in a wide array of
samples that are included in the CLS Gastrointestinal Campylobacter sp., C. difficile toxin A /B, Enteroaggregative E. col, E. coli O157,
scheme, from the Bacteriology, Panel (multiplex) Plesiomonas shigelloides, Salmonella, Shigella,Shiga Toxin, Vibrio, Entamoeba
Mycobacteriology, Mycology, histolytica, Astrovirus, Sapovirus.
Parasitology, Virology and
Molecular Multiplex disciplines. Meningitis Panel Escherichia coli K1, Haemophilus influenza, Listeria monocytogenes, Neisseria
(multiplex) meningitides, Streptococcus agalactiae, Streptococcus pneumoniae,
Cytomegalovirus, Enterovirus, Herpes simplex virus, Human parechovirus,
Varicella zoster virus.

Respiratory Panel Bordetella holmesii, Bordetella pertussis, Chlamydophila pneumoniae,


(multiplex) Mycoplasma pneumoniae, Adenovirus, Coronavirus, Human Metapneumovirus
(hMPV), Influenza A, Influenza B, Parainfluenza, Respiratory Syncytial Virus, RSV A,
RSV B, Rhinovirus.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

** Please note that the CLS scheme is currently not included in our scope of accreditation.

44 lgcstandards.com/pt lgcstandards.com/pt 45
Consumer Safety 48

49
PHARMASSURE
Pharmaceutical

COSMETICS
Cosmetics & Toiletries
Consumer Safety
Scheme Selector

50 TOYTEST Scheme Distribution Test Test Material Matrix* Analyte Group*


Toy Safety per year

51 NiMS
Nickel Migration PHARMASSURE 4 Chemical, Pharmaceutical Basic and advanced chemical
Pharmaceutical Physical and products and standard analysis, microbiological
Microbiological solutions. analysis and sterility testing.

COSMETICS 4 Chemical and Cream, lipstick, lipgloss, Chemical parameters of


Cosmetics Microbiological liquids, mouthwash, relevance to the cosmetics
& Toiletries and toothpaste. and toiletries testing industries.
Microbiological tests including
spoilage and indicator
organisms.

TOYTEST 4 Chemical, Toys, paper exercises, Interpretation of toy safety


Toy Safety Microbiological, real materials and standards, various physical
Physical and standard solutions. measurements, azo-dyes,
Instrument metals and phthalates.
Techniques

NiMS 2 Chemical Alloy disks, jewellery Nickel release and surface


Nickel and Physical or other appropriate area.
Migration articles.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added
or removed. For accredited and non-accredited status please see current application form/scheme description.

Consumer Safety
46 lgcstandards.com/pt 47
PHARMASSURE COSMETICS
The LGC PHARMASSURE Regular participation in a LGC
proficiency testing scheme has Proficiency Testing scheme offers
been specifically designed to meet a truly independent assessment of
Pharmaceutical the needs of the pharmaceutical measurement quality, which enables
Cosmetics & Toiletries
industry. The test materials are participants to compare their
provided for chemical and analytical capabilities with peers.
microbiological analysis including Managers are able to monitor trends
sterility testing. in their laboratory’s performance
over time and enhance the training
The regulations surrounding the of individuals as they participate in
manufacture of pharmaceutical frequent assessment.
products and laboratories testing
them are wide ranging, and Successful participation in
compliance with GMP/GLP PHARMASSURE is recognised as
requirements is aimed at ensuring a demonstration of laboratory quality
the safety and efficacy of all and competency by a range of third
pharmaceutical preparations. parties, customers, regulators and
accreditation bodies.

Chemistry* Analyte* The LGC COSMETICS proficiency Manufacturers have a duty to ensure
testing scheme is intended for that potentially harmful products are
Format depends Acid/base titration, Density, Melting point, Other basic titration (actual analytes chemists and microbiologists not placed on the market. Products
upon test type (oil, dependant on test), pH, Refractive index. performing product and ingredient must undergo chemical,
powder, solution) testing in the beauty and personal microbiological and physical testing
care products industries. to ensure safety, quality and
Format depends Advanced titration (potentiometric, non-aqueous), Flame spectroscopy, GC, legislative requirements are met.
upon test type IR/FTIR, LOD, Moisture by Karl Fischer, Polarimetry, TLC, UV, Viscosity, NMR Cosmetics have been in use for
(powder, solution) spectroscopy and X-ray Powder Diffraction (XRPD). thousands of years, and the potential If a laboratory performs these
for harm to the wearer has been analyses, participation in the LGC
Powder or solution HPLC analysis. present ever since the use of toxic COSMETICS scheme can provide
chemicals such as lead sulfite confidence that results are
Powder Arsenic, Cadmium, Chromium, Copper, Lead, Mercury, Zinc. (galena) as an eye make-up by meaningful, accurate and will
the ancient Egyptians. allow for comparison to peers.
Tablets Dissolution, Physical measurements.
Consumer Safety

Solutions Low level conductivity, Particulate determination.

Consumer Safety
Microbiology* Analyte* Chemistry* Analyte*

Lyophilised Enumeration and/or identification of a single microorganism. Lipstick, lip gloss Arsenic, Cadmium, Chromium, Lead, Mercury, Nickel.
material and powder
(low-level for direct
culture or filtration) Cream Hydroquinone.

Lyophilised Enumeration of bile-tolerant Gram-negative bacteria, Candida albicans, Liquid cosmetic Density, pH, Viscosity.
material Escherichia coli, Mould, Staphylococcus aureus, Total aerobic microbial count,
(Mixed Total bacterial count, Total yeast and mould, Yeast. Detection of bile-tolerant Mouthwash, Antimony, Arsenic, Barium, Copper, Fluoride, Mercury, Selenium, Zinc.
microorganisms) Gram-negative bacteria, Candida albicans, Escherichia coli, Pseudomonas toothpaste
aeruginosa, Staphylococcus aureus.

Lyophilised Sterility testing and identification of isolated microorganisms.


material Microbiology* Analyte*
(5 vials for
sterility testing) Cream liquid Enumeration and detection of aerobic mesophilic bacteria, Enterobacteriaceae,
and powder Pseudomonas aeruginosa, Staphylococcus aureus, Burkholderia capacia,
* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed. Candida albicans, Escherichia coli, Yeast and mould (total count).
For accredited and non-accredited status please see current application form/scheme description.
* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

48 lgcstandards.com/pt lgcstandards.com/pt 49
TOYTEST NiMS
The LGC TOYTEST proficiency A combination of physical toys and
testing scheme is designed to work product information is provided over
with the strict safety regulations that the scheme year for assessment and
Toy Safety are in place to ensure that toys are testing according to the standards.
Nickel Migration
appropriate for the target age group
of children, and do not pose a Additional materials are also
hazard in use. provided for analyses ranging from
solutions and paint flakes for heavy
The scheme is intended to support metals, materials for kinetic testing,
laboratories testing to the key flammability testing, and dye
regulations in place in Europe and analysis.
America, namely the EN71 standard
in Europe and the ASTM F963
standard in America.

Test Material* Analyte* The LGC NiMS Proficiency Testing Many ordinary items such as
scheme is designed to assess the buttons, coins, spectacle frames,
Toy product Paper exercise covering the scope of EN71-1 and ASTM F963 (Mechanical performance of laboratories watchstraps and zips may also
and physical testing). undertaking the determination of contain nickel and as such is hard
nickel release from articles intended for sufferers to avoid.
Cords, plastic Measurement testing according to EN71-1 and ASTM F963. to come into direct and prolonged
films, toys or toy contact with the skin according to The method for the determination
components the European Regulation (EC) of nickel release from such products
1907/2006. is defined in European standard
Toy product Kinetic energy testing EN71-1 and ASTM F963, Acoustic testing EN71-1. EN 1811 (2011). The article to be
The release of nickel from jewellery tested is suspended in an artificial
Magnetic toys Flux testing EN71-1 and ASTM F963. products, in close contact or sweat solution for a period of
or components pierced through the skin is the a week, after which time the
most widespread cause of allergic concentration of dissolved nickel
Sections of Flammability testing EN71-2. contact dermatitis - which affects in the solution is determined by
an estimated 10% to 20% of the ICP-MS or a similarly accurate
Consumer Safety

fabric or toy
product population. and precise technique.

Consumer Safety
Paint flakes, Migration of elements EN71-3.
crayons, fabric
or finger paint
plus standard
solutions Test Material* Analyte*

Information Activity toys EN71-8. Alloy disks, Nickel release and surface area measurement.
and/or toy jewellery or
product for other
paper exercise appropriate
articles
Toy or other Electrical testing EN62115.
electrical item * The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.
Section A zo-dyes EN14362-1 and EN14362-3.
of fabric

Dried paint Cadmium (total), Lead (total), Chromium (total).


flakes

Section of Phthalates.
plastic plus
standard
solutions

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

50 lgcstandards.com/pt lgcstandards.com/pt 51
Forensics 54

55
QUARTZ
Forensic Blood Toxicology

FAE
Forensic Analysis for Explosives
Forensics
Scheme Selector

56 FIRMS Scheme Distribution Test Test Material Matrix* Analyte Group*


Forensic Isotope Ratio per year
Mass Spectrometry

QUARTZ 4 Toxicology and Blood and urine. Alcohol Technical Defense


Forensic Blood Case Study case study.
Toxicology

FAE 1 Chemical Range of relevant Explosive, trace explosives


Forensic Analysis materials. and unknowns.
for Explosives

FIRMS 2 Chemical Range of products in Variations in isotope ratios.


Forensic Isotope sealed amber vials.
Ratio Mass
Spectrometry

* The full range and availability of test materials and analytes is determined on an annual basis and may be added
or removed. For accredited and non-accredited status please see current application form/scheme description.

Forensics
52 lgcstandards.com/pt 53
QUARTZ The LGC QUARTZ scheme is aimed
at laboratories undertaking forensic
toxicology and coroners work. Test
Participation in QUARTZ will
provide independent performance
assessment and confidence that
FAE
Forensic Blood analytes and case scenarios included results are meaningful and accurate.
Forensic Analysis
Toxicology in the scheme are discussed regularly Consistent good performance will for Explosives
with the Advisory Group. allow laboratories to demonstrate to
third parties, customers, regulators
The scheme offers the choice of a and accreditation bodies the quality
number of test materials comprising of their results.
blood and urine spiked with drugs
and metabolites. Case scenarios The operation of our QUARTZ
provided for interpretation covered scheme is supported by an Advisory
include sudden and suspicious Group consisting of members of the
deaths, drug facilitated sexual professional bodies, scheme
assaults (DFSA), impaired driving participants, and others experienced
and other relevant cases. in the field.

There is an Alcohol Technical


Defence (ATD) exercise that allows
practitioners to demonstrate
competency in performing these
types of calculations.

The LGC Forensic Analysis for Forensic examination for explosives


Explosives (FAE) scheme aims may include the analysis of raw
Test Material* Analyte* to provide information depicting materials found at a scene, the
realistic scenarios and test materials identification of potentially explosive
Blood Forensic drug identification, quantification and case study covering the following: to allow participating laboratories to substances and the forensic
Anaesthetics, Anticholinergics, Anticonvulsants, Antidepressants, Antihistamines, demonstrate the competent analysis identification of post-blast explosive
Antipsychotics, Barbiturates, Benzodiazepines, Cannabinoids, of trace explosives and associated residues.
Carboxyhaemoglobin, Cardiovascular drugs, Erectile dysfunction, Hypnotic drugs, chemicals.
Non steroidal anti-Inflammatory analgesics, Opioid analgesics, Stimulants. Participation in FAE will allow
The European Network of Forensic laboratories to monitor performance
Abuse and prescribed drug quantification of commonly encountered drugs Science Institute (ENFSI) Working and compare it with that of peers
(alternate rounds of drugs of abuse and prescription drugs). Group on Explosives provides against the international standards
technical advice to LGC Proficiency ISO/IEC 17025 and ISO/IEC 17020.
Alcohol in blood quantification of Ethanol and fluoride. Testing on the organisation of this
scheme.
Interpretation of a case study (with analytical data, and a scenario or witness
statement) to determine the potential blood alcohol level in a given time (Alcohol
Technical Defence).

Quantification of up to 4 New Psychoactive Substances (NPS).

Identification of one of the most common synthetic cannabinoids.


Forensics

Urine Identification of up to 4 drugs or metabolites relevant to forensic toxicology. Test Material* Analyte*

Identification of Synthetic Cannabanoids. Range of Explosives, trace explosives and unknowns.


relevant test

Forensics
Identification of New Psychoactive Substances. materials

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed. * The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description. For accredited and non-accredited status please see current application form/scheme description.

54 lgcstandards.com/pt lgcstandards.com/pt 55
FIRMS Isotope Ratio Mass Spectrometry
(IRMS) is a specialised technique
that precisely measures small
Participation in the LGC FIRMS
scheme will help laboratories
demonstrate competence in this
Forensic Isotope Ratio differences in the abundances of analytical technique. The scheme is
Mass Spectrometry isotopes such as 2H/1H, 13C/12C, operated by LGC Proficiency Testing
15N/14N and 18O/16O. Subtle and is supported by the FIRMS
variations to the ‘natural’ abundance Network which provides input for the
of these isotopes may be introduced choice of test materials and scheme
during biological, chemical and performance.
physical processes.

These changes enable the


differentiation of materials that
otherwise may not be separated
such that IRMS is used in many
fields, such as archeology, medicine,
geology, food authenticity and
forensics.

Test Material* Analyte*

Range of products Variations in isotope ratios.


in sealed amber
vials

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

LGC is the accredited provider of the PT scheme.


Forensics

Forensics
56 lgcstandards.com/pt 57
Petroleum 60 OIL
Oils & Fuels
Petroleum
Scheme Selector

Scheme Distribution Test Test Material Matrix* Analyte Group*


per year

OIL** 3 Chemical and Oils & Fuels. Various chemical and physical
Oils & Fuels Physical as per ASTM, IP and ISO
protocols.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added
or removed. For accredited and non-accredited status please see current application form/scheme description.

** Please note that the OIL scheme is currently not included in our scope of accreditation.

Petroleum
58 lgcstandards.com/pt 59
OIL** The LGC OIL scheme is designed
specifically to assist chemists and
engineers working in the refinery,
many more, mean it is essential
that laboratories performing these
measurements are capable of
Oils and Fuels fuel, used oil and lubricant producing accurate data.
laboratories.
If a laboratory is performing the
Petroleum products, such as oils analysis of oils and fuels according
and fuels, are tested throughout their to ASTM, IP and ISO protocols,
life span from the time the oil is taken participating in the LGC OIL
from the ground to beyond the proficiency testing scheme will
petroleum recyclers. The enable it to monitor performance
concentration of contaminants and and compare it with that of other
trace elements is vital in ensuring laboratories worldwide. Consistent
the quality of oil and petroleum good performance will allow
products. laboratories to demonstrate to third
parties, customers, regulators and
Regulations related to cleanliness accreditation bodies the quality
standards in engines, contamination of their results.
particles and water in diesel fuel, and

Test Material* Analyte*

#2 Diesel fuel Acid number, Ash, Base number, BP distribution, Carbon, Carbon residue, Cloud
point, Cold filter plugging point, Colour, Copper corrosion, Density, Distillation,
Flash point, Heat content, High temp stability, Hydrocarbon type(s), Hydrogen,
Lubricity (HFRR) wear scar diameter, Nitrogen, Particulate contamination by
filtration, Pour point, Sediment, Sulfur content, Viscosity, Water.

Crude oil Acid number (total - potentiometric), API gravity, Asphaltenes, Density, HTSD, Iron,
Micro carbon residue, Nickel, Nitrogen (total), Pour point, Reid vapour pressure,
Relative density, Salt, Sediment, Sulfur, Vanadium, Viscosity, Water.

Engine oil Acid number (potentiometric), Ash, Ash sulfated, Barium, Base number, Calcium,
lubricants Colour, Demulsibility, Density, Evaporation loss (Noack), Flash point, Gelation,
Magnesium, Molybdenum, Nitrogen, Phosphorous, Potassium, Pour point,
Saponification number, Shear stability, Silicon, Sodium, Sulfur content, Viscosity
(HTHS, kinematic, low temperature, tapered bearing, tapered plug), Volatility (GC),
Water, Water content, Zinc.

Simulated in Acid number, Aluminium, Antimony, Barium , Base number, Boron, Cadmium,
service engine oil Calcium, Chromium, Copper, Flash point, FTIR (Fuel dilution, Glycol, Nitration,
Oxidation, Phosphate, Sulfation, Water), Fuel dilution Glycol, Insoluble, Iron, Lead,
Magnesium, Manganese, Molybdenum, Nickel, Particle count, Phosphorous,
Potassium, Silicon, Silver, Sodium, Sulphur content, Tin, Titanium, Vanadium,
Viscosity, Water content, Zinc.

* The full range and availability of test materials and analytes is determined on an annual basis and may be added or removed.
For accredited and non-accredited status please see current application form/scheme description.

** Please note that the OIL scheme is currently not included in our scope of accreditation.
Petroleum

Petroleum
60 lgcstandards.com/pt 61
FAQS About Proficiency Testing

What is Proficiency Testing? Why enrol in a Proficiency


Testing scheme?
Proficiency Testing (PT) provides a regular
independent assessment of the the technical • Compare your laboratory’s results
performance of a laboratory to assure the to those of others performing the
validity of measurements and tests, which same test or measurement.
should form part of an overall quality strategy.
PT is often referred to as external quality • Demonstrate and identify performance
assessment (EQA), especially in the medical/ trends.
clinical arena.
• Monitor test performance across all
The practice of testing unknown test materials of your organisation’s laboratories.
from an outside source provides an additional,
independent, means to assure the quality of • Complement internal check sample
laboratory test results. programs.

One of the most common designs for a PT • Demonstrate competency to customers,


scheme is for the Proficiency Testing provider accreditation bodies and other regulatory
to designate specific dates throughout the bodies.
year when it will send test materials to all
participants at the same time. • Fulfil accreditation requirements.

The test materials, whose expected values are • Verify methods and instrumentation.
unknown to the subscribers, are analysed by
the laboratory staff who return their results to • Manage risk through early warning
the Proficiency Testing provider. of potential problems.

The results are reviewed (using statistical • Educate and train staff.
techniques described in ISO 13528) to
determine acceptable performance levels, • Check the reasonableness of the
and an evaluation is issued to each participant. laboratory’s estimated measurement
uncertainty.
The evaluation and accompanying statistical
data not only capture the laboratory’s current
performance, but over time allow the quality
team to analyse trends and improve the
laboratory’s long term performance.

Proficiency Testing is a key element in the


laboratory accreditation process, alongside
reference materials, enabling laboratories to
monitor the quality of their analytical results
as stipulated in ISO/IEC 17025 and ISO 15189. 

About Proficiency
Testing
62 lgcstandards.com/pt lgcstandards.com/pt 63
About LGC About the LGC Proficiency
Proficiency Testing Testing process

Which international standards  o you run PT schemes that are jointly


D How do I join a PT scheme? Participants are asked to check the contents
are relevant to LGC PT schemes? managed? of packages immediately on receipt and to
Participants are advised to take part in the contact LGC Standards if there are any
In terms of stipulating the use of Proficiency Yes, some PT schemes are operated jointly PT scheme(s) that are most fitting to their own problems with the condition of the test
Testing, the main standards are ISO/IEC 17025 with a partner organisation. Where schemes area of testing. Where necessary, appropriate materials or accompanying documentation.
- General requirements for the competence are operated jointly, a Management Committee staff at LGC Standards can advise on which
of testing and calibration laboratories; and may be set up to address operational issues scheme is most suitable for participants. How do I treat my PT test material?
the clinical standard ISO 15189 - Medical for the scheme.
laboratories – requirements for quality and For each scheme, a scheme description and It is important for laboratories to understand
competence. All our PT schemes are operated W hat are the fees for participation? application form will be available, containing how to get the optimum benefit from PT
in accordance with the international standard information about the test materials included participation. To do this, a laboratory must
ISO/IEC 17043. The statistical analysis Fees for participation are reviewed annually in the scheme, and the intended distribution participate in an open and honest fashion,
undertaken is in accordance with the and the current fees for each PT scheme are dates. This information is available on our being prepared to, on occasion, be evaluated
international standard ISO 13528. LGC available on application. Payment terms are website: lgcstandards.com/pt as unsatisfactory. If PT is to achieve its aims,
is accredited by the United Kingdom detailed on the application form and invoice. laboratories need to treat the test materials the
Accreditation Service (UKAS) for the Participants are advised that delays with Participants are invited to place orders via same as routine test materials, and staff must
provision of proficiency testing schemes payments may result in test materials and/or our webshop at lgcstandards.com/pt by be encouraged to treat them appropriately and
against ISO/IEC 17043; a copy of our reports being withheld until payments are made. selecting which test materials they wish to learn from their results in a constructive
current scope of accreditation which lists receive in the PT scheme year. Alternatively, manner.
the accredited schemes is available on our Where do you source your PT test it is possible to complete an application form.
website: lgcstandards.com materials?  o I have to use specific methods to
D
Once a completed webshop order or analyse the PT test materials?
How are your PT schemes organised? The vast majority of test materials are application form is received, an order
manufactured by LGC Standards. Where this confirmation will be sent to the participant, Unless otherwise instructed, participants
The day-to-day operation of each PT scheme is not possible, test materials are carefully confirming the test materials selected and should analyse the test materials using any
is the responsibility of LGC. Individual sourced to meet the needs of participants. distribution date. method that they feel is appropriate.
schemes are managed by a team of Scheme Wherever practical, test materials will be as Participants are asked to treat the test material
Coordinators, to cover reporting, customer similar as possible to those samples routinely How often do I need to participate? in the same way as a routine sample.
service and technical functions. For some tested by participating laboratories. However,
schemes, external advisors may also be used in some cases, in order to achieve the required The frequency that a laboratory needs to Participants may be asked to state their
to provide the full range of relevant knowledge degree of homogeneity and stability, test participate in Proficiency Testing depends method when reporting results. It is important
and expertise needed to operate the scheme materials may be in the form of simulated on a wide range of factors specific to each that this information is accurate as results are
effectively. A small number of schemes are run matrices or concentrated spiking solutions. individual laboratory, such as other quality analysed and reported according to the
in collaboration with other organisations. tools used, the volume of work undertaken method stated.
The analyte concentration range of test and the risk associated to the measurements.
D o you use Advisors and Advisory Groups? materials will usually be varied from round to Therefore every individual laboratory may have Do I have to report my results within
round in order to be realistic and challenging. a different need, which is why PT schemes a specific timescale?
Yes, depending upon the PT scheme in Details of individual test material types are provided by LGC Standards offer flexible
question. Advisors are selected on the basis available in the relevant scheme description. participation, although some do have a Deadlines are specified for the return of
of their technical knowledge and experience minimum participation level. Third parties, results, to ensure the timely issue of assigned
of the industry to which the scheme is related. How is PT test material stability affected such as regulatory bodies, may recommend values and reports to participants. For each
Advisors may be used on an ad-hoc basis and by time, distance and temperature? minimum levels of participation. To gain the PT scheme a closure date will therefore be
contacted when specific issues need to be benefit from trend analysis, participation in specified. For certain tests there may also be a
addressed. The test materials are all stable at the stated a minimum of four rounds over a scheme year date specified by which examination of the test
storage temperatures for at least the period is normally recommended. material is recommended to have been
Alternatively, formal Advisory Groups may be of the PT scheme round. Studies have shown commenced. This is to ensure that sufficient
used. Advisory Groups consist of members there is no significant difference between  ow are PT test materials packaged
H time is available to complete the test and
who may or may not be participants on the results of test materials tested the day after and transported? report results in time for the deadline date.
scheme but who are experienced in the field despatch and those tested on the deadline
of testing covered by the PT scheme. date. There is also no evidence that results Test materials are packaged appropriately
are influenced by different climatic conditions to protect the contents during transit. The
The composition and terms of reference of participating countries. majority of test materials are sent using priority
of each Advisory Group will be agreed on courier. Overseas customers must provide
a scheme-by-scheme basis. Distance travelled does not affect test material relevant documents to prevent delay in
results. We have undertaken studies on a customs such as import permits and may
number of our PT test materials comparing the be required to pay import duties locally.

About the LGC Proficiency


Testing
About LGC Proficiency

average result according to distance travelled,


and no correlations have been found. Stability Once packages have been delivered,

Testing process
consideration is an important part of the LGC Standards cannot be held responsible
design and feasibility process for a PT if they subsequently fail to reach the correct
scheme, where transport conditions such as personnel or are not stored under the
temperature, humidity, pressure, exposure to recommended conditions.
x-rays etc are taken into account.

64 lgcstandards.com/pt lgcstandards.com/pt 65
About LGC Proficiency About reporting
Testing schemes and evaluating results

How should I report my results using this can be corrected using PORTAL until How is the assigned value established? There are two specific guides that are
PORTAL? the round closes. internationally recognised:
ISO 13528: ‘Statistical Methods for use
For the majority of PT schemes, results are How many results may I submit? in Proficiency Testing by Interlaboratory • ISO (BIPM, IEC, IFCC, IUPAC, IUPAP and
returned through our bespoke electronic Comparisons’ sets out how the assigned value OIML) ‘Guide to the Expression of Uncertainty
reporting software, PORTAL. Once you are Although it is desirable for participants to and performance assessment criteria can be in Measurement’
ready to report your results, please go to: submit multiple results in order to compare established and describes the options for the
portal.lgcstandards.com You will need results between different analysts, methods various performance scoring systems. • EURACHEM/CITAC Guide ‘Quantifying
to log in using your lab ID, username and or instruments, a single laboratory reporting Uncertainty in Analytical Measurement’
password. We advise that prior to using a large number of results could potentially bias The assigned value is the value selected as (available at: www.eurachem.org).
PORTAL you read the user guide which is the dataset. In order to minimise the effects being the best estimate of the ‘true value’ for
available at: portal.lgcstandards.com of bias, LGC Standards therefore limits the the parameter under test. The method used Further information on approaches to
select ‘help’ from the menu. number of results participants are able to to determine the assigned value may vary evaluating measurement uncertainty may
report. Each participant is able to enter up depending upon the particular PT scheme also be available from your national
If you require further assistance please to 13 different results. Of these results a and test material and is detailed in the relevant accreditation body.
contact our support team: maximum of 3 results can be ‘nominated’. scheme description.
Nominated results are included in the Can I use PT data to estimate my
Tel: +44 (0)161 762 2500 statistical analysis of the dataset whilst For quantitative tests, where it is appropriate, measurement uncertainty?
Email: ptsupport@lgcgroup.com non-nominated results are not, however practicable and technically feasible, the
or your local LGC Standards office. all results will receive z performance scores assigned value will be derived through It is possible, but must be regarded as
and assessments as appropriate. formulation (or occasionally through the use of a very rough estimate, and is not an approach
For some schemes (or parts of a scheme) a certified reference material) to provide addressed in many guides to evaluating
alternative reporting mechanisms are Nominated results must be obtained using metrological traceability; the associated measurement uncertainty. However
provided, details of which will be emailed different methods, again to minimise the uncertainty of the value can therefore be documents that do address the use of PT
to participants prior to test materials receipt. effects of bias. estimated. However, in many cases the use of data are:
a consensus value is the only practicable and
It is recommended that results and Further information is available in the PORTAL technically feasible approach to use. When the • EURACHEM/CITAC Guide ‘Quantifying
calculations are checked thoroughly before User Guide and the PORTAL Nominated assigned value is determined from the Uncertainty in Analytical Measurement’
reporting. Results should be reported clearly, Results FAQ, both of these documents are consensus value of participant results, or from (available at www.eurachem.org)
in the format and units detailed in the scheme available for download from the PORTAL expert laboratories, robust statistical methods
description. If calculations are used, unless website and further information is available are used for calculation of the consensus • NORDTEST Report TR 537 ‘Handbook
instructed otherwise, the laboratory is to from ptsupport@lgcgroup.com value, the estimated standard uncertainty for Calculation of Measurement Uncertainty
report only the final calculated result. and the robust standard deviation. in Environmental Laboratories’
Can my results be included in the report
In general, results of zero should not be if I’ve missed the deadline for reporting? For qualitative tests, participant results • ISO/TS 19036 ‘Microbiology of Food and
reported; results should be reported are compared against the intended result Animal Feeding Stuffs - Guidelines for the
depending upon the detection limit of the Participants are asked to return results by (assigned value) based on formulation or Estimation of Measurement Uncertainty for
method used, for example, <10. The exception the given deadline in order to ensure that their expert assessment. Quantitative Determinations’.
is a small number of parameters, where it may results are included in the statistical analysis
be appropriate to report a result of zero, and the scheme report. Results received after For interpretive schemes where the result is What is the Standard Deviation for
depending on the measurement scale being the closure date will not be included in the subjective rather than quantifiable, a model Proficiency Assessment (SDPA)?
used. Results of zero and truncated results, report. answer produced by appropriate experts will
such as < or > cannot often be included in the be published in the report. The SDPA expresses the acceptable
data analysis and therefore allocated a For PT schemes where a generic report is difference between the laboratory result
performance score. issued, this is available to all participants For microbiology test materials, all participant and the assigned value. An acceptable z
subscribing to the round regardless of whether results are transformed by converting them to performance score represents a result that
Results will be rounded up or down to the their results were submitted or not. log10 before the statistical analysis is does not deviate from the assigned value by
number of reporting decimal places stipulated undertaken. more than twice the SDPA. The method used
in the scheme description and may not Are microbiology results obtained from to determine the SDPA may vary depending
therefore be identical to your original reported MPN methods comparable to those How do I evaluate measurement upon the particular PT scheme and test
result. The effects of rounding may also mean obtained using plate count methods? uncertainty? material and is detailed in the relevant scheme
that occasionally percentage totals do not add description.
up exactly to 100%. MPN and plate counts are both estimates The aim when evaluating measurement
of the number of microbial cells in the original uncertainty is to combine the effects of all the A fit for purpose value for SDPA, rather than
Part of the challenge of Proficiency Testing test material and therefore provided all errors that will influence the measurement being derived from participant results, is
is the ability to perform calculations and dilutions and calculations have been result, into a single value. There are many preferable as this enables z scores to be
Testing schemes
About LGC Proficiency

transcribe results correctly. The proficiency performed correctly, results should be different guides available which provide advice compared from round to round to demonstrate

About reporting and


testing team cannot interpret or calculate comparable. on evaluating measurement uncertainty. general trends.

evaluating results
results on participants’ behalf. Once submitted
and received, results cannot be amended and For QWAS and QMS, comparing MPN results For each scheme, the value of SDPA and the
no changes can be made after the report has against results obtained from all other method used to derive it is reported in the
been issued. However, if you notice an error methods show no significant differences. scheme description and/or report.
in your result before the reporting deadline,

66 lgcstandards.com/pt lgcstandards.com/pt 67
About reporting About reporting
and evaluating results and evaluating results

What standard deviation for proficiency How do I interpret my results? What is the estimated uncertainty Do you include outlying results due to
assessment (SDPA) is used in microbiology of the assigned value? ‘errors and blunders’ in the statistical
PT schemes? For quantitative examinations, participant analysis of the data?
performance is assessed using the z score, The assigned value has a standard uncertainty
There are many sources of variation in and the following interpretation is given to (ux) that depends upon the method used to Although robust estimators are used in order
microbiological testing and the SDPA results: derive the assigned value. When the assigned to minimise the influence of outlying results,
used to assess performance therefore needs value is determined by the consensus of extreme results or results that are identifiably
to be fit-for-purpose and take all possible |z| ≤ 2.00 Satisfactory result participants’ results, the estimated standard invalid should not be included in the statistical
sources of variation into account. From uncertainty of the assigned value can be analysis of the data. For example, these may
experience and historical data, LGC PT 2.00 < |z| < 3.00 Questionable result calculated by: be results caused by calculation errors or the
uses a fixed SDPA value of 0.35 log10 for use of incorrect units. However, such results
the majority of microbiological tests. |z| ≥ 3.00 Unsatisfactory result ux = 1.25 x Robust standard deviation/√n can be difficult to identify by the PT organiser.
For this reason, the robust mean and standard
How do I report a ‘presumptive’ For qualitative examinations or semi-qualitative Where n = number of results deviation will be calculated in the usual way,
result in microbiology? results, laboratories reporting the assigned but those results that are out of the range of
result or range of results will be considered When the assigned value is determined the assigned value ± 5 x SDPA will be
Report your result as usual but record in correct, and therefore have satisfactory by formulation, the standard uncertainty is excluded and the robust mean and standard
the comments section that the result is performance. estimated by the combination of uncertainties deviation will then be recalculated. These
‘Presumptive’. of all sources of error, such as gravimetric and recalculated values will be used for the
What are the advantages of using a z score volumetric measurements. statistical analysis. By removing these
What is the purpose of scoring my result? to assess performance? ‘blunders’ from the dataset any influence
If ux is ≤ 0.3 x SDPA, then the uncertainty on the summary statistics is minimised.
Once the assigned value for the parameters • Results can be expressed in a form that is of the assigned value can be considered All results, including excluded results, will
under test has been established, participant easy to interpret and understand. negligible and need not be considered in the be given performance scores.
laboratories are assessed on the difference interpretation of results.
between their result and the assigned value, • Results can be summarised in graphical or How can I graphically plot and analyse
with this difference being represented by tabular form to depict overall performance. If ux is > 0.3 x SDPA, then the uncertainty of trends for qualitative results?
a performance score called a z score. This the assigned value is not negligible in relation
provides a simple and consistent measure of • A z score allows participants to the SDPA and so z’ (z-prime) performance Qualitative results are difficult to depict
performance which is the key to monitoring to directly compare their own result with scores, which take into account the standard graphically as they are not normally allocated
competence and implementing an others. uncertainty of the assigned value in their a performance score. However for qualitative
improvement programme as required. calculation, will be reported in place of results, a correct result could be allocated a
• If consistent statistical values are applied, z scores. performance score of 0 to represent a
How is a z score calculated? a z score enables participants to monitor satisfactory result. A false positive result can
and trend their own performance How is a z’ (z-prime) score calculated? be represented by a performance score of + 3,
The participant’s result, x, is converted into over time. whilst a false negative result can be
a performance score (z score) using the A z’ score incorporates the standard represented by a performance score of - 3.
following formula: It is important to interpret any performance uncertainty of the assigned value and is If plotted graphically over time, this should
score in the full context of the overall results calculated as follows: give a clear visual indicator of performance
and in the context of a laboratory’s own quality in qualitative tests.
z = (x - X) control measures.
z’ = (x - X) How will I receive my report?
SDPA
√ SDPA2 + ux2 Following statistical evaluation of the results,
Where: X = the assigned value the reports will generally be available on the
Where x = participant result website within 4 to 10 working days of round
SDPA = Standard Deviation for Proficiency closure (see specific scheme description).
Assessment X = the assigned value We aim to provide 95% of our reports to
participants within 5 working days.
For small data sets, there will be increased SDPA = Standard Deviation for Proficiency Participants will be emailed when the report
uncertainty around the assigned value if Assessment is available. The content of reports vary from
derived from a consensus value from scheme to scheme but include details of the
participants’ results. In such cases, ux = standard uncertainty of the assigned composition of test materials, the assigned
performance scores may not be provided, value X values, and tabular and / or graphical
or may be given for information only. representations of participants’ results.
A z’ score is interpreted in exactly the same
evaluating results
About reporting and

The z score expresses performance in relation way as a z score, ≤2 is satisfactory, >2 but

About reporting and


to the assigned value and the standard <3 is questionable and ≥3 is unsatisfactory.

evaluating results
deviation for proficiency assessment (SDPA).
A z score of 2 represents a result that is a
distance of 2 x SDPA from the assigned value.

68 lgcstandards.com/pt lgcstandards.com/pt 69
About reporting About privacy About driving
and evaluating results and confidentiality quality together

How do I assess the reproducibility Can you guarantee my laboratory’s What could be the cause of my  ow can I measure my laboratory’s
H
standard deviation from the PT report? confidentiality? poor performance? performance over time?

The robust standard deviation provided in the In order to ensure confidentiality, participants A single poor result is not indicative of overall You can do this by trend analysis. A single
PT report for a specific method can be taken in all PT schemes are allocated a unique laboratory performance but neither is a single result simply reflects the performance of the
as an estimate of the reproducibility standard laboratory reference number. This number good result. Ideally, PT results should be laboratory on the particular day that the test
deviation for the PT round for that specific enables results to be reported without monitored over time to detect potential bias or was carried out and therefore gives limited
method. divulging the identities of participant repeated unsatisfactory results. There are information. Frequent participation in PT
laboratories. Only staff within the proficiency many possible reasons for a single poor result. schemes over time can give greater insight
Can I have a report that only includes my testing team and the laboratory itself will know It is therefore important to interpret the results into long-term performance and can help
group laboratories? this number. from PT schemes within the context of an identify where internal bias may be occurring.
all-round quality assurance programme,
Yes, we can produce reports tailored to a How do you prevent collusion and including internal quality control, use of One of the best methods of summarising
customer’s specific requirement. There may falsification of results? validated methods and reference materials. performance scores over time is graphically
be an additional charge for administration and There are numerous potential causes of poor as this gives a clear overview and is less prone
computer programming costs. It defeats the objective of taking part in performance in a PT scheme which may to misinterpretation than numerical methods.
proficiency testing if participants are not include analytical and non-analytical errors. Participants are therefore advised to monitor
 y results have not been included in the
M returning genuine results. Certain measures their PT results over time.
report. Can I calculate my performance are built into the PT schemes to try and Analytical errors
score (z or z’ score)? prevent collusion but, ultimately the An online trend analysis tool is included in the
responsibility rests with each participating • Calibration / instrument problems cost of your PT participation with LGC. The
To calculate your performance score laboratory to behave in a professional manner. online tool is built into the PORTAL reporting
please visit: portal.lgcstandards.com • Extraction / clean-up system and allows you to quickly plot your
Select ‘submit results’ from the menu. results over a range of rounds and easily
• Interferences / matrix effects download the charts for further circulation.

• Diagnostic kits / reagents More information regarding interpretation


and trend analysis of proficiency testing results
• Analyst / method performance is given in the Eurachem guide on ‘Selection,
Use and Interpretation of Proficiency Testing
Non-analytical errors (PT) schemes (available at www.eurachem.
org), IUPAC ‘International Harmonised Protocol
• Calculation / transcription for the Proficiency Testing of Analytical
Chemistry Laboratories’, 2006 and ISO 13528.
• Reporting format / units
 ow can I receive advice
H
• Poor / incorrect storage and feedback?

• Test material defects Communication with participants will be


carried out through PT scheme-related
Test materials are subjected to rigorous quality documentation, emails, letters, or through
control testing before being distributed to local LGC Standards offices. Open meetings
participants, and are unlikely to be the cause may also be organised and all interested
of a poor performance score. All possible parties invited to attend.
reasons for a poor performance should be
investigated fully in order to identify the most How can I send feedback?
likely cause and to enable action to be taken
to prevent recurrence. Repeat test materials Comments on any aspect of our products
are available after every distribution, but it is and services are welcome either by phone,
most important to investigate and understand fax, letter, email or by contacting your local
the reason(s) for the failure, document this LGC Standards office.
fully, and carry out corrective actions before
repeating a test. Can I suggest a PT scheme or test
material?

We welcome suggestions any time. Please


confidentiality
About privacy and

complete the ‘Wish list’ form on our website:

About driving quality


lgcstandards.com/pt

together
70 lgcstandards.com/pt lgcstandards.com/pt 71
Proficiency Testing
Proficiency Testing
LGC
LGC

LGC
A global leader in measurement standards,
reference materials, laboratory services and
proficiency testing.

2,600 21
professionals working in countries

We are the UK’s designated National Measurement Institute


for chemical and bioanalytical measurement.

With 2,600 professionals working in 21 countries, our analytical


measurement and quality control services are second-to-none.

As a global leader, we provide the widest range of reference


materials available from any single supplier.

When you make a decision using our resources, you can be sure
it’s based on precise, robust data. And together, we’re creating fairer,
safer, more confident societies worldwide.

lgcstandards.com

Science for a safer world.

72 73
Order your LGC Proficiency
Testing schemes online
Identify proficiency testing schemes to fit your requirements.
Search and order online now at lgcstandards.com/pt

Key features include:

01 02 03
Fast renewals: Advanced search: Up-to-date:

Use our fast renewals Allows you to search for a You can find our latest
feature to review and proficiency testing scheme schemes, samples,
place repeat orders at based on a wide range of information and
the click of a button. analytes and matrices. instructions online.

You can also browse, search and order the wide range of LGC reference
materials at lgcstandards.com

lgcstandards.com/pt
Whilst every effort has been made to ensure the accuracy of the information in this catalogue, customers are directed to their local sales office or the LGC
Standards website for further details and to verify product information. Specifications, terms and pricing are subject to change. LGC does not guarantee
availability and reserves the right to discontinue any product. LGC does not accept liability for any loss that is caused by inaccurate product information,
customer selection or inappropriate use of a product. Unless otherwise stated all trademarks are the property of LGC or its affiliated group companies. No part
of this publication may be reproduced or transmitted in any form or by any means, electronic or mechanical, including photocopying, recording or any retrieval
system, without the written permission of the copyright holder. © LGC Limited, 2019. All rights reserved.

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